CN113018213B - Lead-in type beauty mask and application thereof - Google Patents
Lead-in type beauty mask and application thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61N—ELECTROTHERAPY; MAGNETOTHERAPY; RADIATION THERAPY; ULTRASOUND THERAPY
- A61N1/00—Electrotherapy; Circuits therefor
- A61N1/18—Applying electric currents by contact electrodes
- A61N1/20—Applying electric currents by contact electrodes continuous direct currents
- A61N1/30—Apparatus for iontophoresis, i.e. transfer of media in ionic state by an electromotoric force into the body, or cataphoresis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/87—Application Devices; Containers; Packaging
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Abstract
The invention relates to a novel leading-in type beauty mask which is prepared from a biological cellulose composite film with conductive performance. The invention adopts the biological cellulose membrane as a base material, and the biological cellulose membrane is coated with conductive polymer to ensure that the biological cellulose membrane has conductive performance, and can realize effective micro-current effect at the using part of the mask after being connected with a micro-current generator or a pulse generator, thereby achieving the effects of skin care and beauty.
Description
Technical Field
The invention relates to the technical field of skin care products, in particular to an imported cosmetic mask and application thereof.
Background
The beauty and medical industry is born in the 90 s of the 20 th century and is based on the expansion of the fields of medicine, optics, electricity, chemistry and the like. Cosmetic instruments have also undergone a further update. The beauty instrument is a machine for regulating and improving the body and the face according to the physiological functions of a human body, and has various functions such as whitening, skin tendering, freckle removal, wrinkle removal, hair removal, weight reduction and the like, and has the functions of an ultrasonic face cleaner, a micro-current face tightening instrument, a blue light acne removal beauty bar, a face thinning electric beauty instrument, an ion leading-in instrument, a face steaming instrument, a hair removal instrument, a nano water supplementing instrument, an ultrasonic color light toxin expelling beauty instrument, a PMD microcrystalline skin grinder, an ion tooth whitening instrument, a laser hair removal instrument, a photon skin tendering instrument and the like. The volume of the device is gradually changed from huge instruments to medium-sized, medium-sized and small-sized instruments, and the small-sized and micro-sized instruments are gradually changed into a trend nowadays. The functions of the hair remover are gradually developed from single depilation, whitening and the like to one machine with multiple functions, the functions tend to be more and more perfect, the development of scientific technology and the application of the hair remover on a cosmetic instrument lead the functions of the hair remover to be more and more diversified and finer. However, these instruments have the disadvantages of high price, large volume, inapplicability to household and personal consumption, etc.
The microcurrent beauty instrument in the prior art is a beauty instrument which acts on a human body through computer microwaves, supplements bioelectricity of the human body, activates cells and recovers skin elasticity, thereby achieving the effects of solving some skin problems and delaying skin aging. Such instruments are commonly used in many care sessions in beauty parlors, such as tightening skin, removing wrinkles, lightening dark circles, etc., with the following cosmetic functions: 1. enhancing cell activity, promoting muscle movement, and recovering skin elasticity; 2. accelerating blood circulation of the capillary, enhancing cell permeability, and effectively supplying nutrients to muscle tissues and skin; 3. the electric ions generated by the micro-current can deeply permeate the skin, and supplement the moisture of the skin to restore and moisten, smooth and tender; 4. the microwave current makes the electric stimulation go deep into subcutaneous tissue to muscle, and helps to repair skin elastic fiber and colloid layer tissue, thereby stretching and weakening wrinkles.
CN105611965a discloses a portable iontophoresis system using a mask, which is to provide an iontophoresis device having two electrodes, one electrode is in contact with the skin of a human body, and the other electrode is connected to one corner of a general mask using forceps, so as to transfer micro-current to the mask; however, the common mask cannot conduct electricity, so that an effective micro-current effect cannot be realized on the face, and the skin beautifying effect is achieved; meanwhile, common metal is in contact with the mask liquid in an electrified state, so that ionic reaction is very easy to occur, and the introduction effect cannot be realized.
Disclosure of Invention
In order to solve the technical defects, the invention provides a novel leading-in type beauty mask which is prepared from a biological cellulose composite film with conductive performance.
Biocellulose (biocellose), also known as bacterial cellulose (Bacterial cellulose, BC), is cellulose synthesized by certain microorganisms of the genus acetobacter, agrobacterium, rhizobium, and the like. Unlike plant cellulose, biological cellulose is not a structural component of bacterial cell walls, but a product secreted by bacteria to the outside of cells, is in an independent filiform fiber form, is cellulose formed by the condensation polymerization of pure glucose, has extremely high cellulose content, is not doped with lignin, hemicellulose and other polysaccharide impurities, and has a very different microfibril mode from plant cellulose. Common bacteria of the biological cellulose producing strain are acetobacter xylinum, acetobacter xylosoxidans and the like. The ultra-high-purity cellulose structure of the biological cellulose gel has gel characteristics and appearance, and the biological cellulose gel has high crystallinity (up to 95%) and high polymerization degree (DP value 2000-8000); has ultra-fine net structure and tensile strength, and also has excellent water holding capacity, high biocompatibility and degradability. Currently, the method is widely applied to various fields such as foods, medicines and the like.
The invention adopts the biological cellulose membrane as a base material, and the biological cellulose membrane is coated with conductive polymer to ensure that the biological cellulose membrane has conductive performance, and can realize effective micro-current effect at the using part of the mask after being connected with a micro-current generator or a pulse generator, thereby achieving the effects of skin care and beauty. The diameter of the biological cellulose fiber is in the nanometer range, the formed pore diameter is also in the nanometer range, and the porous structure and a certain nanoscale pore diameter distribution can be used as templates to control and synthesize the nanometer material or the nanometer structure with the expected specific shape and size, thereby obtaining new different functional materials. The biological cellulose is used as a template, and the nano-scale composite material with the three-dimensional network structure can be synthesized through synthesis routes such as in-situ synthesis and the like by utilizing the nano-scale superfine network structure and a large number of active hydroxyl groups on the surface of the biological cellulose. The invention preferably adopts an in-situ chemical oxidation polymerization method to prepare the biological cellulose film coated with the conductive polymer, wherein the conductive polymer comprises polyacetylene, polypyrrole, polythiophene, poly-p-styrene, polyaniline and the like.
Furthermore, the invention also provides a more excellent technical scheme, namely, when the biological cellulose film coated with the conductive polymer is prepared, an alkali treatment step is added before the in-situ chemical oxidation polymerization step is carried out. The alkali treatment step is preferably to soak the biological cellulose membrane in 2-10wt% sodium hydroxide solution or potassium hydroxide solution at 80-100deg.C for 1-5 hr. The invention innovatively discovers that the biological cellulose can form a more complete core-shell structure with conductive polymers such as polypyrrole after alkali treatment. The method is characterized in that after the biological cellulose is subjected to alkali treatment, more surface active hydroxyl groups are released, polypyrrole forms a more perfect continuous coating structure under the guidance of the active hydroxyl groups in the polymerization process, so that the agglomeration phenomenon is greatly reduced, and the surface smoothness of the fiber is also greatly improved. By detection, the conductivity of the biological cellulose composite membrane before alkali treatment is more than 0.5S/cm, and generally only 0.5-0.7S/cm. The conductivity of the biological cellulose composite membrane prepared after alkali treatment is generally more than 1.5S/cm and can reach 2.5S/cm at most.
The preparation method of the biological cellulose composite membrane with the conductive performance provided by the invention comprises the following steps:
(1) Washing the biological cellulose wet film obtained by fermentation with distilled water or deionized water, and mechanically compressing to remove free water in the biological cellulose film until the water content is below 30-50wt%;
(2) Immersing the treated biological cellulose membrane in a solution containing 0.2-1.0 mol/L pyrrole monomer, magnetically stirring for 2-3 hours, and fully adsorbing the pyrrole monomer by the biological cellulose membrane after the action;
(3) Dropwise adding a proper amount of oxidant solution (the oxidant can be ferric trichloride, ammonium persulfate and the like, and the molar ratio of the oxidant to the pyrrole is 1:2-1:3), reacting at room temperature, polymerizing the pyrrole on the surface of the biological cellulose membrane, and uniformly coating the surface of the biological cellulose nanofiber;
(4) And (3) sequentially cleaning the product obtained in the step (3) by using 75wt% ethanol and distilled water, and then freeze-drying for about 24 hours to obtain the biological cellulose composite membrane with the conductive performance.
The method can be used for coating polypyrrole, and is also suitable for in-situ chemical oxidative polymerization coating of conductive polymers such as polyacetylene, polythiophene, poly-p-styrene, polyaniline and the like. Meanwhile, in order to further improve the conductivity, the above method preferably further comprises an alkali treatment step between the steps (1) and (2), such as immersing the biological cellulose membrane in an alkali solution by using a sodium hydroxide solution or potassium hydroxide solution with a concentration (2-10 wt%, preferably 5 wt%) and placing the biological cellulose membrane in a boiling water bath with a temperature of about 100 ℃ for 1-2 hours, cooling, and washing with deionized water until the biological cellulose membrane is neutral for standby.
Still preferably, the present invention provides an introducing type cosmetic device, comprising an introducing type cosmetic mask, and further comprising a micro-current generator or pulse generator electrically connected to the mask, a mask storage box, a cosmetic liquid, a power supply and a power supply connection line. The leading-in type beauty mask is made into a shape which is attached to a human face or other areas needing beauty care and is electrically connected with a micro-current generator or a pulse generator; the micro-current generator or pulse generator is connected to a power source (with a control switch) through a power source connection line, and the power source connection line can be made into separate type. When the facial mask is not used at ordinary times, the facial mask is placed in a facial mask storage box, when the facial mask is used, the facial mask is soaked in the beauty treatment liquid firstly, and then is applied to the face of a user or other areas needing beauty treatment after being fully soaked for a period of time, then the power supply of a micro-current generator or a pulse generator is connected, and low-frequency micro-current or ultrasonic waves of about 50 Hz are generated, so that the low-frequency micro-current or the ultrasonic waves act on the face of the user or other areas needing beauty treatment, and the low-frequency micro-current can promote skin metabolism, restore elasticity, exercise muscles and promote blood circulation; the ultrasonic wave can promote metabolism, accelerate blood and lymph circulation, improve the ischemia and hypoxia state of cells, improve tissue nutrition, improve regeneration function and the like; simultaneously, the beauty components in the beauty liquid can be guided into the skin surface layer to achieve better absorption effect. The used facial mask can be cleaned with clear water or light salt water and then placed in a storage box.
Detailed Description
To further illustrate the invention, the following examples are provided in connection with:
the wet biological cellulose membrane of the present invention is prepared by the prior art, such as static tray fermentation or dynamic fermenter fermentation, and one preparation method of the wet biological cellulose membrane in the examples is: preparing a biological cellulose fermentation culture medium, wherein the culture medium contains a proper amount of carbon sources such as glucose and sucrose, a proper amount of nitrogen sources and microelements are added, the pH value is regulated to 3.5-5.0, and 10% (volume ratio) of fermentation bacteria are inoculated after the culture medium is sterilized, wherein the fermentation bacteria can be acetobacter xylinum or acetobacter xylinum; fermenting at 34 deg.C for 7 days in a tray, and obtaining a biological cellulose hydrogel film with a thickness of at least 2cm on the surface of the tray. Washing with ethanol or water for use.
Example 1:
the embodiment provides a preparation method of a biological cellulose composite membrane with conductive performance by taking polypyrrole as a conductive polymer, which comprises the following steps:
(1) Washing the biological cellulose wet film obtained by fermentation with distilled water or deionized water, and mechanically compressing to remove free water in the biological cellulose film until the water content is below 50wt%;
(2) Preparing 5wt% sodium hydroxide solution, soaking the biological cellulose membrane in the sodium hydroxide solution, boiling in boiling water bath for 1h, and cooling; washing the cooled biological cellulose membrane to be neutral by deionized water for standby;
(3) Immersing the treated biological cellulose membrane in a solution containing 0.4 mol/L pyrrole monomer, magnetically stirring for 2-3 hours, and fully adsorbing the pyrrole monomer by the biological cellulose membrane after the action;
(4) And (3) dropwise adding a proper amount of saturated solution of ferric trichloride (the molar ratio of the ferric trichloride to the pyrrole is 1:2), reacting at room temperature, polymerizing the pyrrole on the surface of the biological cellulose membrane, and uniformly coating the surface of the biological cellulose nanofiber.
(5) The obtained product is washed by 75wt% ethanol and distilled water in turn, and then freeze-dried for about 24 hours to obtain the biological cellulose composite membrane with conductive performance.
The conductivity of the biological cellulose composite membrane prepared in the embodiment is 1.8S/cm.
Example 2:
the embodiment provides a preparation method of a biological cellulose composite membrane with conductive performance by taking polypyrrole as a conductive polymer, which comprises the following steps:
(1) Washing the biological cellulose wet film obtained by fermentation with distilled water or deionized water, and mechanically compressing to remove free water in the biological cellulose film until the water content is below 40wt%;
(2) Preparing 5wt% sodium hydroxide solution, soaking the biological cellulose membrane in the sodium hydroxide solution, boiling in boiling water bath for 1h, and cooling; washing the cooled biological cellulose membrane to be neutral by deionized water for standby;
(3) Immersing the treated biological cellulose membrane in a solution containing 0.6mol/L pyrrole monomer, magnetically stirring for 2-3 hours, and fully adsorbing the pyrrole monomer by the biological cellulose membrane after the action;
(4) And (3) dropwise adding a proper amount of saturated solution of ferric trichloride (the molar ratio of the ferric trichloride to the pyrrole is 1:3), reacting at room temperature, polymerizing the pyrrole on the surface of the biological cellulose membrane, and uniformly coating the surface of the biological cellulose nanofiber.
(5) The obtained product is washed by 75wt% ethanol and distilled water in turn, and then freeze-dried for about 24 hours to obtain the biological cellulose composite membrane with conductive performance.
The conductivity of the biological cellulose composite membrane prepared in the embodiment is 2.45S/cm.
Example 3:
the embodiment provides a preparation method of a biological cellulose composite membrane with conductive performance by taking polyaniline as a conductive polymer, which comprises the following steps:
(1) Washing the biological cellulose wet film obtained by fermentation with distilled water or deionized water, and mechanically compressing to remove free water in the biological cellulose film until the water content is below 30wt%;
(2) Preparing 10wt% potassium hydroxide solution, soaking the biological cellulose membrane in the potassium hydroxide solution, boiling in boiling water bath for 1.5h, and cooling; washing the cooled biological cellulose membrane to be neutral by deionized water for standby;
(3) Immersing the treated biological cellulose membrane in a hydrochloric acid solution containing 0.6mol/L aniline monomer, magnetically stirring for 2-3 hours, and fully adsorbing the aniline monomer by the biological cellulose membrane after the action;
(4) And (3) dropwise adding a proper amount of ammonium persulfate saturated solution (the molar ratio of ammonium persulfate to aniline is 1:3), reacting at room temperature, polymerizing the aniline on the surface of the biological cellulose membrane, and uniformly coating the surface of the biological cellulose nanofiber.
(5) The obtained product is washed by 75wt% ethanol and distilled water in turn, and then freeze-dried for about 24 hours to obtain the biological cellulose composite membrane with conductive performance.
The conductivity of the biological cellulose composite membrane prepared in the embodiment is 1.5S/cm.
Example 4:
the biological cellulose composite membrane prepared in the embodiment 1-3 is made into a shape which is attached to the face or other areas needing to be beautified and is electrically connected with a microcurrent generator or a pulse generator, so that the leading-in beautifying facial mask is prepared.
Example 5:
an imported cosmetic device comprises an imported cosmetic facial mask, and further comprises a micro-current generator or pulse generator, a facial mask storage box, a cosmetic liquid, a power supply and a power supply connecting wire, wherein the micro-current generator or pulse generator is electrically connected with the facial mask. The lead-in type beauty mask of example 4 was used, electrically connected to a microcurrent generator or pulse generator; the micro-current generator or pulse generator is connected to a power source (with a control switch) through a power source connection line, and the power source connection line can be made into separate type. When the facial mask is not used at ordinary times, the facial mask is placed in a facial mask storage box, when the facial mask is used, the facial mask is soaked in the beauty treatment liquid firstly, and then is applied to the face of a user or other areas needing beauty treatment after being fully soaked for a period of time, then the power supply of a micro-current generator or a pulse generator is connected, and low-frequency micro-current or ultrasonic waves of about 50 Hz are generated, so that the low-frequency micro-current or the ultrasonic waves act on the face of the user or other areas needing beauty treatment, and the low-frequency micro-current can promote skin metabolism, restore elasticity, exercise muscles and promote blood circulation; the ultrasonic wave can promote metabolism, accelerate blood and lymph circulation, improve the ischemia and hypoxia state of cells, improve tissue nutrition, improve regeneration function and the like; simultaneously, the beauty components in the beauty liquid can be guided into the skin surface layer to achieve better absorption effect. The cosmetic liquid can be selected and prepared into various types of cosmetic liquids according to the needs, such as cosmetic care liquid with the effects of whitening, removing freckle, tightening skin, moisturizing, and the like. The used facial mask can be cleaned with clear water or light salt water and then placed in a storage box.
Although the embodiments of the present invention have been disclosed above, it is not limited to the above embodiments, and various modifications may be made by those skilled in the art without departing from the spirit of the invention and the scope of the appended claims.
Claims (4)
1. An introduced beauty mask, characterized in that it is made of a bio-cellulose composite film having conductive properties, which has a conductivity of 0.7-2.5S/cm, made in a shape to be fitted to a human face and electrically connected to a microcurrent generator or a pulse generator, is prepared by a method comprising the steps of:
(1) Washing the biological cellulose wet film obtained by fermentation with distilled water or deionized water, and mechanically compressing to remove free water in the biological cellulose film until the water content is below 30-50wt%;
(2) Soaking the biological cellulose membrane in 2-10wt% sodium hydroxide solution or potassium hydroxide solution at 80-100deg.C for 1-5 hr, cooling, and washing with deionized water to neutrality;
(3) Immersing the treated biological cellulose membrane in a solution containing 0.2-1.0 mol/L pyrrole monomer, magnetically stirring for 2-3 hours, and fully adsorbing the pyrrole monomer by the biological cellulose membrane after the action;
(4) Dropwise adding an oxidant ammonium persulfate solution, wherein the molar ratio of the oxidant to the pyrrole is 1:2-1:3, reacting at room temperature to polymerize the pyrrole on the surface of the biological cellulose membrane, and uniformly coating the surface of the biological cellulose nanofiber;
(5) The obtained product was washed with 75wt% ethanol and distilled water in this order, and then freeze-dried for 24 hours to obtain a biocellulose composite film having conductive properties.
2. The lead-in cosmetic facial mask of claim 1, wherein the preparation method of the biological cellulose composite film with conductive performance comprises the following steps: step (1), cleaning a biological cellulose wet film obtained by fermentation by distilled water or deionized water, and mechanically compressing to remove free water in the biological cellulose film until the water content is below 50 wt%; step (2) soaking the biological cellulose membrane in 5wt% sodium hydroxide solution, placing the biological cellulose membrane in a boiling water bath, boiling for 1h, cooling, and washing the biological cellulose membrane with deionized water to be neutral for later use; step (3) soaking the treated biological cellulose membrane in a solution containing 0.4 mol/L pyrrole monomer, magnetically stirring for 2-3 hours, and fully adsorbing the pyrrole monomer by the biological cellulose membrane after the action; dropwise adding an oxidant ammonium persulfate solution, wherein the molar ratio of the oxidant to the pyrrole is 1:2, reacting at room temperature to polymerize the pyrrole on the surface of the biological cellulose membrane, and uniformly coating the surface of the biological cellulose nanofiber; and (5) sequentially washing the obtained product with 75wt% ethanol and distilled water, and then freeze-drying for 24 hours to obtain the biological cellulose composite membrane with the conductive performance.
3. The leading-in type beauty mask is characterized in that the beauty mask is made of a biological cellulose composite film with conductive performance, which is made into a shape fitting a human face and is electrically connected with a microcurrent generator or a pulse generator, the conductivity of the biological cellulose composite film with conductive performance is 1.5S/cm, and the preparation method is as follows: step (1), cleaning a biological cellulose wet film obtained by fermentation by distilled water or deionized water, and mechanically compressing to remove free water in the biological cellulose film until the water content is below 30wt%; step (2) preparing 10wt% potassium hydroxide solution, soaking the biological cellulose membrane in the potassium hydroxide solution, placing in a boiling water bath, boiling for 1.5h, and cooling; washing the cooled biological cellulose membrane to be neutral by deionized water for standby; (3) Immersing the treated biological cellulose membrane in a hydrochloric acid solution containing 0.6mol/L aniline monomer, magnetically stirring for 2-3 hours, and fully adsorbing the aniline monomer by the biological cellulose membrane after the action; dropwise adding a saturated ammonium persulfate solution, wherein the molar ratio of ammonium persulfate to aniline is 1:3, reacting at room temperature to polymerize aniline on the surface of a biological cellulose membrane, and uniformly coating the surface of the biological cellulose nanofiber; and (5) sequentially washing the obtained product with 75wt% ethanol and distilled water, and then freeze-drying for 24 hours to obtain the biological cellulose composite membrane with the conductive performance.
4. An introduced cosmetic device comprising the introduced cosmetic mask of any one of claims 1-3, further comprising a microcurrent generator or pulse generator electrically connected to the mask, a mask case, a cosmetic liquid, a power source, and a power source connection line.
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| CN102219997B (en) * | 2011-04-29 | 2013-06-26 | 南京理工大学 | Method for preparing polypyrrole coated bacterial cellulose nanometer electric-conduction composite material by utilizing bacterial cellulose as template |
| CN102212210B (en) * | 2011-04-29 | 2014-06-11 | 南京理工大学 | Method for preparing polyaniline-coated bacteria cellulose nano conductive composite by in-situ polymerization |
| CN105797197B (en) * | 2016-04-25 | 2018-09-21 | 华中科技大学 | A kind of dressing for skin and preparation method thereof |
| CN206526402U (en) * | 2016-08-31 | 2017-09-29 | 广州风速信息技术有限公司 | Intelligent beautifying face device |
| CN106310515B (en) * | 2016-08-31 | 2018-10-23 | 广州风速信息技术有限公司 | Intelligent beautifying face device |
| CN107913067A (en) * | 2017-11-15 | 2018-04-17 | 江南大学 | A kind of electronic skin based on native cellulose nanofiber and preparation method thereof |
| CN109091412B (en) * | 2018-09-20 | 2021-08-10 | 江南大学 | ALA-PDT light skin-tendering mask and preparation method thereof |
| CN109180978A (en) * | 2018-10-10 | 2019-01-11 | 华南理工大学 | A kind of polyaniline/cellulose conductive composite film and its preparation method and application |
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|---|---|---|---|---|
| CN102361623A (en) * | 2009-03-23 | 2012-02-22 | 意大利嘉利化工有限责任公司 | Sunscreen product comprising hydroxyapatite as physical filter |
| CN106519275A (en) * | 2016-11-16 | 2017-03-22 | 陕西聚洁瀚化工有限公司 | Preparation method of bacterial cellulose based composite membrane with electromagnetic function |
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