CN113501859A - Lycium barbarum glycopeptide purification and standing equipment and use method thereof - Google Patents
Lycium barbarum glycopeptide purification and standing equipment and use method thereof Download PDFInfo
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- CN113501859A CN113501859A CN202110745633.5A CN202110745633A CN113501859A CN 113501859 A CN113501859 A CN 113501859A CN 202110745633 A CN202110745633 A CN 202110745633A CN 113501859 A CN113501859 A CN 113501859A
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- C07K1/34—Extraction; Separation; Purification by filtration, ultrafiltration or reverse osmosis
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07K—PEPTIDES
- C07K1/00—General methods for the preparation of peptides, i.e. processes for the organic chemical preparation of peptides or proteins of any length
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Abstract
The invention provides a medlar glycopeptide purification standing device and a use method thereof, relating to the technical field of medlar glycopeptide purification, the medlar glycopeptide purification standing device comprises a bottom plate, wherein the upper surface of the bottom plate is fixedly provided with a heat preservation liquid circulating tube through a support, two ends of the heat preservation liquid circulating tube are respectively provided with a connecting pipeline, the two connecting pipelines are respectively and fixedly connected with a first heat preservation liquid circulating pipeline and a second heat preservation liquid circulating pipeline, the first heat preservation liquid circulating pipeline and the second heat preservation liquid circulating pipeline are respectively and fixedly connected on an inlet and an outlet of a heat preservation liquid circulating water pump, the joint of a feeding pipeline and an upper cover is provided with a first pumping pump, the standing tube is fixed on the upper surface of the bottom plate, the medlar glycopeptide dialysis area is reduced, meanwhile, the medlar glycopeptide can be filtered for multiple times, and the purity of the medlar glycopeptide is improved, the device avoids the problem of blockage of the dialysis membrane, accelerates the production rate and improves the production quality of the lycium barbarum glycopeptide.
Description
Technical Field
The invention relates to the technical field of lycium barbarum glycopeptide purification, in particular to lycium barbarum glycopeptide purification and standing equipment and a using method thereof.
Background
The lycium barbarum glycopeptide is 5 glycoconjugates with stronger immunological activity and anti-aging effect obtained by further separating and purifying lycium barbarum polysaccharide, after the lycium barbarum glycopeptide is prepared in a series of ways, further purification is needed to meet the market demand due to low internal concentration, the existing lycium barbarum glycopeptide purification method is a method of centrifugation, filtration and the like, and still standing is needed for 8-10 hours after purification is finished, so that the preparation of the lycium barbarum glycopeptide is completed.
When matrimony vine glycopeptide filters, adopt the mode of dialysis membrane, but current filter equipment is processing, can have the problem of dialysis membrane jam to influence matrimony vine glycopeptide's production procedure, consume a large amount of time and maintain, and still can have matrimony vine glycopeptide too big at equipment pressure during the filtration, the velocity of flow produces inside temperature at the excessive speed higher, thereby influenced matrimony vine glycopeptide's production quality, and the cold-stored temperature is difficult to remain stable when stewing, influences matrimony vine glycopeptide's production quality equally.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides medlar glycopeptide purification and standing equipment and a using method thereof, and solves the problems that when an existing filtering device is processed, a dialysis membrane is blocked, so that the production flow of medlar glycopeptide is influenced, a large amount of time is consumed for maintenance, and during filtering, the medlar glycopeptide has the problems that the internal temperature is higher due to overlarge equipment pressure and too high flow speed, so that the production quality of the medlar glycopeptide is influenced, the temperature is difficult to keep stable during cold storage and standing, and the production quality of the medlar glycopeptide is also influenced.
