CN112704653A - Floral water with sleeping-aiding and insect-expelling effects - Google Patents
Floral water with sleeping-aiding and insect-expelling effects Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
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- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P25/00—Drugs for disorders of the nervous system
- A61P25/20—Hypnotics; Sedatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q13/00—Formulations or additives for perfume preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q15/00—Anti-perspirants or body deodorants
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/02—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings containing insect repellants
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Abstract
The invention discloses floral water with sleep-aiding and insect-expelling effects, which comprises the following raw materials: ethanol, deionized water, lavender, traditional Chinese medicine extract, tween-80, citronella oil and tea tree oil. The preparation method comprises the following steps: firstly, extracting essential oil from lavender and traditional Chinese medicines, then adding ethanol, tea tree oil, tween-80 and citronella oil, and stirring to obtain floral water.
Description
Technical Field
The invention discloses floral water, and particularly relates to floral water with sleeping-aiding and insect-expelling effects.
Background
Floral water is a unique perfume product in China, and firstly, floral oil is used as a main perfume, and the perfume product is prepared from ethanol and mainly has the functions of covering smell and sterilizing and decontaminating. The prescription is about 3% of essence, about 70% of alcohol and 25% of distilled water. Since the proportion is easy to permeate into bacteria, the floral water can also be used as a fragrant disinfectant. The prescription and the process of the prior floral water are continuously improved, and on the basis of keeping the original main formula, some traditional Chinese medicine components with the functions of clearing away heat and toxic materials, relieving swelling and pain are added, so that the floral water has the effects of removing miliaria, relieving itching, treating skin diseases, refreshing and restoring consciousness and the like besides the original effects. For example, the components such as menthol and the like are added into the floral water to make the floral water cool; the mosquito repellent is added to make the mosquito repellent have mosquito repellent effect. In addition, a small amount of chelating agent, antioxidant, pigment and other components are often added to the floral water, so that the ornamental value, safety, stability and efficacy of the floral water are improved. At present, floral water becomes a necessary product for solving skin diseases such as miliaria, heat, dryness and itching in summer.
However, most of toilet water in the market at present uses anophelifuge ester and deet as mosquito repellents in order to achieve a mosquito repelling effect, although the mosquito repelling performance of the toilet water can be improved, the anophelifuge ester and the deet contain toxic substances, and can affect the health of people after long-term use.
Disclosure of Invention
The invention discloses floral water with sleep-aiding and insect-expelling effects, which specifically comprises the following raw materials: 20-40 parts of ethanol, 10-20 parts of deionized water, 5-10 parts of lavender, 5-10 parts of traditional Chinese medicine extracts (spina date seed, white paeony root and poria cocos), 1-3 parts of citronella oil, 1-2 parts of tween-80 and 1-3 parts of tea tree oil.
Preferably, the traditional Chinese medicine extract is prepared from spina date seed, white paeony root and poria cocos.
Preferably, the preparation method of the floral water comprises the following steps:
s1: washing lavender, drying in the air, cutting into pieces, sieving with a 60-80 mesh sieve to obtain lavender powder, then placing the lavender powder into a round-bottom flask containing distilled water, placing the round-bottom flask into a constant-temperature electric heating sleeve, heating after a distillation extraction device is installed, heating until the solution is boiled, and performing distillation extraction by using water vapor;
s2: dissolving citronella oil, tea tree oil and tween-80 in ethanol, and stirring for 1 h;
s3: respectively pulverizing semen Ziziphi Spinosae, radix Paeoniae alba and Poria 10 parts by weight with plant pulverizer to 60-80 mesh, soaking in 20 parts by weight of deionized water for 30min, heating the above 3 Chinese medicinal materials and soaking solution to boiling, decocting in water for 2 times, filtering, mixing filtrates for 2 times, and concentrating to obtain Chinese medicinal extract;
s4: adding products S1 and S3 into S2, stirring for 2h, placing into a centrifuge, centrifuging for 10min at 6000-8000rpm/min, taking the supernatant after centrifugation, standing for 4h, and filtering to obtain the floral water.
