CN113693989B - A Chinese medicinal composition for eliminating turbid pathogen and relieving itching, and its application in personal care product - Google Patents
A Chinese medicinal composition for eliminating turbid pathogen and relieving itching, and its application in personal care product Download PDFInfo
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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Abstract
The invention provides a traditional Chinese medicine composition for removing turbid and relieving itching and application thereof in personal care products, wherein the traditional Chinese medicine composition comprises the following components: cortex Phellodendri extract, folium Citri Grandis extract, lantana leaf extract, folium Eriobotryae extract and flos Lonicerae extract. The traditional Chinese medicine composition has the effect of relieving itching, and is applied to personal care products, and has good effect of relieving itching, safety, low toxic and side effects and low irritation.
Description
Technical Field
The invention relates to the technical field of traditional Chinese medicine nursing products, in particular to a traditional Chinese medicine composition for removing turbid and relieving itching and application of the traditional Chinese medicine composition to personal care products.
Background
Personal care products are a type of daily product that can be divided into: bathing articles, shampoo articles and hand washing articles. Conventional personal care products have limited functionality to the human body, and in order to broaden the functionality of the personal care products to the human body, people have been provided with chemical substances having corresponding functions in the personal care products so that some personal care products have other additional functions, such as itching relieving personal care products, in addition to the basic personal care functions.
At present, chemical bactericides such as ketoconazole, zinc pyrithione, hexamidine di (hydroxyethyl sulfonate), ganbazole, pyridone ethanolamine salt, triclosan and the like are mainly added into the itching relieving personal care products on the market, and most of the chemical bactericides are high in irritation and harmful to health after long-term use. And with the continuous development of economy, consumers pay more and more attention to the safety of products, so that natural and safe products are more and more favored. Therefore, a personal care product added with a natural, safe and turbidity-expelling and itching-relieving substance would be more suitable for consumers, and is favored.
Disclosure of Invention
The invention provides a traditional Chinese medicine composition for removing turbid and relieving itching and application thereof to personal care products.
In order to achieve the above purpose, the invention adopts the following technical scheme:
a traditional Chinese medicine composition for removing turbid and relieving itching comprises the following components in parts by weight: the wampee tree extract, the grapefruit leaf extract, the lantana leaf extract, the loquat leaf extract and the honeysuckle flower extract are respectively 0.5-2:1.5-3:1.5-3:0.5-2:0.5-2.
Preferably, the turbidity-removing itching-relieving traditional Chinese medicine composition comprises the following components in parts by weight: the wampee tree extract, the grapefruit leaf extract, the lantana leaf extract, the loquat leaf extract and the honeysuckle flower extract are respectively 0.5-2:1.5-3:1.5-3:0.5-2:0.5-2.
Preferably, the wampee tree extract is wampee tree leaf extract.
The invention also provides application of the turbidity-removing itching-relieving traditional Chinese medicine composition in personal care products.
Preferably, the personal care product comprises a bath product, a shampoo product, a hand wash product, a body care product, a soap cosmetic.
Preferably, the soap cosmetics include perfumed soaps, handmade soaps and liquid soaps.
Preferably, the weight percentage of the traditional Chinese medicine composition for eliminating turbid and relieving itching in the personal care product is 1-30%.
More preferably, the weight percentage of the traditional Chinese medicine composition for eliminating turbid and relieving itching in the personal care product is 1-10%.
The Chinese medicine is called wampee tree, is a plant of the genus phellodendron of the family ruaceae, and can be used as a medicine. The invention preferably uses the extract of the wampee tree leaves, which has the effects of expelling turbidity, relieving exterior syndrome, dissipating heat, dispelling wind and removing toxin (heat toxin, mange and snake and insect bites).
The pomelo leaf extract disclosed by the invention can remove toxic materials and detumescence (mastitis and tonsillitis), and has the effects of removing turbid and detoxifying.
The lantana camara is named as lantana camara, and the Chinese medicinal materials are lantana camara, common sage herb, ruyi grass and lantana camara, and are dicotyledoneae plants. The whole plant of the root, leaf and flower can be used as medicine, and the whole plant extract has the effects of clearing heat and detoxicating, resolving hard mass and relieving pain, dispelling wind and relieving itching.