(II) technical scheme
In order to achieve the purpose, the invention is realized by the following technical scheme: the wolfberry glycopeptide purification standing equipment comprises a bottom plate, wherein a heat preservation liquid circulating cylinder is fixedly mounted on the upper surface of the bottom plate through a support, connecting pipelines are arranged at two ends of the heat preservation liquid circulating cylinder, the two connecting pipelines are respectively and fixedly connected with a first heat preservation liquid circulating pipeline and a second heat preservation liquid circulating pipeline, the first heat preservation liquid circulating pipeline and the second heat preservation liquid circulating pipeline are respectively and fixedly connected to an inlet and an outlet of a heat preservation liquid circulating water pump and a water outlet of the heat preservation liquid circulating water pump, a filtering assembly is arranged at the upper end of a spiral filtering pipeline, a filtrate collecting assembly is arranged on the filtering assembly, a first flow collecting ball is arranged between a discharge port of the spiral filtering pipeline and a feeding pipeline, a first material pumping pump is arranged at the joint of the feeding pipeline and an upper cover, the upper cover is clamped at the upper end of the standing cylinder, and the standing cylinder is fixed on the upper surface of the bottom plate.
Preferably, the upper end of the heat-preservation liquid circulation cylinder is provided with an upper supporting groove, one side of the upper supporting groove is provided with a clamping groove, the upper supporting groove is tightly attached to an upper supporting plate, a connecting plate on one side of the upper supporting plate is provided with a second screw hole fixedly connected with the heat-preservation liquid circulation cylinder, and the clamping plate is provided with a first screw hole fixedly connected with the heat-preservation liquid circulation cylinder.
Preferably, the filtering component comprises a cutting groove, filtering sleeves, a sealing ring, a dialysis membrane, a fixing plate and a pipeline groove, each filtering sleeve is fixedly connected with the upper support plate through the fixing plate at the lower end, the filtering sleeves are distributed at equal intervals, and each filtering sleeve corresponds to the cutting groove formed in the spiral filtering pipeline.
Preferably, a sealing ring is arranged at the joint of the two ends of each filtering sleeve and the spiral filtering pipeline, a dialysis membrane is fixed on one side of the inner wall of each filtering sleeve, and a pipeline groove connected with a filtrate collecting component is formed in the upper end of each filtering sleeve.
Preferably, the filtrate collecting assembly comprises a plurality of filtrate inflow pipelines, a filtrate suction pump and a filtrate collecting box, each filtrate inflow pipeline is fixedly connected to each pipeline slot, each filtrate inflow pipeline is fixedly connected with the filtrate collecting assembly fixed on the upper surface of the bottom plate, and each filtrate inflow pipeline is provided with the filtrate suction pump.
Preferably, the inner wall of the standing barrel is fixedly connected with an inner barrel through a plurality of connecting rods, each inner barrel and a hollow groove of the standing barrel are provided with an ice block placing groove, and the standing barrel is provided with a discharging pipe and a water discharging pipe.
Preferably, the lower end of the upper cover is fixedly connected with a first sealing ring and a second sealing ring, two sides of the first sealing ring are attached to the ice block placing groove, the outer wall of the second sealing ring is attached to the inner wall of the inner barrel, and the upper cover is further provided with an air pumping pipe, an air valve pipe and a water inflow pipe.
Preferably, the first heat preservation liquid circulating pipeline comprises a first direct current pipeline, a straight pipe, a second flow collecting ball, a first curve flow pipe and a second direct current pipeline, the straight pipe is fixed on the connecting pipeline, the second flow collecting ball is fixedly connected with the joint of one end, far away from the connecting pipeline, of the straight pipe and the first curve flow pipe, the first curve flow pipe is connected with the first direct current pipeline, the second heat preservation liquid circulating pipeline comprises a third direct current pipeline, a second curve flow pipe and a fourth direct current pipeline, and the third direct current pipeline and the fourth direct current pipeline are connected with the second curve flow pipe.
