CN113550751A - Method for recovering near-surface caving ore body - Google Patents

Method for recovering near-surface caving ore body Download PDF

Info

Publication number
CN113550751A
CN113550751A CN202110840824.XA CN202110840824A CN113550751A CN 113550751 A CN113550751 A CN 113550751A CN 202110840824 A CN202110840824 A CN 202110840824A CN 113550751 A CN113550751 A CN 113550751A
Authority
CN
China
Prior art keywords
caving
ore body
grouting
ore
seamless steel
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN202110840824.XA
Other languages
Chinese (zh)
Other versions
CN113550751B (en
Inventor
刘东锐
***
***
李永辉
李晓辉
朱青凌
王亚军
邹平
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Changsha Institute of Mining Research Co Ltd
Original Assignee
Changsha Institute of Mining Research Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Changsha Institute of Mining Research Co Ltd filed Critical Changsha Institute of Mining Research Co Ltd
Priority to CN202110840824.XA priority Critical patent/CN113550751B/en
Publication of CN113550751A publication Critical patent/CN113550751A/en
Application granted granted Critical
Publication of CN113550751B publication Critical patent/CN113550751B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21CMINING OR QUARRYING
    • E21C41/00Methods of underground or surface mining; Layouts therefor
    • E21C41/16Methods of underground mining; Layouts therefor
    • E21C41/22Methods of underground mining; Layouts therefor for ores, e.g. mining placers
    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B33/00Sealing or packing boreholes or wells
    • E21B33/10Sealing or packing boreholes or wells in the borehole
    • E21B33/13Methods or devices for cementing, for plugging holes, crevices or the like
    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B7/00Special methods or apparatus for drilling
    • E21B7/04Directional drilling
    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B7/00Special methods or apparatus for drilling
    • E21B7/20Driving or forcing casings or pipes into boreholes, e.g. sinking; Simultaneously drilling and casing boreholes
    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21FSAFETY DEVICES, TRANSPORT, FILLING-UP, RESCUE, VENTILATION, OR DRAINING IN OR OF MINES OR TUNNELS
    • E21F15/00Methods or devices for placing filling-up materials in underground workings

Landscapes

  • Engineering & Computer Science (AREA)
  • Mining & Mineral Resources (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Geochemistry & Mineralogy (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Fluid Mechanics (AREA)
  • Remote Sensing (AREA)
  • Geophysics And Detection Of Objects (AREA)

Abstract

The invention discloses a method for recovering an ore body caving from the near surface, which comprises the steps of firstly, exploring occurrence conditions of the ore body caving, then, constructing a row of follow pipe drill holes along the artery connecting lane from one side of the ore body caving by adopting a follow pipe drilling machine in a direction perpendicular to the ore body, and installing a seamless steel pipe with a round hole in each drill hole. And grouting the caving ore body region through a seamless steel pipe by adopting a single-liquid grouting pump, forming a layer of grouting cementing body in the upper region and the lower region of the seamless steel pipe, and forming a route isolation layer in the whole caving ore body range below the grouting cementing body in a downward layered route filling method mode from a vein-along connecting roadway perpendicular to the ore body trend. And then under the protection of the overlying grouting cementing body and the access isolation layer, recovering the ore body from the lower caving and filling the empty area. The invention has the advantages of simple process and principle, low cost, high recovery rate, safety, good reliability and the like.

