CN112763654A - Glufosinate-ammonium synergist synthesis purity detection device and detection method - Google Patents

Glufosinate-ammonium synergist synthesis purity detection device and detection method Download PDF

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Publication number
CN112763654A
CN112763654A CN202011515975.XA CN202011515975A CN112763654A CN 112763654 A CN112763654 A CN 112763654A CN 202011515975 A CN202011515975 A CN 202011515975A CN 112763654 A CN112763654 A CN 112763654A
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China
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detection
glufosinate
synergist
ammonium
shaped
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钱前
先斌
傅胜辉
胡其钊
王丹
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ANHUI COSTAR BIO-CHEMICAL CO LTD
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ANHUI COSTAR BIO-CHEMICAL CO LTD
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/90Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms 
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B3/00Cleaning by methods involving the use or presence of liquid or steam
    • B08B3/02Cleaning by the force of jets or sprays

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Cleaning By Liquid Or Steam (AREA)
  • Accessories For Mixers (AREA)

Abstract

The invention discloses a glufosinate-ammonium synergist synthesis purity detection device and a glufosinate-ammonium synergist synthesis purity detection method, and belongs to the technical field of purity detection. According to the glufosinate synergist synthetic purity detection device and the detection method, detection data are uploaded and recorded by the detection head every 1s, the air cylinder drives the piston rod to be reduced to the minimum distance, the piston rod seals a through hole for detection of the stirring shell, the detection head is located in the lantern ring, cleaning liquid in the water tank fills the T-shaped ring groove and is sprayed out from the nozzle along the water spray pipe, the gear rotates along the gear ring in the spraying process, the detection head is cleaned through 360-degree rotating spraying, the detection head is cleaned in an all-around mode, and the detection degree is improved.

