CN113995158A - Preparation method of plant-aroma-containing electronic cigarette solid particle atomized matter - Google Patents
Preparation method of plant-aroma-containing electronic cigarette solid particle atomized matter Download PDFInfo
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- CN113995158A CN113995158A CN202111605293.2A CN202111605293A CN113995158A CN 113995158 A CN113995158 A CN 113995158A CN 202111605293 A CN202111605293 A CN 202111605293A CN 113995158 A CN113995158 A CN 113995158A
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- electronic cigarette
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- 239000003571 electronic cigarette Substances 0.000 title claims abstract description 43
- 239000002245 particle Substances 0.000 title claims abstract description 43
- 239000007787 solid Substances 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 241000196324 Embryophyta Species 0.000 claims abstract description 46
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 33
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 24
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 20
- 235000013599 spices Nutrition 0.000 claims abstract description 16
- 238000002156 mixing Methods 0.000 claims abstract description 14
- 239000003205 fragrance Substances 0.000 claims abstract description 13
- 239000007921 spray Substances 0.000 claims abstract description 12
- 244000269722 Thea sinensis Species 0.000 claims abstract description 11
- 239000000654 additive Substances 0.000 claims abstract description 11
- 230000000996 additive effect Effects 0.000 claims abstract description 11
- 239000000843 powder Substances 0.000 claims abstract description 11
- 238000000889 atomisation Methods 0.000 claims abstract description 6
- 244000061176 Nicotiana tabacum Species 0.000 claims abstract 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 18
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 16
- 229930195729 fatty acid Natural products 0.000 claims description 16
- 239000000194 fatty acid Substances 0.000 claims description 16
- -1 -isopropyl butanamide Chemical compound 0.000 claims description 15
- 238000000855 fermentation Methods 0.000 claims description 15
- 239000007788 liquid Substances 0.000 claims description 15
- 239000000243 solution Substances 0.000 claims description 14
- 239000003795 chemical substances by application Substances 0.000 claims description 12
- 239000008139 complexing agent Substances 0.000 claims description 12
- 239000003995 emulsifying agent Substances 0.000 claims description 12
- 230000004151 fermentation Effects 0.000 claims description 12
- 239000000047 product Substances 0.000 claims description 12
- 239000002994 raw material Substances 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 238000001914 filtration Methods 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 9
- 229920001214 Polysorbate 60 Polymers 0.000 claims description 8
- 238000007493 shaping process Methods 0.000 claims description 8
- 244000144730 Amygdalus persica Species 0.000 claims description 6
- 235000005979 Citrus limon Nutrition 0.000 claims description 6
- 244000131522 Citrus pyriformis Species 0.000 claims description 6
- 241001672694 Citrus reticulata Species 0.000 claims description 6
- 235000005976 Citrus sinensis Nutrition 0.000 claims description 6
- 240000002319 Citrus sinensis Species 0.000 claims description 6
- 235000006040 Prunus persica var persica Nutrition 0.000 claims description 6
- 241000533293 Sesbania emerus Species 0.000 claims description 6
- CBOQJANXLMLOSS-UHFFFAOYSA-N ethyl vanillin Chemical compound CCOC1=CC(C=O)=CC=C1O CBOQJANXLMLOSS-UHFFFAOYSA-N 0.000 claims description 6
- 239000000706 filtrate Substances 0.000 claims description 6
- 239000000796 flavoring agent Substances 0.000 claims description 6
- 235000013355 food flavoring agent Nutrition 0.000 claims description 6
- UWKAYLJWKGQEPM-LBPRGKRZSA-N linalyl acetate Chemical compound CC(C)=CCC[C@](C)(C=C)OC(C)=O UWKAYLJWKGQEPM-LBPRGKRZSA-N 0.000 claims description 6
- 239000011259 mixed solution Substances 0.000 claims description 6
- 239000003960 organic solvent Substances 0.000 claims description 6
- 238000000926 separation method Methods 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 5
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 claims description 4
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 4
- 229930006000 Sucrose Natural products 0.000 claims description 4
- 239000004327 boric acid Substances 0.000 claims description 4
- 125000005619 boric acid group Chemical group 0.000 claims description 4
