CN114041529A - Preparation method of picromerite and picromerite feed - Google Patents
Preparation method of picromerite and picromerite feed Download PDFInfo
- Publication number
- CN114041529A CN114041529A CN202111429170.8A CN202111429170A CN114041529A CN 114041529 A CN114041529 A CN 114041529A CN 202111429170 A CN202111429170 A CN 202111429170A CN 114041529 A CN114041529 A CN 114041529A
- Authority
- CN
- China
- Prior art keywords
- parts
- picromerite
- schoenite
- meshes
- ore
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 claims abstract description 23
- GMLLYEDWRJDBIT-UHFFFAOYSA-J magnesium;dipotassium;disulfate Chemical compound [Mg+2].[K+].[K+].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O GMLLYEDWRJDBIT-UHFFFAOYSA-J 0.000 claims abstract description 20
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000000463 material Substances 0.000 claims abstract description 12
- 229910052943 magnesium sulfate Inorganic materials 0.000 claims abstract description 11
- 239000012535 impurity Substances 0.000 claims abstract description 7
- 229910052742 iron Inorganic materials 0.000 claims abstract description 7
- 238000012216 screening Methods 0.000 claims abstract description 6
- 229910000831 Steel Inorganic materials 0.000 claims abstract description 4
- 238000001035 drying Methods 0.000 claims abstract description 4
- 239000010959 steel Substances 0.000 claims abstract description 4
- 238000003860 storage Methods 0.000 claims abstract description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 16
- 235000002639 sodium chloride Nutrition 0.000 claims description 15
- 235000013339 cereals Nutrition 0.000 claims description 9
- 239000011780 sodium chloride Substances 0.000 claims description 8
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 7
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 claims description 7
- 229910052939 potassium sulfate Inorganic materials 0.000 claims description 7
- 229940045109 genistein Drugs 0.000 claims description 6
- TZBJGXHYKVUXJN-UHFFFAOYSA-N genistein Natural products C1=CC(O)=CC=C1C1=COC2=CC(O)=CC(O)=C2C1=O TZBJGXHYKVUXJN-UHFFFAOYSA-N 0.000 claims description 6
- 235000006539 genistein Nutrition 0.000 claims description 6
- ZCOLJUOHXJRHDI-CMWLGVBASA-N genistein 7-O-beta-D-glucoside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1=CC(O)=C2C(=O)C(C=3C=CC(O)=CC=3)=COC2=C1 ZCOLJUOHXJRHDI-CMWLGVBASA-N 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- 244000068988 Glycine max Species 0.000 claims description 5
- 235000010469 Glycine max Nutrition 0.000 claims description 5
- 240000008042 Zea mays Species 0.000 claims description 5
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 claims description 5
- 235000002017 Zea mays subsp mays Nutrition 0.000 claims description 5
- 150000001413 amino acids Chemical class 0.000 claims description 5
- 235000005822 corn Nutrition 0.000 claims description 5
- 235000013312 flour Nutrition 0.000 claims description 5
- 235000012424 soybean oil Nutrition 0.000 claims description 5
- 239000003549 soybean oil Substances 0.000 claims description 5
- 239000004575 stone Substances 0.000 claims description 5
- 235000013343 vitamin Nutrition 0.000 claims description 5
- 239000011782 vitamin Substances 0.000 claims description 5
- 229940088594 vitamin Drugs 0.000 claims description 5
- 229930003231 vitamin Natural products 0.000 claims description 5
- 150000003722 vitamin derivatives Chemical class 0.000 claims description 5
- 235000019341 magnesium sulphate Nutrition 0.000 claims description 4
- 239000001103 potassium chloride Substances 0.000 claims description 4
- 235000011164 potassium chloride Nutrition 0.000 claims description 4
- 235000011151 potassium sulphates Nutrition 0.000 claims description 4
- 238000000034 method Methods 0.000 claims 1
- 241001465754 Metazoa Species 0.000 abstract description 10
- 230000008901 benefit Effects 0.000 abstract description 6
- 244000144977 poultry Species 0.000 abstract description 5
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 abstract description 4
- 239000011777 magnesium Substances 0.000 abstract description 4
- 229910052749 magnesium Inorganic materials 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 206010012735 Diarrhoea Diseases 0.000 abstract description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 abstract description 2
- 239000011591 potassium Substances 0.000 abstract description 2
- 229910052700 potassium Inorganic materials 0.000 abstract description 2
- 238000007873 sieving Methods 0.000 abstract 1
- BMQVDVJKPMGHDO-UHFFFAOYSA-K magnesium;potassium;chloride;sulfate;trihydrate Chemical compound O.O.O.[Mg+2].[Cl-].[K+].[O-]S([O-])(=O)=O BMQVDVJKPMGHDO-UHFFFAOYSA-K 0.000 description 6
- OJXVUEMVNWMNCR-UHFFFAOYSA-L magnesium;potassium;sulfate Chemical class [Mg+2].[K+].[O-]S([O-])(=O)=O OJXVUEMVNWMNCR-UHFFFAOYSA-L 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 239000011738 major mineral Substances 0.000 description 2