Description

Glufosinate-ammonium synergist synthesis purity detection device and detection method
Technical Field
The invention relates to the technical field of purity detection, and particularly relates to a device and a method for detecting the synthesis purity of a glufosinate-ammonium synergist.
Background
The liquid chemical industry refers to a chemical product in a liquid state, the relationship between human beings and the chemical industry is very close, the liquid chemical industry is popularized to the aspects of life, in modern life, the chemical product can not be opened almost at any time and any place, some chemical products play epoch-making important roles in the human development history, the production and the application of the liquid chemical industry and even represent a certain history stage of human civilization, but the purity of the liquid chemical industry needs to be detected before the liquid chemical industry is used, although the existing purity detector can meet the use of people, certain problems still exist, and the specific problems are as follows:
traditional purity detector design is fairly simple, directly inserts the detector inside liquid and detects, because liquid has the mobility, leads to the data of detection to deviate probably to current purity detector can't heat liquid chemicals, leads to can't be in according to liquid chemicals and can't compare the data that detect under the temperature, causes the detectivity singleness.
Disclosure of Invention
The invention aims to provide a device and a method for detecting the synthesis purity of a glufosinate-ammonium synergist, so as to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme: a glufosinate-ammonium synergist synthesis purity detection device comprises a base and a stirring shell, wherein the bottom of the base is connected with rollers, the top of the base is respectively connected with an outer frame and the stirring shell, a motor and a movable stirring shaft are fixed on the top surface of the outer frame, the motor is connected with the stirring shaft through a belt, and the stirring shaft penetrates into the stirring shell and is connected with stirring blades;
the side wall of the outer frame is connected with a detection mechanism which stretches into the stirring shell, the detection mechanism stretches into the stirring shell to detect the purity of the glufosinate-ammonium synergist, the detection mechanism retracts into the outer portion of the stirring shell, an annular rotating mechanism fixed with the stirring shell is sleeved outside the detection mechanism, a cleaning mechanism is installed on the annular rotating mechanism, and the cleaning mechanism rotates around the annular rotating mechanism to clean the detection mechanism.
Furthermore, a water pump connected to the stirring shell is fixed on the base, and the water pump pumps or conveys the glufosinate-ammonium synergist into the stirring shell.
Furthermore, the detection mechanism comprises an air cylinder, an air cylinder frame and a detection head, wherein the air cylinder frame is fixed on the side wall of the outer frame, the air cylinder is inserted into the air cylinder frame for fixing, a piston rod of the air cylinder is inserted into a through hole for detection of the stirring shell, and the detection head is embedded into the piston rod;
the cylinder drives the piston rod to extend to the maximum distance, and the detection head is positioned in the stirring shell;
the cylinder drives the piston rod to reduce to the minimum distance, the piston rod seals the through hole used for detection of the stirring shell, and the detection head is located in the annular rotating mechanism.
Further, the annular rotating mechanism comprises a lantern ring, a U-shaped frame and a T-shaped sealing ring, the lantern ring is fixed on the outer wall of the stirring shell through a support column, ring grooves which are symmetrical to each other are machined on the peripheral surfaces of the two sides of the lantern ring, a gear ring is sleeved on each ring groove, the U-shaped frame is sleeved from the inner side of the lantern ring, gears are inserted into bearings at the two ends of the U-shaped frame, and the U-shaped frame is meshed with the gear rings at the two sides through the gears;
the inner peripheral surface of the lantern ring is provided with a T-shaped annular groove, the T-shaped sealing ring is clamped into the T-shaped annular groove and fixed with the U-shaped frame, and the T-shaped sealing ring rotates around the T-shaped annular groove along with the U-shaped frame and is in a sealing state in the rotating process.
Furthermore, the cleaning mechanism comprises a water tank, a water pipe, a water spray pipe and a nozzle, wherein the water tank is fixed on the top surface of the outer frame, the water pipe connected with the water tank penetrates through the outer frame and extends into the T-shaped ring groove, one end of the water spray pipe is fixed on the T-shaped sealing ring, the other end of the water spray pipe is connected with the nozzle, through holes arranged in the water spray pipe, the nozzle and the T-shaped sealing ring are communicated with the T-shaped ring groove, and the water tank is used for filling the T-shaped ring groove with cleaning liquid and spraying the cleaning liquid to the detection head from the nozzle through rotation of.