- 150000004665 fatty acids Chemical class 0.000 claims description 4
- 239000005720 sucrose Substances 0.000 claims description 4
- 240000000560 Citrus x paradisi Species 0.000 claims description 3
- 235000009917 Crataegus X brevipes Nutrition 0.000 claims description 3
- 235000013204 Crataegus X haemacarpa Nutrition 0.000 claims description 3
- 235000009685 Crataegus X maligna Nutrition 0.000 claims description 3
- 235000009444 Crataegus X rubrocarnea Nutrition 0.000 claims description 3
- 235000009486 Crataegus bullatus Nutrition 0.000 claims description 3
- 235000017181 Crataegus chrysocarpa Nutrition 0.000 claims description 3
- 235000009682 Crataegus limnophila Nutrition 0.000 claims description 3
- 240000000171 Crataegus monogyna Species 0.000 claims description 3
- 235000004423 Crataegus monogyna Nutrition 0.000 claims description 3
- 235000002313 Crataegus paludosa Nutrition 0.000 claims description 3
- 235000009840 Crataegus x incaedua Nutrition 0.000 claims description 3
- 102000004190 Enzymes Human genes 0.000 claims description 3
- 108090000790 Enzymes Proteins 0.000 claims description 3
- YIKYNHJUKRTCJL-UHFFFAOYSA-N Ethyl maltol Chemical compound CCC=1OC=CC(=O)C=1O YIKYNHJUKRTCJL-UHFFFAOYSA-N 0.000 claims description 3
- 235000006679 Mentha X verticillata Nutrition 0.000 claims description 3
- 235000002899 Mentha suaveolens Nutrition 0.000 claims description 3
- 235000001636 Mentha x rotundifolia Nutrition 0.000 claims description 3
- 241000320412 Ogataea angusta Species 0.000 claims description 3
- 240000000851 Vaccinium corymbosum Species 0.000 claims description 3
- 235000003095 Vaccinium corymbosum Nutrition 0.000 claims description 3
- 235000017537 Vaccinium myrtillus Nutrition 0.000 claims description 3
- 235000009754 Vitis X bourquina Nutrition 0.000 claims description 3
- 235000012333 Vitis X labruscana Nutrition 0.000 claims description 3
- 240000006365 Vitis vinifera Species 0.000 claims description 3
- 235000014787 Vitis vinifera Nutrition 0.000 claims description 3
- 229940069765 bean extract Drugs 0.000 claims description 3
- 235000021014 blueberries Nutrition 0.000 claims description 3
- 229940055416 blueberry extract Drugs 0.000 claims description 3
- 235000019216 blueberry extract Nutrition 0.000 claims description 3
- 238000009835 boiling Methods 0.000 claims description 3
- 230000000593 degrading effect Effects 0.000 claims description 3
- 229940093503 ethyl maltol Drugs 0.000 claims description 3
- 229940073505 ethyl vanillin Drugs 0.000 claims description 3
- 229940038487 grape extract Drugs 0.000 claims description 3
- 229940065115 grapefruit extract Drugs 0.000 claims description 3
- 235000020717 hawthorn extract Nutrition 0.000 claims description 3
- UWKAYLJWKGQEPM-UHFFFAOYSA-N linalool acetate Natural products CC(C)=CCCC(C)(C=C)OC(C)=O UWKAYLJWKGQEPM-UHFFFAOYSA-N 0.000 claims description 3
- 229940105902 mint extract Drugs 0.000 claims description 3
- 230000001376 precipitating effect Effects 0.000 claims description 3
- 239000006185 dispersion Substances 0.000 claims 2
- 235000012907 honey Nutrition 0.000 claims 1
- 239000000779 smoke Substances 0.000 abstract description 4
- 230000000391 smoking effect Effects 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 2
- 241000208125 Nicotiana Species 0.000 description 13
- 238000010438 heat treatment Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 3
- 235000019504 cigarettes Nutrition 0.000 description 2
- 239000002304 perfume Substances 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/20—Biochemical treatment
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
Abstract
The invention relates to the technical field of electronic cigarette products, in particular to a preparation method of an electronic cigarette solid particle atomized substance containing plant fragrance. A preparation method of an electronic cigarette solid particle spray containing plant aroma comprises the following components in parts by mass: 20-70 parts of tea powder, 5-35 parts of glycerol, 5-20 parts of propylene glycol, 1-20 parts of 85% tobacco extract, 0.5-2 parts of 85% plant spice and 0.5-2 parts of additive, and mixing to prepare the electronic cigarette particle atomization product with plant fragrance. The preparation method is simple to operate and low in preparation cost, and when the electronic cigarette particle atomized prepared by the invention is applied to an electronic cigarette, fragrance can be released and flows out along with smoke, so that the smoking experience of a user is improved.