The loquat of the invention is prepared from loquat, chinese medicinal herbs such as Jinwan, rumex, lu Jie, lu Ju, etc. and is a plant of the genus Eriobotrya of the family Rosaceae. The folium Eriobotryae extract has effects of clearing heat and detoxicating.
The honeysuckle, the Chinese medicinal name honeysuckle, the honeysuckle stem, the bicolor flower stem, the Erbao stem, the right-turn stem and the like are plants of the lonicera genus of the honeysuckle family. The honeysuckle has the effects of clearing heat and detoxicating, resisting inflammation, tonifying deficiency and treating wind, and is mainly used for treating distending and fullness diseases, warm diseases and fever, heat toxin carbuncle and ulcer, tumor and other symptoms. The honeysuckle flower external application has a certain treatment effect on skin itch such as eczema of children and the like.
The bath product is bath foam/dew/oil/cream/gel/foam, foot bath liquid, hand cleanser or hand soap.
The shampoo product is shampoo/liquid/cream or shampoo soap.
The body skin care product is body milk/essence cream/essence.
The invention provides a preferable extraction method, which comprises the steps of mixing and crushing corresponding compound traditional Chinese medicines according to weight ratio, heating and refluxing with 70-80 vol.% ethanol with the amount of 3-5 times for extraction, and then concentrating the extracting solution under reduced pressure and drying the extracting solution into powder; of course, the extraction method is not limited to the above method, and extraction may be performed by supercritical extraction, ultrasonic extraction, or the like; the extractant or extractant is not limited to ethanol, and may be extracted or extracted with water or other substances.
In addition, the above-mentioned Chinese medicinal extract used in the present invention is preferably pure extract powder with 100% of the corresponding active ingredient, but is not limited to extract powder, but may be other forms such as extract solution or extract, etc., and when applied to personal care products in other forms, the addition amount in the formulation should be converted into the amount of pure extract form disclosed in the present invention.
By adopting the technical scheme, the invention has the beneficial effects that:
the itching relieving auxiliary component adopted by the invention is a turbidity-removing itching relieving traditional Chinese medicine composition, namely five traditional Chinese medicine mixed extracts of a wampee tree extract, a shaddock leaf extract, a lantana leaf extract, a loquat leaf extract and a honeysuckle flower extract. The wampee tree extract plays roles in expelling turbidity, relieving exterior syndrome, dissipating heat, dispelling wind and removing toxin in the formula, the pomelo leaf extract plays roles in removing toxin and relieving swelling, the lantana camara leaf extract plays roles in clearing away heat and toxic materials, resolving masses, relieving pain, dispelling wind and relieving itching, the loquat leaf extract plays roles in clearing away heat and toxic materials, and the honeysuckle plays roles in clearing away heat and toxic materials, resisting inflammation, tonifying deficiency and treating wind. The traditional Chinese medicine composition for removing turbid and relieving itching has natural raw materials, is safe, has less toxic and side effects and irritation, and is not easy to cause the condition of skin micro-ecosystem imbalance such as skin allergy, inflammation and the like; in addition, the turbid-removing itching-relieving composition is not easy to accumulate on the skin and scalp, but can be decomposed quickly, has no residue, and does not have adverse effect on the skin even if being absorbed by the skin in a small amount.
Detailed Description
The present invention will be further described in detail with reference to the following examples, but the scope of the present invention is not limited to the following examples.
Experiment 1 application of turbid discharge antipruritic traditional Chinese medicine composition in liquid soap
1.1 preparation of Chinese medicinal composition for eliminating turbid and relieving itching and liquid soap
Table 1 Chinese medicinal composition for eliminating turbid pathogen and relieving itching
The preparation method of the extract comprises the following steps: mixing and pulverizing the corresponding compound Chinese medicines according to the weight ratio, extracting with 5 times of 75% ethanol under reflux, concentrating the extractive solution under reduced pressure, and drying to obtain powder.
Table 2 method for preparing liquid soap using Chinese medicinal composition for eliminating turbid and relieving itching on liquid soap: adding dodecanoic acid into formula water, heating for dissolving, adding potassium hydroxide for saponification,
after saponification is completed, adding AES, CAB, potassium cocoyl glycinate, white sugar, glycerol and an amino acid humectant, mixing and dissolving, cooling to normal temperature, adding antiseptic and essence, and Chinese medicinal components for removing turbid and relieving itching, mixing uniformly, standing and defoaming.
