CN113735057A - 一种免活化储氢材料及其制备方法和装置 - Google Patents
一种免活化储氢材料及其制备方法和装置 Download PDFInfo
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- CN113735057A CN113735057A CN202111014637.2A CN202111014637A CN113735057A CN 113735057 A CN113735057 A CN 113735057A CN 202111014637 A CN202111014637 A CN 202111014637A CN 113735057 A CN113735057 A CN 113735057A
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- 239000001257 hydrogen Substances 0.000 title claims abstract description 130
- 229910052739 hydrogen Inorganic materials 0.000 title claims abstract description 130
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 title claims abstract description 129
- 239000011232 storage material Substances 0.000 title claims abstract description 58
- 238000002360 preparation method Methods 0.000 title claims abstract description 36
- 239000000956 alloy Substances 0.000 claims abstract description 104
- 229910045601 alloy Inorganic materials 0.000 claims abstract description 99
- 239000000843 powder Substances 0.000 claims abstract description 45
- 229910052751 metal Inorganic materials 0.000 claims abstract description 40
- 239000002184 metal Substances 0.000 claims abstract description 40
- 238000003723 Smelting Methods 0.000 claims abstract description 31
- 238000002156 mixing Methods 0.000 claims abstract description 28
- 238000000137 annealing Methods 0.000 claims abstract description 20
- 239000000463 material Substances 0.000 claims abstract description 20
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 16
- 238000007873 sieving Methods 0.000 claims abstract description 16
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims abstract description 6
- 238000003860 storage Methods 0.000 claims description 61
- 238000006243 chemical reaction Methods 0.000 claims description 59
- 230000004048 modification Effects 0.000 claims description 42
- 238000012986 modification Methods 0.000 claims description 42
- 239000012298 atmosphere Substances 0.000 claims description 24
- 238000000034 method Methods 0.000 claims description 21
- 238000001035 drying Methods 0.000 claims description 16
- 230000001681 protective effect Effects 0.000 claims description 15
- 239000007788 liquid Substances 0.000 claims description 12
- 229910000531 Co alloy Inorganic materials 0.000 claims description 11
- 238000011049 filling Methods 0.000 claims description 11
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 11
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 11
- 239000007787 solid Substances 0.000 claims description 11
- 239000001307 helium Substances 0.000 claims description 10
- 229910052734 helium Inorganic materials 0.000 claims description 10
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 claims description 10
- 239000010936 titanium Substances 0.000 claims description 9
- GYHNNYVSQQEPJS-UHFFFAOYSA-N Gallium Chemical compound [Ga] GYHNNYVSQQEPJS-UHFFFAOYSA-N 0.000 claims description 8
- 229910001069 Ti alloy Inorganic materials 0.000 claims description 8
- 229910052733 gallium Inorganic materials 0.000 claims description 8
- YXUQHTDQKKCWNG-UHFFFAOYSA-N gallium titanium Chemical compound [Ti].[Ga] YXUQHTDQKKCWNG-UHFFFAOYSA-N 0.000 claims description 8
- 229910052742 iron Inorganic materials 0.000 claims description 8
- 239000011572 manganese Substances 0.000 claims description 8
- 230000007246 mechanism Effects 0.000 claims description 8
- 229910052759 nickel Inorganic materials 0.000 claims description 8
- 238000000926 separation method Methods 0.000 claims description 8
- 229910052684 Cerium Inorganic materials 0.000 claims description 7
- 239000012300 argon atmosphere Substances 0.000 claims description 7
- 238000000967 suction filtration Methods 0.000 claims description 7
- 229910052720 vanadium Inorganic materials 0.000 claims description 7
- 229910052726 zirconium Inorganic materials 0.000 claims description 7
- 229910001080 W alloy Inorganic materials 0.000 claims description 6
- 238000000498 ball milling Methods 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 239000003607 modifier Substances 0.000 claims description 6
- 239000002245 particle Substances 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 229910052719 titanium Inorganic materials 0.000 claims description 6
- 229910000640 Fe alloy Inorganic materials 0.000 claims description 4
- 239000002202 Polyethylene glycol Substances 0.000 claims description 4
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 4
- JSUIEZRQVIVAMP-UHFFFAOYSA-N gallium iron Chemical compound [Fe].[Ga] JSUIEZRQVIVAMP-UHFFFAOYSA-N 0.000 claims description 4
- 239000004519 grease Substances 0.000 claims description 4
- 229910052748 manganese Inorganic materials 0.000 claims description 4