Preferably, in the step S1, the ratio of material to liquid during distillation is 1 g: (15-25) ml.
Preferably, in step S2, the mass ratio of the citronella oil, the tea tree oil, the tween 80 and the ethanol is 1: 1: (0.5-1): (10-20).
Preferably, in step S3, the filtrates are combined and concentrated to 30-40% of the original volume.
Compared with the prior art, the invention has the following beneficial effects:
the invention discloses floral water with sleep-aiding and insect-expelling effects, which is simple in preparation method, wide in raw material source and easy for large-scale production. The tea tree oil contains the components such as the p-menthane-1-ol-4-1, 8-cineole and the like, can effectively repel mosquitoes, and achieves the effects of sterilization and mosquito repelling by utilizing the tea tree oil and the citronella oil; the lavender essential oil contains linalool, and after a certain amount of linalool is inhaled, the sleep time induced by pentobarbital sodium can be prolonged; the main components of the spina date seed, the white paeony root and the tuckahoe contain triterpenes, so that the spina date seed, the white paeony root and the tuckahoe have the effects of tranquilizing and hypnotizing, resisting anxiety, resisting convulsion and resisting arrhythmia, and the effect of helping sleep is achieved by adding the substances.
Detailed description of the preferred embodiments
Example 1:
a floral water with effects of improving sleep and expelling parasites is prepared by the following steps:
s1: washing 10 parts of lavender, drying in the air, cutting into pieces, sieving with a 60-80-mesh sieve to obtain lavender powder, and then filling the lavender powder into a round-bottom flask filled with distilled water, wherein the material-liquid ratio is 1 g: 20ml, placing the round-bottom flask in a constant-temperature electric heating sleeve, heating after the distillation extraction device is installed, heating until the solution boils, and performing distillation extraction by using water vapor;
s2: dissolving 2 parts of citronella oil, 2 parts of tea tree oil and 1.5 parts of tween-80 in 30 parts of ethanol, and stirring for 1 hour for later use;
s3: respectively pulverizing semen Ziziphi Spinosae, radix Paeoniae alba and Poria 10 parts by weight with plant pulverizer to 60-80 mesh, soaking in 20 parts by weight of deionized water for 30min, heating the above 3 Chinese medicinal materials and soaking solution to boiling, decocting in water for 2 times, filtering, mixing filtrates for 2 times, concentrating to 30% of original volume, and making into Chinese medicinal extract;
s4: adding products S1 and S3 into S2, stirring for 2h, placing into a centrifuge, centrifuging at 7000rpm/min for 10min, taking the centrifuged supernatant, standing for 4h, and filtering to obtain the floral water.
Example 2:
a floral water with effects of improving sleep and expelling parasites is prepared by the following steps:
s1: washing 8 parts of lavender, drying in the air, cutting into pieces, sieving with a 60-80-mesh sieve to obtain lavender powder, and then filling the lavender powder into a round-bottom flask filled with distilled water, wherein the material-liquid ratio is 1 g: 15ml, placing the round-bottom flask in a constant-temperature electric heating sleeve, heating after the distillation extraction device is installed, heating until the solution boils, and performing distillation extraction by using water vapor;
s2: dissolving 3 parts of citronella oil, 3 parts of tea tree oil and 2 parts of tween-80 in 30 parts of ethanol, and stirring for 1 hour for later use;
s3: respectively pulverizing semen Ziziphi Spinosae, radix Paeoniae alba and Poria 10 parts by weight with plant pulverizer to 60-80 mesh, soaking in 20 parts by weight of deionized water for 30min, heating the above 3 Chinese medicinal materials and soaking solution to boil, decocting in water for 2 times, filtering, mixing filtrates for 2 times, concentrating to 40% of original volume, and making into Chinese medicinal extract;
s4: adding products S1 and S3 into S2, stirring for 2h, placing into a centrifuge, centrifuging at 6000rpm/min for 10min, taking the centrifuged supernatant, standing for 4h, and filtering to obtain the floral water.