Furthermore, the gear is connected with an external power device, the power of the gear and the air cylinder are uniformly controlled by the PLC, and when the air cylinder is in the shortest stroke, the power of the gear triggers the rotary water spraying cleaning.
The invention provides another technical scheme, which comprises a detection method of a glufosinate-ammonium synergist synthesis purity detection device, and comprises the following steps:
s1: liquid injection: the water pump 7 works to pump the glufosinate-ammonium synergist into the stirring shell, and the injected glufosinate-ammonium synergist submerges the detection head;
s2: stirring; the motor drives the stirring shaft to rotate through the belt, the stirring blade drives the glufosinate synergist to rotate continuously, and the detection head uploads and records detected data every 1 s;
s3: cleaning: the cylinder drives the piston rod to reduce to minimum distance, the piston rod seals the through hole that the agitator shell is used for detecting, detects the head and is located the lantern ring, and T type annular is filled to the washing liquid in the water tank to spout from the nozzle along the spray pipe, at spun in-process gear along the ring gear rotation, through 360 rotatory spouts to detecting the head and accomplish the washing.
Further, in S3, the cleaned probe is inserted into the stirring housing for testing, the data of the test is uploaded and recorded every 1S, and steps S2 to S3 are repeated three times.
Compared with the prior art, the invention has the beneficial effects that: the invention provides a glufosinate-ammonium synergist synthetic purity detection device and a detection method, a water pump works to pump a glufosinate-ammonium synergist into a stirring shell, an injected glufosinate-ammonium synergist submerges a detection head, a motor drives a stirring shaft to rotate through a belt, stirring blades drive the glufosinate-ammonium synergist to continuously rotate, the detection head uploads and records detected data every 1s, a cylinder drives a piston rod to reduce to a minimum distance, the piston rod seals a through hole for detection of the stirring shell, the detection head is positioned in a lantern ring, cleaning liquid in a water tank fills a T-shaped ring groove and is sprayed out from a nozzle along a water spraying pipe, a gear rotates along a gear ring in the spraying process, the detection head is cleaned through 360-degree rotation in all directions, the detection head is cleaned by a method, and the detection degree is improved.
Drawings
FIG. 1 is an overall block diagram of the present invention;
FIG. 2 is a view showing the internal structure of the stirring shell of the present invention;
FIG. 3 is an overall side view of the present invention;
FIG. 4 is a perspective view of the ring rotating mechanism and the cleaning mechanism of the present invention;
FIG. 5 is a view of the detection head of the present invention in a retracted state;
FIG. 6 is a view of the test head of the present invention in an extended state;
fig. 7 is an enlarged view of fig. 5 a according to the present invention.
In the figure: 1. a base; 11. a stirring shell; 12. a motor; 13. an outer frame; 2. a roller; 3. a stirring shaft; 31. stirring blades; 4. a detection mechanism; 41. a cylinder; 42. a cylinder frame; 43. a detection head; 5. a ring-shaped rotating mechanism; 51. a collar; 511. a ring groove; 5111. a ring gear; 52. a U-shaped frame; 521. a gear; 53. a T-shaped sealing ring; 6. a cleaning mechanism; 61. a water tank; 62. a water delivery pipe; 63. a water spray pipe; 64. a nozzle; 7. and (4) a water pump.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-2, a glufosinate-ammonium synergist synthetic purity detection device comprises a base 1 and a stirring shell 11, wherein the bottom of the base 1 is connected with a roller 2, the roller 2 drives the base 1 to move, the top of the base 1 is respectively connected with an outer frame 13 and the stirring shell 11, a motor 12 and a stirring shaft 3 which is movably mounted are fixed on the top surface of the outer frame 13, the stirring shaft 3 rotates around the outer frame 13, the motor 12 is connected with the stirring shaft 3 through a belt, the stirring shaft 3 penetrates through the stirring shell 11 and is connected with a stirring blade 31, and the motor 12 drives the stirring blade 31 to rotate and stir the glufosinate-ammonium synergist.
Be connected with detection mechanism 4 flexible to stirring in the shell 11 on the lateral wall of outrigger 13, detection mechanism 4 stretches into the purity that detects the glufosinate-ammonium synergist in stirring shell 11, and detection mechanism 4 withdraws the outside of stirring shell 11, and detection mechanism 4 outside cover has the annular rotary mechanism 5 fixed with stirring shell 11, installs wiper mechanism 6 on the annular rotary mechanism 5, and wiper mechanism 6 washs detection mechanism 4 around annular rotary mechanism 5 rotation.
The water pump 7 connected to the stirring shell 11 is fixed on the base 1, the water pump 7 pumps or conveys the glufosinate-ammonium synergist to the stirring shell 11, and the glufosinate-ammonium synergist is pumped by the water pump 7.
