CN113907140B - Camel milk powder and preparation method thereof - Google Patents

Camel milk powder and preparation method thereof Download PDF

Info

Publication number
CN113907140B
CN113907140B CN202111318344.3A CN202111318344A CN113907140B CN 113907140 B CN113907140 B CN 113907140B CN 202111318344 A CN202111318344 A CN 202111318344A CN 113907140 B CN113907140 B CN 113907140B
Authority
CN
China
Prior art keywords
parts
biomass charcoal
camel milk
vitamin
milk powder
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN202111318344.3A
Other languages
Chinese (zh)
Other versions
CN113907140A (en
Inventor
刘音波
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Inner Mongolia Sunite Camel Industry Biotechnology Co ltd
Original Assignee
Inner Mongolia Sunite Camel Industry Biotechnology Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Inner Mongolia Sunite Camel Industry Biotechnology Co ltd filed Critical Inner Mongolia Sunite Camel Industry Biotechnology Co ltd
Priority to CN202111318344.3A priority Critical patent/CN113907140B/en
Publication of CN113907140A publication Critical patent/CN113907140A/en
Application granted granted Critical
Publication of CN113907140B publication Critical patent/CN113907140B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C9/00Milk preparations; Milk powder or milk powder preparations
    • A23C9/16Agglomerating or granulating milk powder; Making instant milk powder; Products obtained thereby
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C7/00Other dairy technology
    • A23C7/04Removing unwanted substances other than lactose or milk proteins from milk
    • A23C7/043Removing unwanted substances other than lactose or milk proteins from milk using chemicals in liquid or solid state, e.g. flocculating, adsorbing or extracting agents
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C9/00Milk preparations; Milk powder or milk powder preparations
    • A23C9/152Milk preparations; Milk powder or milk powder preparations containing additives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C9/00Milk preparations; Milk powder or milk powder preparations
    • A23C9/152Milk preparations; Milk powder or milk powder preparations containing additives
    • A23C9/1522Inorganic additives, e.g. minerals, trace elements; Chlorination or fluoridation of milk; Organic salts or complexes of metals other than natrium or kalium; Calcium enrichment of milk
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C9/00Milk preparations; Milk powder or milk powder preparations
    • A23C9/152Milk preparations; Milk powder or milk powder preparations containing additives
    • A23C9/1526Amino acids; Peptides; Protein hydrolysates; Nucleic acids; Derivatives thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C9/00Milk preparations; Milk powder or milk powder preparations
    • A23C9/152Milk preparations; Milk powder or milk powder preparations containing additives
    • A23C9/1528Fatty acids; Mono- or diglycerides; Petroleum jelly; Paraffine; Phospholipids; Derivatives thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C9/00Milk preparations; Milk powder or milk powder preparations
    • A23C9/152Milk preparations; Milk powder or milk powder preparations containing additives
    • A23C9/156Flavoured milk preparations ; Addition of fruits, vegetables, sugars, sugar alcohols or sweeteners
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C9/00Milk preparations; Milk powder or milk powder preparations
    • A23C9/152Milk preparations; Milk powder or milk powder preparations containing additives
    • A23C9/158Milk preparations; Milk powder or milk powder preparations containing additives containing vitamins or antibiotics
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/20Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising free carbon; comprising carbon obtained by carbonising processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/3078Thermal treatment, e.g. calcining or pyrolizing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/32Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/05Preparation or purification of carbon not covered by groups C01B32/15, C01B32/20, C01B32/25, C01B32/30
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00Aspects relating to sorbent materials
    • B01J2220/40Aspects relating to the composition of sorbent or filter aid materials
    • B01J2220/48Sorbents characterised by the starting material used for their preparation
    • B01J2220/4812Sorbents characterised by the starting material used for their preparation the starting material being of organic character
    • B01J2220/4825Polysaccharides or cellulose materials, e.g. starch, chitin, sawdust, wood, straw, cotton
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P60/00Technologies relating to agriculture, livestock or agroalimentary industries
    • Y02P60/80Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
    • Y02P60/87Re-use of by-products of food processing for fodder production

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Nutrition Science (AREA)
  • Biophysics (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • General Chemical & Material Sciences (AREA)
  • Molecular Biology (AREA)
  • Biochemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Dairy Products (AREA)