Description
Technical Field
The invention relates to the technical field of electronic cigarette products, in particular to a preparation method of an electronic cigarette solid particle atomized substance containing plant fragrance.
Background
The electronic cigarette is an electronic product simulating a cigarette, and has the same appearance, smoke, taste and sensation as the cigarette. It is a product which is absorbed by users after nicotine and the like are changed into steam by means of atomization and the like.
Along with the improvement of the living standard of people, the requirements of people on the use experience of electronic cigarette products are higher and higher. In order to improve the use experience of electronic cigarette products, a component containing aroma is generally added into a cartridge of an electronic cigarette to meet various efficacy requirements of users.
Disclosure of Invention
The present invention aims to overcome the above-mentioned shortcomings and provide a technical solution to solve the above-mentioned problems.
A preparation method of an electronic cigarette solid particle spray containing plant aroma is used for preparing the electronic cigarette solid particle spray containing the plant aroma and comprises the following components in parts by weight: 20-70 parts of tea powder, 5-35 parts of glycerol, 5-20 parts of propylene glycol, 1-20 parts of 85% tobacco extract, 0.5-2 parts of 85% plant spice, 0.5-2 parts of additive and 5-10 parts of shaping agent, and mixing to prepare the electronic cigarette solid particle atomization agent with plant fragrance.
Further, the plant perfume is one of coffee bean extract, mint extract, lemon extract, blueberry extract, sweet orange extract, juicy peach extract, grape extract, grapefruit extract, mandarin orange extract, preserved plum extract and hawthorn extract.
Further, the additive comprises the following components in parts by mass: 0.5-5 parts of flavoring agent and 0.2-5 parts of N.2.3 trimethyl-2-isopropyl butanamide.
Further, the flavoring agent is one or a mixture of more of ethyl maltol, ethyl vanillin and linalyl acetate.
Further, the tobacco extract is prepared by the following method: mixing tobacco raw materials, water and degrading enzyme at 40-50 deg.C, and performing enzymolysis for 4-8 hr to obtain zymolyte; mixing the zymolyte with hansenula polymorpha for anaerobic fermentation to obtain a fermented product; carrying out solid-liquid separation on the fermentation product to obtain a separation liquid; concentrating the separated liquid to obtain fermentation liquid; the density of the fermentation liquor is 1.1-1.4 mg/mL; adsorbing the fermentation liquid, precipitating with mixed ethanol solution of ethanol and propylene glycol, and removing ethanol to obtain tobacco extract.
Further, the plant spice is prepared by the following method: the plant spice extract is prepared by smashing one of coffee beans, mint, lemon, blueberry, sweet orange, juicy peach, grape, grapefruit, green tangerine, preserved plum and hawthorn to obtain a plant raw material, putting the plant raw material into water according to the mass ratio of 1:10, stewing and boiling the plant raw material for 2 hours at 70-75 ℃ in a sealed environment, filtering, retaining filtrate, distilling and concentrating the filtrate.
Further, the shaping agent comprises 0.05-0.2 part of complexing agent and 5-10 parts of emulsifier, wherein the complexing agent is boric acid, the emulsifier is at least one of fatty acid monoglyceride, sodium dodecyl sulfate, sucrose fatty acid ester, polyoxyethylene sorbitan fatty acid ester and polyoxyethylene sorbitan fatty acid ester, and the rest components are mixed to prepare the electronic cigarette solid particle atomization product with plant fragrance.