Description

Method for recovering near-surface caving ore body
Technical Field
The invention relates to the technical field of underground metal mine mining, in particular to a method for recovering near-surface caving ore bodies.
Background
The underground mining difficulty of the near-surface ore body is small, the effect is quick, the near-surface ore body is easy to steal, and the ore rock is easy to collapse to the surface due to disordered and non-filling mining in the early stage of mining, so that a large amount of ore (body) left in the inner part and the lower part of the ore body cannot be recovered, and generally, the grade and the value of the part of the ore body are higher, and the amount of the ore body is larger. The ground surface is continuously collapsed due to the trade recovery, the environment is irreversibly influenced, and meanwhile, a large amount of waste rocks and a fourth system are doped in the discharged ore, so that the dilution rate of the discharged ore is high. The conventional mode for recovering the part of ore is two modes, namely pre-grouting secondary recovery and surface filling underground recovery, wherein when the caving area is too large, the required slurry amount is too large, and the problems of slurry leakage and slurry leakage cannot be effectively avoided; the latter risks depletion losses and this solution cannot be implemented when there are fixed buildings in the vicinity. In addition, methods such as in-situ leaching have problems of high cost, low success rate, low recovery efficiency, and the like.
In view of the defects of the methods, a method with wide application range, simple process and low cost is needed, and the problems of high cost, poor dilution rate control, low reliability and the like in the process of recovering the near-surface caving ore body are solved.
Disclosure of Invention
In order to solve the technical problem, the invention provides a method for recovering a near-surface caving ore body, which comprises the following steps:
step 1, constructing a vein-following connection roadway in upper and lower plate rock masses of a caving ore body along the trend, constructing a vein-following connection roadway perpendicular to the trend of the ore body at a certain interval from the vein-following connection roadway, and exploring the caving range of the caving ore body, the relative position relation of the caving range and the ground surface and the surrounding stope, and the ore block size distribution condition in a caving area by combining the mining data of the ore body in the early period through exploration drilling, roadway engineering and geophysical prospecting methods;
step 2, in a vein-following connection roadway on one side of the self-caving ore body, a pipe-following drilling machine is adopted to construct a row of pipe-following drill holes in a direction perpendicular to the ore body, the pipe-following drill holes need to exceed a caving area and are constructed into stable original rock on the other side of the caving area, the specific length of the pipe-following drill holes is determined according to mechanical calculation, the seamless steel pipes are synchronously installed in the whole length of the drill holes along with the drilling of the pipe-following drill holes, and circular holes for grouting are reserved on the seamless steel pipes;
step 3, adopting a single-liquid grouting pump to perform grouting on the caving ore body region through the seamless steel pipe, and forming a layer of grouting cementing body in the upper region and the lower region of the seamless steel pipe;
step 4, after the maintenance design period of the grouting cementing body, sampling the grouting cementing body by a drilling machine in a vein-following connection roadway, detecting mechanical parameters, and performing the next operation after the design index is reached;
step 5, forming a route isolation layer in the whole caving ore body range in a downward layered route filling method mode from the artery-following connecting roadway perpendicular to the direction of the ore body, wherein the distance between the top of the route isolation layer and the seamless steel pipe is 50-100 cm;
step 6, under the protection of the upper grouting cementing body and the access isolation layer, recovering the lower collapse ore body, constructing corresponding ore drawing engineering at the ore drawing level, discharging the collapse ore below the access isolation layer, and determining the height of the single recovered ore according to the size of a collapse area in the ore drawing process to prevent secondary collapse caused by overlarge exposed area in the ore drawing process;
and 7, immediately filling the empty area after the ores to be collapsed are completely discharged.
Preferably, the pipe following drilling distance is 50-100 cm, the thickness of the seamless steel pipes is 3-6 mm, the diameter of the seamless steel pipes is 90-126 mm, each seamless steel pipe is 1.0-1.5 m long, the seamless steel pipes are connected through threads, and the connection length is not less than 100 mm.
Preferably, the circular holes reserved for grouting on the seamless steel pipes are arranged in a quincunx shape, and the aperture is 3-5 mm.
Preferably, during grouting in the step 3, the grouting slurry is made of 42.5 cement, and the water-cement ratio is 0.6: 1-1: 1, the grouting pressure is 0.6-2.0 Mpa, and the diffusion range of single-hole grouting is not less than half of the distance between two holes.
Further, when the approach isolation layer is formed in the step 5, a wood board matched with a steel bracket is adopted for supporting in the downward approach, after the approach is formed, film laying and rib laying are carried out, then two ends of the approach are sealed, and then C30 high-grade concrete or high-strength filling slurry is adopted for filling.
Furthermore, the number of the access layers of the access isolation layer is determined by adopting a theoretical calculation and numerical simulation method, and is generally 2-4.
Preferably, when the reinforcement is paved in the downward access way, the reinforcement is adopted
Figure BDA0003176580100000031
And the length of the reinforcing steel bars is reserved at two sides of the transverse bar by 20cm, and the transverse bar is made into a hook which is connected with the reinforcing steel bars of adjacent routes.
Advantageous effects
Compared with the prior art and the method, the method for recovering the near-surface caving ore body provided by the invention has the following beneficial effects:
1. simple process and principle