Abstract

The invention relates to camel milk powder and a preparation method thereof. The camel milk powder comprises the following raw materials in parts by weight: 200-250 parts of fresh camel milk, 10-30 parts of glucose, 10-30 parts of lactose oligosaccharide, 20-50 parts of whey protein, 3-7 parts of whole wheat dietary fiber, 0.8-1.2 parts of lecithin, 0.1-0.3 part of vitamin A, 0.3-0.4 part of vitamin D, 0.15-0.2 part of vitamin E and 0.1-0.2 part of whey calcium. According to the method, on the basis of the existing conventional preparation of camel milk powder, the adsorption step of biomass charcoal is added, so that the content of biomass alkali is effectively reduced, the bitter and fishy smell of the camel milk powder is obviously reduced, and the taste is better. Simultaneously, biomass alkali can be adsorbed in the biomass charcoal more stably by modifying the biomass charcoal, because aluminum sulfate and ferric phosphate enable the biomass alkali to form a more stable complex on the surface of the biomass charcoal.

Description

Camel milk powder and preparation method thereof
Technical Field
The invention relates to camel milk powder and a preparation method thereof.
Background
The camel milk has rich nutrition, low fat content and easy digestion, and is an ideal animal edible drink. The protein content in camel milk is higher than that of milk by more than 3.5%, and the milk fat content is also higher than 6.5%. The camel milk is easy to digest, quick to absorb and stomach-invigorating. The heat content is higher than that of milk, and the milk contains abundant vitamins B1, B2 and C and enough nutrients such as calcium, iron and zinc. The content of vitamin C in camel milk is 3-4 times that of equivalent cow milk, and the insulin content of camel milk is more than 3 times that of equivalent cow milk. In addition, the calcium content of the camel milk is higher than that of cow milk, and the camel milk also contains a large amount of unsaturated fatty acids and B vitamins required by human bodies; the content of iron element is 8 times of that of cow milk. Proved by the fact, the camel milk has good effect on feeding infants, can promote digestion and absorption of intestines and stomach, and can strengthen the body and whiten and lubricate the skin after long-term drinking. Meanwhile, camel milk can treat edema, rheumatism, allergic purpura, dyspepsia and the like. The camel milk can be used for processing traditional dairy products such as milk skin, milk curd, butter and the like, and according to analysis, the camel milk contains casein, lactoferrin, immunoglobulin, vitamins, minerals, fatty acids, amino acids and various bioactive substances. The chemical composition of camel milk is affected by various factors such as camel variety, age, health condition, season, climate, grassland quality, forage supplement, drinking water, management, etc.
The main food of the camel is the prismatic grass, the thorn, the euphorbia lathyris or the reed and the like in the desert or semiarid areas, and the food usually ensures that the camel milk contains a certain amount of alkaloids, namely an organic matter of an azacyclic ring, has alkalinity and specific physiological activities, most of alkaloids have bitter taste and even have certain pungency, and the camel milk has certain bitter taste, so that the taste of the camel milk after processing is influenced to a certain extent.
Disclosure of Invention
The invention provides camel milk powder and a preparation method thereof, which are used for solving the technical problems of bitter taste and poor mouthfeel of camel milk powder.
In order to solve the technical problems, the invention adopts the following technical scheme:
the camel milk powder comprises the following raw materials in parts by weight: 200-250 parts of fresh camel milk, 10-30 parts of glucose, 10-30 parts of lactose oligosaccharide, 20-50 parts of whey protein, 3-7 parts of whole wheat dietary fiber, 0.8-1.2 parts of lecithin, 0.1-0.3 part of vitamin A, 0.3-0.4 part of vitamin D, 0.15-0.2 part of vitamin E and 0.1-0.2 part of whey calcium.
The preparation method of the camel milk powder is characterized by comprising the following steps of:
1. adding 200-250 parts of fresh camel milk into a centrifuge according to parts by weight, centrifugally separating at a rotating speed of 3000-5000 r/min for 20-30 min, keeping the temperature at room temperature during centrifugation, and centrifugally separating to obtain the defatted camel milk.
2. And (3) delivering the defatted camel milk into an adsorption column, wherein the adsorption column is prepared from modified biomass charcoal, and the modified biomass charcoal is prepared by sequentially soaking the biomass charcoal in aluminum sulfate and ferric phosphate solution and then drying.
3. And (3) performing high-pressure sterilization on the defatted camel milk adsorbed in the second step, wherein the sterilization temperature is 60-70 ℃ and the pressure is 80-100MP.