- 229920001223 polyethylene glycol Polymers 0.000 claims description 4
- 229920001296 polysiloxane Polymers 0.000 claims description 4
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 4
- 238000012216 screening Methods 0.000 claims description 4
- 239000010935 stainless steel Substances 0.000 claims description 4
- 229910001220 stainless steel Inorganic materials 0.000 claims description 4
- 238000005538 encapsulation Methods 0.000 claims description 3
- 238000002844 melting Methods 0.000 claims description 3
- 230000008018 melting Effects 0.000 claims description 3
- 150000002739 metals Chemical class 0.000 claims description 3
- 239000006258 conductive agent Substances 0.000 claims description 2
- 230000004913 activation Effects 0.000 abstract description 12
- 230000009467 reduction Effects 0.000 abstract description 9
- 238000005984 hydrogenation reaction Methods 0.000 abstract description 8
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract description 6
- 230000007547 defect Effects 0.000 abstract description 6
- 239000001301 oxygen Substances 0.000 abstract description 6
- 229910052760 oxygen Inorganic materials 0.000 abstract description 6
- 238000002161 passivation Methods 0.000 abstract description 6
- 239000002994 raw material Substances 0.000 description 9
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 7
- 229910052802 copper Inorganic materials 0.000 description 7
- 239000010949 copper Substances 0.000 description 7
- 238000010521 absorption reaction Methods 0.000 description 6
- 238000004806 packaging method and process Methods 0.000 description 6
- 230000008569 process Effects 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 5
- 239000002131 composite material Substances 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 5
- 239000002803 fossil fuel Substances 0.000 description 5
- 229910052761 rare earth metal Inorganic materials 0.000 description 5
- 150000002910 rare earth metals Chemical class 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 230000009286 beneficial effect Effects 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 238000005266 casting Methods 0.000 description 3
- 238000003795 desorption Methods 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 241000282414 Homo sapiens Species 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 150000002431 hydrogen Chemical class 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 238000011031 large-scale manufacturing process Methods 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 125000004429 atom Chemical group 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000010981 drying operation Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000003682 fluorination reaction Methods 0.000 description 1
- 150000004678 hydrides Chemical class 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 229910001404 rare earth metal oxide Inorganic materials 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000009489 vacuum treatment Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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Classifications
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
- C01B3/0005—Reversible uptake of hydrogen by an appropriate medium, i.e. based on physical or chemical sorption phenomena or on reversible chemical reactions, e.g. for hydrogen storage purposes ; Reversible gettering of hydrogen; Reversible uptake of hydrogen by electrodes
- C01B3/001—Reversible uptake of hydrogen by an appropriate medium, i.e. based on physical or chemical sorption phenomena or on reversible chemical reactions, e.g. for hydrogen storage purposes ; Reversible gettering of hydrogen; Reversible uptake of hydrogen by electrodes characterised by the uptaking medium; Treatment thereof
- C01B3/0031—Intermetallic compounds; Metal alloys; Treatment thereof
- C01B3/0047—Intermetallic compounds; Metal alloys; Treatment thereof containing a rare earth metal; Treatment thereof
- C01B3/0057—Intermetallic compounds; Metal alloys; Treatment thereof containing a rare earth metal; Treatment thereof also containing nickel
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/02—Making metallic powder or suspensions thereof using physical processes
- B22F9/04—Making metallic powder or suspensions thereof using physical processes starting from solid material, e.g. by crushing, grinding or milling
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
- C01B3/0005—Reversible uptake of hydrogen by an appropriate medium, i.e. based on physical or chemical sorption phenomena or on reversible chemical reactions, e.g. for hydrogen storage purposes ; Reversible gettering of hydrogen; Reversible uptake of hydrogen by electrodes