1.2 clinical trials
1.2.1 Effect on Hartley guinea pig histamine phosphate itching response
The experimental method comprises the following steps:
experimental test article: liquid soap for eliminating turbid and relieving itching.
Three-ingredient heat-clearing itching-relieving lotion, produced by Guangxi Baiyunshan Yingkang pharmaceutical industry Co.
Histamine phosphate, manufactured by national pharmaceutical group chemical company, inc.
Experimental animals: hartley guinea pigs weighing 250g-400g.
Method and results
Effect on the itching response of histamine phosphate in Hartley guinea pigs.
80 healthy Hartley guinea pigs with the weight of 250-400 g are selected and randomly divided into 10 groups of 10 male and female parts. Blank control group (distilled water 0.1ml/100 g), positive control test sample three-flavor heat-clearing and itching-relieving lotion group (three-flavor heat-clearing and itching-relieving lotion 0.1ml/100 g), turbid-discharging itching-relieving liquid soap group (0.1 ml/100 g). Shaving the backs of the right back feet of the Hartley guinea pigs of each group 2 days before the experiment, and externally coating corresponding experiment test objects at the shaving positions of the animals of each group for 2 days for 1 time a day; on day 3, on the experimental day, animals of each group scratch the shaved parts of the backs of the right feet with coarse sand paper to damage the epidermis, the skin is slightly permeated with blood to the extent that the area is 1cm 2 After the corresponding experimental test objects are coated on the parts of the animals of each group for 1 time, the experimental test objects are coated for 10 minutes at last time, 0.05 ml/dose of 0.01% histamine phosphate solution is started to be dripped on the wound surface, the concentration is gradually increased by 0.02%, 0.03% and 0.04% … … … … every 3 minutes, each time, the concentration is 0.05 ml/dose until the Hartley guinea pig licks the right hind foot, the total amount (mug) of histamine phosphate which is given when the Hartley guinea pig licks the right hind foot last occurs is taken as an itching threshold, each group of data is recorded, and the data are subjected to statistical t and t' tests, and the results are shown in Table 1.
TABLE 3 influence of 10 groups of turbid discharge antipruritic liquid soap samples on the itching response of Hartley guinea pig histamine phosphate
n＝10)
Note that: comparison to the blank control group: * P < 0.05, P < 0.01, P < 0.001.
Experimental results show that 0.1ml/100g of the liquid soap group (example 3, example 4 and example 5) for eliminating turbid and relieving itching can obviously improve the itching threshold value of the histamine phosphate on guinea pigs when being externally used, and has obvious effects of eliminating turbid and relieving itching. However, in example 1, the effect is obviously inferior to that of examples 3, 4 and 5 because the adding ratio of the sample is too small, and the itching threshold of the single medicinal materials of the wampee tree extract, the pomelo leaf extract, the lantana camara leaf extract, the loquat leaf extract and the honeysuckle extract on guinea pigs is relatively low. The experimental results show that the mixture of the five traditional Chinese medicine extracts has stronger turbidity-removing and itching-relieving effects than the single traditional Chinese medicine extract. The experimental results show that the mixing ratio of the five traditional Chinese medicines is between 0.5-2:1.5-3:1.5-3:0.5-2:0.5-2, and a good turbidity-removing and itching-relieving effect can be achieved. The antipruritic effect of examples 3 to 5 is far greater than the one-way effect of examples 6 to 10.
1.2.2 antibacterial Property experiments
The test was performed using the QB/T2738-2012 (7.3) method. The action concentration and time are as follows: 10% strength and 20 minutes of action time. The experimental results are as follows:
table 4 results of antibacterial property test
Experiments show that the antibacterial performance of the five traditional Chinese medicine mixed extract solutions of examples 1-5 containing lantana camara, naria leaf, loquat leaf extract, honeysuckle and wampee is obviously higher than that of examples 6-10, and the antibacterial effect is obviously reduced by only using a single traditional Chinese medicine extract solution. When the implementation concentration of the mixed extract of the traditional Chinese medicines containing lantana camara, naringin leaf, loquat leaf extract, honeysuckle and wampee tree is gradually increased from 1% to 10%, the antibacterial rate is also increased from 50% to 90%, and the antibacterial effect is related to the used concentration. In examples 3 to 5, the composition ratio of the five traditional Chinese medicines is within the range (0.5-2:1.5-3:1.5-3:0.5-2:0.5-2), so that the antibacterial performance of the product can be ensured.