4. Sequentially adding 10-30 parts of glucose, 10-30 parts of lactose oligomer, 20-50 parts of whey protein, 3-7 parts of whole wheat dietary fiber, 0.8-1.2 parts of lecithin, 0.1-0.3 part of vitamin A, 0.3-0.4 part of vitamin D, 0.15-0.2 part of vitamin E and 0.1-0.2 part of whey calcium obtained after sterilization in the step three into a homogenizer for homogenization, wherein the homogenization temperature is 50 ℃.
5. And (3) carrying out vacuum concentration on the homogenized camel milk component, and then carrying out spray granulation to obtain the camel milk powder.
The biomass charcoal raw material is wood or bamboo.
The preparation method of the modified biomass charcoal comprises the following steps:
1. placing the cleaned wood into a calciner, and carbonizing for 2 hours at 350 ℃ to obtain biomass charcoal;
2. after cooling the biomass charcoal, screening the biomass charcoal by using a grinder, wherein the screen mesh is 12 meshes;
3. washing biomass charcoal with deionized water until water is clear, and performing constant-temperature drying at 120 ℃ in an incubator to obtain biomass charcoal;
4. adding biomass charcoal particles into 2000ml of aluminum sulfate solution, soaking for 1 hour, then washing with deionized water, and drying at a constant temperature of 120 ℃ in a constant temperature box to obtain aluminum sulfate modified biomass charcoal;
5. adding the ferric sulfate modified biomass charcoal into the ferric phosphate solution, soaking for 1 hour, then washing with deionized water, and drying at a constant temperature of 120 ℃ in a constant temperature box to obtain the aluminum sulfate and ferric phosphate modified biomass charcoal.
6. Loading aluminum sulfate and ferric phosphate modified biomass charcoal into an adsorption column.
The concentration of the aluminum sulfate is 2-5wt%. The concentration of the ferric phosphate is 2-6wt%.
The invention has the beneficial effects that:
according to the method, on the basis of the existing conventional preparation of camel milk powder, the adsorption step of biomass charcoal is added, so that the content of biomass alkali is effectively reduced, the bitter and fishy smell of the camel milk powder is obviously reduced, and the taste is better. Simultaneously, biomass alkali can be adsorbed in the biomass charcoal more stably by modifying the biomass charcoal, because aluminum sulfate and ferric phosphate enable the biomass alkali to form a more stable complex on the surface of the biomass charcoal.
Detailed Description
For a better understanding of the present invention, reference is made to the following examples, which are included within the scope of the present invention, but are not intended to limit the scope of the present invention.
Example 1
The preparation method of the camel milk powder is characterized by comprising the following steps of:
1. adding 200 parts of fresh camel milk into a centrifuge according to parts by weight, centrifugally separating for 30min at a rotating speed of 3000-5000 r/min, keeping the temperature at room temperature during centrifugation, and centrifugally separating to obtain the defatted camel milk.
2. And (3) delivering the defatted camel milk into an adsorption column, wherein the adsorption column is prepared from modified biomass charcoal, and the modified biomass charcoal is prepared by sequentially soaking the biomass charcoal in aluminum sulfate and ferric phosphate solution and then drying.
3. And (3) performing high-pressure sterilization on the defatted camel milk adsorbed in the second step, wherein the sterilization temperature is 70 ℃ and the pressure is 80MP.
4. Sequentially adding the defatted camel milk, 20 parts of glucose, 200 parts of lactose oligosaccharide, 30 parts of whey protein, 5 parts of whole wheat dietary fiber, 1 part of lecithin, 0.2 part of vitamin A, 0.2 part of vitamin D, 0.2 part of vitamin E and 0.2 part of whey calcium which are obtained after sterilization in the step three into a homogenizer for homogenization, wherein the homogenization temperature is 50 ℃.
5. And (3) carrying out vacuum concentration on the homogenized camel milk component, and then carrying out spray granulation to obtain the camel milk powder.
The preparation method of the modified biomass charcoal comprises the following steps:
1. placing 10kg of cleaned bamboo into a roasting furnace, and carbonizing for 2 hours at 350 ℃ to obtain biomass charcoal;
2. after cooling the biomass charcoal, screening the biomass charcoal by using a grinder, wherein the screen mesh is 12 meshes;
3. washing biomass charcoal with deionized water until water is clear, and performing constant-temperature drying at 120 ℃ in an incubator to obtain biomass charcoal;
4. adding biomass charcoal particles into 2000ml of 2wt% aluminum sulfate solution, soaking for 1 hour, then washing with deionized water, and drying at a constant temperature of 120 ℃ in a constant temperature box to obtain aluminum sulfate modified biomass charcoal;
5. the method comprises the steps of adding ferric sulfate modified biomass charcoal into 2000ml of 3wt% ferric phosphate solution, immersing for 1 hour, then washing with deionized water, and drying at a constant temperature of 120 ℃ in a constant temperature box to obtain aluminum sulfate and ferric phosphate modified biomass charcoal.