Referring to fig. 3, the detecting mechanism 4 includes an air cylinder 41, an air cylinder frame 42 and a detecting head 43, the air cylinder frame 42 is fixed on the side wall of the outer frame 13, the air cylinder 41 is inserted into the air cylinder frame 42 and fixed, a piston rod of the air cylinder 41 is inserted into a through hole for detection of the stirring shell 11, the detecting head 43 is embedded into the piston rod, the surface of the detecting head 43 is flush with the piston rod, the surface of the detecting head 43 is not affected in the sliding process, and the detecting head is flush and clean to avoid residue.
The cylinder 41 drives the piston rod to extend to the maximum distance, and the detection head 43 is located in the stirring shell 11.
The cylinder 41 drives the piston rod to reduce to the minimum distance, the piston rod seals the through hole of the stirring shell 11 for detection, and the detection head 43 is positioned in the annular rotating mechanism 5.
Referring to fig. 4-7, the ring rotating mechanism 5 includes a collar 51, a U-shaped frame 52 and a T-shaped sealing ring 53, the collar 51 is fixed on the outer wall of the agitator housing 11 through a pillar, ring grooves 511 that are symmetrical to each other are formed on the circumferential surfaces of both sides of the collar 51, a gear ring 5111 is sleeved on the ring grooves 511, the U-shaped frame 52 is sleeved from the inner side of the collar 51, a gear 521 is inserted into bearings at both ends of the U-shaped frame 52, the U-shaped frame 52 is engaged with the gear rings 5111 at both sides through the gear 521, and the gear ring 5111 and the gear 521 are engaged with each other to complete.
A T-shaped ring groove 511 is processed on the inner circumferential surface of the collar 51, and a T-shaped sealing ring 53 is clamped in the T-shaped ring groove 511 and fixed with the U-shaped frame 52, so that the T-shaped sealing ring 53 rotates around the T-shaped ring groove 511 along with the U-shaped frame 52 and is in a sealing state in the rotating process.
The cleaning mechanism 6 comprises a water tank 61, a water pipe 62, a water spray pipe 63 and a nozzle 64, wherein the water tank 61 is fixed on the top surface of the outer frame 13, the water pipe 62 connected with the water tank 61 penetrates through the outer frame 13 and extends into the T-shaped ring groove 511, one end of the water spray pipe 63 is fixed on the T-shaped sealing ring 53, the other end of the water spray pipe 63 is connected with the nozzle 64, through holes arranged in the water spray pipe 63, the nozzle 64 and the T-shaped sealing ring 53 are communicated with the T-shaped ring groove 511, and the water tank 61 is used for filling the T-shaped ring groove 511 with cleaning liquid and spraying the cleaning liquid to the detection head 43 from the nozzle 64 along the water.
The gear 521 is connected with an external power device, the power of the gear 521 and the cylinder 41 are controlled by a PLC in a unified mode, and when the cylinder 41 is in the shortest stroke, the power of the gear 521 triggers the rotary water spraying cleaning.
The detection method of the glufosinate-ammonium synergist synthesis purity detection device comprises the following steps:
s1: liquid injection: the water pump 7 works to pump the glufosinate-ammonium synergist into the stirring shell 11, and the injected glufosinate-ammonium synergist submerges the detection head 43;
s2: stirring; the motor 12 drives the stirring shaft 3 to rotate through a belt, the stirring blade 31 drives the glufosinate-ammonium synergist to continuously rotate, and the detection head 43 uploads and records detected data every 1 s;
s3: cleaning: the cylinder 41 drives the piston rod to reduce to the minimum distance, the piston rod seals the through hole of the stirring shell 11 for detection, the detection head 43 is positioned on the lantern ring 51, the cleaning solution in the water tank 61 fills the T-shaped ring groove 511 and is sprayed out from the nozzle 64 along the spray pipe 63, the gear 521 rotates along the gear ring 5111 in the spraying process, and the cleaning is completed by being sprayed to the detection head 43 through 360-degree rotation.
Further, in S3, the cleaned probe 43 is inserted into the stirring housing 11 and tested, the data of the test is uploaded and recorded every 1S, and steps S2 to S3 are repeated three times.
In summary, the following steps: the glufosinate-ammonium synergist synthesis purity detection device and the detection method are characterized in that the water pump 7 works to pump the glufosinate-ammonium synergist into the stirring shell 11, the injected glufosinate-ammonium synergist submerges the detection head 43, the motor 12 drives the stirring shaft 3 to rotate through a belt, the stirring blade 31 drives the glufosinate-ammonium synergist to continuously rotate, the detection head 43 uploads and records detected data every 1s, the cylinder 41 drives the piston rod to reduce to a minimum distance, the piston rod seals a through hole for detection of the stirring shell 11, the detection head 43 is located in the lantern ring 51, a T-shaped ring groove 511 is filled with cleaning liquid in the water tank 61 and is sprayed out from a nozzle 64 along a water spraying pipe 63, the gear 521 rotates along the gear ring 5111 in the spraying process, the detection head 43 is cleaned through 360-degree rotating spraying, the detection head 43 is cleaned in an all-round method, and the detection degree.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be able to cover the technical solutions and the inventive concepts of the present invention within the technical scope of the present invention.