Meanwhile, the invention also discloses a use method of the lycium barbarum glycopeptide purification and standing equipment, which comprises the following operation steps:
s1: connecting a pipeline of equipment for storing the primarily processed lycium barbarum glycopeptide with a spiral filtering pipeline, starting a first material pumping pump to drive the lycium barbarum glycopeptide to a discharge port in the spiral filtering pipeline, filtering impurities contained in the lycium barbarum glycopeptide through a dialysis membrane when the lycium barbarum glycopeptide passes through the upper part of the spiral filtering pipeline, and starting a filtrate material pumping pump to adsorb the impurities in front of the dialysis membrane to a filtrate collecting box when the equipment for accumulating more impurities in front of the dialysis membrane is difficult to filter;
s2: when the lycium barbarum glycopeptide is filtered, the heat preservation liquid circulating water pump is started at the same time, and the heat preservation liquid circulating cylinder is circulated through the operation of the heat preservation liquid circulating water pump, so that the internal environment temperature of the tightly attached spiral filtering pipeline is stable, meanwhile, the first curve flow pipe and the second curve flow pipe can slow the flow speed of the heat preservation liquid, the effect of the heat preservation liquid on the spiral filtering pipeline is further improved, and the first flow collecting ball can prevent the lycium barbarum glycopeptide from being blocked;
s3: fill in the ice-cube standing groove inside and be full of the ice-cube, the height and the ice-cube standing groove parallel and level of ice-cube, then with the upper cover chucking in a section of thick bamboo that stews, then pour into water through the water inflow pipe, take out through the air and press the union coupling pump to manage to find time the air of inside to at the lycium barbarum glycopeptide including a section of thick bamboo stand and reach vacuum and cold-stored effect.
(III) advantageous effects
The invention provides a medlar glycopeptide purification and standing device, which has the following beneficial effects:
1. the pipeline of the equipment that will deposit the matrimony vine glycopeptide that the preliminary working is good links to each other with spiral filter tube, then start first pump of drawing material and carry out the matrimony vine glycopeptide to the discharge gate in spiral filter tube, can filter the impurity that contains in the matrimony vine glycopeptide through the dialysis membrane in the top of matrimony vine glycopeptide process spiral filter tube every time, pile up more impurity equipment before the dialysis membrane and filter the difficulty, start the impurity that the material pump of drawing material of straining adsorbs to straining the thing collecting box before the dialysis membrane face, through the inside circulation matrimony vine glycopeptide of spiral tube, matrimony vine glycopeptide dialysis area has been reduced, make matrimony vine glycopeptide can carry out a lot of filtration simultaneously, the purity that the matrimony vine glycopeptide was prepared has been improved, make equipment avoid the problem that the dialysis membrane blocks up, the production rate has been accelerated, the quality of matrimony vine glycopeptide production has been improved.
2. Operation through heat preservation liquid circulating water pump will be located a heat preservation liquid circulation section of thick bamboo and carry out circulation, thereby make the stability of the internal environment temperature who pastes the spiral filtration pipeline tightly, the first bend flow tube that is equipped with simultaneously, the velocity of flow of second bend flow tube can slow heat preservation liquid, make heat preservation liquid further improve spiral filtration pipeline's effect, the jam of matrimony vine glycopeptide can be prevented to the first mass flow ball that is equipped with, thereby improved the heat absorption of heat preservation liquid to the inside temperature of spiral filtration pipeline, the temperature of internal environment has been kept, avoided leading to the production quality of matrimony vine glycopeptide low because of the temperature is overheated.
3. Fill in at the ice-cube standing groove is inside to be full of the ice-cube, the height and the ice-cube standing groove parallel and level of ice-cube, then with the upper cover chucking in a section of thick bamboo that stews, then pour into water through the water inflow pipe, take out through the air and press the union coupling and take out the pump and manage to find time the air of inside to a section of thick bamboo stews including matrimony vine glycopeptide and reaches vacuum and cold-stored effect, because the temperature of ice water mixture is zero degree usually, the stability of keeping inside temperature that can be fine has improved the practicality of equipment.
Drawings
FIG. 1 is a schematic view of the overall structure of the present invention;
FIG. 2 is a schematic diagram of the construction of the spiral filtration duct of the present invention;
FIG. 3 is a schematic view of the filter cartridge of the present invention;
FIG. 4 is a schematic structural view of a first heat-retaining liquid circulation pipeline according to the present invention;
FIG. 5 is a schematic structural view of a second insulating liquid circulation pipeline according to the present invention;
FIG. 6 is a schematic view of a resting cartridge of the present invention;
fig. 7 is a schematic view of the upper cover of the present invention.