6. Loading aluminum sulfate and ferric phosphate modified biomass charcoal into an adsorption column.
Example 2
The preparation method of the camel milk powder is characterized by comprising the following steps of:
1. adding 230 parts of fresh camel milk into a centrifuge according to parts by weight, centrifugally separating for 30min at the rotating speed of 4000 rpm, keeping the temperature at room temperature during centrifugation, and obtaining the defatted camel milk after centrifugal separation.
2. And (3) delivering the defatted camel milk into an adsorption column, wherein the adsorption column is prepared from modified biomass charcoal, and the modified biomass charcoal is prepared by sequentially soaking the biomass charcoal in aluminum sulfate and ferric phosphate solution and then drying.
3. And (3) performing high-pressure sterilization on the defatted camel milk adsorbed in the second step, wherein the sterilization temperature is 65 ℃ and the pressure is 90MP.
4. Sequentially adding the defatted camel milk, 10 parts of glucose, 10 parts of lactose oligosaccharide, 20 parts of whey protein, 3 parts of whole wheat dietary fiber, 0.8 part of lecithin, 0.1 part of vitamin A, 0.3 part of vitamin D, 0.15 part of vitamin E and 0.1 part of whey calcium which are obtained after sterilization in the step three into a homogenizer for homogenization, wherein the homogenization temperature is 50 ℃.
5. And (3) carrying out vacuum concentration on the homogenized camel milk component, and then carrying out spray granulation to obtain the camel milk powder.
The preparation method of the modified biomass charcoal comprises the following steps:
1. placing 10kg of cleaned bamboo into a roasting furnace, and carbonizing for 2 hours at 350 ℃ to obtain biomass charcoal;
2. after cooling the biomass charcoal, screening the biomass charcoal by using a grinder, wherein the screen mesh is 12 meshes;
3. washing biomass charcoal with deionized water until water is clear, and performing constant-temperature drying at 120 ℃ in an incubator to obtain biomass charcoal;
4. adding biomass charcoal particles into 2000ml of 3wt% aluminum sulfate solution, soaking for 1 hour, then washing with deionized water, and drying at a constant temperature of 120 ℃ in a constant temperature box to obtain aluminum sulfate modified biomass charcoal;
5. the method comprises the steps of adding ferric sulfate modified biomass charcoal into 2000ml of 4wt% ferric phosphate solution, immersing for 1 hour, then washing with deionized water, and drying at a constant temperature of 120 ℃ in a constant temperature box to obtain aluminum sulfate and ferric phosphate modified biomass charcoal.
6. Loading aluminum sulfate and ferric phosphate modified biomass charcoal into an adsorption column.
Example 3
The preparation method of the camel milk powder is characterized by comprising the following steps of:
1. adding 250 parts of fresh camel milk into a centrifuge according to parts by weight, centrifugally separating for 30min at the rotating speed of 4000 rpm, keeping the temperature at room temperature during centrifugation, and obtaining the defatted camel milk after centrifugal separation.
2. And (3) delivering the defatted camel milk into an adsorption column, wherein the adsorption column is prepared from modified biomass charcoal, and the modified biomass charcoal is prepared by sequentially soaking the biomass charcoal in aluminum sulfate and ferric phosphate solution and then drying.
3. And (3) performing high-pressure sterilization on the defatted camel milk adsorbed in the second step, wherein the sterilization temperature is 65 ℃ and the pressure is 90MP.
4. Sequentially adding the defatted camel milk, 30 parts of glucose, 30 parts of lactose oligosaccharide, 50 parts of whey protein, 6 parts of whole wheat dietary fiber, 1.2 parts of lecithin, 0.3 part of vitamin A, 0.4 part of vitamin D, 0.2 part of vitamin E and 0.2 part of whey calcium which are obtained after sterilization in the step three into a homogenizer for homogenization, wherein the homogenization temperature is 50 ℃.
5. And (3) carrying out vacuum concentration on the homogenized camel milk component, and then carrying out spray granulation to obtain the camel milk powder.
The preparation method of the modified biomass charcoal comprises the following steps:
1. placing 10kg of cleaned bamboo into a roasting furnace, and carbonizing for 2 hours at 350 ℃ to obtain biomass charcoal;
2. after cooling the biomass charcoal, screening the biomass charcoal by using a grinder, wherein the screen mesh is 12 meshes;
3. washing biomass charcoal with deionized water until water is clear, and performing constant-temperature drying at 120 ℃ in an incubator to obtain biomass charcoal;
4. adding biomass charcoal particles into 2000ml of 5wt% aluminum sulfate solution, soaking for 1 hour, then washing with deionized water, and drying at a constant temperature of 120 ℃ in a constant temperature box to obtain aluminum sulfate modified biomass charcoal;
