CN113514382A - 评价含膨胀粘土气藏岩石水相渗吸返排后水膜厚度的方法 - Google Patents
评价含膨胀粘土气藏岩石水相渗吸返排后水膜厚度的方法 Download PDFInfo
- Publication number
- CN113514382A CN113514382A CN202110447946.2A CN202110447946A CN113514382A CN 113514382 A CN113514382 A CN 113514382A CN 202110447946 A CN202110447946 A CN 202110447946A CN 113514382 A CN113514382 A CN 113514382A
- Authority
- CN
- China
- Prior art keywords
- water
- flowback
- rock
- core sample
- imbibition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 94
- 239000011435 rock Substances 0.000 title claims abstract description 90
- 238000005213 imbibition Methods 0.000 title claims abstract description 46
- 238000000034 method Methods 0.000 title claims abstract description 36
- 239000004927 clay Substances 0.000 title claims abstract description 19
- 230000008961 swelling Effects 0.000 title claims description 10
- 239000011148 porous material Substances 0.000 claims abstract description 52
- 238000005481 NMR spectroscopy Methods 0.000 claims abstract description 27
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 25
- 238000009826 distribution Methods 0.000 claims abstract description 18
- 238000012360 testing method Methods 0.000 claims abstract description 18
- 238000002474 experimental method Methods 0.000 claims abstract description 14
- 229920006395 saturated elastomer Polymers 0.000 claims abstract description 11
- 238000001035 drying Methods 0.000 claims abstract description 6
- 239000000523 sample Substances 0.000 claims description 75
- 239000007789 gas Substances 0.000 claims description 27
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 18
- 239000012530 fluid Substances 0.000 claims description 18
- 238000002347 injection Methods 0.000 claims description 14
- 239000007924 injection Substances 0.000 claims description 14
- 238000005070 sampling Methods 0.000 claims description 12
- 229910052757 nitrogen Inorganic materials 0.000 claims description 9
- XLYOFNOQVPJJNP-ZSJDYOACSA-N Heavy water Chemical compound [2H]O[2H] XLYOFNOQVPJJNP-ZSJDYOACSA-N 0.000 claims description 8
- 239000007788 liquid Substances 0.000 claims description 4
- 238000005259 measurement Methods 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 230000000704 physical effect Effects 0.000 claims description 4
- 230000008569 process Effects 0.000 claims description 4
- 239000012267 brine Substances 0.000 claims description 2
- 238000004364 calculation method Methods 0.000 claims description 2
- 239000012153 distilled water Substances 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 claims description 2
- 230000000087 stabilizing effect Effects 0.000 claims description 2
- 239000002734 clay mineral Substances 0.000 abstract description 5
- 230000036571 hydration Effects 0.000 abstract description 5
- 238000006703 hydration reaction Methods 0.000 abstract description 5
- 235000019441 ethanol Nutrition 0.000 abstract description 4
- 238000010521 absorption reaction Methods 0.000 abstract 1
- 239000012071 phase Substances 0.000 description 31
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 9
- 229910052753 mercury Inorganic materials 0.000 description 9
- 238000003825 pressing Methods 0.000 description 5
- 238000001179 sorption measurement Methods 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 2
- 238000000418 atomic force spectrum Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 238000013507 mapping Methods 0.000 description 2
- 230000035699 permeability Effects 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 238000005553 drilling Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000013508 migration Methods 0.000 description 1
- 230000005012 migration Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000000696 nitrogen adsorption--desorption isotherm Methods 0.000 description 1