Wherein, 1, a bottom plate; 2. a heat preservation liquid circulating water pump; 3. a filter assembly; 301. grooving; 302. a filter cartridge; 303. a seal ring; 304. a dialysis membrane; 305. a fixing plate; 306. a pipe chase; 4. a first current collecting ball; 5. a second heat preservation liquid circulation pipeline; 501. a third direct current conduit; 502. a second curved flow tube; 503. a fourth direct current conduit; 6. a feed line; 7. a spiral filtration duct; 8. a filtrate collection assembly; 801. the filtered materials flow into a pipeline; 802. a filtrate pump; 803. a filtrate collection box; 9. a first pump; 10. a heat preservation liquid circulation cylinder; 1001. a card slot; 1002. a first screw hole; 1003. clamping a plate; 1004. an upper support plate; 1005. an upper supporting groove; 1006. a connecting plate; 1007. a second screw hole; 11. connecting a pipeline; 12. a first heat-preserving fluid circulation pipeline; 1201. a first direct current conduit; 1202. a straight pipe; 1203. a second current collecting ball; 1204. a first curved flow tube; 1205. a second direct current conduit; 13. an upper cover; 1301. an air pressure pipe; 1302. an air valve tube; 1303. a water inflow pipe; 1304. a first seal ring; 1305. a second seal ring; 14. a standing cylinder; 1401. an ice block placing groove; 1402. a connecting rod; 1403. an inner barrel; 1404. a discharge pipe; 1405. a water discharge pipe.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example (b):
as shown in fig. 1, 2, 3, 4, 5, 6, and 7, an embodiment of the present invention provides a lycium barbarum glycopeptide purification standing apparatus, which includes a bottom plate 1, an insulation liquid circulation cylinder 10 is fixedly installed on an upper surface of the bottom plate 1 through a support, connection pipes 11 are respectively installed at two ends of the insulation liquid circulation cylinder 10, a first insulation liquid circulation pipe 12 and a second insulation liquid circulation pipe 5 are respectively and fixedly connected to the two connection pipes 11, the first insulation liquid circulation pipe 12 and the second insulation liquid circulation pipe 5 are respectively and fixedly connected to an inlet and an outlet of the insulation liquid circulation water pump 2, a filter assembly 3 is installed at an upper end of a spiral filter pipe 7, a filter collection assembly 8 is installed on the filter assembly 3, a first flow-collecting ball 4 is installed between a discharge port of the spiral filter pipe 7 and a feeding pipe 6, a first pumping pump 9 is installed at a connection between the feeding pipe 6 and an upper cover 13, the upper cover 13 is tightly clamped at an upper end of the standing cylinder 14, the standing cylinder 14 is fixed on the upper surface of the bottom plate 1.
According to the technical scheme, the pipeline of the equipment for storing the primarily processed lycium barbarum glycopeptide is connected with the spiral filtering pipeline 7, then the first material pumping pump 9 is started to drive the lycium barbarum glycopeptide to the discharge hole in the spiral filtering pipeline 7, when the lycium barbarum glycopeptide passes through the upper part of the spiral filtering pipeline 7, impurities contained in the lycium barbarum glycopeptide can be filtered through the dialysis membrane 304, when more impurities are accumulated in front of the dialysis membrane 304 and the filtration is difficult, the filtrate material pumping pump 802 is started to adsorb the impurities in front of the dialysis membrane 304 to the filtrate collection box 803, the lycium barbarum glycopeptide circulates through the spiral pipe, the lycium barbarum glycopeptide dialysis area is reduced, meanwhile, the lycium barbarum glycopeptide can be filtered for multiple times, the purity of the lycium barbarum glycopeptide preparation is improved, the quality of the lycium barbarum glycopeptide production is improved, and the lycium barbarum glycopeptide circulating circulation cylinder 10 is positioned through the operation of the heat preservation liquid circulating water pump 2, thereby make the stability of the internal environment temperature who pastes tight spiral filtration pipeline 7, the first bend flow tube 1204 that is equipped with simultaneously, the velocity of flow of second bend flow tube 502 can slow heat preservation liquid, make heat preservation liquid further improve spiral filtration pipeline 7's effect, the jam of matrimony vine glycopeptide can be prevented to first mass flow ball 4 that is equipped with, thereby improved the heat absorption of heat preservation liquid to the inside temperature of spiral filtration pipeline, the temperature of internal environment has been kept, avoided leading to the production quality of matrimony vine glycopeptide low because of the temperature is overheated.