5. the method comprises the steps of adding ferric sulfate modified biomass charcoal into 2000ml of 6wt% ferric phosphate solution, immersing for 1 hour, then washing with deionized water, and drying at a constant temperature of 120 ℃ in a constant temperature box to obtain aluminum sulfate and ferric phosphate modified biomass charcoal.
6. Loading aluminum sulfate and ferric phosphate modified biomass charcoal into an adsorption column.
Comparative example 1
The preparation method of the camel milk powder is characterized by comprising the following steps of:
1. adding 250 parts of fresh camel milk into a centrifuge according to parts by weight, centrifugally separating for 30min at the rotating speed of 4000 rpm, keeping the temperature at room temperature during centrifugation, and obtaining the defatted camel milk after centrifugal separation.
2. And (3) performing high-pressure sterilization on the defatted camel milk adsorbed in the second step, wherein the sterilization temperature is 65 ℃ and the pressure is 90MP.
3. Sequentially adding the defatted camel milk, 30 parts of glucose, 30 parts of lactose oligosaccharide, 50 parts of whey protein, 6 parts of whole wheat dietary fiber, 1.2 parts of lecithin, 0.3 part of vitamin A, 0.4 part of vitamin D, 0.2 part of vitamin E and 0.2 part of whey calcium which are obtained after sterilization in the step three into a homogenizer for homogenization, wherein the homogenization temperature is 50 ℃.
4. And (3) carrying out vacuum concentration on the homogenized camel milk component, and then carrying out spray granulation to obtain the camel milk powder.
Comparative example 2
The preparation method of the camel milk powder is characterized by comprising the following steps of:
1. adding 250 parts of fresh camel milk into a centrifuge according to parts by weight, centrifugally separating for 30min at the rotating speed of 4000 rpm, keeping the temperature at room temperature during centrifugation, and obtaining the defatted camel milk after centrifugal separation.
2. And (3) delivering the defatted camel milk into an adsorption column, wherein the adsorption column is filled with adsorption materials such as biomass charcoal, and the biomass charcoal is unmodified biomass charcoal.
3. And (3) performing high-pressure sterilization on the defatted camel milk adsorbed in the second step, wherein the sterilization temperature is 65 ℃ and the pressure is 90MP.
4. Sequentially adding the defatted camel milk, 30 parts of glucose, 30 parts of lactose oligosaccharide, 50 parts of whey protein, 6 parts of whole wheat dietary fiber, 1.2 parts of lecithin, 0.3 part of vitamin A, 0.4 part of vitamin D, 0.2 part of vitamin E and 0.2 part of whey calcium which are obtained after sterilization in the step three into a homogenizer for homogenization, wherein the homogenization temperature is 50 ℃.
5. And (3) carrying out vacuum concentration on the homogenized camel milk component, and then carrying out spray granulation to obtain the camel milk powder.
The preparation method of the modified biomass charcoal comprises the following steps:
1. placing 10kg of cleaned bamboo into a roasting furnace, and carbonizing for 2 hours at 350 ℃ to obtain biomass charcoal;
2. after cooling the biomass charcoal, screening the biomass charcoal by using a grinder, wherein the screen mesh is 12 meshes;
3. washing biomass charcoal with deionized water until water is clear, and performing constant-temperature drying at 120 ℃ in an incubator to obtain biomass charcoal;
4. loading the aluminum sulfate modified biomass charcoal into an adsorption column.
Comparative example 3
The preparation method of the camel milk powder is characterized by comprising the following steps of:
1. adding 250 parts of fresh camel milk into a centrifuge according to parts by weight, centrifugally separating for 30min at the rotating speed of 4000 rpm, keeping the temperature at room temperature during centrifugation, and obtaining the defatted camel milk after centrifugal separation.
2. And (3) delivering the defatted camel milk into an adsorption column, wherein the adsorption column is prepared from modified biomass charcoal, and the modified biomass charcoal is prepared by soaking the biomass charcoal in an aluminum sulfate solution and then drying.
3. And (3) performing high-pressure sterilization on the defatted camel milk adsorbed in the second step, wherein the sterilization temperature is 65 ℃ and the pressure is 90MP.
4. Sequentially adding the defatted camel milk, 30 parts of glucose, 30 parts of lactose oligosaccharide, 50 parts of whey protein, 6 parts of whole wheat dietary fiber, 1.2 parts of lecithin, 0.3 part of vitamin A, 0.4 part of vitamin D, 0.2 part of vitamin E and 0.2 part of whey calcium which are obtained after sterilization in the step three into a homogenizer for homogenization, wherein the homogenization temperature is 50 ℃.
5. And (3) carrying out vacuum concentration on the homogenized camel milk component, and then carrying out spray granulation to obtain the camel milk powder.
The preparation method of the modified biomass charcoal comprises the following steps:
