CN113651641A - Volcano lava-imitated glaze ceramic and preparation method thereof - Google Patents
Volcano lava-imitated glaze ceramic and preparation method thereof Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/24—Manufacture of porcelain or white ware
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
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Abstract
The invention relates to the field of ceramic products and preparation methods thereof, in particular to a volcano-imitated lava glaze ceramic which comprises a green body, wherein the surface of the green body is provided with a grain crack glaze layer, a lava glaze layer, a floating ash glaze layer and a matte transparent glaze layer. Forming cracks by applying crack glaze with feldspar and without feldspar particles, then immersing the cracks into a granulated sugar solution, immersing the granulated sugar solution into the cracks, drying at low temperature to carbonize granulated sugar in the cracks, expanding the cracks and forming a three-dimensional texture of cracked rock similar to that after volcanic ignition; applying lava glaze to form a red-like volcanic rock slurry; the inside of the crack of the particle crack glaze layer is provided with lava glaze which flows like magma; in the firewood burning kiln, granulated sugar and rice husk are used as fuels, ash floating glaze is formed on the surface after smoking to form the effect similar to volcanic ash floating, and copper powder is sprayed on the surface to form the local flame flash effect; the effect similar to volcanic rock slurry spraying is formed by composite glazing, and the ornamental value is strong.
Description
Technical Field
The invention relates to the field of ceramic products and preparation methods thereof, in particular to volcano lava-imitated glaze ceramic and a preparation method thereof.
Background
The fancy glaze has different glaze formulas, different firing temperatures and atmospheres or different glazing methods, forms a texture effect of overlapping a plurality of colors on the glaze surface after firing, and has strong decoration. The fancy glaze belongs to a compound color system of the colored glaze, most fancy glazes are formed by stacking the colored glazes, and the traditional kiln change glaze has large temperature difference and atmosphere change due to the structure of a kiln, so that the color tone change range is large, the stability and the repeatability are poor, the effect of a smooth surface is more realized, the stereoscopic impression is not good, and the scheme is generated.
Disclosure of Invention
An object of the present invention is to solve at least the above problems by an imitated volcanic lava glaze ceramic and a method for preparing the same.
In order to solve the technical problems, the technical scheme adopted by the invention is as follows: the volcanic lava-imitated glaze ceramic is characterized in that: the green body is a small-sized and big-sized cone, the surface of the green body is provided with a particle crack glaze layer, a lava glaze layer, a floating ash glaze layer and a matte transparent glaze layer, cracks and particles are arranged on the particle crack glaze layer, the lava glaze layer comprises a top area and a bottom area, the top area covers the top of the green body, the bottom area is in a strip shape and partially covers the lower part of the green body, the floating ash glaze covers the bottom area of the lava glaze layer, and the matte transparent glaze layer covers the particle crack glaze layer, the lava glaze layer and the floating ash glaze layer.
Preferably, the particle crack glaze layer is made of a particle crack glaze, the particle crack glaze is black, and the raw materials of the particle crack glaze comprise the following components in parts by weight: 20-25 parts of nickel oxide, 10-15 parts of copper oxide, 12-15 parts of ferric oxide, 20-22 parts of chromium oxide, 40-45 parts of feldspar and 5-8 parts of quartz.
Preferably, the lava glaze layer is made of lava glaze, the lava glaze layer is red, and the lava glaze layer comprises the following components in parts by weight: 25-28 parts of silica, 12-15 parts of ferrous sulfate, 30-35 parts of silicon dioxide, 5-6 parts of sodium fluoride, 2-3 parts of sodium chloride, 25-26 parts of light calcium carbonate and 4-5 parts of potassium dichromate.
Preferably, the lava glaze is arranged in the cracks of the particle crack glaze layer.
Preferably, the floating ash glaze layer is made of floating ash glaze, the floating ash glaze is gray, and the raw material of the floating ash glaze is natural ash.
Preferably, the natural ash is prepared by firing granulated sugar and rice husk.
Preferably, the matte transparent glaze layer is made of matte transparent glaze, and comprises the following components in parts by weight: 10-12 parts of calcium carbonate, 5-8 parts of nepheline syenite, 20-26 parts of quartz, 3-5 parts of lithium carbonate and 32-35 parts of cryolite.