It should be noted that, the upper end of the thermal insulation liquid circulation cylinder 10 is provided with an upper supporting groove 1005, one side of the upper supporting groove 1005 is provided with a clamping groove 1001, the upper supporting groove 1005 is tightly attached to an upper supporting plate 1004, a connecting plate 1006 at one side of the upper supporting plate 1004 is provided with a second screw hole 1007 fixedly connected to the thermal insulation liquid circulation cylinder 10, a first screw hole 1002 fixed to the thermal insulation liquid circulation cylinder 10 is provided on a clamping plate 1003, the filter assembly 3 comprises a cutting groove 301, a filter sleeve 302, a sealing ring 303, a dialysis membrane 304, a fixing plate 305 and a pipeline groove 306, each filter sleeve 302 is fixedly connected to the upper supporting plate 1004 through the fixing plate 305 at the lower end, each filter sleeve 302 is distributed at equal intervals, each filter sleeve 302 corresponds to the cutting groove 301 provided on the spiral filter pipeline 7, the ice block placing groove 1401 is filled with ice blocks, the height of the ice blocks is flush with the ice block placing groove 1401, then the upper cover 13 is tightly clamped in the standing cylinder 14, and water is poured through a water inflow pipe 1303, the pressure pumping pump is connected with the pressure pumping pump through the air pressure pumping pipe 1301 to evacuate the air inside, so that the lycium barbarum glycopeptide stands still on the inner barrel 1403 to achieve the effects of vacuum and refrigeration, and because the temperature of the ice-water mixture is always zero, the stability of the internal temperature can be well kept, and the practicability of the equipment is improved.
Wherein, the joint of the two ends of each filtering sleeve 302 and the spiral filtering pipe 7 is provided with a sealing ring 303, one side of the inner wall of the filtering sleeve 302 is fixed with a dialysis membrane 304, the upper end of the filtering sleeve 302 is provided with a pipe groove 306 connected with a filtering material collecting component 8, the filtering material collecting component 8 comprises a plurality of filtering material inflow pipes 801, a filtering material pumping pump 802 and a filtering material collecting box 803, each filtering material inflow pipe 801 is fixedly connected with each pipe groove 306, each filtering material inflow pipe 801 is fixedly connected with the filtering material collecting component 8 fixed on the upper surface of the bottom plate 1, each filtering material inflow pipe 801 is provided with the filtering material pumping pump 802, the pipe of the device storing the primarily processed medlar glycopeptide is connected with the spiral filtering pipe 7, then the first pumping pump 9 is started to drive the medlar to a discharge port in the spiral filtering pipe 7, when the medlar passes through the upper part of the spiral filtering pipe 7, impurities contained in the medlar can be filtered through the dialysis membrane 304, pile up more impurity equipment before dialysis membrane 304 and filter when difficult, start to filter thing pump 802 and adsorb the impurity in front of dialysis membrane 304 to filtering thing collecting box 803, through the inside circulation matrimony vine glycopeptide of spiral pipe, reduced matrimony vine glycopeptide dialysis area, make matrimony vine glycopeptide can carry out a lot of filtration simultaneously, improved the purity that matrimony vine glycopeptide was prepared.