1. placing 10kg of cleaned bamboo into a roasting furnace, and carbonizing for 2 hours at 350 ℃ to obtain biomass charcoal;
2. after cooling the biomass charcoal, screening the biomass charcoal by using a grinder, wherein the screen mesh is 12 meshes;
3. washing biomass charcoal with deionized water until water is clear, and performing constant-temperature drying at 120 ℃ in an incubator to obtain biomass charcoal;
4. adding biomass charcoal particles into 2000ml of 5wt% aluminum sulfate solution, soaking for 1 hour, then washing with deionized water, and drying at a constant temperature of 120 ℃ in a constant temperature box to obtain aluminum sulfate modified biomass charcoal;
5. loading the aluminum sulfate modified biomass charcoal into an adsorption column.
Comparative example 4
The preparation method of the camel milk powder is characterized by comprising the following steps of:
1. adding 250 parts of fresh camel milk into a centrifuge according to parts by weight, centrifugally separating for 30min at the rotating speed of 4000 rpm, keeping the temperature at room temperature during centrifugation, and obtaining the defatted camel milk after centrifugal separation.
2. And (3) delivering the defatted camel milk into an adsorption column, wherein the adsorption column is prepared from modified biomass charcoal, and the modified biomass charcoal is prepared by sequentially drying the biomass charcoal in the form of ferric phosphate solution.
3. And (3) performing high-pressure sterilization on the defatted camel milk adsorbed in the second step, wherein the sterilization temperature is 65 ℃ and the pressure is 90MP.
4. Sequentially adding the defatted camel milk, 30 parts of glucose, 30 parts of lactose oligosaccharide, 50 parts of whey protein, 6 parts of whole wheat dietary fiber, 1.2 parts of lecithin, 0.3 part of vitamin A, 0.4 part of vitamin D, 0.2 part of vitamin E and 0.2 part of whey calcium which are obtained after sterilization in the step three into a homogenizer for homogenization, wherein the homogenization temperature is 50 ℃.
5. And (3) carrying out vacuum concentration on the homogenized camel milk component, and then carrying out spray granulation to obtain the camel milk powder.
The preparation method of the modified biomass charcoal comprises the following steps:
1. placing 10kg of cleaned bamboo into a roasting furnace, and carbonizing for 2 hours at 350 ℃ to obtain biomass charcoal;
2. after cooling the biomass charcoal, screening the biomass charcoal by using a grinder, wherein the screen mesh is 12 meshes;
3. washing biomass charcoal with deionized water until water is clear, and performing constant-temperature drying at 120 ℃ in an incubator to obtain biomass charcoal;
5. the biomass charcoal is added into 2000ml of 6wt% ferric phosphate solution to be soaked for 1 hour, then the biomass charcoal is washed by deionized water, and the biomass charcoal is dried at the constant temperature of 120 ℃ in a constant temperature box to obtain the ferric phosphate modified biomass charcoal.
6. Loading the ferric phosphate modified biomass charcoal into an adsorption column.
The method for alkaloid content comprises the following steps:
for the defatted camel milk in the first step, an alkaloid extraction method commonly used in the art, such as an aqueous solution extraction method, an organic solvent extraction method, a percolation extraction method, a supercritical fluid extraction method, and the like, may be used, and since the present application is a defatted camel milk, an alcohol solvent extraction method is used, wherein a 75% ethanol solution is used as an extractant. Table 1 shows the alkaloid content of the camel milk after degreasing of examples 1-3 and comparative examples 1-3.
TABLE 1
Alkaloid content (mg/kg)
Example 1 0.39
Example 2 0.31
Example 3 0.26
Comparative example 1 0.85
Comparative example 2 0.67
Comparative example 3 0.56
Comparative example 4 0.53
Since comparative examples 1 to 4 used the same conditions as in example 3, it was confirmed by comparing comparative example 1 with examples 1 to 3 that the biomass content in the modified biochar-treated defatted camel milk was significantly reduced. By comparing the comparative example 1 with the comparative examples 2, 3 and 4, it can be determined that the modified or unmodified biomass charcoal has an effect of reducing alkaloids in the defatted camel milk, and the modified effect is more obvious; comparing comparative examples 1-4 with example 3, it was determined that the effect of reducing alkaloids in skim camel milk by aluminum sulfate and ferric phosphate modified biomass charcoal was most pronounced.
The protection scope of the present invention is not limited to the above embodiments, and all technical solutions belonging to the concept of the present invention belong to the protection scope of the present invention. It should be noted that modifications and adaptations to the present invention may occur to one skilled in the art without departing from the principles of the present invention and are intended to be within the scope of the present invention.

Claims (4)

1. A preparation method of camel milk powder is characterized in that:
the camel milk powder comprises the following raw materials in parts by weight: 200-250 parts of fresh camel milk, 10-30 parts of glucose, 10-30 parts of lactose oligosaccharide, 20-50 parts of whey protein, 3-7 parts of whole wheat dietary fiber, 0.8-1.2 parts of lecithin, 0.1-0.3 part of vitamin A, 0.3-0.4 part of vitamin D, 0.15-0.2 part of vitamin E and 0.1-0.2 part of whey calcium;
the method comprises the following steps:
1. adding 200-250 parts of fresh camel milk into a centrifuge according to parts by weight, centrifugally separating at a rotating speed of 3000-5000 r/min for 20-30 min, keeping the temperature at room temperature during centrifugation, and obtaining defatted camel milk after centrifugal separation;
2. the defatted camel milk is sent into an adsorption column, wherein the adsorption column is made of modified biomass charcoal, and the modified biomass charcoal is obtained by sequentially soaking the biomass charcoal in aluminum sulfate and ferric phosphate solution and then drying;
3. sterilizing the defatted camel milk adsorbed in the second step under high pressure at 60-70 ℃ and 80-100MP;
4. sequentially adding the defatted camel milk obtained after sterilization in the step three, 10-30 parts of glucose, 10-30 parts of lactose oligomer, 20-50 parts of whey protein, 3-7 parts of whole wheat dietary fiber, 0.8-1.2 parts of lecithin, 0.1-0.3 part of vitamin A, 0.3-0.4 part of vitamin D, 0.15-0.2 part of vitamin E and 0.1-0.2 part of whey calcium into a homogenizer for homogenization, wherein the homogenization temperature is 50 ℃;
5. vacuum concentrating the homogenized camel milk component, and then performing spray granulation to obtain camel milk powder.
2. The method for preparing camel milk powder according to claim 1, characterized in that the method for preparing the modified biomass charcoal comprises the following steps:
1. placing the cleaned wood into a calciner, and carbonizing for 2 hours at 350 ℃ to obtain biomass charcoal;
2. after cooling the biomass charcoal, screening the biomass charcoal by using a grinder, wherein the screen mesh is 12 meshes;
3. washing biomass charcoal with deionized water until water is clear, and performing constant-temperature drying at 120 ℃ in an incubator to obtain biomass charcoal;
4. adding the biomass charcoal obtained in the step 3 into 2000ml of aluminum sulfate solution, soaking for 1 hour, then washing with deionized water, and drying at a constant temperature of 120 ℃ in a constant temperature box to obtain aluminum sulfate modified biomass charcoal;
5. adding aluminum sulfate modified biomass charcoal into ferric phosphate solution, soaking for 1 hour, then washing with deionized water, and drying at constant temperature under the condition of a constant temperature oven at 120 ℃ to obtain aluminum sulfate and ferric phosphate modified biomass charcoal;
6. loading aluminum sulfate and ferric phosphate modified biomass charcoal into an adsorption column.
3. The method for preparing camel milk powder according to claim 1, wherein the raw material of the biomass charcoal is wood or bamboo.
4. A method of preparing camel milk powder according to claim 1, characterized in that the concentration of aluminium sulphate is 2-5wt% and the concentration of iron phosphate is 2-6wt%.
CN202111318344.3A 2021-11-09 2021-11-09 Camel milk powder and preparation method thereof Active CN113907140B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202111318344.3A CN113907140B (en) 2021-11-09 2021-11-09 Camel milk powder and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202111318344.3A CN113907140B (en) 2021-11-09 2021-11-09 Camel milk powder and preparation method thereof