Claims (8)

1. A glufosinate-ammonium synergist synthesis purity detection device is characterized by comprising a base (1) and a stirring shell (11), wherein the bottom of the base (1) is connected with rollers (2), the top of the base (1) is respectively connected with an outer frame (13) and the stirring shell (11), a motor (12) and a stirring shaft (3) which is movably mounted are fixed on the top surface of the outer frame (13), the motor (12) is connected with the stirring shaft (3) through a belt, and the stirring shaft (3) penetrates into the stirring shell (11) and is connected with stirring blades (31);
be connected with detection mechanism (4) flexible in to stirring shell (11) on the lateral wall of outrigger (13), detection mechanism (4) stretch into the purity that detects the glufosinate-ammonium synergist in stirring shell (11), the outside of detection mechanism (4) withdrawal stirring shell (11), detection mechanism (4) outside cover has annular rotary mechanism (5) fixed with stirring shell (11), install wiper mechanism (6) on annular rotary mechanism (5), wiper mechanism (6) are around annular rotary mechanism (5) rotatory cleaning detection mechanism (4).
2. The device for detecting the synthesis purity of the glufosinate-ammonium synergist according to claim 1, wherein a water pump (7) connected to the stirring shell (11) is fixed on the base (1), and the water pump (7) pumps or conveys the glufosinate-ammonium synergist into the stirring shell (11).
3. The device for detecting the synthesis purity of the glufosinate-ammonium synergist according to claim 1, wherein the detection mechanism (4) comprises a cylinder (41), a cylinder frame (42) and a detection head (43), the cylinder frame (42) is fixed on the side wall of the outer frame (13), the cylinder (41) is inserted into the cylinder frame (42) for fixation, a piston rod of the cylinder (41) is inserted into a through hole of the stirring shell (11) for detection, and the detection head (43) is embedded into the piston rod;
the cylinder (41) drives the piston rod to extend to the maximum distance, and the detection head (43) is positioned in the stirring shell (11);
the cylinder (41) drives the piston rod to be reduced to the minimum distance, the piston rod seals the through hole of the stirring shell (11) for detection, and the detection head (43) is positioned in the annular rotating mechanism (5).
4. The glufosinate-ammonium synergist synthesis purity detection device as claimed in claim 1, wherein the annular rotating mechanism (5) comprises a lantern ring (51), a U-shaped frame (52) and a T-shaped sealing ring (53), the lantern ring (51) is fixed on the outer wall of the stirring shell (11) through a support, annular grooves (511) which are symmetrical to each other are formed in the peripheral surfaces of the two sides of the lantern ring (51), a gear ring (5111) is sleeved on the annular grooves (511), the U-shaped frame (52) is sleeved from the inner side of the lantern ring (51), gears (521) are inserted into bearings at the two ends of the U-shaped frame (52), and the U-shaped frame (52) is meshed with the gear rings (5111) at the two sides through the gears (521);
the inner circumferential surface of the lantern ring (51) is provided with a T-shaped ring groove (511), the T-shaped sealing ring (53) is clamped into the T-shaped ring groove (511) and fixed with the U-shaped frame (52) and used for enabling the T-shaped sealing ring (53) to rotate around the T-shaped ring groove (511) along with the U-shaped frame (52) and be in a sealing state in the rotating process.