It can be understood that in the present application, the inner wall of the standing barrel 14 is fixedly connected with the inner barrel 1403 through a plurality of connecting rods 1402, the empty slot existing between each inner barrel 1403 and the standing barrel 14 is set as an ice block placing slot 1401, the standing barrel 14 is provided with a discharge pipe 1404 and a discharge pipe 1405, the lower end of the upper cover 13 is fixedly connected with a first sealing ring 1304 and a second sealing ring 1305, two sides of the first sealing ring 1304 are attached to the ice block placing slot 1401, the outer wall of the second sealing ring 1305 is attached to the inner wall of the inner barrel 1403, the upper cover 13 is further provided with an air pumping pipe 1301, an air valve pipe 1302 and a water inflow pipe 1303, the first insulating liquid circulating pipe 12 comprises a first straight pipe 1201, a straight pipe 1202, a second collecting ball 1203, a first straight pipe 1204 and a second straight pipe 1205, the straight pipe 1202 is fixed on the connecting pipe 11, one end of the straight pipe 1202 far away from the connecting pipe 11 is fixedly connected with the second collecting ball 1203 at the connection with the first pipe 1204, the first curve flow pipe 1204 is connected with the first straight flow pipe 1201, the second heat preservation liquid circulation pipe 5 comprises a third straight flow pipe 501, a second curve flow pipe 502 and a fourth straight flow pipe 503, the third straight flow pipe 501 and the fourth straight flow pipe 503 are connected with the second curve flow pipe 502, the pipe of the equipment for storing the primarily processed lycium barbarum glycopeptide is connected with the spiral filtering pipe 7, then the first pumping pump 9 is started to drive the lycium barbarum glycopeptide in the spiral filtering pipe 7 to the discharge port, whenever the lycium barbarum glycopeptide passes through the upper part of the spiral filtering pipe 7, more impurities contained in the lycium barbarum glycopeptide can be filtered through the dialysis membrane 304, when the impurity equipment accumulated in front of the dialysis membrane 304 is difficult to filter, the filter pumping pump 802 is started to absorb the impurities in front of the dialysis membrane 304 to the filter collection box 803, the lycium barbarum glycopeptide circulates in the spiral pipe, the dialysis area of the lycium barbarum glycopeptide is reduced, meanwhile, the lycium barbarum glycopeptide can be filtered for multiple times, and the purity of the lycium barbarum glycopeptide is improved.
Meanwhile, the invention also discloses a use method of the lycium barbarum glycopeptide purification and standing equipment, which comprises the following operation steps:
s1: connecting a pipeline of equipment for storing the primarily processed lycium barbarum glycopeptide with a spiral filtering pipeline 7, starting a first pumping pump 9 to drive the lycium barbarum glycopeptide in the spiral filtering pipeline 7 to a discharge port, filtering impurities contained in the lycium barbarum glycopeptide through a dialysis membrane 304 when the lycium barbarum glycopeptide passes through the upper part of the spiral filtering pipeline 7, and starting a filtrate pumping pump 802 to adsorb the impurities in front of the dialysis membrane 304 to a filtrate collecting box 803 when the equipment for accumulating more impurities in front of the dialysis membrane 304 is difficult to filter;
s2: when the lycium barbarum glycopeptide is filtered, the heat preservation liquid circulating water pump 2 is started at the same time, the heat preservation liquid circulating cylinder 10 is circulated through the operation of the heat preservation liquid circulating water pump 2, so that the internal environment temperature of the tightly attached spiral filtering pipeline 7 is stable, meanwhile, the first bent flow pipe 1204 and the second bent flow pipe 502 are arranged to slow the flow speed of the heat preservation liquid, the effect of the heat preservation liquid on the spiral filtering pipeline 7 is further improved, and the first flow collecting ball 4 is arranged to prevent the lycium barbarum glycopeptide from being blocked;
s3: the ice cube placing groove 1401 is filled with ice cubes, the height of the ice cubes is flush with the ice cube placing groove 1401, the upper cover 13 is clamped in the standing barrel 14, water is poured into the standing barrel 1303 through the water inflow pipe, the air inside the standing barrel is pumped out through the air pumping and pressing pipe 1301 connected with the pumping pump, and therefore the lycium barbarum glycopeptide stands in the inner barrel 1403 to achieve the vacuum and refrigeration effect.
The working principle is as follows: the pipeline that will deposit the equipment of the good matrimony vine glycopeptide of preliminary processing links to each other with spiral filter tube 7, then start first pump 9 of drawing material and exercise the matrimony vine glycopeptide to the discharge gate in spiral filter tube 7, can filter the impurity that contains the matrimony vine glycopeptide through dialysis membrane 304 in the top of spiral filter tube 7 every time, pile up more impurity equipment before dialysis membrane 304 and filter when difficult, start filter pump 802 of drawing material and adsorb the impurity in front of dialysis membrane 304 to filter thing collecting box 803, through the inside circulation matrimony vine glycopeptide of spiral pipe, matrimony vine glycopeptide dialysis area has been reduced, make the matrimony vine glycopeptide can carry out a lot of filtration simultaneously, the purity that the matrimony vine glycopeptide was prepared has been improved, the quality of matrimony vine glycopeptide production has been improved.
Operation through heat preservation liquid circulating water pump 2 will be located heat preservation liquid circulation section of thick bamboo 10 and carry out the circulation, thereby make the stability of the internal environment temperature who pastes tight spiral filtration pipeline 7, the first bend flow tube 1204 that is equipped with simultaneously, the velocity of flow of second bend flow tube 502 can slow heat preservation liquid, make heat preservation liquid further improve spiral filtration pipeline 7's effect, the jam of matrimony vine glycopeptide can be prevented to first mass flow ball 4 that is equipped with, thereby it absorbs heat to the inside temperature of spiral filtration pipeline to have improved heat preservation liquid, the temperature of internal environment has been kept, avoided leading to the production quality of matrimony vine glycopeptide low because of the temperature is overheated.
Fill in the ice-cube standing groove 1401 inside and be full of the ice-cube, the height and the ice-cube standing groove 1401 parallel and level of ice-cube, then with upper cover 13 chucking in a section of thick bamboo 14 that stews, then pour into water through water inflow pipe 1303, take out through the air and press pipe 1301 to connect the pump and manage to find time the air of inside to stew at inner tube 1403 and reach vacuum and cold-stored effect, because the temperature of ice-water mixture is zero degree usually, the stability of the inside temperature of maintenance that can be fine, the practicality of equipment has been improved.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation, an element defined by the phrase "comprising a reference structure" does not exclude the presence of other similar elements in a process, method, article, or apparatus that comprises the element.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (9)
1. The utility model provides a matrimony vine glycopeptide purification equipment of stewing, includes bottom plate (1), its characterized in that: the upper surface of the bottom plate (1) is fixedly provided with a heat preservation liquid circulating cylinder (10) through a support, two ends of the heat preservation liquid circulating cylinder (10) are respectively provided with a connecting pipeline (11), the two connecting pipelines (11) are respectively and fixedly connected with a first heat preservation liquid circulating pipeline (12) and a second heat preservation liquid circulating pipeline (5), the first heat preservation liquid circulating pipeline (12) and the second heat preservation liquid circulating pipeline (5) are respectively and fixedly connected to an inlet and an outlet of a heat preservation liquid circulating water pump (2) and a water outlet, the upper end of the spiral filtering pipeline (7) is provided with a filtering component (3), the filtering component (3) is provided with a filtrate collecting component (8), a first flow collecting ball (4) is arranged between a discharge port of the spiral filtering pipeline (7) and the feeding pipeline (6), and a first material pumping pump (9) is arranged at the joint of the feeding pipeline (6) and the upper cover (13), the upper cover (13) is tightly clamped at the upper end of the standing barrel (14), and the standing barrel (14) is fixed on the upper surface of the bottom plate (1).
2. The lycium barbarum glycopeptide purification and resting device according to claim 1, characterized in that: an upper supporting groove (1005) is formed in the upper end of the heat preservation liquid circulation cylinder (10), a clamping groove (1001) is formed in one side of the upper supporting groove (1005), an upper supporting plate (1004) is attached to the upper supporting groove (1005), a second screw hole (1007) fixedly connected with the heat preservation liquid circulation cylinder (10) is formed in a connecting plate (1006) on one side of the upper supporting plate (1004), and a first screw hole (1002) fixed to the heat preservation liquid circulation cylinder (10) is formed in the clamping plate (1003).
3. The lycium barbarum glycopeptide purification and resting device according to claim 2, characterized in that: the filter assembly (3) comprises a cutting groove (301), filter sleeves (302), a sealing ring (303), a dialysis membrane (304), a fixing plate (305) and a pipeline groove (306), each filter sleeve (302) is fixedly connected with an upper support plate (1004) through the fixing plate (305) at the lower end, the filter sleeves (302) are distributed at equal intervals, and each filter sleeve (302) corresponds to the cutting groove (301) formed in the spiral filter pipeline (7).
4. The lycium barbarum glycopeptide purification and resting device according to claim 3, characterized in that: every the junction of the both ends of filtering sleeve (302) and spiral filtration pipeline (7) is provided with sealing washer (303), it is fixed with dialysis membrane (304) to filter sleeve (302) inner wall one side, filter sleeve (302) upper end and seted up pipeline groove (306) of connecting filtrations thing collection component (8).