- 238000009659 non-destructive testing Methods 0.000 description 1
- 238000001225 nuclear magnetic resonance method Methods 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Images
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/08—Investigating permeability, pore-volume, or surface area of porous materials
- G01N15/088—Investigating volume, surface area, size or distribution of pores; Porosimetry
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N24/00—Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects
- G01N24/08—Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects by using nuclear magnetic resonance
- G01N24/081—Making measurements of geologic samples, e.g. measurements of moisture, pH, porosity, permeability, tortuosity or viscosity
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N24/00—Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects
- G01N24/08—Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects by using nuclear magnetic resonance
- G01N24/082—Measurement of solid, liquid or gas content
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/24—Earth materials
- G01N33/246—Earth materials for water content
Landscapes
- Physics & Mathematics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Pathology (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- High Energy & Nuclear Physics (AREA)
- Engineering & Computer Science (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Geology (AREA)
- Geochemistry & Mineralogy (AREA)
- Dispersion Chemistry (AREA)
- Remote Sensing (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Sampling And Sample Adjustment (AREA)
- Geophysics And Detection Of Objects (AREA)
Abstract
Description
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202110447946.2A CN113514382B (zh) | 2021-04-25 | 2021-04-25 | 评价含膨胀粘土气藏岩石水相渗吸返排后水膜厚度的方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202110447946.2A CN113514382B (zh) | 2021-04-25 | 2021-04-25 | 评价含膨胀粘土气藏岩石水相渗吸返排后水膜厚度的方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN113514382A true CN113514382A (zh) | 2021-10-19 |
CN113514382B CN113514382B (zh) | 2024-04-05 |
Family
ID=78061517
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN202110447946.2A Active CN113514382B (zh) | 2021-04-25 | 2021-04-25 | 评价含膨胀粘土气藏岩石水相渗吸返排后水膜厚度的方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN113514382B (zh) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114048695A (zh) * | 2021-11-10 | 2022-02-15 | 西南石油大学 | 一种基于返排数据的页岩气有效缝网体积反演方法 |
CN114778410A (zh) * | 2022-04-24 | 2022-07-22 | 西安石油大学 | 一种岩石孔隙结构的化验设备 |
CN114858683A (zh) * | 2022-05-20 | 2022-08-05 | 西南石油大学 | 一种评价储气库岩心结盐后孔隙结构变化的方法 |
CN115078438A (zh) * | 2022-06-19 | 2022-09-20 | 西南石油大学 | 一种基于核磁共振测试数字岩心建立孔隙网络模型的方法 |
Citations (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20120136578A1 (en) * | 2010-10-20 | 2012-05-31 | The Petroleum Institute | Rise in core wettability characterization method |
CN103018153A (zh) * | 2012-12-25 | 2013-04-03 | 上海大学 | 一种渗流流场端部效应的评价方法 |
CN104034645A (zh) * | 2014-06-07 | 2014-09-10 | 向丹 | 一种页岩气储层孔隙结构的检测算法 |
CN104200105A (zh) * | 2014-09-05 | 2014-12-10 | 中国石油大学(华东) | 确定致密砂岩气充注物性下限的方法 |
CN104237957A (zh) * | 2014-10-20 | 2014-12-24 | 中国石油大学 | 一种核磁共振测井t2截止值的确定方法 |
US20150198036A1 (en) * | 2014-01-13 | 2015-07-16 | Schlumberger Technology Corporation | Method for estimating irreducible water saturation from mercury injection capillary pressure |
CN104990851A (zh) * | 2015-06-23 | 2015-10-21 | 西南石油大学 | 一种新的页岩敏感性实验研究方法 |
CN108414424A (zh) * | 2018-05-08 | 2018-08-17 | 中国石油天然气股份有限公司 | 一种确定储层边界层厚度的方法、装置及*** |
CN109781765A (zh) * | 2019-01-18 | 2019-05-21 | 西南石油大学 | 一种计算致密储层束缚水液膜厚度的新方法 |
EP3569755A1 (en) * | 2018-04-24 | 2019-11-20 | LG Electronics Inc. | Washing machine and control method thereof |