The preparation method of the volcano lava-imitated glaze ceramic is characterized by comprising the following steps of: the method comprises the following steps:
step a, forming and firing a blank;
b, applying granular crack glaze on the surface of the blank, firing at 700 ℃, taking out the ceramic, and rapidly cooling at 0 ℃ to form cracks;
c, pasting a paster on the ceramic surface at a place where the lava glaze does not need to be applied, applying the lava glaze in a glaze dipping mode, tearing off the paster after drying at low temperature, repeatedly dipping the glaze to fill cracks with the lava glaze, wiping off the glaze on the particle surfaces except the cracks, drying at low temperature, and finally sintering at 1100-plus 1150 ℃;
d, placing the ceramic in a firewood kiln, smoking for 1-2h by taking granulated sugar and rice husk as fuels, forming ash floating glaze on the surface, and spraying copper powder on the surface at the last 10min of smoking;
and e, applying matte transparent glaze on the surface of the ceramic, heating to 1200 ℃ in a kiln at the speed of 50 ℃/h, preserving heat for 0.5h, and slowly preparing the volcano lava-imitated glaze ceramic at the speed of 100 ℃/h.
Preferably, the step b is performed twice, feldspar is not added into the first particle crack glaze, and feldspar is added into the second particle crack glaze after drying.
Preferably, in the step b, the fired ceramic is immersed in a granulated sugar solution at 10 ℃ for 30-40 minutes to immerse the granulated sugar solution in the cracks, the solubility of the granulated sugar solution is 100g/100g, and then the ceramic surface is taken out and cleaned, and baked at 300 ℃ for 3-4 hours to carbonize the granulated sugar in the cracks and expand the cracks.
As can be seen from the above description, the volcanic lava-imitated glaze ceramic and the preparation method thereof provided by the invention have the following beneficial effects: forming cracks by applying crack glaze with feldspar and without feldspar particles, then immersing the cracks into a granulated sugar solution, immersing the granulated sugar solution into the cracks, drying at low temperature to carbonize granulated sugar in the cracks, expanding the cracks and forming a three-dimensional texture of cracked rock similar to that after volcanic ignition; applying lava glaze to form a red-like volcanic rock slurry; the inside of the crack of the particle crack glaze layer is provided with lava glaze which flows like magma; in the firewood burning kiln, granulated sugar and rice husk are used as fuels, ash floating glaze is formed on the surface after smoking to form the effect similar to volcanic ash floating, and copper powder is sprayed on the surface to form the local flame flash effect; the effect similar to volcanic rock slurry spraying is formed by composite glazing, and the ornamental value is strong.
Detailed Description
The invention is further described below by means of specific embodiments.
In order to make the technical means, the creation characteristics, the achievement purposes and the effects of the invention easy to understand, the invention is further described with the specific embodiments.
The volcano lava imitating glaze ceramic is characterized in that: the green body is a small-sized and big-sized cone, the surface of the green body is provided with a particle crack glaze layer, a lava glaze layer, a floating ash glaze layer and a matte transparent glaze layer, cracks and particles are arranged on the particle crack glaze layer, the lava glaze layer comprises a top area and a bottom area, the top area covers the top of the green body, the bottom area is in a strip shape and partially covers the lower part of the green body, the floating ash glaze covers the bottom area of the lava glaze layer, and the matte transparent glaze layer covers the particle crack glaze layer, the lava glaze layer and the floating ash glaze layer.
The particle crack glaze layer is made of particle crack glaze, the particle crack glaze is black, and the raw materials of the particle crack glaze comprise the following components in parts by weight: 20-25 parts of nickel oxide, 10-15 parts of copper oxide, 12-15 parts of ferric oxide, 20-22 parts of chromium oxide, 40-45 parts of feldspar and 5-8 parts of quartz.
The lava glaze layer is made of lava glaze, the lava glaze layer is red, and the lava glaze layer comprises the following components in parts by weight: 25-28 parts of silica, 12-15 parts of ferrous sulfate, 30-35 parts of silicon dioxide, 5-6 parts of sodium fluoride, 2-3 parts of sodium chloride, 25-26 parts of light calcium carbonate and 4-5 parts of potassium dichromate.
And a lava glaze is arranged in the cracks of the particle crack glaze layer.
The floating ash glaze layer is made of floating ash glaze, the floating ash glaze is gray, and the raw material of the floating ash glaze is natural ash.
The natural ash is prepared by baking granulated sugar and rice husk.
The matte transparent glaze layer is made of matte transparent glaze, and comprises the following components in parts by weight: 10-12 parts of calcium carbonate, 5-8 parts of nepheline syenite, 20-26 parts of quartz, 3-5 parts of lithium carbonate and 32-35 parts of cryolite.
The preparation method of the volcano lava-imitated glaze ceramic is characterized by comprising the following steps of: the method comprises the following steps:
step a, forming and firing a blank;
b, applying granular crack glaze on the surface of the blank, firing at 700 ℃, taking out the ceramic, and rapidly cooling at 0 ℃ to form cracks;
c, pasting a paster on the ceramic surface at a place where the lava glaze does not need to be applied, applying the lava glaze in a glaze dipping mode, tearing off the paster after drying at low temperature, repeatedly dipping the glaze to fill cracks with the lava glaze, wiping off the glaze on the particle surfaces except the cracks, drying at low temperature, and finally sintering at 1100-plus 1150 ℃;
d, placing the ceramic in a firewood kiln, smoking for 1-2h by taking granulated sugar and rice husk as fuels, forming ash floating glaze on the surface, and spraying copper powder on the surface at the last 10min of smoking;
and e, applying matte transparent glaze on the surface of the ceramic, heating to 1200 ℃ in a kiln at the speed of 50 ℃/h, preserving heat for 0.5h, and slowly preparing the volcano lava-imitated glaze ceramic at the speed of 100 ℃/h.
And c, glazing twice in the step b, wherein feldspar is not added into the first particle crack glaze, and after drying, feldspar is added into the second particle crack glaze.
And b, immersing the fired ceramic into a granulated sugar solution at 10 ℃ for 30-40 minutes to immerse the granulated sugar solution into the cracks, wherein the solubility of the granulated sugar solution is 100g/100g, taking out and cleaning the surface of the ceramic, baking at 300 ℃ for 3-4 hours to carbonize the granulated sugar in the cracks, and expanding the cracks.
Forming cracks by applying crack glaze with feldspar and without feldspar particles, then immersing the cracks into a granulated sugar solution, immersing the granulated sugar solution into the cracks, drying at low temperature to carbonize granulated sugar in the cracks, expanding the cracks and forming a three-dimensional texture of cracked rock similar to that after volcanic ignition; applying lava glaze to form a red-like volcanic rock slurry; the inside of the crack of the particle crack glaze layer is provided with lava glaze which flows like magma; in the firewood burning kiln, granulated sugar and rice husk are used as fuels, ash floating glaze is formed on the surface after smoking to form the effect similar to volcanic ash floating, and copper powder is sprayed on the surface to form the local flame flash effect; the effect similar to volcanic rock slurry spraying is formed by composite glazing, and the ornamental value is strong.
The above description is only a few specific embodiments of the present invention, but the design concept of the present invention is not limited thereto, and any insubstantial modifications made by the design concept should fall within the scope of the present invention.
Claims (10)
1. The volcanic lava-imitated glaze ceramic is characterized in that: the green body is a small-sized and big-sized cone, the surface of the green body is provided with a particle crack glaze layer, a lava glaze layer, a floating ash glaze layer and a matte transparent glaze layer, cracks and particles are arranged on the particle crack glaze layer, the lava glaze layer comprises a top area and a bottom area, the top area covers the top of the green body, the bottom area is in a strip shape and partially covers the lower part of the green body, the floating ash glaze covers the bottom area of the lava glaze layer, and the matte transparent glaze layer covers the particle crack glaze layer, the lava glaze layer and the floating ash glaze layer.
2. The volcano lava-imitated glazed ceramic as claimed in claim 1, wherein: the particle crack glaze layer is made of particle crack glaze, the particle crack glaze is black, and the raw materials of the particle crack glaze comprise the following components in parts by weight: 20-25 parts of nickel oxide, 10-15 parts of copper oxide, 12-15 parts of ferric oxide, 20-22 parts of chromium oxide, 40-45 parts of feldspar and 5-8 parts of quartz.
3. The volcano lava-imitated glazed ceramic as claimed in claim 1, wherein: the lava glaze layer is made of lava glaze, the lava glaze layer is red, and the lava glaze layer comprises the following components in parts by weight: 25-28 parts of silica, 12-15 parts of ferrous sulfate, 30-35 parts of silicon dioxide, 5-6 parts of sodium fluoride, 2-3 parts of sodium chloride, 25-26 parts of light calcium carbonate and 4-5 parts of potassium dichromate.
4. The volcano lava-imitated glazed ceramic as claimed in claim 4, wherein: and a lava glaze is arranged in the cracks of the particle crack glaze layer.
5. The volcano lava-imitated glazed ceramic as claimed in claim 1, wherein: the floating ash glaze layer is made of floating ash glaze, the floating ash glaze is gray, and the raw material of the floating ash glaze is natural ash.
6. The volcano lava-imitated glazed ceramic as claimed in claim 5, wherein: the natural ash is prepared by baking granulated sugar and rice husk.
7. The volcano lava-imitated glazed ceramic as claimed in claim 1, wherein: the matte transparent glaze layer is made of matte transparent glaze, and comprises the following components in parts by weight: 10-12 parts of calcium carbonate, 5-8 parts of nepheline syenite, 20-26 parts of quartz, 3-5 parts of lithium carbonate and 32-35 parts of cryolite.
8. The method for preparing the volcano lava-imitated glazed ceramic according to any one of claims 1 to 8, wherein: the method comprises the following steps:
step a, forming and firing a blank;
b, applying granular crack glaze on the surface of the blank, firing at 700 ℃, taking out the ceramic, and rapidly cooling at 0 ℃ to form cracks;
c, pasting a paster on the ceramic surface at a place where the lava glaze does not need to be applied, applying the lava glaze in a glaze dipping mode, tearing off the paster after drying at low temperature, repeatedly dipping the glaze to fill cracks with the lava glaze, wiping off the glaze on the particle surfaces except the cracks, drying at low temperature, and finally sintering at 1100-plus 1150 ℃;
d, putting the ceramic into a firewood kiln, smoking for 1-2h by taking granulated sugar and rice husk as fuels, forming ash floating glaze on the surface, and spraying copper powder on the surface for 10min at the end of smoking;
and e, applying matte transparent glaze on the surface of the ceramic, heating to 1200 ℃ in a kiln at the speed of 50 ℃/h, preserving heat for 0.5h, and slowly preparing the volcano lava-imitated glaze ceramic at the speed of 100 ℃/h.
9. The preparation method of the volcano lava-imitated glazed ceramic according to claim 1, wherein: and c, glazing twice in the step b, wherein feldspar is not added into the first particle crack glaze, and after drying, feldspar is added into the second particle crack glaze.
10. The preparation method of the volcano lava-imitated glazed ceramic according to claim 9, wherein: and b, immersing the fired ceramic into a granulated sugar solution at 10 ℃ for 30-40 minutes to immerse the granulated sugar solution into the cracks, wherein the solubility of the granulated sugar solution is 100g/100g, taking out and cleaning the surface of the ceramic, baking at 300 ℃ for 3-4 hours to carbonize the granulated sugar in the cracks, and expanding the cracks.
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| CN114702242A (en) * | 2022-04-13 | 2022-07-05 | 广东道氏陶瓷材料有限公司 | Star diamond crack glaze, glaze slip and ceramic thereof |
| CN115159849A (en) * | 2022-08-11 | 2022-10-11 | 福建省德化县华茂陶瓷有限公司 | Antique yellow secret color celadon and preparation process thereof |
| CN117105697A (en) * | 2023-09-06 | 2023-11-24 | 福建省德化县腾艺陶瓷有限公司 | Thick glazed firewood fired glaze ceramic with flash and rust spots and preparation method thereof |
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| CN1609043A (en) * | 2004-11-09 | 2005-04-27 | 成都再建装饰材料有限公司 | Ceramic tile and mosaic and their production process |
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| CN117105697A (en) * | 2023-09-06 | 2023-11-24 | 福建省德化县腾艺陶瓷有限公司 | Thick glazed firewood fired glaze ceramic with flash and rust spots and preparation method thereof |
| CN117105697B (en) * | 2023-09-06 | 2024-03-19 | 福建省德化县腾艺陶瓷有限公司 | Thick glazed firewood fired glaze ceramic with flash and rust spots and preparation method thereof |
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| CN113651641B (en) | 2022-12-30 |
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