5. The lycium barbarum glycopeptide purification and resting device according to claim 3, characterized in that: the filtered material collecting assembly (8) comprises a plurality of filtered material inflow pipelines (801), a filtered material pumping pump (802) and a filtered material collecting box (803), each filtered material inflow pipeline (801) is fixedly connected to each pipeline groove (306), each filtered material inflow pipeline (801) is fixedly connected with the filtered material collecting assembly (8) fixed on the upper surface of the bottom plate (1), and each filtered material inflow pipeline (801) is provided with the filtered material pumping pump (802).
6. The lycium barbarum glycopeptide purification and resting device and the use method thereof according to claim 1, characterized in that: the inner wall of the standing barrel (14) is fixedly connected with an inner barrel (1403) through a plurality of connecting rods (1402), each inner barrel (1403) and an empty groove of the standing barrel (14) are set to be an ice block placing groove (1401), and the standing barrel (14) is provided with a discharge pipe (1404) and a discharge pipe (1405).
7. The lycium barbarum glycopeptide purification and resting device according to claim 5, characterized in that: the ice cube placing device is characterized in that a first sealing ring (1304) and a second sealing ring (1305) are fixedly connected to the lower end of the upper cover (13), two sides of the first sealing ring (1304) are attached to an ice cube placing groove (1401), the outer wall of the second sealing ring (1305) is attached to the inner wall of the inner barrel (1403), and an air pressure pumping pipe (1301), an air valve pipe (1302) and a water inflow pipe (1303) are further arranged on the upper cover (13).
8. The lycium barbarum glycopeptide purification and resting device according to claim 1, characterized in that: the first heat preservation liquid circulating pipeline (12) comprises a first direct current pipeline (1201), a straight pipe (1202), a second flow collecting ball (1203), a first curve flow pipe (1204) and a second direct current pipeline (1205), the straight pipe (1202) is fixed on the connecting pipeline (11), the straight pipe (1202) is far away from the second flow collecting ball (1203) at the joint of one end of the connecting pipeline (11) and the first curve flow pipe (1204), the first curve flow pipe (1204) is connected with the first direct current pipeline (1201), the second heat preservation liquid circulating pipeline (5) comprises a third direct current pipeline (501), a second curve flow pipe (502) and a fourth direct current pipeline (503), and the third direct current pipeline (501) and the fourth direct current pipeline (503) are connected with the second curve flow pipe (502).
9. The use method of the device for purifying and standing lycium barbarum glycopeptide according to any one of claims 1-8, wherein the device comprises: the method comprises the following operation steps:
s1: connecting a pipeline of equipment for storing the primarily processed lycium barbarum glycopeptide with a spiral filtering pipeline (7), then starting a first pumping pump (9) to drive the lycium barbarum glycopeptide to a discharge port in the spiral filtering pipeline (7), filtering impurities contained in the lycium barbarum glycopeptide through a dialysis membrane (304) whenever the lycium barbarum glycopeptide passes through the upper part of the spiral filtering pipeline (7), and starting a filtrate pumping pump (802) to adsorb the impurities in front of the dialysis membrane (304) to a filtrate collecting box (803) when the filtration is difficult due to the equipment for accumulating more impurities in front of the dialysis membrane (304);
s2: when the lycium barbarum glycopeptide is filtered, the heat preservation liquid circulating water pump (2) is started at the same time, and the heat preservation liquid circulating cylinder (10) is located for circulating through the operation of the heat preservation liquid circulating water pump (2), so that the internal environment temperature of the tightly attached spiral filtering pipeline (7) is stable, meanwhile, the first curve flow pipe (1204) and the second curve flow pipe (502) are arranged to slow the flow speed of the heat preservation liquid, the effect of the heat preservation liquid on the spiral filtering pipeline (7) is further improved, and the first flow collecting ball (4) is arranged to prevent the lycium barbarum glycopeptide from being blocked;
s3: the ice cube placing groove (1401) is filled with ice cubes, the height of the ice cubes is flush with the ice cube placing groove (1401), then the upper cover (13) is clamped in the standing barrel (14), water is poured in through the water inflow pipe (1303), the air inside the ice cube placing groove is pumped out through the air pumping pipe (1301) connected with the pumping pump, and therefore the lycium barbarum glycopeptide stands in the inner barrel (1403) to achieve the effects of vacuum and refrigeration.
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