According to the principle of the beam, a steel pipe and rock-soil mixture nearby the steel pipe are formed into a composite beam by adopting a mode of drilling along with the pipe and matching grouting; and then under the protection of the beam, a downward access construction method is adopted, and a high-strength filling body is matched to form the strong-support simply supported beam, so that the process and the principle are simple.
2. Low cost and high recovery rate
Through the segmentation implementation isolation project, high-grade ore is retrieved in segments, has guaranteed the safety of recovery process promptly, has reduced whole construction cost again, compares in directly adopting the access way method to build, and the security is higher, compares in directly forming the isolation layer at the earth's surface, and the cost is lower, and the rate of recovery is higher.
3. High safety and good reliability
The method forms a double-layer safety isolation layer by establishing a pipe following isolation layer and an access isolation layer, ensures the safe recovery of ore bodies in the lower caving region, and is reliable and new.
Drawings
The present invention will be described in further detail with reference to the accompanying drawings.
FIG. 1 is a front view of a method for recovering near-surface caving ore body provided by the invention;
FIG. 2 is a sectional view taken along line II-II of FIG. 1;
FIG. 3 is a cross-sectional view III-III of FIG. 1;
in the figure: 1-connecting lane along vein; 2-exploration drilling; 3-a loose mass; 4-grouting a cementing body; 5-connecting lane of thoroughfare; 6-a route isolation layer; 7-caving ore body; 8-collapse zone boundary; 9-downward route; 10-seamless steel tube; 11-virgin rock.
Detailed Description
The technical solutions of the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings, and it is to be understood that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments; all other embodiments, which can be derived by a person skilled in the art from the embodiments of the present invention without any inventive step, are within the scope of the present invention.
As shown in fig. 1-3, the method for recovering near-surface caving ore body provided by the invention comprises the following steps:
step 1, constructing a vein-following connection lane 1 in upper and lower plate rock masses of a caving ore body 7 along the trend, constructing a vein-following connection lane 5 from the vein-following connection lane 1 in a manner of being perpendicular to the trend of the ore body at a certain interval, and exploring the caving range of the caving ore body 7, the relative position relation of the caving range and the ground surface and the peripheral stope, and the ore block size distribution condition in a caving area through an exploration drilling hole 2, a roadway engineering and a geophysical prospecting method by combining early-stage ore body mining data;
and 2, constructing a row of pipe following drill holes in the connecting roadway 1 along the vein on one side of the self-caving roof ore body 7 by adopting a pipe following drilling machine to be vertical to the direction of the ore body, wherein the distance between the pipe following drill holes is 50-100 cm. The pipe-following drilling needs to exceed the caving area and is constructed into the stable original rock 11 on the other side of the caving area, the specific length of the pipe-following drilling is determined according to mechanical calculation, the seamless steel pipes 10 are synchronously installed in the whole length of the drilling along with the drilling of the pipe-following drilling, the thickness of each seamless steel pipe 10 is 3-6 mm, the diameter of each seamless steel pipe 10 is 90-126 mm, each seamless steel pipe 10 is 1.0-1.5 m long, the seamless steel pipes 10 are connected through threads, and the connection length is not less than 100 mm. A circular hole for grouting is reserved in the seamless steel tube 10, the circular hole is arranged in a quincunx shape, and the aperture is 3-5 mm.
And 3, adopting a single-liquid grouting pump to perform grouting on the area of the caving ore body 7 through the seamless steel pipe 10, and forming a layer of grouting cement 4 on the upper area and the lower area of the seamless steel pipe 10. The grouting slurry is prepared from 42.5 cement, and the water-cement ratio is 0.6: 1-1: 1, the grouting pressure is 0.6-2.0 Mpa, and the diffusion range of single-hole grouting is not less than half of the distance between two holes.
Step 4, after the maintenance design period of the grouting cementing body 4, sampling the grouting cementing body 4 by a drilling machine in the artery-following connecting roadway 1, detecting mechanical parameters, and performing the next operation after the design index is reached;
and 5, forming a route isolation layer 6 in the range of the whole caving ore body 7 in a downward layered route filling method mode from the artery-following connecting roadway 1 perpendicular to the direction of the ore body, wherein the distance between the top of the route isolation layer 6 and the seamless steel pipe is 1050-100 cm. The number of the access layers of the access isolation layer 6 is determined by adopting a theoretical calculation and numerical simulation method, and is generally 2-4. When the route isolation layer 6 is formed, the downward route 9 is supported by a wood plate matched with a steel bracket, the film and the reinforcing steel bars are paved after the route is formed, and when the reinforcing steel bars are paved, the reinforcing steel bars are adopted
Figure BDA0003176580100000051
The reinforcing steel bars, the length of which is 20cm reserved on the two sides of the transverse bar, are made into hooks to be connected with the reinforcing steel bars of adjacent approaches, then the two ends of the approach are sealed, and C30 high-grade concrete or high-strength filling slurry is adopted for fillingAnd (6) filling.
Step 6, under the protection of the upper grouting cementing body 4 and the access isolation layer 6, recovering the lower caving ore body 7, constructing corresponding ore drawing engineering at the ore drawing level, discharging the caving ore below the access isolation layer 6, determining the height of single ore recovery according to the size of a caving area in the ore drawing process, and preventing secondary collapse caused by overlarge exposed area in the ore drawing process;
and 7, immediately filling the empty area after the ores to be collapsed are completely discharged.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.