Example 3:
a floral water with effects of improving sleep and expelling parasites is prepared by the following steps:
s1: washing 5 parts of lavender, drying in the air, cutting into pieces, sieving with a 60-80-mesh sieve to obtain lavender powder, and then filling the lavender powder into a round-bottom flask filled with distilled water, wherein the material-liquid ratio is 1 g: 25ml, placing the round-bottom flask in a constant-temperature electric heating sleeve, heating after the distillation extraction device is installed, heating until the solution boils, and performing distillation extraction by using water vapor;
s2: dissolving 1 part of citronella oil, 1 part of tea tree oil and 1 part of tween-80 in 20 parts of ethanol, and stirring for 1 hour for later use;
s3: respectively pulverizing semen Ziziphi Spinosae, radix Paeoniae alba and Poria 10 parts by weight with plant pulverizer to 60-80 mesh, soaking in 20 parts by weight of deionized water for 30min, heating the above 3 Chinese medicinal materials and soaking solution to boiling, decocting in water for 2 times, filtering, mixing filtrates for 2 times, concentrating to 35% of original volume, and making into Chinese medicinal extract;
s4: adding products S1 and S3 into S2, stirring for 2h, placing into a centrifuge, centrifuging at 8000rpm/min for 10min, taking the centrifuged supernatant, standing for 4h, and filtering to obtain the floral water.
Example 4:
a floral water with effects of improving sleep and expelling parasites is prepared by the following steps:
s1: washing 10 parts of lavender, drying in the air, cutting into pieces, sieving with a 60-80-mesh sieve to obtain lavender powder, and then filling the lavender powder into a round-bottom flask filled with distilled water, wherein the material-liquid ratio is 1 g: 15ml, placing the round-bottom flask in a constant-temperature electric heating sleeve, heating after the distillation extraction device is installed, heating until the solution boils, and performing distillation extraction by using water vapor;
s2: dissolving 2 parts of citronella oil, 2 parts of tea tree oil and 2 parts of tween-80 in 30 parts of ethanol, and stirring for 1 hour for later use;
s3: respectively pulverizing semen Ziziphi Spinosae, radix Paeoniae alba and Poria 10 parts by weight with plant pulverizer to 60-80 mesh, soaking in 20 parts by weight of deionized water for 30min, heating the above 3 Chinese medicinal materials and soaking solution to boil, decocting in water for 2 times, filtering, mixing filtrates for 2 times, concentrating to 40% of original volume, and making into Chinese medicinal extract;
s4: adding products S1 and S3 into S2, stirring for 2h, placing into a centrifuge, centrifuging at 6000rpm/min for 10min, taking the centrifuged supernatant, standing for 4h, and filtering to obtain the floral water.
Comparative example 1
S1: washing 10 parts of lavender, drying in the air, cutting into pieces, sieving with a 60-80-mesh sieve to obtain lavender powder, and then filling the lavender powder into a round-bottom flask filled with distilled water, wherein the material-liquid ratio is 1 g: 20ml, placing the round-bottom flask in a constant-temperature electric heating sleeve, heating after the distillation extraction device is installed, heating until the solution boils, and performing distillation extraction by using water vapor;
s2: dissolving 2 parts of citronella oil, 2 parts of tea tree oil and 1 part of tween-80 in 30 parts of ethanol, and stirring for 1 hour for later use;
s3: and adding the product S1 into S2, stirring for 2h, putting into a centrifuge, centrifuging at 7000rpm/min for 10min, taking the centrifuged supernatant, standing for 4h, and filtering to obtain the floral water.