Specifically, the preparation method of the electronic cigarette solid particle spray containing the plant aroma comprises the following steps:
s1: putting glycerol and propylene glycol in the mass parts into 100 parts of water, and uniformly mixing and stirring to obtain an organic solvent;
s2: taking tea powder, a tobacco extract and plant spice according to the mass parts, putting the tea powder, the tobacco extract and the plant spice into the organic solvent obtained in the step S1, uniformly stirring, standing for 24 hours, and filtering to obtain an organic solution;
s3: adding the additive, the complexing agent and the emulsifier in parts by mass into the organic solution obtained in the step S2, and uniformly stirring to obtain a mixed solution;
s4: and (4) adding a weak base solution into the mixed solution obtained in the step S3 until particles are not separated out, filtering out the particles, and drying to obtain the electronic cigarette solid particle atomized matter.
Compared with the prior art, the invention has the following beneficial effects: the preparation method is simple to operate and low in preparation cost, and when the electronic cigarette particle atomizer prepared by the invention is applied to an electronic cigarette, fragrance can be released and flows out along with smoke, so that the smoking experience of a user is improved.
Additional aspects and advantages of the invention will be set forth in part in the description which follows and, in part, will be obvious from the description, or may be learned by practice of the invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
A preparation method of an electronic cigarette solid particle spray containing plant aroma is used for preparing the electronic cigarette solid particle spray containing the plant aroma and comprises the following components in parts by weight: 20-70 parts of tea powder, 5-35 parts of glycerol, 5-20 parts of propylene glycol, 1-20 parts of 85% tobacco extract, 0.5-2 parts of 85% plant spice, 0.5-2 parts of additive and 5-10 parts of shaping agent, and mixing to prepare the electronic cigarette solid particle atomization agent with plant fragrance.
Further, the plant perfume is one of coffee bean extract, mint extract, lemon extract, blueberry extract, sweet orange extract, juicy peach extract, grape extract, grapefruit extract, mandarin orange extract, preserved plum extract and hawthorn extract.
Further, the additive comprises the following components in parts by mass: 0.5-5 parts of flavoring agent and 0.2-5 parts of N.2.3 trimethyl-2-isopropyl butanamide.
Further, the flavoring agent is one or a mixture of more of ethyl maltol, ethyl vanillin and linalyl acetate.
Further, the tobacco extract is prepared by the following method: mixing tobacco raw materials, water and degrading enzyme at 40-50 deg.C, and performing enzymolysis for 4-8 hr to obtain zymolyte; mixing the zymolyte with hansenula polymorpha for anaerobic fermentation to obtain a fermented product; carrying out solid-liquid separation on the fermentation product to obtain a separation liquid; concentrating the separated liquid to obtain fermentation liquid; the density of the fermentation liquor is 1.1-1.4 mg/mL; adsorbing the fermentation liquid, precipitating with mixed ethanol solution of ethanol and propylene glycol, and removing ethanol to obtain tobacco extract.
Further, the plant spice is prepared by the following method: the plant spice extract is prepared by smashing one of coffee beans, mint, lemon, blueberry, sweet orange, juicy peach, grape, grapefruit, green tangerine, preserved plum and hawthorn to obtain a plant raw material, putting the plant raw material into water according to the mass ratio of 1:10, stewing and boiling the plant raw material for 2 hours at 70-75 ℃ in a sealed environment, filtering, retaining filtrate, distilling and concentrating the filtrate.