CN110687155A (zh) * | 2019-10-22 | 2020-01-14 | 长安大学 | 一种土壤薄膜水厚度的测试方法 |
US20200132584A1 (en) * | 2018-10-29 | 2020-04-30 | University Of Manitoba | Characterization of Porous Materials Using Gas Expansion Induced Water Intrusion Porosimetry |
US20200173902A1 (en) * | 2018-03-27 | 2020-06-04 | Min Wang | Evaluation method for hydrogen-bearing components, porosity and pore size distribution of organic-rich shale |
CN111521532A (zh) * | 2019-02-01 | 2020-08-11 | 中国石油天然气股份有限公司 | 一种致密储层含气饱和度的测定方法 |
CN111650108A (zh) * | 2020-06-19 | 2020-09-11 | 中国石油天然气股份有限公司 | 一种测定泥页岩岩石有效孔隙度的方法及装置 |
CN111751242A (zh) * | 2020-06-19 | 2020-10-09 | 中国石油天然气股份有限公司 | 一种泥页岩油气储层岩石油水饱和度准确测量方法 |
CN112147049A (zh) * | 2019-06-11 | 2020-12-29 | 中国石油化工股份有限公司 | 一种岩心水膜厚度的确定方法 |
CA3152100A1 (en) * | 2019-09-30 | 2021-04-08 | Wenyi Huang | Polyolefin-based microporous films via sequential cold and hot stretching of unannealed polypropylene copolymer films |
-
2021
- 2021-04-25 CN CN202110447946.2A patent/CN113514382B/zh active Active
Patent Citations (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20120136578A1 (en) * | 2010-10-20 | 2012-05-31 | The Petroleum Institute | Rise in core wettability characterization method |
CN103018153A (zh) * | 2012-12-25 | 2013-04-03 | 上海大学 | 一种渗流流场端部效应的评价方法 |
US20150198036A1 (en) * | 2014-01-13 | 2015-07-16 | Schlumberger Technology Corporation | Method for estimating irreducible water saturation from mercury injection capillary pressure |
CN104034645A (zh) * | 2014-06-07 | 2014-09-10 | 向丹 | 一种页岩气储层孔隙结构的检测算法 |
CN104200105A (zh) * | 2014-09-05 | 2014-12-10 | 中国石油大学(华东) | 确定致密砂岩气充注物性下限的方法 |
CN104237957A (zh) * | 2014-10-20 | 2014-12-24 | 中国石油大学 | 一种核磁共振测井t2截止值的确定方法 |
CN104990851A (zh) * | 2015-06-23 | 2015-10-21 | 西南石油大学 | 一种新的页岩敏感性实验研究方法 |
US20200173902A1 (en) * | 2018-03-27 | 2020-06-04 | Min Wang | Evaluation method for hydrogen-bearing components, porosity and pore size distribution of organic-rich shale |
EP3569755A1 (en) * | 2018-04-24 | 2019-11-20 | LG Electronics Inc. | Washing machine and control method thereof |
CN108414424A (zh) * | 2018-05-08 | 2018-08-17 | 中国石油天然气股份有限公司 | 一种确定储层边界层厚度的方法、装置及*** |
US20200132584A1 (en) * | 2018-10-29 | 2020-04-30 | University Of Manitoba | Characterization of Porous Materials Using Gas Expansion Induced Water Intrusion Porosimetry |
CN109781765A (zh) * | 2019-01-18 | 2019-05-21 | 西南石油大学 | 一种计算致密储层束缚水液膜厚度的新方法 |
CN111521532A (zh) * | 2019-02-01 | 2020-08-11 | 中国石油天然气股份有限公司 | 一种致密储层含气饱和度的测定方法 |
CN112147049A (zh) * | 2019-06-11 | 2020-12-29 | 中国石油化工股份有限公司 | 一种岩心水膜厚度的确定方法 |
CA3152100A1 (en) * | 2019-09-30 | 2021-04-08 | Wenyi Huang | Polyolefin-based microporous films via sequential cold and hot stretching of unannealed polypropylene copolymer films |
CN110687155A (zh) * | 2019-10-22 | 2020-01-14 | 长安大学 | 一种土壤薄膜水厚度的测试方法 |
CN111650108A (zh) * | 2020-06-19 | 2020-09-11 | 中国石油天然气股份有限公司 | 一种测定泥页岩岩石有效孔隙度的方法及装置 |
CN111751242A (zh) * | 2020-06-19 | 2020-10-09 | 中国石油天然气股份有限公司 | 一种泥页岩油气储层岩石油水饱和度准确测量方法 |
Non-Patent Citations (7)
Title |
---|
CHENG YEN-BEN: "Estimating vegetation water content with hyperspectral data for different canopy scenarios: Relationships between AVIRIS and MODIS indexes", 《REMOTE SENSING OF ENVIRONMENT》, vol. 105, no. 4, 30 December 2006 (2006-12-30), pages 354 - 366 * |
DALKILIC A. S.: "Effect of void fraction models on the film thickness of R134a during downward condensation in a vertical smooth tube", 《INTERNATIONAL COMMUNICATIONS IN HEAT AND MASS TRANSFER》, vol. 36, no. 2, 1 February 2009 (2009-02-01), pages 172 - 179, XP025917443, DOI: 10.1016/j.icheatmasstransfer.2008.10.015 * |
LI YING: "Analysis of Spectral Characteristics of Oil Film on Water Based on Wavelet Transform", 《SPECTROSCOPY AND SPECTRAL ANALYSIS》, vol. 32, no. 7, 2 October 2012 (2012-10-02), pages 1923 - 1927 * |
丁娱娇: "基于核磁共振T_2谱集中度的低孔隙度低渗透率储层饱和度参数研究", 《测井技术》, no. 04, 20 August 2017 (2017-08-20), pages 26 - 32 * |
俞缙: "水化学与冻融循环共同作用下砂岩细观损伤与力学性能劣化试验研究", 《 岩土力学》, vol. 40, no. 2, 13 July 2018 (2018-07-13), pages 455 - 464 * |
唐洪明: "克拉苏气田超致密砂岩气储层水锁损害", 《断块油气田》, vol. 24, no. 4, 25 July 2017 (2017-07-25), pages 541 - 545 * |
邓少贵: "致密含气砂岩核磁共振—声波速度联合实验", 《石油学报》, vol. 37, no. 6, 31 December 2016 (2016-12-31), pages 768 - 776 * |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114048695A (zh) * | 2021-11-10 | 2022-02-15 | 西南石油大学 | 一种基于返排数据的页岩气有效缝网体积反演方法 |
CN114048695B (zh) * | 2021-11-10 | 2022-09-09 | 西南石油大学 | 一种基于返排数据的页岩气有效缝网体积反演方法 |
CN114778410A (zh) * | 2022-04-24 | 2022-07-22 | 西安石油大学 | 一种岩石孔隙结构的化验设备 |
CN114858683A (zh) * | 2022-05-20 | 2022-08-05 | 西南石油大学 | 一种评价储气库岩心结盐后孔隙结构变化的方法 |
CN115078438A (zh) * | 2022-06-19 | 2022-09-20 | 西南石油大学 | 一种基于核磁共振测试数字岩心建立孔隙网络模型的方法 |
Also Published As
Publication number | Publication date |
---|---|
CN113514382B (zh) | 2024-04-05 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN113514382B (zh) | 评价含膨胀粘土气藏岩石水相渗吸返排后水膜厚度的方法 | |
Cheng et al. | New insights into spontaneous imbibition in tight oil sandstones with NMR | |
CN100594369C (zh) | 评估采自地下库藏的岩石切割物的物理参数的方法及装置 | |
Yuan et al. | Spontaneous imbibition in coal: Experimental and model analysis | |
CN109001243B (zh) | 一种采用低场核磁共振评价煤的动态水锁效应的方法与装置 | |
CN106153662A (zh) | 岩心应力敏感性的测量方法 | |
CN107727679A (zh) | 一种表征深层碳酸盐岩岩石物理学特征方法 | |
Niu et al. | Experimental study of permeability changes and its influencing factors with CO2 injection in coal | |
CN106501144A (zh) | 一种基于核磁共振双截止值的致密砂岩渗透率计算方法 | |
CN109283029B (zh) | 一种测量黏土结合水和力学参数的方法、装置及黏土制备仪 | |
Chang et al. | Behavior and mechanism of water imbibition and its influence on gas permeability during hydro-fracturing of a coalbed methane reservoir | |
Liu et al. | The impacts of flow velocity on permeability and porosity of coals by core flooding and nuclear magnetic resonance: implications for coalbed methane production | |
CN113866069B (zh) | 一种页岩岩心渗透率实验装置和方法 | |
CN105547958A (zh) | 一种用于页岩的自发渗吸测量方法 | |
Carles et al. | Low permeability measurements using steady-state and transient methods | |
Xu et al. | Quantitatively study on imbibition of fracturing fluid in tight sandstone reservoir under high temperature and high pressure based on NMR technology | |
Xiong et al. | Experimental investigation of foam-assisted N2 huff-n-puff enhanced oil recovery in fractured shale cores | |
Zhou et al. | The determination of surface relaxivity and application to coal spontaneous imbibition | |
Jiang et al. | Study on spontaneous imbibition and displacement characteristics of mixed-wet tight sandstone reservoir based on high-precision balance and NMR method | |
CN113916745B (zh) | 一种无损测量水驱气藏微观孔隙结构变化规律的实验方法 | |
CN212748663U (zh) | 一种非稳态气水相渗测试装置 | |
Zeng et al. | Pore-fracture network alteration during forced and spontaneous imbibition processes in shale formation | |
Vogt et al. | Magnetic resonance measurements of flow-path enhancement during supercritical CO2 injection in sandstone and carbonate rock cores | |
Blöcher et al. | Impact of poroelastic response of sandstones on geothermal power production | |
CN104948150A (zh) | 一种确定地层排驱压力的方法和装置 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
CB03 | Change of inventor or designer information |
Inventor after: Li Ying Inventor after: Luo Yiyuan Inventor after: Li Haitao Inventor after: Zhang Qihui Inventor after: Luo Hongwen Inventor after: Ye Kairui Inventor after: Chen Mingjun Inventor before: Li Ying Inventor before: Luo Yiyuan Inventor before: Li Haitao Inventor before: Zhang Qihui Inventor before: Luo Hongwen Inventor before: Ye Kairui Inventor before: Chen Mingjun |
|
CB03 | Change of inventor or designer information |