Comparative example 2:
s1: washing 10 parts of lavender, drying in the air, cutting into pieces, sieving with a 60-80-mesh sieve to obtain lavender powder, and then filling the lavender powder into a round-bottom flask filled with distilled water, wherein the material-liquid ratio is 1 g: 20ml, placing the round-bottom flask in a constant-temperature electric heating sleeve, heating after the distillation extraction device is installed, heating until the solution boils, and performing distillation extraction by using water vapor;
s2: respectively pulverizing semen Ziziphi Spinosae, radix Paeoniae alba and Poria 10 parts by weight with plant pulverizer to 60-80 mesh, soaking in 20 parts by weight of deionized water for 30min, heating the above 3 Chinese medicinal materials and soaking solution to boiling, decocting in water for 2 times, filtering, mixing filtrates for 2 times, concentrating to 30% of original volume, and making into Chinese medicinal extract;
s4: adding products S1 and S2 into 30 parts of ethanol, stirring for 2h, placing into a centrifuge, centrifuging at 7000rpm/min for 10min, taking the centrifuged supernatant, standing for 4h, and filtering to obtain the floral water.
And (3) performance testing:
the floral water prepared in the above examples 1 to 4 and comparative examples 1 to 2 was preliminarily examined according to the national light industry standards of the people's republic of China QB/T4147-2010 mosquito repellent floral water.
(1) Appearance: the toilet water prepared in examples 1-4 and comparative examples 1-2 has clear water quality, no obvious impurities and black spots, and fresh visual feeling.
(2) Sensory: the two types of floral water are both green transparent solution, and the floral water is uniformly smeared on the skin, so that the prepared floral water has fresh fragrance and brings people a relatively comfortable cool feeling.
(3) Low-temperature stability: 50ml of the floral water prepared in examples 1-4 and comparative examples 1-2 was measured, placed in a 150ml triangular flask, kept at 0 + -2 deg.C for 1 hour in a refrigerator, stirred with a glass rod for 1 time every 15min for 15s each time, placed in a refrigerator for 7 hours, taken out after 7 hours, placed at room temperature, and observed for several floral water types within 24 hours. Several floral water samples were found to remain clear, indicating that the low temperature stability of these several floral water samples was better.
And (3) testing the mosquito repelling effect by referring to GB/T17322.10-1998:
selecting 60 qualified subjects in the attack force test, dividing the subjects into 6 groups, exposing skin of 5cm multiplied by 5cm on the backs of the hands of the 60 qualified subjects in the attack force test respectively, and covering the rest parts of the subjects tightly. Wherein 1 hand was used as a blank control, and the other 1 hand was used to prepare toilet water of 1.5. mu.l/cm from examples 1-4 and comparative examples 1-22The protective agent is uniformly smeared on the exposed skin of the back of a hand, the hand is stretched into a mosquito cage qualified in an attack force test for 2min after 2h, whether mosquitoes suck blood or not is observed, the test is carried out for 1 time every hour later, the mosquito protective agent is invalid as long as 1 mosquito sucks blood in the future, and the effective protection rates of 4h, 6h, 8h, 10h and 12h are observed and calculated.
After the floral water prepared in example 1 was applied, the number of bites was 0 in 8 hours, 4 after 10 hours, and 7 after 12 hours.
After the floral water prepared in example 2 was applied, the number of bites was 0 in 6 hours, 4 after 8 hours, 6 after 10 hours, and 11 after 12 hours.
After the floral water prepared in example 3 was applied, the number of bites was 0 in 4 hours, 5 after 8 hours, 9 after 10 hours, and 14 after 12 hours.
After the floral water prepared in example 4 was applied, the number of bites was 0 in 4 hours, 7 after 8 hours, 10 after 10 hours, and 15 after 12 hours.
After the floral water prepared in comparative example 1 was applied, the number of bites was 15 within 4 hours, 20 after 8 hours, 28 after 10 hours, and 32 after 12 hours.
After the floral water prepared in comparative example 2 was applied, the number of bites was 17 within 4 hours, 28 after 8 hours, 41 after 10 hours, and 47 after 12 hours.
The results are shown in Table 1.