- 235000011963 major mineral Nutrition 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 230000001850 reproductive effect Effects 0.000 description 2
- 208000035240 Disease Resistance Diseases 0.000 description 1
- 241000588724 Escherichia coli Species 0.000 description 1
- 241000607142 Salmonella Species 0.000 description 1
- 239000003674 animal food additive Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 229910052564 epsomite Inorganic materials 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229910052930 hexahydrite Inorganic materials 0.000 description 1
- 230000009545 invasion Effects 0.000 description 1
- 229910052928 kieserite Inorganic materials 0.000 description 1
- WRUGWIBCXHJTDG-UHFFFAOYSA-L magnesium sulfate heptahydrate Chemical compound O.O.O.O.O.O.O.[Mg+2].[O-]S([O-])(=O)=O WRUGWIBCXHJTDG-UHFFFAOYSA-L 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/116—Heterocyclic compounds
- A23K20/121—Heterocyclic compounds containing oxygen or sulfur as hetero atom
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/142—Amino acids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/158—Fatty acids; Fats; Products containing oils or fats
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/174—Vitamins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
- A23K20/24—Compounds of alkaline earth metals, e.g. magnesium
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K50/00—Feeding-stuffs specially adapted for particular animals
- A23K50/70—Feeding-stuffs specially adapted for particular animals for birds
- A23K50/75—Feeding-stuffs specially adapted for particular animals for birds for poultry
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Animal Husbandry (AREA)
- Zoology (AREA)
- Food Science & Technology (AREA)
- Birds (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Botany (AREA)
- Molecular Biology (AREA)
- Mycology (AREA)
- Physiology (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Biotechnology (AREA)
- Fodder In General (AREA)
- Feed For Specific Animals (AREA)
Abstract
The invention discloses a preparation method of schoenite and schoenite feed, comprising the following steps: 1. selecting picromerite ore in salt lake, sorting in a screw machine to remove iron impurity, and sieving to remove plastic paperOpening sundries; 2. crushing the picromerite ore screened clean in the step 1 by a crusher, removing iron by magnetic steel, and drying in an air-cooled dryer by using low temperature; 3. the dried material is sent into a grading square sieve for screening, the material with the grain diameter smaller than 20 meshes is taken by the sieve and enters a storage bin, the material with the grain diameter larger than 20 meshes is crushed by a hammer mill until the grain diameter is smaller than 20 meshes, and the picromerite (K) is finally obtained2SO4·MgSO4·6H2Content of O)>90 percent. The picromerite feed has the advantages that the ratio of potassium to magnesium is more suitable for animals, the content of magnesium is lower, animal diarrhea is avoided, the picromerite feed is more suitable for animals to eat, and the production performance and the economic benefit of animals, poultry and the like are improved.
Description
Technical Field
The invention relates to the technical field of feeds, in particular to a preparation method of schoenite and a schoenite feed.
Background
One of the major mineral products in salt lakes is picromerite (picromerite), which is one of the major mineral components of sylvite ores. Monoclinic system, the crystal is short column or thick plate, the aggregate is block, powder, and shell. Transparent and colorless or white, and light red, light yellow or gray when containing impurities. Glass gloss. Hardness 2.5, density 2.03g/cm 3. The water is easy to lose by heating. At lower temperatures, schoenite primary precipitates are formed in brines containing kainite and kainite. It may also be weathered products of kainite and kainite anhydrous, which are associated with kieserite, epsomite, glaserite, etc.
Schoenite is a double salt of potassium sulfate and magnesium sulfate. At present, most of magnesium potassium sulfate salts (picromerite, kainite and anhydrous kainite) are used for fertilizer production, and with the continuous deepening of research and exploration, about 8 percent of magnesium potassium sulfate salts are used for feed additives, and the safety and the effectiveness of the magnesium potassium sulfate salts are long known.
In order to prepare picromerite suitable for animal feed, the invention develops a preparation method of picromerite and picromerite feed.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide a preparation method of schoenite and a schoenite feed, wherein the proportion of potassium to magnesium is more suitable for animals, the content of magnesium is lower, animal diarrhea is not caused, the schoenite feed is more suitable for animals to eat, and the production performance and the economic benefit of animals, poultry and the like are improved.
In order to achieve the purpose, the invention is realized by the following technical scheme: a preparation method of schoenite comprises the following steps:
1. selecting picromerite ore in a salt lake, entering a screw machine for sorting, removing iron impurities in the picromerite ore, and then screening plastic paper impurities through a sieve;
2. crushing the picromerite ore screened clean in the step 1 by a crusher, removing iron by magnetic steel, and drying in an air-cooled dryer by using low temperature;
3. the dried material is sent into a grading square sieve for screening, the material with the grain diameter smaller than 20 meshes is taken by the sieve and enters a storage bin, the material with the grain diameter larger than 20 meshes is crushed by a hammer mill until the grain diameter is smaller than 20 meshes, and the picromerite (K) is finally obtained2SO4·MgSO4·6H2Content of O)>90％。
The picromerite ore in the step 1 is K2SO4·MgSO4·6H2Content of O>95 percent of sodium chloride, potassium sulfate, potassium chloride and magnesium sulfate.
The picromerite feed consists of the following components in parts by weight: 5-8 parts of schoenite, 20-25 parts of corn, 15-20 parts of soybean, 10-15 parts of amino acid, 5-10 parts of vitamin, 10-20 parts of flour, 5-8 parts of soybean oil, 10-15 parts of stone powder, 5-10 parts of sodium chloride and 3-5 parts of genistein.
The invention has the beneficial effects that: the invention utilizes the natural ore of the salt lake to extract the picromerite, and adds the picromerite into the feed, thereby promoting the growth and reproductive performance of poultry and improving the economic benefit.
Detailed Description
In order to make the technical means, the creation characteristics, the achievement purposes and the effects of the invention easy to understand, the invention is further described with the specific embodiments.
The specific implementation mode adopts the following technical scheme: a preparation method of schoenite comprises the following steps:
1. selecting picromerite ore in salt lake, sorting in screw machine to remove ironRemoving impurities of the plastic paper by a sieve; wherein the schoenite ore is K2SO4·MgSO4·6H2Content of O>95 percent of sodium chloride, potassium sulfate, potassium chloride and magnesium sulfate.
2. Crushing the picromerite ore screened clean in the step 1 by a crusher, removing iron by magnetic steel, and drying in an air-cooled dryer by using low temperature;
3. the dried material is sent into a grading square sieve for screening, the material with the grain diameter smaller than 20 meshes is taken by the sieve and enters a storage bin, the material with the grain diameter larger than 20 meshes is crushed by a hammer mill until the grain diameter is smaller than 20 meshes, and the picromerite (K) is finally obtained2SO4·MgSO4·6H2Content of O)>90％。
Example 1:
the picromerite feed consists of the following components in parts by weight: 5 parts of schoenite, 20 parts of corn, 15 parts of soybean, 10 parts of amino acid, 5 parts of vitamin, 10 parts of flour, 5 parts of soybean oil, 10 parts of stone powder, 5 parts of sodium chloride and 3 parts of genistein.
Example 2:
the picromerite feed consists of the following components in parts by weight: 8 parts of schoenite, 25 parts of corn, 20 parts of soybean, 15 parts of amino acid, 10 parts of vitamin, 20 parts of flour, 8 parts of soybean oil, 15 parts of stone powder, 10 parts of sodium chloride and 5 parts of genistein.
Example 3:
the picromerite feed consists of the following components in parts by weight: 5-8 parts of schoenite, 22 parts of corn, 18 parts of soybean, 12 parts of amino acid, 8 parts of vitamin, 15 parts of flour, 6 parts of soybean oil, 12 parts of stone powder, 8 parts of sodium chloride and 4 parts of genistein.
The invention prepares the picromerite (K) by using the picromerite ore in the salt lake2SO4·MgSO4·6H2O,) content>90 percent, improves the growth efficiency of poultry, reduces the death rate, can improve the egg yield of laying hens, improves the reproductive capacity of sows and dyes the sows when being added into the feedThe genistein can inhibit the invasion of Escherichia coli and Salmonella to IPEC-1 cells. Ensures the disease resistance of poultry animals, has good use effect and greatly improves economic benefit.
The foregoing shows and describes the general principles and broad features of the present invention and advantages thereof. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the invention as claimed. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (3)
1. The preparation method of schoenite is characterized by comprising the following steps:
(1) selecting picromerite ore in a salt lake, entering a screw machine for sorting, removing iron impurities in the picromerite ore, and then screening plastic paper impurities by a sieve;
(2) crushing the schoenite ore screened clean in the step (1) by a crusher, removing iron by magnetic steel, and drying in an air-cooled dryer by using low temperature;
(3) the dried material is sent into a grading square sieve for screening, the material with the grain diameter smaller than 20 meshes is taken by the sieve and enters a storage bin, the material with the grain diameter larger than 20 meshes is crushed by a hammer mill until the grain diameter is smaller than 20 meshes, and finally the picromerite (K) is obtained2SO4·MgSO4·6H2Content of O)>90％。
2. The process according to claim 1, wherein the schoenite ore in step (1) is K2SO4·MgSO4·6H2Content of O>95 percent of sodium chloride, potassium sulfate, potassium chloride and magnesium sulfate.
3. The picromerite feed is characterized by comprising the following components in parts by weight: 5-8 parts of schoenite, 20-25 parts of corn, 15-20 parts of soybean, 10-15 parts of amino acid, 5-10 parts of vitamin, 10-20 parts of flour, 5-8 parts of soybean oil, 10-15 parts of stone powder, 5-10 parts of sodium chloride and 3-5 parts of genistein.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111429170.8A CN114041529A (en) | 2021-11-29 | 2021-11-29 | Preparation method of picromerite and picromerite feed |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111429170.8A CN114041529A (en) | 2021-11-29 | 2021-11-29 | Preparation method of picromerite and picromerite feed |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN114041529A true CN114041529A (en) | 2022-02-15 |
Family
ID=80211441
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202111429170.8A Pending CN114041529A (en) | 2021-11-29 | 2021-11-29 | Preparation method of picromerite and picromerite feed |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN114041529A (en) |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1724374A (en) * | 2005-07-17 | 2006-01-25 | 青海中信国安科技发展有限公司 | Process for producing soft potassium magnesium vanadium |
| CN102320867A (en) * | 2011-08-31 | 2012-01-18 | 张万里 | Sulphate-potassium magnesium fertilizer and preparation method thereof |
| CN103156071A (en) * | 2013-04-03 | 2013-06-19 | 左刚 | Sulphate-potassium magnesium and application of sulphate-potassium magnesium contained mixture as animal feed additive |
| CN107021501A (en) * | 2017-05-04 | 2017-08-08 | 山西晋坤矿产品股份有限公司 | A kind of method that gangue prepares high oil absorption value calcined kaolin |
| CN107080098A (en) * | 2017-06-22 | 2017-08-22 | 中国农业大学 | A kind of Breeder hens feed for improving growth of meat chicken and meat production |
| CN109368669A (en) * | 2018-11-22 | 2019-02-22 | 青海蓝湖善成生物技术有限公司 | A kind of preparation method and picromerite feed of picromerite |
| CN110012970A (en) * | 2019-04-19 | 2019-07-16 | 青海蓝湖善成生物技术有限公司 | Coating type mineral additive for feed and preparation method thereof |
| CN110947514A (en) * | 2019-12-23 | 2020-04-03 | 佛山市高明星源机械有限公司 | Iron removing method for non-metallic ore system |
-
2021
- 2021-11-29 CN CN202111429170.8A patent/CN114041529A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1724374A (en) * | 2005-07-17 | 2006-01-25 | 青海中信国安科技发展有限公司 | Process for producing soft potassium magnesium vanadium |
| CN102320867A (en) * | 2011-08-31 | 2012-01-18 | 张万里 | Sulphate-potassium magnesium fertilizer and preparation method thereof |
| CN103156071A (en) * | 2013-04-03 | 2013-06-19 | 左刚 | Sulphate-potassium magnesium and application of sulphate-potassium magnesium contained mixture as animal feed additive |
| CN107021501A (en) * | 2017-05-04 | 2017-08-08 | 山西晋坤矿产品股份有限公司 | A kind of method that gangue prepares high oil absorption value calcined kaolin |
| CN107080098A (en) * | 2017-06-22 | 2017-08-22 | 中国农业大学 | A kind of Breeder hens feed for improving growth of meat chicken and meat production |
| CN109368669A (en) * | 2018-11-22 | 2019-02-22 | 青海蓝湖善成生物技术有限公司 | A kind of preparation method and picromerite feed of picromerite |
| CN110012970A (en) * | 2019-04-19 | 2019-07-16 | 青海蓝湖善成生物技术有限公司 | Coating type mineral additive for feed and preparation method thereof |
| CN110947514A (en) * | 2019-12-23 | 2020-04-03 | 佛山市高明星源机械有限公司 | Iron removing method for non-metallic ore system |
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Application publication date: 20220215 |