Claims (7)

1. The method for recovering the near-surface caving ore body is characterized by comprising the following steps of:
step 1, constructing a vein-following connection roadway in upper and lower plate rock masses of a caving ore body along the trend, constructing a vein-following connection roadway perpendicular to the trend of the ore body at a certain interval from the vein-following connection roadway, and exploring the caving range of the caving ore body, the relative position relation of the caving range and the ground surface and the surrounding stope, and the ore block size distribution condition in a caving area by combining the mining data of the ore body in the early period through exploration drilling, roadway engineering and geophysical prospecting methods;
step 2, in a vein-following connection roadway on one side of the self-caving ore body, a pipe-following drilling machine is adopted to construct a row of pipe-following drill holes in a direction perpendicular to the ore body, the pipe-following drill holes need to exceed a caving area and are constructed into stable original rock on the other side of the caving area, the specific length of the pipe-following drill holes is determined according to mechanical calculation, the seamless steel pipes are synchronously installed in the whole length of the drill holes along with the drilling of the pipe-following drill holes, and circular holes for grouting are reserved on the seamless steel pipes;
step 3, adopting a single-liquid grouting pump to perform grouting on the caving ore body region through the seamless steel pipe, and forming a layer of grouting cementing body in the upper region and the lower region of the seamless steel pipe;
step 4, after the maintenance design period of the grouting cementing body, sampling the grouting cementing body by a drilling machine in a vein-following connection roadway, detecting mechanical parameters, and performing the next operation after the design index is reached;
step 5, forming a route isolation layer in the whole caving ore body range in a downward layered route filling method mode from the artery-following connecting roadway perpendicular to the direction of the ore body, wherein the distance between the top of the route isolation layer and the seamless steel pipe is 50-100 cm;
step 6, under the protection of the upper grouting cementing body and the access isolation layer, recovering the lower collapse ore body, constructing corresponding ore drawing engineering at the ore drawing level, discharging the collapse ore below the access isolation layer, and determining the height of the single recovered ore according to the size of a collapse area in the ore drawing process to prevent secondary collapse caused by overlarge exposed area in the ore drawing process;
and 7, immediately filling the empty area after the ores to be collapsed are completely discharged.
2. The method for recovering the near-surface caving ore body according to claim 1, wherein: the pipe following drilling distance is 50-100 cm, the thickness of the seamless steel pipes is 3-6 mm, the diameter of the seamless steel pipes is 90-126 mm, the length of each seamless steel pipe is 1.0-1.5 m, the seamless steel pipes are connected through threads, and the connection length is not less than 100 mm.
3. The method for recovering the near-surface caving ore body according to claim 1, wherein: the circular holes reserved for grouting on the seamless steel pipes are arranged in a quincunx shape, and the hole diameter is 3-5 mm.
4. The method for recovering the near-surface caving ore body according to claim 1, wherein: during grouting in the step 3, the grouting slurry is made of 42.5 cement, and the water cement ratio is 0.6: 1-1: 1, the grouting pressure is 0.6-2.0 Mpa, and the diffusion range of single-hole grouting is not less than half of the distance between two holes.
5. The method for recovering the near-surface caving ore body according to claim 1, wherein: and (5) when the approach isolation layer is formed in the step (5), supporting the downward approach by adopting a wood board matched with a steel bracket, laying a film and a rib after the approach is formed, then sealing two ends of the approach, and then filling by adopting C30 high-grade concrete or high-strength filling slurry.
6. The method for recovering the near-surface caving ore body according to claim 1, wherein: the number of the access layers of the access isolation layer is determined by adopting a theoretical calculation and numerical simulation method, and is generally 2-4.
7. The method for recovering near-surface caving ore body according to claim 5, wherein: when the reinforcing steel bars are paved in the downward access, the reinforcing steel bars are adopted
Figure FDA0003176580090000021
And the length of the reinforcing steel bars is reserved at two sides of the transverse bar by 20cm, and the transverse bar is made into a hook which is connected with the reinforcing steel bars of adjacent routes.
CN202110840824.XA 2021-07-23 2021-07-23 Method for recovering near-surface caving ore body Active CN113550751B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202110840824.XA CN113550751B (en) 2021-07-23 2021-07-23 Method for recovering near-surface caving ore body

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202110840824.XA CN113550751B (en) 2021-07-23 2021-07-23 Method for recovering near-surface caving ore body

Publications (2)

Publication Number Publication Date
CN113550751A true CN113550751A (en) 2021-10-26
CN113550751B CN113550751B (en) 2022-06-03

Family

ID=78132732

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202110840824.XA Active CN113550751B (en) 2021-07-23 2021-07-23 Method for recovering near-surface caving ore body

Country Status (1)

Country Link
CN (1) CN113550751B (en)

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1314066A1 (en) * 1986-01-22 1987-05-30 Новочеркасский Политехнический Институт Им.Серго Орджоникидзе Method of mining ore bodies
SU1608345A1 (en) * 1988-12-09 1990-11-23 Московский Геологоразведочный Институт Им.Серго Орджоникидзе Method of mining mineral deposits
CN203452793U (en) * 2013-07-10 2014-02-26 济南钢城矿业有限公司 Room structure of shallow-hole shrinkage mining method for mining near-surface thick, large and more oblique ore body
CN110656939A (en) * 2019-09-12 2020-01-07 北京科技大学 Large-stage efficient mining method for steeply inclined medium-thickness ore body meeting water argillization surrounding rock
CN110952981A (en) * 2019-11-14 2020-04-03 南华大学 Residual ore mining method for gently inclined medium-thick and large ore body

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1314066A1 (en) * 1986-01-22 1987-05-30 Новочеркасский Политехнический Институт Им.Серго Орджоникидзе Method of mining ore bodies
SU1608345A1 (en) * 1988-12-09 1990-11-23 Московский Геологоразведочный Институт Им.Серго Орджоникидзе Method of mining mineral deposits
CN203452793U (en) * 2013-07-10 2014-02-26 济南钢城矿业有限公司 Room structure of shallow-hole shrinkage mining method for mining near-surface thick, large and more oblique ore body
CN110656939A (en) * 2019-09-12 2020-01-07 北京科技大学 Large-stage efficient mining method for steeply inclined medium-thickness ore body meeting water argillization surrounding rock
CN110952981A (en) * 2019-11-14 2020-04-03 南华大学 Residual ore mining method for gently inclined medium-thick and large ore body

Also Published As

Publication number Publication date
CN113550751B (en) 2022-06-03

Similar Documents

Publication Publication Date Title
CN103089275B (en) Control method of surrounding rocks in water-rich very-broken surrounding rock tunnel collapse sections
CN105422170B (en) Middle deep goaf grouting reinforcing and processing method under a kind of building foundation
CN104612695B (en) One acutely collapses shaft wall restoring and fastening method
CN104358572B (en) Non-pillar mining technology by spontaneous caving filling roadway at large inclined angle steeply inclined seam
CN104929666A (en) Top breaking gob-side entry retaining method for tender roofs
CN106150508B (en) A kind of tunnel drilling operation method in karst strata
CN104532818A (en) Treatment method for strip mine goaf
CN114837663B (en) Construction method for improving recovery rate of fault waterproof coal pillar through ground pre-grouting
WO2022247176A1 (en) Filling caving mining method
CN111997616B (en) Method for continuously recycling residual top-bottom column by adopting large section
CN103046955A (en) Large-range goaf group filling method
CN112610218B (en) Thick coal seam fully-mechanized top-tunneling top-cutting pressure relief automatic roadway forming method
CN108952732A (en) A kind of excavation construction method suitable for rich water fault belt large cross-section tunnel
CN113202471B (en) In-situ leaching mining method for pillar ore body of underground mine
CN113175325A (en) Coal and intergrown sandstone type uranium ore coordinated mining method based on key layer protection
CN109611146B (en) Separation layer water drainage grouting method
CN105804748A (en) Method for mining hanging wall ore by subareas under open-air transportation system
CN104088637A (en) Method for second mining of upper-group shallow residual coal under coal seam group conditions
CN113550751B (en) Method for recovering near-surface caving ore body
CN111663945A (en) Open roof cutting roadway type upward wide drift filling mining method
CN113818882B (en) Method for recycling stope jack posts under loose tailing filling body
CN110552701A (en) Partitioned combined filling mining method
CN113217044B (en) Upward and oblique scattering type grouting water plugging method for deep large fault tunnel
CN112302718B (en) Method for protecting water resource of water-bearing stratum of coal seam roof
CN116335665B (en) Mining method for constructing near-horizontal thin ore body under top-protection layer stoping water body

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant