CN112825994A - Fresh and alive normal-heat-clearing drink formula for discharging oil and discharging stubborn stool and preparation method thereof - Google Patents

Fresh and alive normal-heat-clearing drink formula for discharging oil and discharging stubborn stool and preparation method thereof Download PDF

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Publication number
CN112825994A
CN112825994A CN202110161733.3A CN202110161733A CN112825994A CN 112825994 A CN112825994 A CN 112825994A CN 202110161733 A CN202110161733 A CN 202110161733A CN 112825994 A CN112825994 A CN 112825994A
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parts
hawthorn
cordyceps militaris
sea buckthorn
cassia seed
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陆国胜
王思棋
贾景然
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Guangzhou Huimei Biotechnology Co ltd
Zhejiang Jianfeng Health Tech Co ltd
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Guangzhou Huimei Biotechnology Co ltd
Zhejiang Jianfeng Health Tech Co ltd
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Priority to CN202110161733.3A priority Critical patent/CN112825994A/en
Publication of CN112825994A publication Critical patent/CN112825994A/en
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    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/38—Other non-alcoholic beverages
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/42—Preservation of non-alcoholic beverages
    • A23L2/44—Preservation of non-alcoholic beverages by adding preservatives
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52—Adding ingredients
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52—Adding ingredients
    • A23L2/60—Sweeteners
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • A23L2/72—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration
    • A23L2/74—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration using membranes, e.g. osmosis, ultrafiltration
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/105—Plant extracts, their artificial duplicates or their derivatives
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
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    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/20—Reducing nutritive value; Dietetic products with reduced nutritive value
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    • A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs

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Abstract

The invention relates to the technical field of drinking agents, in particular to a fresh and alive normal clear drink formula for discharging oil and discharging stubborn stool and a preparation method thereof, wherein the normal clear drink formula comprises the following raw materials, by weight, 10-15 parts of hawthorn, 8-12 parts of semen cassiae, 8-10 parts of chrysanthemum, 5-10 parts of sea buckthorn, 10-20 parts of cordyceps militaris, 5-10 parts of isomaltooligosaccharide, 6-8 parts of fructo-oligosaccharide, 8-12 parts of stachyose, 6-10 parts of soybean dietary fiber, 2-6 parts of sucralose and 350 parts of deionized water.

Description

Fresh and alive normal-heat-clearing drink formula for discharging oil and discharging stubborn stool and preparation method thereof
Technical Field
The invention relates to the technical field of potables, in particular to a fresh and alive normally clear beverage formula for discharging oil and discharging stubborn stool and a preparation method thereof.
Background
The gastrointestinal tract is an important digestive organ, and the human body must provide main energy by means of the food digested by the gastrointestinal tract to maintain normal physiological and biochemical functions, immune function, growth and development, metabolism and other life activities. The gastrointestinal system supplies energy to the human body through activities such as food intake, transport, digestion and absorption, and residue excretion, and in addition, the gastrointestinal system has partial endocrine and immune functions. The diversity of the gastrointestinal system functions determines that both disturbances and decline of gastrointestinal function will cause a series of significant clinical symptoms. Specifically, three main aspects are included: (1) gastroparesis and paralytic ileus caused by gastrointestinal motility disorder; (2) ulcer and inflammation caused by the damage of the normal mucosa protection function; (3) diarrhea and constipation due to malabsorption and secretion disorder. The normal function of the gastrointestinal tract has important significance for maintaining other functions of the body, however, with the acceleration of the modern life rhythm, the change of the dietary structure and the increase of the competitive pressure, the incidence rate of the gastrointestinal tract diseases is rising year by year at present.
Constipation is the most common and easily overlooked bowel disease, and recent data show that constipation has a prevalence of up to 27% in the population, i.e., one constipation patient out of every 4. Constipation is the condition that wastes and toxins in a human body cannot be normally discharged to form accumulated stubborn stool in an intestinal tract, the toxins in the stubborn stool are repeatedly absorbed by the intestinal tract to cause the problems of inappetence, gastrointestinal discomfort, abdominal swelling, chloasma, palsy, acne and the like on the skin, and even colon cancer may be induced.
At present, a plurality of health care products for treating constipation generally have side effects, such as damage to the body caused by strong excretion and easy formation of dependence, and potables generally have short storage life and cannot be stored for a long time, and if the potables are stored for a long time, effective components are easy to lose efficacy.
Disclosure of Invention
In view of the above, the present invention aims to provide a fresh and alive drink formula for discharging oil and discharging stool and a preparation method thereof, wherein the drink formula has functions of discharging oil and discharging stool, and improving intestinal micro-ecological environment, has a long shelf life, and can effectively improve constipation, thereby recovering intestinal health.
The invention solves the technical problems by the following technical means:
a fresh and alive normal clear drink formula for discharging oil and discharging stubborn stool comprises the following raw materials, by weight, 10-15 parts of hawthorn, 8-12 parts of semen cassiae, 8-10 parts of chrysanthemum, 5-10 parts of sea buckthorn, 10-20 parts of cordyceps militaris, 5-10 parts of isomaltooligosaccharide, 6-8 parts of fructo-oligosaccharide, 8-12 parts of stachyose, 6-10 parts of soybean dietary fiber, 2-6 parts of sucralose and 350 parts of deionized water.
Specifically, the Changqing drink formula comprises the following raw materials, by weight, 13 parts of hawthorn, 10 parts of cassia seed, 9 parts of chrysanthemum, 8 parts of sea buckthorn, 15 parts of cordyceps militaris, 8 parts of isomaltose hypgather, 7 parts of fructo-oligosaccharide, 10 parts of stachyose, 8 parts of soybean dietary fiber, 4 parts of sucralose and 300 parts of deionized water.
The hawthorn has the functions of promoting digestion, invigorating stomach, promoting qi circulation, removing blood stasis, eliminating turbid pathogen and reducing blood fat. Semen Cassiae can enter liver, kidney, and large intestine meridians; loosening bowel to relieve constipation, reducing blood lipid and improving eyesight, treating constipation and hyperlipemia, hypertension, removing liver fire for improving eyesight, promoting diuresis and relaxing bowels, and has laxative effect, and lowering blood pressure and reducing blood lipid. The chrysanthemum has the functions of dispelling wind and clearing heat, calming the liver and improving eyesight, and clearing heat and removing toxicity, and the sea buckthorn has the functions of strengthening spleen and helping digestion, relieving cough and eliminating phlegm, and activating blood and dissipating blood stasis. The Cordyceps militaris has multiple active components, and has effects of enhancing immunity, resisting cancer, resisting bacteria, relieving fatigue, resisting anoxia, and resisting aging.
The isomaltooligosaccharide is difficult to digest by gastric enzyme, has low sweetness and low heat, does not increase blood sugar and blood fat basically, can promote the proliferation of bifidobacteria in intestinal tracts, inhibits the formation of harmful bacteria and putrefactive substances in the intestinal tracts, increases the vitamin content, improves the immunity of organisms, can not be absorbed by the stomach and the small intestine, but directly enters the large intestine, is preferentially utilized by the bifidobacteria to help the mass propagation of the bifidobacteria, and is a bifidobacteria proliferation factor; other harmful bacteria in the intestines cannot be utilized, so that the growth of the harmful bacteria can be inhibited, and the microecology in the intestines can be adjusted to a benign cycle. The fructo-oligosaccharide cannot be directly digested and absorbed by human body, and can only be used by beneficial bacteria such as bifidobacterium and the like, namely, the bifidobacterium (pathogenic bacteria) only proliferates by 10-100 times, so that the bifidobacterium has the effect of bidirectional regulation, and after the fructo-oligosaccharide is taken by the human body, the quantity of the beneficial bacteria in the body can inhibit the growth and the propagation of exogenous pathogenic bacteria and intrinsic putrefying bacteria such as salmonella in intestines, reduce the growth and the accumulation of putrefying substances in the intestines, promote the intestinal peristalsis, and prevent constipation and diarrhea. Stachyose is functional oligosaccharide, has no dependence, can be used for targeting colonization, can directly colonize each part of intestinal tract, can proliferate beneficial bacteria such as bifidobacterium at an increasing speed of 40 times, has quick effect, does not cause abdominal distension and discomfort, is extracted from plants, and has no side effect. The soybean dietary fiber can safely regulate the blood sugar level of a human body, prevent constipation, increase satiety, and simultaneously has the physiological functions of preventing obesity, promoting the proliferation of bifidobacteria and aerobic bacteria, enhancing the function of macrophages and improving the disease resistance. The sucralose has good stability, can not react with other substances, can not influence the transparency, color and flavor of the beverage, and also has the performances of heat sterilization and long-term storage.
The beverage has the advantages that the functions of discharging oil and discharging stubborn stool can be achieved through the mutual matching of the traditional Chinese medicine components of the hawthorn, the cassia seed, the chrysanthemum, the sea buckthorn and the cordyceps militaris, the functions of discharging oil and discharging stubborn stool can be achieved, the intestinal micro-ecological environment can be improved through the mutual matching of the isomaltooligosaccharide, the fructooligosaccharide, the stachyose, the soybean dietary fiber and the sucralose, and no side effect exists.
The invention also discloses a preparation method of the fresh and alive normal clear beverage for discharging oil and defecation, which comprises the following steps,
a1: pretreating fructus crataegi, semen Cassiae, flos Chrysanthemi, fructus Hippophae and Cordyceps militaris;
a2: boiling flos Chrysanthemi, fructus crataegi, semen Cassiae, fructus Hippophae and Cordyceps militaris, filtering, concentrating to obtain first extractive solution,
a3: puffing the hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris extracted by the A2, and then performing heavy percolation extraction to obtain a second extracting solution;
a4: pulverizing the hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris which are subjected to the heavy percolation extraction in the A3, and performing the heavy percolation extraction again to obtain a third extracting solution;
a5: adding deionized water into isomaltose hypgather, fructo-oligosaccharide, stachyose, soybean dietary fiber and sucralose, stirring and dissolving to obtain a first intermediate liquid for later use;
a6: stirring and mixing the first extracting solution, the second extracting solution and the third extracting solution to obtain a second intermediate liquid, mixing the first intermediate liquid and the second intermediate liquid to obtain a mixed liquid, passing the mixed liquid through an electromagnetic field, adding deionized water to a constant volume, filling and sterilizing to obtain a finished product.
By pretreating the hawthorn, the cassia seed, the chrysanthemum, the sea buckthorn and the cordyceps militaris in the step A1, the effective ingredients in the hawthorn, the cassia seed, the chrysanthemum, the sea buckthorn and the cordyceps militaris can be effectively preserved. In the step A2, in the boiling extraction process, firstly, 8 times of deionized water in parts by weight of chrysanthemum, hawthorn, cassia seed, sea buckthorn and cordyceps militaris is added, boiling is carried out for 2 hours to obtain a primary extracting solution, then 6 times of deionized water in parts by weight of traditional Chinese medicinal materials is added into the primary extracting solution, boiling is carried out for 2 times, the traditional Chinese medicinal materials are filtered and concentrated to obtain a first extracting solution. In the step A3, the hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris are puffed, so that the effective ingredients in the hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris are activated, and more effective ingredients can be extracted during the percolation. In the step A4, the hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris which are extracted in the step A3 are crushed and subjected to percolation extraction again, so that the content of the effective ingredients in the hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris is completely extracted, and the loss of the effective ingredients is avoided.
After the effective components in the traditional Chinese medicinal materials are completely extracted, the effective components of the traditional Chinese medicinal materials are mixed together and then mixed with the mixed solution of isomaltooligosaccharide, fructo-oligosaccharide, stachyose, soybean dietary fiber and sucralose, after an electromagnetic field is passed, on one hand, the first intermediate liquid and the second intermediate liquid are fully mixed, on the other hand, the electron polarity in the mixed solution is enhanced, electrons can stimulate the effective components in the mixed solution for a long time, and the activity of the effective components is kept.
Specifically, in the step a1, the pretreatment step includes cleaning hawthorn, cassia seed, chrysanthemum, sea buckthorn and cordyceps militaris, drying in the shade, and then performing gradient temperature rise to dryness after drying in the shade, wherein the gradient temperature rise is 10 ℃ per hour, and the final temperature rise is 40 ℃.
The traditional Chinese medicinal materials are dried in the shade to avoid direct irradiation or baking of sunlight, so that the effective components in the traditional Chinese medicinal materials are damaged, and then the traditional Chinese medicinal materials are processed through gradient heating, so that the traditional Chinese medicinal materials can be stored for a longer time without losing the effective components.
Specifically, in the step a3, the puffing treatment specifically comprises the steps of placing the hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris in liquid carbon dioxide, keeping the pressure for 3-5H under the air pressure of 0.5-1MPa, and then opening a gate to release the pressure to obtain the puffed hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris.
Through the puffing treatment, the physical forms of the boiled hawthorn, cassia seed, sea buckthorn and cordyceps militaris are changed, so that the residual effective ingredients in the hawthorn, cassia seed, sea buckthorn and cordyceps militaris can be uniformly distributed, and the heavy percolation extraction is facilitated.
Specifically, in the process of extracting the second extracting solution and the third extracting solution from the A3 and the A4 by a double percolation method, hawthorn, cassia seed, sea buckthorn and cordyceps militaris are wrapped by a filter membrane, and the filter membrane is prepared by placing activated carbon fiber into an ethanol water solution, adding coco glucoside, stirring uniformly, adding sodium peroxide, reacting for 8-10H at 40-60 ℃, after the reaction is finished, introducing 10-20mA current for 10min, concentrating, coating, and freeze-drying.
The hawthorn, the cassia seed, the sea-buckthorn and the cordyceps militaris are wrapped by a special filter membrane, so that electrons in the filter membrane can enter the extracting solution more easily in the percolation process. In the preparation process of the filter membrane, sodium ions are grafted on the activated carbon fiber, then the power is supplied, electrons on the sodium ions are in an excited state by the power, and when the filtration is carried out, the leaching liquor passes through the filter membrane to impact the electrons in the excited state, so that the electrons in the excited state are combined with effective components in the extracting solution, the extracting solution is provided with the electrons, and the storage time of the extracting solution is prolonged.
Specifically, in the step A4, the hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris are crushed into 30-60 meshes.
By crushing the traditional Chinese medicinal materials, the effective content of the extract is more sufficient when the heavy percolation extraction is carried out.
Specifically, in the step a6, the voltage of the electromagnetic field is 18V, and the current is 0.3A.
Through carrying out the electromagnetic field to the mixed solution and handling, make liquid intensive mixing in the middle of first middle liquid and the second on the one hand, the intensity of electric current is greater than the intensity of filter membrane preparation in-process electric current to can further strengthen the polarity of electron in the mixed solution, increase the energy storage intensity of electron, make the active time of electron longer, make the electron can stimulate the active ingredient in the mixed solution for a long time, keep the activity of active ingredient, and voltage, electric current are safe voltage, avoid accidentally causing the injury to the human body.
The invention has the beneficial effects that: the invention discloses a Changqing drink formula and a preparation method thereof, and the drink prepared by the preparation method has the functions of discharging oil, discharging stubborn stool and improving intestinal micro-ecological environment, can keep the activity of effective components for a long time, and is convenient to drink at any time.
Detailed Description
The present invention will be described in detail with reference to specific examples below:
the invention relates to a fresh and alive normal clear drink formula for discharging oil and discharging stubborn stool, which comprises the following raw materials, by weight, 10-15 parts of hawthorn, 8-12 parts of cassia seed, 8-10 parts of chrysanthemum, 5-10 parts of sea buckthorn, 10-20 parts of cordyceps militaris, 5-10 parts of isomaltooligosaccharide, 6-8 parts of fructo-oligosaccharide, 8-12 parts of stachyose, 6-10 parts of soybean dietary fiber, 2-6 parts of sucralose and 350 parts of deionized water, wherein the hawthorn, the cassia seed, the chrysanthemum, the sea buckthorn and the cordyceps militaris are subjected to boiling extraction, the hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris are screened out, the puffing treatment is carried out again, the first percolation extraction is carried out after the puffing treatment, then the hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris are crushed, the second percolation extraction is carried out, and during the percolation extraction, extracting with a special filter membrane, dissolving isomaltooligosaccharide, fructo-oligosaccharide, stachyose, soybean dietary fiber and sucralose in deionized water, mixing the extractive solution with the first intermediate liquid, mixing, passing through an electromagnetic field, adding deionized water to a constant volume, filling, and sterilizing to obtain the final product.
Example 1 preparation of filtration Membrane
Taking 20 parts by weight of activated carbon fiber, placing the activated carbon fiber in 50 parts by weight of ethanol aqueous solution until the activated carbon fiber is completely dissolved, adding 4 parts by weight of coco glucoside, stirring uniformly, adding 2 parts by weight of sodium peroxide, reacting for 8H at 60 ℃, after the reaction is finished, introducing 10mA current for 10min, heating to 70 ℃ for concentration after electrifying, coating the concentrated solution on a plate while the concentrated solution is hot after the concentration is finished, and freeze-drying the coated plate at-5 ℃ to obtain the filter membrane.
Example 2 preparation of the Filter Membrane
Putting 25 parts by weight of activated carbon fiber into 60 parts by weight of ethanol water solution until the activated carbon fiber is completely dissolved, adding 5 parts by weight of coco-glucoside, uniformly stirring, adding 4 parts by weight of sodium peroxide, reacting at 50 ℃ for 9H, after the reaction is finished, introducing 15mA current for 10min, after electrifying, heating to 70 ℃ for concentration, after the concentration is finished, coating the concentrated solution on a plate while hot, and freeze-drying the coated plate at-5 ℃ to obtain the filter membrane.
Example 3 preparation of the Filter Membrane
Putting 30 parts by weight of activated carbon fiber into 75 parts by weight of ethanol aqueous solution until the activated carbon fiber is completely dissolved, adding 6 parts by weight of coco-glucoside, uniformly stirring, adding 6 parts by weight of sodium peroxide, reacting for 10 hours at 40 ℃, introducing 20mA current for 10 minutes after the reaction is finished, heating to 70 ℃ for concentration after electrifying, coating the concentrated solution on a plate while hot after the concentration is finished, and freeze-drying the coated plate at-5 ℃ to obtain the filter membrane.
Example 4 preparation of Changqing drink 1
A1: cleaning fructus crataegi, semen Cassiae, flos Chrysanthemi, fructus Hippophae and Cordyceps militaris, drying in the shade, and performing gradient heating to evaporate to dryness, wherein the gradient heating is increased by 10 deg.C per hour, and the final temperature is increased to 40 deg.C.
A2: putting 8 parts of chrysanthemum, 10 parts of hawthorn, 8 parts of semen cassiae, 5 parts of sea buckthorn and 10 parts of cordyceps militaris into a container, adding 8 times of deionized water by weight of traditional Chinese medicinal materials, heating to boil, keeping the boiling state for 1.5H to obtain a primary extracting solution, adding 6 times of deionized water by weight of traditional Chinese medicinal materials into the primary extracting solution, heating to boil, keeping the boiling state for 1.5H, filtering the traditional Chinese medicinal materials, and heating and concentrating to obtain a first extracting solution for later use;
a3: screening the hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris in the step A2, primarily drying, then placing the hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris in liquid carbon dioxide, keeping the pressure for 5H under 0.5MPa, then opening a gate to release pressure to obtain a puffed traditional Chinese medicinal material, then wrapping the puffed traditional Chinese medicinal material with a filter membrane, then placing the puffed traditional Chinese medicinal material into a heavy percolation extraction container, placing the heavy percolation extraction container in an electromagnetic field, wherein the voltage of the electromagnetic field is 18V, the current is 0.3A, using 0.2mol/L edible acetic acid as an extracting solution, then performing heavy percolation extraction for 18H to obtain a second extracting solution for later use;
a4: drying the hawthorn, the cassia seed, the sea-buckthorn and the cordyceps militaris which are subjected to the heavy percolation extraction in the A3, then crushing the dried hawthorn, the cassia seed, the sea-buckthorn and the cordyceps militaris to 60 meshes, performing the heavy percolation extraction again under the same condition, and keeping the intensity of electromagnetic field unchanged during the heavy percolation extraction to obtain a third extracting solution for later use;
a5: adding deionized water into isomaltose hypgather, fructo-oligosaccharide, stachyose, soybean dietary fiber and sucralose, stirring and dissolving to obtain a first intermediate liquid for later use;
a6: stirring and mixing the first extracting solution, the second extracting solution and the third extracting solution to obtain a second intermediate liquid, regulating the pH of the second intermediate liquid to 7-7.2, mixing the first intermediate liquid and the second intermediate liquid to obtain a mixed liquid, passing the mixed liquid through an electromagnetic field, keeping the strength of the electromagnetic field unchanged, adding deionized water to the mixed liquid to fix the volume, filling, sterilizing and obtaining a finished product, wherein the finished product is 30 ml/bag.
Example 5 preparation of Changqing drink II
A1: cleaning fructus crataegi, semen Cassiae, flos Chrysanthemi, fructus Hippophae and Cordyceps militaris, drying in the shade, and performing gradient heating to evaporate to dryness, wherein the gradient heating is increased by 10 deg.C per hour, and the final temperature is increased to 40 deg.C.
A2: putting 9 parts of chrysanthemum, 13 parts of hawthorn, 10 parts of semen cassiae, 8 parts of sea buckthorn and 15 parts of cordyceps militaris into a container, adding 8 parts by weight of deionized water of a traditional Chinese medicine, heating to boil, keeping the boiling state for 2H to obtain a primary extracting solution, adding 6 parts by weight of deionized water of the traditional Chinese medicine into the primary extracting solution, heating to boil, keeping the boiling state for 2H, filtering the traditional Chinese medicine, heating and concentrating to obtain a first extracting solution for later use;
a3: screening the hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris in the step A2, primarily drying, then placing the hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris in liquid carbon dioxide, keeping the pressure at 0.8MPa for 4H, then opening a gate to release pressure to obtain a puffed traditional Chinese medicinal material, then wrapping the puffed traditional Chinese medicinal material with a filter membrane, then placing the puffed traditional Chinese medicinal material into a heavy percolation extraction container, placing the heavy percolation extraction container in an electromagnetic field, wherein the voltage of the electromagnetic field is 18V, the current is 0.3A, using 0.2mol/L edible acetic acid as an extracting solution, then performing heavy percolation extraction for 20H to obtain a second extracting solution for later use;
a4: drying the hawthorn, the cassia seed, the sea-buckthorn and the cordyceps militaris which are subjected to the heavy percolation extraction in the A3, then crushing the dried hawthorn, the cassia seed, the sea-buckthorn and the cordyceps militaris to 40 meshes, performing the heavy percolation extraction again under the same condition, and keeping the intensity of electromagnetic field unchanged during the heavy percolation extraction to obtain a third extracting solution for later use;
a5: adding deionized water into isomaltose hypgather, fructo-oligosaccharide, stachyose, soybean dietary fiber and sucralose, stirring and dissolving to obtain a first intermediate liquid for later use;
a6: stirring and mixing the first extracting solution, the second extracting solution and the third extracting solution to obtain a second intermediate liquid, regulating the pH of the second intermediate liquid to 7-7.2, mixing the first intermediate liquid and the second intermediate liquid to obtain a mixed liquid, passing the mixed liquid through an electromagnetic field, keeping the strength of the electromagnetic field unchanged, adding deionized water to the mixed liquid to fix the volume, filling, sterilizing and obtaining a finished product, wherein the finished product is 30 ml/bag.
Example 6 preparation of Changqing drink III
A1: cleaning fructus crataegi, semen Cassiae, flos Chrysanthemi, fructus Hippophae and Cordyceps militaris, drying in the shade, and performing gradient heating to evaporate to dryness, wherein the gradient heating is increased by 10 deg.C per hour, and the final temperature is increased to 40 deg.C.
A2: putting 10 parts of chrysanthemum, 15 parts of hawthorn, 12 parts of semen cassiae, 10 parts of sea buckthorn and 20 parts of cordyceps militaris into a container, adding 8 parts by weight of deionized water of a traditional Chinese medicinal material, heating to boil, keeping the boiling state for 2.5H to obtain a primary extracting solution, adding 6 parts by weight of deionized water of the traditional Chinese medicinal material into the primary extracting solution, heating to boil, keeping the boiling state for 2.5H, filtering the traditional Chinese medicinal material, and heating and concentrating to obtain a first extracting solution for later use;
a3: screening the hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris in the step A2, primarily drying, then placing the hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris in liquid carbon dioxide, keeping the pressure for 3H under the air pressure of 1MPa, then opening a gate to release the pressure to obtain a puffed traditional Chinese medicinal material, then wrapping the puffed traditional Chinese medicinal material with a filter membrane, then placing the puffed traditional Chinese medicinal material into a re-percolation extraction container, placing the re-percolation extraction container in an electromagnetic field, setting the voltage of the electromagnetic field to be 18V and the current to be 0.3A, using 0.2mol/L edible acetic acid as an extracting solution, then performing re-percolation extraction for 24H to obtain a second extracting solution for later use;
a4: drying the hawthorn, the cassia seed, the sea-buckthorn and the cordyceps militaris which are subjected to the heavy percolation extraction in the A3, then crushing the dried hawthorn, the cassia seed, the sea-buckthorn and the cordyceps militaris to 30 meshes, performing the heavy percolation extraction again under the same condition, and keeping the intensity of electromagnetic field unchanged during the heavy percolation extraction to obtain a third extracting solution for later use;
a5: adding deionized water into isomaltose hypgather, fructo-oligosaccharide, stachyose, soybean dietary fiber and sucralose, stirring and dissolving to obtain a first intermediate liquid for later use;
a6: stirring and mixing the first extracting solution, the second extracting solution and the third extracting solution to obtain a second intermediate liquid, regulating the pH of the second intermediate liquid to 7-7.2, mixing the first intermediate liquid and the second intermediate liquid to obtain a mixed liquid, passing the mixed liquid through an electromagnetic field, keeping the strength of the electromagnetic field unchanged, adding deionized water to the mixed liquid to fix the volume, filling, sterilizing and obtaining a finished product, wherein the finished product is 30 ml/bag.
Randomly selecting 50 volunteers with constipation, dividing 50 volunteers into A, B, C, D, E five groups, wherein A, B, C, D four groups of volunteers are experimental groups, E group of volunteers are control groups, the experimental groups are normally fed, and respectively drink one bag of the normally clear drink prepared in the embodiments 4, 5 and 6 at 8 am and 8 am respectively, the control groups respectively drink 30ml of warm water at corresponding time, continuously drink for half a month, and detect the defecation condition by taking 3 days as a node, and the test results are as follows:
Figure BDA0002936944160000071
Figure BDA0002936944160000081
from the test results, the normal clear drinking preparations prepared by the implementation of the steps 4, 5 and 6 can discharge oil, defecate and improve the function of intestinal micro-ecological environment, so that the constipation patients can recover to the defecation condition of normal people.
The potables prepared in examples 4, 5 and 6 were subjected to retention time test under conditions of 10-25 ℃ and stored in the dark, wherein the control group was a product obtained by wrapping the Chinese medicinal materials with ordinary gauze without adding the filter membrane prepared in the present invention and subjecting the wrapped materials to percolation, and then the content and activity of the effective components were measured, and the test results were as follows:
Figure BDA0002936944160000082
from the test results, the examples 4, 5 and 6 adopt the special filter membranes, so that the active ingredients and the activity of the active ingredients in the normal clear beverage can be maintained for a longer time, and the example 5 has the best effect, so that the beverage can still have the functions of oil discharge, defecation and intestinal micro-ecological environment improvement after being stored for a longer time for drinking.
In the process of preparing the potables of examples 4, 5 and 6, in the process of preparing the potables of examples 4 and 5, the steps A3 and A6 were activated and charged by using an electromagnetic field, and in the steps A3 and A6 of example 6, neither was activated and charged by using an electromagnetic field, and then the potables prepared in examples 4, 5 and 6 were tested for storage time under the conditions of 10-25 ℃ and protected from light, and the test results were as follows:
Figure BDA0002936944160000091
from the test results, it was found that examples 4 and 5 were able to maintain the content of the active ingredient after long-term storage, and the activity of the active ingredient was slightly lowered, and were able to be stored for a longer period of time without losing the medicinal efficacy, compared with the drinkable preparation prepared without electromagnetic field activation and charging in example 6.
Although the present invention has been described in detail with reference to the preferred embodiments, it will be understood by those skilled in the art that various changes may be made and equivalents may be substituted without departing from the spirit and scope of the invention as defined in the appended claims. The techniques, shapes, and configurations not described in detail in the present invention are all known techniques.

Claims (8)

1. The formula of the fresh and alive normal clear beverage for discharging oil and discharging stubborn stool is characterized by comprising the following raw materials, by weight, 10-15 parts of hawthorn, 8-12 parts of semen cassiae, 8-10 parts of chrysanthemum, 5-10 parts of sea buckthorn, 10-20 parts of cordyceps militaris, 5-10 parts of isomaltooligosaccharide, 6-8 parts of fructo-oligosaccharide, 8-12 parts of stachyose, 6-10 parts of soybean dietary fiber, 2-6 parts of sucralose and 350 parts of deionized water.
2. The fresh and alive normal-clear drink formula for discharging oil and defecation as claimed in claim 1, wherein the normal-clear drink formula comprises the following raw materials, by weight, 13 parts of hawthorn, 10 parts of semen cassiae, 9 parts of chrysanthemum, 8 parts of sea buckthorn, 15 parts of cordyceps militaris, 8 parts of isomaltooligosaccharide, 7 parts of fructo-oligosaccharide, 10 parts of stachyose, 8 parts of soybean dietary fiber, 4 parts of sucralose and 300 parts of deionized water.
3. The method for preparing a fresh and alive beverage for draining oil and defecation according to any one of claims 1-2, which comprises the following steps,
a1: pretreating fructus crataegi, semen Cassiae, flos Chrysanthemi, fructus Hippophae and Cordyceps militaris;
a2: boiling and extracting chrysanthemum, hawthorn, cassia seed, sea buckthorn and cordyceps militaris, filtering and concentrating to obtain a first extracting solution;
a3: puffing the hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris extracted by the A2, and then performing heavy percolation extraction to obtain a second extracting solution;
a4: pulverizing the hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris which are subjected to the heavy percolation extraction in the A3, and performing the heavy percolation extraction again to obtain a third extracting solution;
a5: adding deionized water into isomaltose hypgather, fructo-oligosaccharide, stachyose, soybean dietary fiber and sucralose, stirring and dissolving to obtain a first intermediate liquid for later use;
a6: stirring and mixing the first extracting solution, the second extracting solution and the third extracting solution to obtain a second intermediate liquid, mixing the first intermediate liquid and the second intermediate liquid to obtain a mixed liquid, passing the mixed liquid through an electromagnetic field, adding deionized water to a constant volume, filling and sterilizing to obtain a finished product.
4. The method for preparing the fresh and alive normal clear beverage for discharging the oil and the stool as claimed in claim 3, wherein in the step A1, the pretreatment step comprises the steps of cleaning the hawthorn, the cassia seed, the chrysanthemum, the sea buckthorn and the cordyceps militaris, drying in the shade, and then performing gradient temperature rise for evaporation, wherein the gradient temperature rise is 10 ℃ per hour, and the final temperature rise is 40 ℃.
5. The preparation method of the fresh and alive normal clear beverage for discharging oil and defecation, as claimed in claim 4, wherein in the step A3, the puffing treatment comprises the specific steps of placing the hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris in liquid carbon dioxide, keeping for 3-5H under the air pressure of 0.5-1MPa, then opening a gate and releasing pressure to obtain the puffed hawthorn, the cassia seed, the sea buckthorn and the cordyceps militaris.
6. The preparation method of the fresh and alive normal clear beverage for oil drainage and defecation according to claim 5, wherein in the process of extracting the second extract and the third extract by the double percolation method in the A3 and the A4, hawthorn, cassia seed, sea buckthorn and cordyceps militaris are wrapped by using a filter membrane, the preparation method of the filter membrane comprises the following steps of putting activated carbon fibers into an ethanol solution, adding coco glucoside, stirring uniformly, adding sodium peroxide, reacting for 8-10H at 40-60 ℃, after the reaction is finished, introducing 10-20mA current for 10min, concentrating, coating, and freeze-drying.
7. The method for preparing a fresh and alive normal clear beverage for discharging oil and defecation according to claim 6, wherein in the step A4, hawthorn, cassia seed, sea buckthorn and cordyceps militaris are crushed into 30-60 meshes.
8. The method according to claim 7, wherein in the step A6, the voltage of the electromagnetic field is 18V and the current is 0.3A.
CN202110161733.3A 2021-02-05 2021-02-05 Fresh and alive normal-heat-clearing drink formula for discharging oil and discharging stubborn stool and preparation method thereof Pending CN112825994A (en)

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Application publication date: 20210525