Experiment 2 application of turbidity-expelling and itching-relieving traditional Chinese medicine composition in shampoo
Table 5 1 application of extract in shampoo
In examples 11-13, the shampoo was prepared using the conventional shampoo formulation: adding APG into deionized water, further adding citric acid, adding fatty alcohol disodium succinate, CAB, triisostearate PEG-120 methyl glucose, olive oil, jojoba oil ester, camellia seed oil and the traditional Chinese medicine composition for removing turbid and relieving itching, sequentially adding the raw materials, stirring while adding, heating to about 75 ℃, cooling to about 40 ℃ in the next step, and adding preservative and essence.
Experiment 3 application of turbid discharge antipruritic traditional Chinese medicine composition in bath foam
Table 6 1 application of extract in bath lotion
In examples 14-16, the conventional shower gel production formulation process was used: adding AES into deionized water, further adding APG, citric acid, CAB, cocamidomethyl MEA, glycerol, amino acid humectant, and Chinese medicinal composition for eliminating turbid pathogen and relieving itching, sequentially adding raw materials, stirring while adding, and finally adding essence and antiseptic.
Experiment 4 application of turbidity-removing and itching-relieving traditional Chinese medicine composition in handmade soap
Table 7 1 application of extract to handmade soap
In examples 17-19, the conventional handmade soap manufacturing recipe procedure was used: adding soap particles into a heating pot to dissolve at 70-80 ℃, adding chelating agent, antioxidant and essential oil, and removing turbid and itching-relieving traditional Chinese medicine components, transferring into a former, placing at low temperature, forming and demoulding.
Experiment 5 application of turbid discharge antipruritic traditional Chinese medicine composition in body milk
Table 8 1 application of extract on body milk
In examples 20-22, the conventional body lotion manufacturing recipe process was used: adding emulsifier, vegetable oil, mineral oil, and polydimethylsiloxane into oil phase pot, heating to 85deg.C, maintaining for 20 min, adding water, carbomer, and amino acid humectant into water phase pot, heating to 85deg.C, and maintaining for 20 min. Then adding the oil phase solution into the water-oil solution, stirring and homogenizing, cooling to 40 ℃, and adding essence and preservative.
Samples prepared in experiments 2-5 were used in clinical trials.
Effect on the itching response of Hartley guinea pig histamine phosphate
30 healthy Hartley guinea pigs with the weight of 250-400 g are selected and randomly divided into 4 groups of 10 male and female halves. Blank (distilled water 0.1ml/100 g), body wash 20% test solution 0.1ml/100g (example 13), shampoo 20% test solution 0.1ml/100g (example 16), handmade soap 20% test solution 0.1ml/100g (example 19)). The backs of the right rear feet of the Hartley guinea pigs of each group were shaved 2 days before the experiment, and the corresponding experiment subjects were applied to the shaved sites of the animals of each group for 1 time,for 2 consecutive days; on day 3, on the experimental day, animals of each group scratch the shaved parts of the backs of the right feet with coarse sand paper to damage the epidermis, the skin is slightly bloodletting to a degree, and the area is 1cm 2 After the corresponding experimental test objects are coated on the animal parts of each group for 1 time, the last experimental test object is coated for 10min, 0.01 ml/part of histamine phosphate solution is dripped on the wound surface, the concentration is gradually increased by 0.02%, 0.03% and 0.04% … … every 3min, and each time is 0.05 ml/part, until the Hartley guinea pig licks the right hind foot back, the total amount (ug) of the histamine phosphate given when the Hartley guinea pig licks the right hind foot back finally is taken as the itching threshold, each group of data is recorded, statistics t and t are carried out, and the results are shown in Table 9.
Table 9 experimental results for examples 13, 16 and 19
Note that: comparison to the blank control group: * P < 0.05, < P < 0.01, < P < 0.001
Experiments show that the bathing product, the shampoo product and the soap cosmetic containing the Chinese medicinal components of the wampee tree extract, the grapefruit leaf extract, the lantana leaf extract, the loquat leaf extract and the honeysuckle flower extract have obvious effects of removing turbidity and relieving itching, and the external application of the bathing product, the shampoo product and the soap cosmetic can obviously improve the itching threshold of the histamine phosphate on the histamine phosphate of Hartley guinea pigs.
The samples prepared in experiments 2-5 were used for crowd use.
According to the requirement of double-blind test, the number of required test samples is between 30 and 50. The skin sub-health population with certain itching and erythema on the skin and scalp of the body is selected for trial, and after 4 weeks of trial (the use frequency is at least 2 times per week), the use intention list is filled in. Experimental data are as follows:
| group (30 persons each group) | Turbid discharge and itching relieving (%) | No effect (%) |
| Blank control group | 10.1 | 89.9 |
| Handmade soap (example 19) | 78.8 | 21.2 |
| Shower gel (example 15) | 76.8 | 23.2 |
| Body lotion (example 22) | 85.6 | 14.4 |
Experiments show that the bathing product, shampoo product and soap and body milk product containing the Chinese herbal medicine ingredients of the wampee tree extract, the grapefruit leaf extract, the lantana leaf extract, the loquat leaf extract and the honeysuckle flower extract have obvious effects of removing itch and reducing erythra when being externally used, namely, have obvious effects of removing turbidity and relieving itch.
Claims (8)
1. The traditional Chinese medicine composition for removing turbid and relieving itching is characterized by comprising the following components in parts by weight: the preparation method comprises the following steps of (1) extracting a wampee tree, namely, extracting a shaddock leaf, namely, extracting a lantana leaf, namely, extracting a loquat leaf, namely, extracting a honeysuckle flower, namely, 0.5-2:1.5-3:1.5-3:0.5-2:0.5-2, wherein the extraction method comprises the following steps: mixing and crushing the corresponding compound traditional Chinese medicines according to the weight ratio, heating and refluxing the mixture by using 70-80 vol.% ethanol with the amount of 3-5 times, and concentrating and drying the extracting solution under reduced pressure to obtain powder.
2. The turbid-removing itching-relieving traditional Chinese medicine composition according to claim 1 is characterized by comprising the following components in parts by weight: the wampee tree extract, the grapefruit leaf extract, the lantana leaf extract, the loquat leaf extract and the honeysuckle flower extract are respectively 1:2:2:1:1.
3. The turbid-removing itching-relieving traditional Chinese medicine composition according to claim 1, wherein the wampee tree extract is wampee tree leaf extract.
4. The use of the turbidity-removing itching-relieving traditional Chinese medicine composition according to any one of claims 1-3 in personal care products.
5. The use according to claim 4, characterized in that: the personal care products include bath products, shampoo products, hand washing products, body skin care products, and soap cosmetics.
6. The use according to claim 5, characterized in that: the soap cosmetics include perfumed soap, handmade soap and liquid soap.
7. The use according to any one of claims 4-6, characterized in that: the weight percentage of the traditional Chinese medicine composition for eliminating turbid and relieving itching in the personal care product is 1% -30%.
8. The use according to claim 7, characterized in that: the weight percentage of the traditional Chinese medicine composition for eliminating turbid and relieving itching in the personal care product is 1% -10%.
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| CN102885737A (en) * | 2012-09-24 | 2013-01-23 | 佛山市梦莎美容化妆品有限公司 | Application of common lantana leaf or branchlet active extract to preparation of cosmetics |
| CN108066238A (en) * | 2017-12-29 | 2018-05-25 | 柳州两面针股份有限公司 | Application of the Chinese medicine composition with antipyretic and itching-stopping on articles for washing |
| CN110856711A (en) * | 2018-08-25 | 2020-03-03 | 蒋成 | Plant itching-relieving and dandruff-removing shampoo |
| CN109010131A (en) * | 2018-10-16 | 2018-12-18 | 江门市君和办公用品有限公司 | A kind of removing miliaria and relieving itching shower cream and preparation method thereof |
| CN112006970B (en) * | 2020-08-14 | 2021-10-22 | 珀莱雅化妆品股份有限公司 | Anti-itch composition and preparation method and application thereof |
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| CN113693989A (en) | 2021-11-26 |
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