5. The device for detecting the synthetic purity of the glufosinate-ammonium synergist according to claim 1, wherein the cleaning mechanism (6) comprises a water tank (61), a water delivery pipe (62), a water spraying pipe (63) and a nozzle (64), the water tank (61) is fixed on the top surface of the outer frame (13), the water delivery pipe (62) connected with the water tank (61) extends into the T-shaped annular groove (511) through the outer frame (13), one end of the water spraying pipe (63) is fixed on the T-shaped sealing ring (53), the other end of the water spraying pipe (63) is connected with the nozzle (64), through holes arranged in the water spraying pipe (63), the nozzle (64) and the T-shaped sealing ring (53) are communicated with the T-shaped annular groove (511), and the water tank (61) is used for filling the T-shaped annular groove (511) with cleaning liquid and is sprayed to the detection head (43) through 360 degrees of the nozzle (64) along the water spraying pipe (63).
6. The device and the method for detecting the synthesis purity of the glufosinate-ammonium synergist according to claim 4, wherein the gear (53) is connected with an external power device, the power of the gear (53) and the cylinder (41) are controlled by a PLC in a unified manner, and when the cylinder (41) is in the shortest stroke, the power of the gear (53) triggers the rotary water spraying cleaning.
7. The detection method of the glufosinate-ammonium synergist synthesis purity detection device according to claim 1, characterized by comprising the following steps:
s1: liquid injection: the water pump (7) works to pump the glufosinate-ammonium synergist into the stirring shell (11), and the injected glufosinate-ammonium synergist submerges the detection head (43);
s2: stirring; the motor (12) drives the stirring shaft (3) to rotate through a belt, the stirring blade (31) drives the glufosinate synergist to continuously rotate, and the detection head (43) uploads and records detected data every 1 s;
s3: cleaning: the cylinder (41) drives the piston rod to reduce to the minimum distance, the piston rod seals a through hole used for detection of the stirring shell (11), the detection head (43) is located on the lantern ring (51), cleaning liquid in the water tank (61) fills the T-shaped annular groove (511) and is sprayed out from the nozzle (64) along the water spray pipe (63), the gear (53) rotates along the gear ring (5111) in the spraying process, and the cleaning is finished by spraying the cleaning liquid to the detection head (43) through 360-degree rotation.
8. The method for detecting the glufosinate-ammonium synergist synthesis purity detection device according to claim 7, wherein the cleaned detection head (43) is inserted into the stirring shell (11) for detection in S3, the detected data is uploaded and recorded every 1S, and the steps S2-S3 are repeated three times.
CN202011515975.XA 2020-12-21 2020-12-21 Glufosinate-ammonium synergist synthesis purity detection device and detection method Pending CN112763654A (en)

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CN210010251U (en) * 2019-03-25 2020-02-04 国网陕西省电力公司咸阳供电公司 Automatic cleaning equipment for detecting insulating porcelain insulator
CN211359793U (en) * 2019-11-18 2020-08-28 凤城市曙光汽车半轴有限责任公司 Cleaning device for automobile parts
CN211148586U (en) * 2019-11-19 2020-07-31 张家港检验认证有限公司 Purity detector for liquid chemicals
CN212068446U (en) * 2020-01-22 2020-12-04 深圳市三神科技有限公司 Glue apparatus for producing convenient to wash
CN211891417U (en) * 2020-03-22 2020-11-10 山东启新新型建材科技有限公司 Portable batching stirring mortar device
CN111751504A (en) * 2020-07-12 2020-10-09 广西壮族自治区特种设备检验研究院 Nondestructive testing device for pressure container
CN212134556U (en) * 2020-11-02 2020-12-11 北京原能细胞生物科技有限公司 Acidimeter with automatic washing function

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114577741A (en) * 2022-01-26 2022-06-03 昆明冠生园食品有限公司 Moon cake component detection device, system and method

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