And (3) testing the sleep-aiding effect:
selecting 60 qualified subjects in the attack force test, dividing the subjects into 6 groups, smearing floral water prepared in the steps of 1-4 and 1-2 before going to sleep at night, investigating the sleep condition of each experimenter by a Pittsburgh sleep quality index questionnaire (PSQI), and continuously testing for one week. PSQI was developed by doctor Buysse, 1989, for assessing sleep quality in psychiatric patients over the last week or month, and is widely used in the general population. The questionnaire consists of 19 items in 7 dimensions. The patients were evaluated for sleep quality, sleep latency, sleep duration, sleep efficiency, sleep disturbance, condition of hypnotics application, daytime dysfunction, etc. Each dimension is scored from 0 (best) to 3 (worst), the total score is 21, the lower the score is, the better the sleep quality is, and the lower the score is, the better the sleep quality is, the lower the score is, the score is less than or equal to 5, the better the sleep quality is. The results are shown in Table 1.
Table 1: mosquito repellent and sleep aid performance data for examples 1-4 and comparative examples 1-2
As can be seen from table 1, the toilet water prepared in examples 1 to 4 has good mosquito repellent and sleep aid effects, and the mosquito repellent effect and sleep aid effect are significantly higher than those of the toilet water prepared in comparative examples 1 to 2, which proves that the mosquito repellent and sleep aid effects of the toilet water are improved by the addition of the traditional Chinese medicine extract and the tea tree oil.
Claims (6)
1. The toilet water with the effects of helping sleep and expelling insects is characterized by comprising the following raw materials in parts by weight: 20-40 parts of ethanol, 10-20 parts of deionized water, 5-10 parts of lavender, 5-10 parts of traditional Chinese medicine extract, 1-3 parts of citronella oil, 1-2 parts of tween-80 and 1-3 parts of tea tree oil.
2. The floral water having the effects of improving sleep and expelling parasites according to claim 1, wherein said herbal extracts are prepared from Zizyphi Spinosae semen, Paeoniae radix and Poria.
3. The floral water having sleep-aiding and insect-repelling effects as claimed in claim 1, wherein said floral water is prepared by a method comprising the steps of:
s1: washing lavender, drying in the air, cutting into pieces, sieving with a 60-80 mesh sieve to obtain lavender powder, then placing the lavender powder into a round-bottom flask containing distilled water, placing the round-bottom flask into a constant-temperature electric heating sleeve, heating after a distillation extraction device is installed, heating until the solution is boiled, and performing distillation extraction by using water vapor;
s2: dissolving citronella oil, tea tree oil and tween-80 in ethanol, and stirring for 1 h;
s3: respectively pulverizing semen Ziziphi Spinosae, radix Paeoniae alba and Poria 10 parts by weight with plant pulverizer to 60-80 mesh, soaking in 20 parts by weight of deionized water for 30min, heating the above 3 Chinese medicinal materials and soaking solution to boiling, decocting in water for 2 times, filtering, mixing filtrates for 2 times, and concentrating to obtain Chinese medicinal extract;
s4: adding products S1 and S3 into S2, stirring for 2h, placing into a centrifuge, centrifuging for 10min at 6000-8000rpm/min, taking the supernatant after centrifugation, standing for 4h, and filtering to obtain the floral water.
4. The toilet water with the effects of helping sleep and expelling insects as claimed in claim 3, wherein in step S1, the ratio of material to liquid in distillation is 1 g: (15-25) ml.
5. The floral water having the effect of helping sleep and expelling parasites according to claim 3, wherein in step S2, the mass ratio of the citronella oil, the tea tree oil, the Tween 80 and the ethanol is 1: 1: (0.5-1): (10-20).
6. The floral water having the effect of helping sleep and expelling parasites according to claim 3, wherein in step S3, the filtrates are combined and concentrated to 30-40% of the original volume.
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| CN102429840A (en) * | 2011-09-22 | 2012-05-02 | 黄馨莹 | Mosquito repellent liquid and preparation method thereof |
| CN103040660A (en) * | 2011-10-12 | 2013-04-17 | 吴博 | Mosquito repellent floral water |
| CN102579288A (en) * | 2012-04-06 | 2012-07-18 | 厦门鼎嘉奇投资管理有限公司 | Natural plant essential oil composition capable of directly serving as mosquito repellent |
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| CN108379122A (en) * | 2018-04-04 | 2018-08-10 | 翟志桦 | A kind of cooling ointment and preparation method thereof |
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