[ example one ] the setting agent comprises 0.05-0.2 part of a complexing agent and 5-10 parts of an emulsifier, wherein the complexing agent is boric acid, the emulsifier is at least one of fatty acid monoglyceride, sodium dodecyl sulfate, sucrose fatty acid ester, polyoxyethylene sorbitan fatty acid ester and polyoxyethylene sorbitan fatty acid ester, and the remaining components are mixed to prepare the electronic cigarette particles with plant fragrance, and the method specifically comprises the following steps:
s1: putting glycerol and propylene glycol in the mass parts into 100 parts of water, and uniformly mixing and stirring to obtain an organic solvent;
s2: taking tea powder, a tobacco extract and plant spice according to the mass parts, putting the tea powder, the tobacco extract and the plant spice into the organic solvent obtained in the step S1, uniformly stirring, standing for 24 hours, and filtering to obtain an organic solution;
s3: adding the additive, the complexing agent and the emulsifier in parts by mass into the organic solution obtained in the step S2, and uniformly stirring to obtain a mixed solution;
s4: and (4) adding a weak base solution into the mixed solution obtained in the step S3 until particles are not separated out, filtering out the particles, and drying to obtain the electronic cigarette solid particle atomized matter.
[ example two ]
The shaping agent comprises 0.05-0.2 part of complexing agent and 5-10 parts of emulsifier, wherein the complexing agent is boric acid, the emulsifier is at least one of fatty acid monoglyceride, sodium dodecyl sulfate, sucrose fatty acid ester, polyoxyethylene sorbitan fatty acid ester and polyoxyethylene sorbitan fatty acid ester, and the shaping agent is mixed with the rest components to prepare the electronic cigarette particles with plant fragrance, and the shaping agent specifically comprises the following steps:
s1': uniformly mixing glycerol, propylene glycol, tea powder, a tobacco extract and plant spice according to the mass parts, adding water according to the mass percent of 50%, heating, keeping the heating temperature at 50-80 ℃, and continuously stirring until the mixture is in a molten state;
s2': adding the additive, the complexing agent and the emulsifier in parts by weight, continuously heating, uniformly stirring, heating to 90-100 ℃, and continuously stirring until solid particles are separated out;
s3': and (5) putting the solid particles obtained in the step (S2') into a drying box, and drying the surface moisture of the solid particles at a constant temperature of 120 ℃ to obtain the electronic cigarette solid particle atomized matter.
In particular, the different plant fragrances comprise the main components as follows:
the electronic cigarette particle atomized matter prepared according to the formula and the preparation method is simple to operate, the preparation cost is low, and when the electronic cigarette particle atomized matter prepared by the invention is applied to an electronic cigarette, fragrance can be released and flows out along with smoke, so that the smoking experience of a user is improved.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.
Claims (8)
1. The preparation method of the plant-aroma-containing electronic cigarette solid particle atomized matter is characterized by comprising the following components in parts by weight: 20-70 parts of tea powder, 5-35 parts of glycerol, 5-20 parts of propylene glycol, 1-20 parts of 85% tobacco extract, 0.5-2 parts of 85% plant spice, 0.5-2 parts of additive and 5-10 parts of shaping agent, and mixing to prepare the electronic cigarette solid particle atomization agent with plant fragrance.
2. The method for preparing the plant aroma-containing electronic cigarette solid particle spray as claimed in claim 1, wherein the plant aroma is one of coffee bean extract, mint extract, lemon extract, blueberry extract, sweet orange extract, honey peach extract, grape extract, grapefruit extract, mandarin orange extract, preserved plum extract and hawthorn extract.
3. The preparation method of the plant-aroma-containing electronic cigarette solid particle spray as claimed in claim 1, wherein the additive comprises the following components in parts by mass: 0.5-5 parts of flavoring agent and 0.2-5 parts of N.2.3 trimethyl-2-isopropyl butanamide.
4. The method for preparing the plant-aroma-containing electronic cigarette solid particle spray according to claim 3, wherein the flavoring agent is one or more of ethyl maltol, ethyl vanillin and linalyl acetate.
5. The preparation method of the plant-aroma-containing electronic cigarette solid particle dispersion as claimed in claim 1, wherein the tobacco extract is prepared by the following method: mixing tobacco raw materials, water and degrading enzyme at 40-50 deg.C, and performing enzymolysis for 4-8 hr to obtain zymolyte; mixing the zymolyte with hansenula polymorpha for anaerobic fermentation to obtain a fermented product; carrying out solid-liquid separation on the fermentation product to obtain a separation liquid; concentrating the separated liquid to obtain fermentation liquid; the density of the fermentation liquor is 1.1-1.4 mg/mL; adsorbing the fermentation liquid, precipitating with mixed ethanol solution of ethanol and propylene glycol, and removing ethanol to obtain tobacco extract.