- C01B3/001—Reversible uptake of hydrogen by an appropriate medium, i.e. based on physical or chemical sorption phenomena or on reversible chemical reactions, e.g. for hydrogen storage purposes ; Reversible gettering of hydrogen; Reversible uptake of hydrogen by electrodes characterised by the uptaking medium; Treatment thereof
- C01B3/0031—Intermetallic compounds; Metal alloys; Treatment thereof
- C01B3/0047—Intermetallic compounds; Metal alloys; Treatment thereof containing a rare earth metal; Treatment thereof
- C01B3/0052—Intermetallic compounds; Metal alloys; Treatment thereof containing a rare earth metal; Treatment thereof also containing titanium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/02—Making non-ferrous alloys by melting
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C14/00—Alloys based on titanium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C28/00—Alloys based on a metal not provided for in groups C22C5/00 - C22C27/00
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C30/00—Alloys containing less than 50% by weight of each constituent
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C2202/00—Physical properties
- C22C2202/04—Hydrogen absorbing
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/32—Hydrogen storage
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Combustion & Propulsion (AREA)
- Inorganic Chemistry (AREA)
- Environmental & Geological Engineering (AREA)
- Powder Metallurgy (AREA)
Abstract
Description
Claims (10)
Priority Applications (1)
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CN202111014637.2A CN113735057A (zh) | 2021-08-31 | 2021-08-31 | 一种免活化储氢材料及其制备方法和装置 |
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Citations (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0726301A (ja) * | 1993-07-09 | 1995-01-27 | Mazda Motor Corp | 水素吸蔵材及びその製造方法 |
JPH08162108A (ja) * | 1994-11-30 | 1996-06-21 | Sanyo Electric Co Ltd | アルカリ蓄電池用水素吸蔵合金の保存方法 |
US5885378A (en) * | 1995-07-12 | 1999-03-23 | Mitsubishi Materials Corporation | Hydrogen occluding alloy and electrode made of the alloy |
US6461766B1 (en) * | 1998-08-27 | 2002-10-08 | Ovonic Battery Company, Inc. | Hydrogen storage powder and process for preparing the same |
JP2004360037A (ja) * | 2003-06-06 | 2004-12-24 | Toyota Central Res & Dev Lab Inc | 水素吸蔵合金および水素吸蔵材料 |
CN2861702Y (zh) * | 2005-10-08 | 2007-01-24 | 北京有色金属研究总院 | 金属氢化物储氢装置 |
CN101108331A (zh) * | 2006-07-17 | 2008-01-23 | 北京有色金属研究总院 | 一种配位氢化物催化可逆贮氢材料及其制备方法 |
CN103145098A (zh) * | 2013-03-04 | 2013-06-12 | 长安大学 | 一种固态储氢材料及其制备方法 |
CN106566965A (zh) * | 2016-10-31 | 2017-04-19 | 安泰科技股份有限公司 | 一种聚合物包覆的纳米镁基储氢材料及其制备方法 |
CN110106426A (zh) * | 2019-04-29 | 2019-08-09 | 北京铂陆氢能科技开发有限公司 | 易活化储氢合金、其制造方法以及熔炼设备 |
CN110405219A (zh) * | 2019-07-29 | 2019-11-05 | 四川大学 | 高功率储氢合金粉末的制备方法及高功率储氢合金粉末 |
CN111636012A (zh) * | 2020-05-20 | 2020-09-08 | 有研工程技术研究院有限公司 | 一种La-Mg-Ni系储氢材料及其制备方法 |
CN113148947A (zh) * | 2021-03-03 | 2021-07-23 | 中国科学院江西稀土研究院 | 一种稀土合金储氢材料及其制备方法 |
-
2021
- 2021-08-31 CN CN202111014637.2A patent/CN113735057A/zh active Pending
Patent Citations (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0726301A (ja) * | 1993-07-09 | 1995-01-27 | Mazda Motor Corp | 水素吸蔵材及びその製造方法 |
JPH08162108A (ja) * | 1994-11-30 | 1996-06-21 | Sanyo Electric Co Ltd | アルカリ蓄電池用水素吸蔵合金の保存方法 |
US5885378A (en) * | 1995-07-12 | 1999-03-23 | Mitsubishi Materials Corporation | Hydrogen occluding alloy and electrode made of the alloy |
US6461766B1 (en) * | 1998-08-27 | 2002-10-08 | Ovonic Battery Company, Inc. | Hydrogen storage powder and process for preparing the same |
JP2004360037A (ja) * | 2003-06-06 | 2004-12-24 | Toyota Central Res & Dev Lab Inc | 水素吸蔵合金および水素吸蔵材料 |
CN2861702Y (zh) * | 2005-10-08 | 2007-01-24 | 北京有色金属研究总院 | 金属氢化物储氢装置 |
CN101108331A (zh) * | 2006-07-17 | 2008-01-23 | 北京有色金属研究总院 | 一种配位氢化物催化可逆贮氢材料及其制备方法 |
CN103145098A (zh) * | 2013-03-04 | 2013-06-12 | 长安大学 | 一种固态储氢材料及其制备方法 |
CN106566965A (zh) * | 2016-10-31 | 2017-04-19 | 安泰科技股份有限公司 | 一种聚合物包覆的纳米镁基储氢材料及其制备方法 |
CN110106426A (zh) * | 2019-04-29 | 2019-08-09 | 北京铂陆氢能科技开发有限公司 | 易活化储氢合金、其制造方法以及熔炼设备 |
CN110405219A (zh) * | 2019-07-29 | 2019-11-05 | 四川大学 | 高功率储氢合金粉末的制备方法及高功率储氢合金粉末 |
CN111636012A (zh) * | 2020-05-20 | 2020-09-08 | 有研工程技术研究院有限公司 | 一种La-Mg-Ni系储氢材料及其制备方法 |
CN113148947A (zh) * | 2021-03-03 | 2021-07-23 | 中国科学院江西稀土研究院 | 一种稀土合金储氢材料及其制备方法 |
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Inventor after: Wang Bin Inventor after: Wang Zhigao Inventor after: Wu Hailei Inventor after: Zhong Miao Inventor before: Wang Bin Inventor before: Wang Zhigao Inventor before: Wu Hailei Inventor before: Ma Chuanlong Inventor before: Zhong Miao |
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