Publications (2)

Publication Number Publication Date
CN113907140A CN113907140A (en) 2022-01-11
CN113907140B true CN113907140B (en) 2023-08-08

Family

ID=79245754

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202111318344.3A Active CN113907140B (en) 2021-11-09 2021-11-09 Camel milk powder and preparation method thereof

Country Status (1)

Country Link
CN (1) CN113907140B (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106111060A (en) * 2016-07-11 2016-11-16 中南大学 A kind of modification biological carbon composite and preparation thereof and application
CN107996715A (en) * 2017-12-10 2018-05-08 长沙无道工业设计有限公司 A kind of camel milk formula and preparation method thereof
CN113019326A (en) * 2021-03-15 2021-06-25 中南大学 Iron-based-carboxyl modified biochar and preparation method and application thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106111060A (en) * 2016-07-11 2016-11-16 中南大学 A kind of modification biological carbon composite and preparation thereof and application
CN107996715A (en) * 2017-12-10 2018-05-08 长沙无道工业设计有限公司 A kind of camel milk formula and preparation method thereof
CN113019326A (en) * 2021-03-15 2021-06-25 中南大学 Iron-based-carboxyl modified biochar and preparation method and application thereof

Also Published As

Publication number Publication date
CN113907140A (en) 2022-01-11

Similar Documents

Publication Publication Date Title
CN103027126B (en) Fermented soybean milk clear juice beverage, high protein viable organism chewable tablet and preparation method thereof
CN110537583A (en) Preparation method of Chinese yam yoghourt
CN113812461A (en) Method for producing yoghourt by two-stage fermentation and probiotic herbal yoghourt
CN113907140B (en) Camel milk powder and preparation method thereof
CN102805150A (en) Live bacteria type lotus seed and corn yoghurt beverage and preparation method thereof
CN112167343A (en) Preparation method of oat yogurt
CN111466441A (en) Instant milk cubilose and preparation method thereof
CN109169897A (en) A kind of donkey fresh milk and its manufacture craft and method
RU2386260C1 (en) Production method of fermented milk drink "acidophilous honey"
CN101816333B (en) Defatted and desugared nutritional formula milk powder and preparation method thereof
CN114514949A (en) Preparation method of nut plant-based fermented milk
CN103300153B (en) Bean beverage and preparation method thereof
CN112841320A (en) Double-embryo vegetable protein beverage and preparation method thereof
CN112155140A (en) Turbid pumpkin fermented beverage added with compound protein and preparation method thereof
CN104905101A (en) Arbutus jam and preparation method thereof
CN110881523A (en) Fingered citron, Chinese yam and poria cocos yoghourt and preparation method thereof
CN110800911A (en) Soybean water lactobacillus dry cargo rehydration agent and preparation method thereof
CN1241496C (en) Fish milk product and its production process
CN107646973A (en) A kind of wormwood Yoghourt and preparation method thereof
CN109329437A (en) A kind of preparation process with burnt odor taste Walnut Milk
CN111480752A (en) Fermented coconut water beverage base material, fermented coconut water beverage and preparation method thereof
CN109258811A (en) A kind of jujube spirulina composite yoghourt and its preparation process
CN107821769A (en) A kind of duckling feed and preparation method thereof
CN106343083B (en) Pickled vegetable flavored sour tea beverage and preparation method thereof
CN105767179A (en) Walnut kernel brain tonifying blueberry yoghourt and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant