CN114075709B - Cold cloth containing zinc jade fiber and preparation method and application thereof - Google Patents
Cold cloth containing zinc jade fiber and preparation method and application thereof Download PDFInfo
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- CN114075709B CN114075709B CN202111249140.9A CN202111249140A CN114075709B CN 114075709 B CN114075709 B CN 114075709B CN 202111249140 A CN202111249140 A CN 202111249140A CN 114075709 B CN114075709 B CN 114075709B
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- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/20—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the material of the fibres or filaments constituting the yarns or threads
- D03D15/292—Conjugate, i.e. bi- or multicomponent, fibres or filaments
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/0007—Electro-spinning
- D01D5/0015—Electro-spinning characterised by the initial state of the material
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/06—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyolefin as constituent
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/18—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from other substances
-
- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/20—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the material of the fibres or filaments constituting the yarns or threads
- D03D15/208—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the material of the fibres or filaments constituting the yarns or threads cellulose-based
- D03D15/217—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the material of the fibres or filaments constituting the yarns or threads cellulose-based natural from plants, e.g. cotton
-
- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/50—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04B—KNITTING
- D04B1/00—Weft knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes
- D04B1/14—Other fabrics or articles characterised primarily by the use of particular thread materials
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04B—KNITTING
- D04B21/00—Warp knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
- D10B2201/01—Natural vegetable fibres
- D10B2201/02—Cotton
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Life Sciences & Earth Sciences (AREA)
- Botany (AREA)
- Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Mechanical Engineering (AREA)
- Artificial Filaments (AREA)
Abstract
The invention discloses a cool cloth containing zinc jade fiber, a preparation method and application thereof, and relates to the technical field of textile preparation; the lignin is a natural aromatic polymer with a three-dimensional network structure, the spinnability of the lignin and the mechanical property of fibers can be improved by utilizing an electrostatic spinning technology after the lignin and the polystyrene are mixed, and the polystyrene has good biocompatibility and can be blended with the lignin and the graphene to form a nanofiber structure, so that nano zinc oxide and jade powder are effectively adsorbed and inlaid on the surface of the nanofiber structure, the cool feeling can be improved, the fiber strength can be enhanced, and the service life of the material is prolonged.
Description
Technical Field
The invention relates to the technical field of textile preparation, in particular to a cool cloth containing zinc jade fibers, and a preparation method and application thereof.
Background
Along with the continuous improvement of living standard, the quality requirements of people on the underwear are increasingly increased, and the underwear with various functions, such as antibiosis, radiation protection, warmth retention and the like, are generated. In hot summer, people are in urgent need of a garment with a rapid cooling effect.
The existing clothes with the cooling function are generally made of jade fibers, the fabric prepared from the jade fibers has good cooling feeling, trace elements of the fabric can be absorbed by a human body, cell tissues are activated, and the immunity of the human body is improved.
However, the jade fiber in the prior art has single functionality, and in order to achieve enough cool feeling, the addition amount of the jade powder in the jade fiber is more, the problems of poor fiber strength and insufficient comfort are easy to occur, the cooling feeling is insufficient due to the reduction of the addition amount, and meanwhile, the spinnability of the fiber is influenced by the addition of more jade powder or other functional particles, so that the breaking strength of the fiber is reduced, and the performance of the fiber is influenced.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provide a cooling cloth containing zinc jade fiber, and a preparation method and application thereof.
In order to solve the technical problems, the invention provides the following technical scheme:
in a first aspect, a method for preparing a cool cloth containing zinc jade fiber is provided, which comprises the following steps:
(1) Weighing the following substances in proportion: graphene material: 20-30 parts of polystyrene: 30-40 parts of lignin: 15-20 parts of organic solvent: 180-200 parts of jade powder: 10-15 parts of nano zinc oxide: 10-12 parts of dispersing agent: 3-5 parts;
(2) Dissolving a graphene material, polystyrene and lignin in an organic solvent, and extruding by a screw to obtain a mixed solution;
(3) Adding jade powder and nano zinc oxide into the mixed solution, stirring for 60-80 min at normal temperature, adding a dispersing agent, and performing ultrasonic dispersion for 30-40 min to obtain mixed dispersion;
(4) Blending and melting the mixed dispersion liquid and the spinning melt to obtain spinning liquid, and carrying out electrospinning treatment on the spinning liquid to obtain zinc jade fibers;
(5) Blending zinc jade fiber and cotton fiber according to a proportion to obtain a cool cloth containing zinc jade fiber; wherein, the content of the zinc jade fiber in the cooling cloth of the zinc jade fiber is 40-50%, and the content of the cotton fiber is 50-60%.
Preferably, the graphene material is selected from one or more of graphene or a graphene derivative.
Preferably, the particle size of the graphene material is less than or equal to 10 mu m. For example 0.1 μm, 0.2 μm, 0.7 μm, 0.8 μm, 1.1 μm, 1.2 μm, 1.5 μm, 2.1 μm, 2.5 μm, 3.5 μm, 4.5 μm, 6 μm, 7 μm, 8 μm, 9 μm, 9.5 μm, etc.
Preferably, the organic solvent is selected from one or more of N, N-dimethylformamide and dimethyl tetrahydrofuran.
More preferably, the organic solvent is a mixture of N, N-dimethylformamide and dimethyltetrahydrofuran.
Preferably, the dispersant comprises sodium tripolyphosphate and stearic acid; the mass ratio of the sodium tripolyphosphate to the stearic acid is 1:1.
Preferably, in the step (4), the temperature of the electrospinning treatment is 24-26 ℃ and the voltage is 10-11 kV.
Preferably, the particle size of the jade powder is less than or equal to 10 mu m. For example 0.1 μm, 0.2 μm, 0.7 μm, 0.8 μm, 1.1 μm, 1.2 μm, 1.5 μm, 2.1 μm, 2.5 μm, 3.5 μm, 4.5 μm, 6 μm, 7 μm, 8 μm, 9 μm, 9.5 μm, etc.
Preferably, in the step (1), the temperature of the screw extrusion is 180-200 ℃.
Preferably, the particle size of the nano zinc oxide is 20-30 μm. For example, 20.1 μm, 20.2 μm, 20.7 μm, 20.8 μm, 21.1 μm, 21.2 μm, 21.5 μm, 22 μm, 23 μm, 25 μm, 27 μm, 28 μm, 29 μm, etc.
In a second aspect, a cool sense fabric containing zinc jade fiber is provided, and the cool sense fabric is prepared by the preparation method in the first aspect.
In a third aspect, the application of the cooling cloth containing zinc jade fiber in the second aspect in preparing textiles is provided. Including but not limited to bed sheets, T-shirts, undershirts, shirts, and sportswear.
Compared with the prior art, the invention has the following beneficial effects:
1. in the preparation method, polystyrene, graphene materials and lignin are added in a specific proportion; the lignin is a natural aromatic polymer with a three-dimensional network structure, the spinnability of the lignin and the mechanical property of fibers can be improved by utilizing an electrostatic spinning technology after the lignin and the polystyrene are mixed, and the polystyrene has good biocompatibility and can be blended with the lignin and the graphene to form a nanofiber structure, so that nano zinc oxide and jade powder are effectively adsorbed and inlaid on the surface of the nanofiber structure, the cool feeling can be improved, the fiber strength can be enhanced, and the service life of the material is prolonged.
2. According to the invention, graphene and jade powder are added into a fiber material at the same time, so that the cool feeling can be improved, and simultaneously, sodium tripolyphosphate and stearic acid can treat the surface of nano zinc oxide, so that the surface of nano zinc oxide is modified to form a compact hydrophobic film, so that the nano zinc oxide is effectively adsorbed on a nano fiber structure, and the net structure of lignin can be combined with polystyrene and a graphene material, so that the fiber strength of the material can be effectively enhanced while the addition amount of the jade powder is increased.
3. The dispersing agent composed of sodium tripolyphosphate and stearic acid can better treat the surface of nano zinc oxide, and can enable the surface of nano zinc oxide to be modified to form a compact hydrophobic film, so that the fiber strength of the material is obviously enhanced.
Additional aspects and advantages of the invention will be set forth in part in the description which follows, and in part will be obvious from the description, or may be learned by practice of the invention.
Detailed Description
For a more complete understanding of the present invention, reference should be made to the following descriptions of the embodiments; it will be apparent that the embodiments described below are only some, but not all, embodiments of the invention; all other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to fall within the scope of the invention.
The features, advantages and advantages of the present invention will become apparent to those skilled in the art from a reading of the present disclosure.
All percentages, fractions and ratios are calculated on the total mass of the composition of the invention, unless otherwise indicated. The term "mass content" is used herein to denote the symbol "%".
In the present invention, the ratio of each component in the composition and the cosmetic is the same.
The terms "comprising," "including," "containing," "having," or other variations thereof herein are intended to cover a non-closed inclusion, without distinguishing between them. The term "comprising" means that other steps and ingredients may be added that do not affect the end result. The term "comprising" also includes the terms "consisting of and" consisting essentially of. The compositions and methods/processes of the present invention can comprise, consist of, and consist essentially of the essential elements and limitations described herein, as well as additional or optional ingredients, components, steps, or limitations of any of the embodiments described herein.
Example 1
The embodiment provides a cool sense cloth containing zinc jade fiber, which is prepared by the following steps:
(1) Weighing the following substances in proportion: graphene: 25 parts of polystyrene: 30 parts of lignin: 16 parts of dimethyl tetrahydrofuran: 180 parts of jade powder: 11 parts of nano zinc oxide: 10 parts of sodium tripolyphosphate: 4 parts;
(2) Dissolving a graphene material, polystyrene and lignin in an organic solvent, and extruding at a screw extrusion temperature of 180 ℃ to obtain a mixed solution;
(3) Adding jade powder and nano zinc oxide into the mixed solution, stirring for 60min at normal temperature, and adding sodium tripolyphosphate for ultrasonic dispersion for 30min to obtain mixed dispersion;
(4) Blending and melting the mixed dispersion liquid and the spinning melt to obtain spinning liquid, and carrying out electrospinning treatment on the spinning liquid at the temperature of 25 ℃ and the voltage of 11kV to obtain zinc jade fibers;
(5) Blending zinc jade fiber and cotton fiber according to a proportion to obtain a cool cloth containing zinc jade fiber; wherein, the content of zinc jade fiber in the cool cloth containing zinc jade fiber is 50 percent, and the content of cotton fiber is 50 percent.
The particle size of the graphene material is less than or equal to 10 mu m, the particle size of the jade powder is less than or equal to 10 mu m, and the particle size of the nano zinc oxide is 20-30 mu m.
Example 2
The embodiment provides a cool sense cloth containing zinc jade fiber, which is prepared by the following steps:
(1) Weighing the following substances in proportion: graphene: 22 parts of polystyrene: 33 parts of lignin: 17 parts of N, N-dimethylformamide: 185 parts of jade powder: 12 parts of nano zinc oxide: 10 parts of sodium tripolyphosphate: 4 parts;
(2) Dissolving a graphene material, polystyrene and lignin in an organic solvent, and extruding at a screw extrusion temperature of 190 ℃ to obtain a mixed solution;
(3) Adding jade powder and nano zinc oxide into the mixed solution, stirring for 70min at normal temperature, and then adding sodium tripolyphosphate for ultrasonic dispersion for 40min to obtain mixed dispersion;
(4) Blending and melting the mixed dispersion liquid and the spinning melt to obtain spinning liquid, and carrying out electrospinning treatment on the spinning liquid at the temperature of 36 ℃ and the voltage of 11kV to obtain zinc jade fibers;
(5) Blending zinc jade fiber and cotton fiber according to a proportion to obtain a cool cloth containing zinc jade fiber; wherein, the content of zinc jade fiber in the cool cloth containing zinc jade fiber is 50 percent, and the content of cotton fiber is 50 percent.
The particle size of the graphene material is less than or equal to 10 mu m, the particle size of the jade powder is less than or equal to 10 mu m, and the particle size of the nano zinc oxide is 20-30 mu m.
Example 3
The embodiment provides a cool sense cloth containing zinc jade fiber, which is prepared by the following steps:
(1) Weighing the following substances in proportion: graphene: 25 parts of polystyrene: 30 parts of lignin: 16 parts of N, N-dimethylformamide: 185 parts of jade powder: 11 parts of nano zinc oxide: 10 parts of stearic acid; 4 parts;
(2) Dissolving a graphene material, polystyrene and lignin in an organic solvent, and extruding at a screw extrusion temperature of 190 ℃ to obtain a mixed solution;
(3) Adding jade powder and nano zinc oxide into the mixed solution, stirring for 80min at normal temperature, adding stearic acid, and performing ultrasonic dispersion for 40min to obtain mixed dispersion;
(4) Blending and melting the mixed dispersion liquid and the spinning melt to obtain spinning liquid, and carrying out electrospinning treatment on the spinning liquid at the temperature of 25 ℃ and the voltage of 11kV to obtain zinc jade fibers;
(5) Blending zinc jade fiber and cotton fiber according to a proportion to obtain a cool cloth containing zinc jade fiber; wherein, the content of zinc jade fiber in the cool cloth containing zinc jade fiber is 50 percent, and the content of cotton fiber is 50 percent.
The particle size of the graphene material is less than or equal to 10 mu m, the particle size of the jade powder is less than or equal to 10 mu m, and the particle size of the nano zinc oxide is 20-30 mu m.
Example 4
The embodiment provides a cool sense cloth containing zinc jade fiber, which is prepared by the following steps:
(1) Weighing the following substances in proportion: graphene: 26 parts of polystyrene: 32 parts of lignin: 15 parts of N, N-dimethylformamide: 100 parts of dimethyl tetrahydrofuran: 90 parts of jade powder: 12 parts of nano zinc oxide: 12 parts of sodium tripolyphosphate: 2 parts of stearic acid; 2 parts;
(2) Dissolving graphene, polystyrene and lignin in an organic solvent, and extruding at a screw extrusion temperature of 200 ℃ to obtain a mixed solution;
(3) Adding jade powder and nano zinc oxide into the mixed solution, stirring for 70min at normal temperature, adding sodium tripolyphosphate and stearic acid, and performing ultrasonic dispersion for 40min to obtain mixed dispersion;
(4) Blending and melting the mixed dispersion liquid and the spinning melt to obtain spinning liquid, and carrying out electrospinning treatment on the spinning liquid at the temperature of 25 ℃ and the voltage of 11kV to obtain zinc jade fibers;
(5) Blending zinc jade fiber and cotton fiber according to a proportion to obtain a cool cloth containing zinc jade fiber; wherein, the content of zinc jade fiber in the cool cloth containing zinc jade fiber is 50 percent, and the content of cotton fiber is 50 percent.
The particle size of the graphene material is less than or equal to 10 mu m, the particle size of the jade powder is less than or equal to 10 mu m, and the particle size of the nano zinc oxide is 20-30 mu m.
Example 5
The embodiment provides a cool sense cloth containing zinc jade fiber, which is prepared by the following steps:
(1) Weighing the following substances in proportion: graphene: 27 parts of polystyrene: 31 parts of lignin: 18 parts of N, N-dimethylformamide: 190 parts of jade powder: 13 parts of nano zinc oxide: 11 parts of sodium tripolyphosphate: 2.5 parts of stearic acid: 2.5 parts;
(2) Dissolving graphene, polystyrene and lignin in an organic solvent, and extruding at a screw extrusion temperature of 200 ℃ to obtain a mixed solution;
(3) Adding jade powder and nano zinc oxide into the mixed solution, stirring for 80min at normal temperature, adding sodium tripolyphosphate and stearic acid, and performing ultrasonic dispersion for 40min to obtain mixed dispersion;
(4) Blending and melting the mixed dispersion liquid and the spinning melt to obtain spinning liquid, and carrying out electrospinning treatment on the spinning liquid at the temperature of 25 ℃ and the voltage of 11kV to obtain zinc jade fibers;
(5) Blending zinc jade fiber and cotton fiber according to a proportion to obtain a cool cloth containing zinc jade fiber; wherein, the content of zinc jade fiber in the cool cloth containing zinc jade fiber is 50 percent, and the content of cotton fiber is 50 percent.
The particle size of the graphene material is less than or equal to 10 mu m, the particle size of the jade powder is less than or equal to 10 mu m, and the particle size of the nano zinc oxide is 20-30 mu m.
Comparative example 1
The difference from example 5 is that: no graphene was added.
Comparative example 2
The difference from example 5 is that: no lignin was added.
Comparative example 3
The difference from example 5 is that: no polystyrene was added.
The cool feeling fabrics prepared in examples 1 to 5 and comparative examples 1 to 3 were subjected to the relevant effect test including the contact cool feeling test, the antibacterial property test and the fiber strength test.
Test of contact Cool feeling coefficient
The test method of the contact cool feeling coefficient is GB/T35263-2017;
antibacterial property test
The antibacterial performance test method is FZ/T73023-2006;
fiber strength test
The test method of the fiber strength is GB/T14337-2008.
The test results are shown in Table 1.
Table 1:
according to the test results of table 1, the dispersants consisting of sodium tripolyphosphate and stearic acid selected in examples 4 and 5 can be obtained in comparative examples 1-5, so that the nano zinc oxide surface can be better treated, and the nano zinc oxide surface can be modified to form a compact hydrophobic film, thereby remarkably enhancing the fiber strength and antibacterial property of the material.
Further, in the comparative examples 5 and 1 to 3, when one of graphene, lignin and polystyrene is not added, the contact cooling coefficient, antibacterial performance and fiber strength of the comparative examples 1 to 3 are remarkably reduced, which indicates that in the scheme of the invention, the graphene, lignin and polystyrene have synergistic effect, and the polystyrene has good biocompatibility and can be blended with the lignin and the graphene to form a nanofiber structure, so that nano zinc oxide and jade powder are effectively adsorbed and embedded on the surface of the nanofiber structure, the cooling feeling can be improved, the fiber strength can be enhanced, and the service life of the material is prolonged.
The foregoing has described in detail the technical solutions provided by the embodiments of the present invention, and specific examples have been applied to illustrate the principles and implementations of the embodiments of the present invention, where the above description of the embodiments is only suitable for helping to understand the principles of the embodiments of the present invention; meanwhile, as for those skilled in the art, according to the embodiments of the present invention, there are variations in the specific embodiments and the application scope, and the present description should not be construed as limiting the present invention.
Claims (9)
1. The preparation method of the cool cloth containing zinc jade fiber is characterized by comprising the following steps of:
(1) Weighing the following substances in proportion: graphene material: 20-30 parts of polystyrene: 30-40 parts of lignin: 15-20 parts of an organic solvent: 180-200 parts of jade powder: 10-15 parts of nano zinc oxide: 10-12 parts of dispersing agent: 3-5 parts of a lubricant;
(2) Dissolving a graphene material, polystyrene and lignin in an organic solvent, and extruding by a screw to obtain a mixed solution;
(3) Adding jade powder and nano zinc oxide into the mixed solution, stirring for 60-80 min at normal temperature, adding a dispersing agent, and performing ultrasonic dispersion for 30-40 min to obtain mixed dispersion;
(4) Blending and melting the mixed dispersion liquid and the spinning melt to obtain spinning liquid, and carrying out electrospinning treatment on the spinning liquid to obtain zinc jade fibers;
(5) Blending zinc jade fiber and cotton fiber according to a proportion to obtain a cool cloth containing zinc jade fiber; the cool sense cloth containing the zinc jade fibers comprises 40-50% of zinc jade fibers and 50-60% of cotton fibers;
wherein the dispersant comprises sodium tripolyphosphate and stearic acid; the mass ratio of the sodium tripolyphosphate to the stearic acid is 1:1.
2. The method for preparing the cooling cloth of zinc-containing jade fiber according to claim 1, wherein the graphene material is one or more selected from graphene or graphene derivatives.
3. The method for preparing the cooling cloth of zinc-containing jade fiber according to claim 1, wherein the particle size of the graphene material is less than or equal to 10 μm.
4. The method for preparing the cool feeling cloth of zinc-containing jade fiber according to claim 1, wherein the organic solvent is one or more selected from the group consisting of N, N-dimethylformamide and dimethyl tetrahydrofuran.
5. The method for preparing the cool cloth of zinc-containing jade fiber according to claim 1, wherein in the step (4), the temperature of the electrospinning treatment is 24-26 ℃ and the voltage is 10-11 kV.
6. The method for preparing a cool feeling cloth of zinc-containing jade fiber according to claim 1, wherein in the step (2), the temperature of screw extrusion is 180-200 ℃.
7. The method for preparing the cool sense fabric of zinc-containing jade fiber according to claim 1, wherein the particle size of the nano zinc oxide is 20-30 μm; the grain diameter of the jade powder is less than or equal to 10 mu m.
8. A cooling cloth comprising zinc-containing jade fiber, which is prepared by the preparation method of any one of claims 1-7.
9. Use of the cooling cloth comprising zinc-containing jade fiber according to claim 8 for preparing textiles.
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| CN104120507B (en) * | 2014-07-22 | 2016-05-18 | 南京工业大学 | Preparation method of lignin-based electrostatic blended material |
| CN105088373A (en) * | 2015-09-17 | 2015-11-25 | 无锡市长安曙光手套厂 | Anti-bacterial fabric and preparation method thereof |
| CN108794997B (en) * | 2017-05-02 | 2021-01-26 | 山东圣泉新材料股份有限公司 | Cool master batch, cool fiber and preparation method and application thereof |
| CN109457362B (en) * | 2018-12-29 | 2021-05-11 | 江苏工程职业技术学院 | Design method and production process of cool moisture-conducting and sweat-releasing fabric |
| CN109930300B (en) * | 2019-02-28 | 2020-05-08 | 文登华绮服装有限公司 | Preparation method of wetting composite fiber fabric material |
| CN113062025B (en) * | 2021-03-03 | 2022-11-15 | 浙江义乌露炜针织内衣有限公司 | Jade zinc ice health-care fabric and preparation method thereof |
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