6. The preparation method of the plant-aroma-containing electronic cigarette solid particle dispersion as claimed in claim 1, wherein the plant aroma is prepared by the following steps: the plant spice extract is prepared by smashing one of coffee beans, mint, lemon, blueberry, sweet orange, juicy peach, grape, grapefruit, green tangerine, preserved plum and hawthorn to obtain a plant raw material, putting the plant raw material into water according to the mass ratio of 1:10, stewing and boiling the plant raw material for 2 hours at 70-75 ℃ in a sealed environment, filtering, retaining filtrate, distilling and concentrating the filtrate.
7. The method for preparing the plant-aroma-containing electronic cigarette solid particle spray is characterized in that the shaping agent comprises 0.05-0.2 part of complexing agent and 5-10 parts of emulsifier, wherein the complexing agent is boric acid, and the emulsifier is at least one of fatty acid monoglyceride, sodium dodecyl sulfate, sucrose fatty acid ester, polyoxyethylene sorbitan fatty acid ester and polyoxyethylene sorbitan fatty acid ester, and is mixed with the rest components to prepare the plant-aroma-containing electronic cigarette solid particle spray.
8. The preparation method of the plant-aroma-containing electronic cigarette solid particle spray as claimed in claim 7, which is characterized by comprising the following steps:
s1: putting glycerol and propylene glycol in the mass parts into 100 parts of water, and uniformly mixing and stirring to obtain an organic solvent;
s2: taking tea powder, a tobacco extract and plant spice according to the mass parts, putting the tea powder, the tobacco extract and the plant spice into the organic solvent obtained in the step S1, uniformly stirring, standing for 24 hours, and filtering to obtain an organic solution;
s3: adding the additive, the complexing agent and the emulsifier in parts by mass into the organic solution obtained in the step S2, and uniformly stirring to obtain a mixed solution;
s4: and (4) adding a weak base solution into the mixed solution obtained in the step S3 until particles are not separated out, filtering out the particles, and drying to obtain the electronic cigarette solid particle atomized matter.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111605293.2A CN113995158A (en) | 2021-12-25 | 2021-12-25 | Preparation method of plant-aroma-containing electronic cigarette solid particle atomized matter |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202111605293.2A CN113995158A (en) | 2021-12-25 | 2021-12-25 | Preparation method of plant-aroma-containing electronic cigarette solid particle atomized matter |
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| CN113995158A true CN113995158A (en) | 2022-02-01 |
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| CN113057363A (en) * | 2019-12-31 | 2021-07-02 | 广东省金叶科技开发有限公司 | Granular tobacco core material and preparation method thereof |
| CN113558273A (en) * | 2021-07-27 | 2021-10-29 | 深圳波顿香料有限公司 | Heating non-combustible smoke pellet and preparation method thereof |
-
2021
- 2021-12-25 CN CN202111605293.2A patent/CN113995158A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2338360A1 (en) * | 2008-09-17 | 2011-06-29 | Yonglin Liang | Alexipharmic cigarette filter material and their praparation |
| CN108669624A (en) * | 2018-05-30 | 2018-10-19 | 重庆中烟工业有限责任公司 | A kind of tobacco extract, preparation method and tobacco product |
| CN113057363A (en) * | 2019-12-31 | 2021-07-02 | 广东省金叶科技开发有限公司 | Granular tobacco core material and preparation method thereof |
| CN113057373A (en) * | 2021-03-16 | 2021-07-02 | 深圳市智叶科技有限公司 | Essential oil particles, preparation method thereof, filter tip and electronic cigarette |
| CN113558273A (en) * | 2021-07-27 | 2021-10-29 | 深圳波顿香料有限公司 | Heating non-combustible smoke pellet and preparation method thereof |
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