CN112675779A - High-temperature-resistant easy-to-disperse emulsifier and preparation method thereof - Google Patents

High-temperature-resistant easy-to-disperse emulsifier and preparation method thereof Download PDF

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CN112675779A
CN112675779A CN202011536776.7A CN202011536776A CN112675779A CN 112675779 A CN112675779 A CN 112675779A CN 202011536776 A CN202011536776 A CN 202011536776A CN 112675779 A CN112675779 A CN 112675779A
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temperature resistant
emulsifier
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邓德贵
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Nantong Hengrun New Mstar Technology Ltd
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Nantong Hengrun New Mstar Technology Ltd
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Abstract

The invention discloses a high temperature resistant easy-to-disperse emulsifier and a preparation method thereof, belonging to the technical field of emulsifier preparation, by adding modified polyether amine, epoxy resin, modified polypropylene resin and polysorbate into the emulsifier formula, the hydrophilicity, stability, solubility and viscosity of the emulsifier are enhanced to a certain extent, meanwhile, a high temperature resistant material is added in the formula of the emulsifier, the high temperature resistant material is subjected to high temperature hot melting diffusion, and is uniformly distributed in the emulsion, effectively improves the thermal stability of the emulsifier, is suitable for high-temperature industry, and the oil phase fiber clusters are uniformly distributed in the emulsion, are in a net-bag-shaped structure and have net-shaped porous gaps, so that the emulsifier is easy to disperse and form in the emulsification work, a large amount of foam is generated to form emulsion, the emulsification effect of the emulsifier in a high-temperature environment is effectively improved, and the application range of the emulsifier is expanded.

Description

High-temperature-resistant easy-to-disperse emulsifier and preparation method thereof
Technical Field
The invention relates to the technical field of emulsifier preparation, in particular to a high-temperature-resistant easily-dispersible emulsifier and a preparation method thereof.
Background
Emulsifiers are substances which improve the surface tension between the various constituent phases of an emulsion to form a uniform and stable dispersion or emulsion. Emulsifiers are surface-active substances which have both hydrophilic and lipophilic groups in the molecule and which accumulate at the oil/water interface and reduce the interfacial tension and the energy required to form an emulsion, thereby increasing the energy of the emulsion.
The existing emulsifier has single component, so that the thermal stability and the emulsifying property are poor, and the common emulsifier is not easy to disperse and form aiming at the use of some high-temperature industries, so that the emulsifying effect under some high-temperature environments cannot be met.
Therefore, a high-temperature-resistant easy-dispersion emulsifier and a preparation method thereof are provided to effectively solve some problems in the prior art.
Disclosure of Invention
1. Technical problem to be solved
Aiming at the problems in the prior art, the invention aims to provide a high-temperature-resistant easily-dispersible emulsifier and a preparation method thereof, wherein modified polyetheramine, epoxy resin, modified polypropylene resin and polysorbate are added into an emulsifier formula to enhance the hydrophilicity, stability, solubility and viscosity of the emulsifier to a certain extent, and meanwhile, a high-temperature-resistant material is added into the emulsifier formula, is subjected to high-temperature hot melting diffusion and is uniformly distributed in an emulsion to effectively improve the thermal stability of the emulsifier, so that the emulsifier is suitable for high-temperature industry, oil-phase fiber clusters are uniformly distributed in the emulsion, are in a net-bag-shaped structure and have net-shaped porous gaps, the emulsifier is easy to disperse and form in the emulsification work, a large amount of foams are generated to form emulsion, and the emulsification effect of the emulsifier in a high-temperature environment is effectively improved, the application range is expanded.
2. Technical scheme
In order to solve the above problems, the present invention adopts the following technical solutions.
2. The high-temperature-resistant easy-to-disperse emulsifier comprises the following components in parts by mass: 15-20 parts of oil phase, 20-30 parts of water phase, 10-15 parts of oil phase fiber cluster, 2-5 parts of modified polyether amine, 30-45 parts of epoxy resin, 10-15 parts of modified polypropylene resin, 7-10 parts of polysorbate, 5-10 parts of sodium alginate and 5-8 parts of high-temperature resistant material, wherein the preparation method comprises the following steps:
s1, placing the oil phase, the modified polyether amine, the epoxy resin and the polysorbate in a stirring kettle, stirring for 1-1.5h at the high temperature of 100-120 ℃, cooling to 50-70 ℃, adding the oil phase fiber cluster, keeping the temperature, and stirring for 0.5-1h to obtain a mixture A;
s2, placing the water phase, the modified polypropylene resin and the sodium alginate in a stirring kettle, and stirring for 0.5-1h at the temperature of 30-50 ℃ to obtain a mixture B;
s3, adding the mixture B into the mixture A, slowly raising the temperature to 80-100 ℃, finally adding the high-temperature resistant material, stirring for 1-1.2h, and carrying out high-temperature hot melting diffusion on the high-temperature resistant material to obtain the high-temperature resistant easily-dispersible emulsifier.
Furthermore, the oil phase is formed by mixing glycerol and vegetable oil, the vegetable oil is stearic acid and oleic acid, the mass ratio of the glycerol to the vegetable oil is 2:1, the water phase is pure water, the glycerol is used as a moisturizing filler of the emulsifier, and the vegetable oil is matched to form the oil phase, so that the physical and chemical properties and the stability of the emulsifier are effectively improved.
Furthermore, the oil phase fiber bundles adopt fiber mesh bags formed by combining aluminum silicate fibers, glass fibers and carbon fibers, and the mass ratio of the aluminum silicate fibers to the glass fibers to the carbon fibers is 1:2: 1.
Furthermore, the fiber net bag comprises a hollow outer bag shell, a plurality of fiber yarns are distributed on the peripheral side wall of the hollow outer bag shell, the hollow outer bag shell is made of aluminum silicate fibers, and the plurality of fiber yarns are made of carbon fibers.
Furthermore, a plurality of fiber balls are filled in the hollow outer capsule shell, the fiber balls are made of glass fibers, the outer diameter of each fiber ball is far larger than the gap distance between every two adjacent fibers, the mesh-bag-shaped structure formed by the hollow outer capsule shell and the fibers is easy to foam the emulsion in the stirring process, and the plurality of fiber balls filled in the hollow outer capsule shell shake in the hollow outer capsule shell along with the emulsion in the stirring process, so that the emulsion effect on the emulsion is further enhanced.
Furthermore, the outer diameter of the hollow outer capsule shell is 2-5mm, and the diameter 1 is set within a certain specification range, so that the influence of the fiber mesh capsule on the use of the emulsifier due to larger particle size is effectively avoided under the action of promoting emulsification.
Furthermore, the high-temperature resistant material adopts hot-melt high-temperature resistant granules with a spherical structure, the hot-melt high-temperature resistant granules comprise hot-melt capsules positioned on the outer side, a plurality of glass beads are filled in the hollow outer capsule shells, the glass beads have the advantages of light weight, low heat conduction, high strength, good chemical stability and the like, the surfaces of the glass beads have oleophylic and hydrophobic properties through special treatment, the glass beads are very easy to disperse in an organic material system, after the hot-melt high-temperature resistant granules are placed in a stirring kettle, the hot-melt capsules positioned on the outer side are heated and fused under a certain temperature condition to release the plurality of glass beads inside the hot-melt capsules, and the plurality of glass beads are dispersed in the emulsion, so that the thermal stability of the emulsion is improved.
Further, the hollow outer capsule shell is made of hot-melt resin, a magnetic ball is embedded in the hollow outer capsule shell, and an air overflow layer is filled between the magnetic ball and the glass beads.
Further, the layer of overflowing gas is including the fixed effervescent disintegration layer of cladding in the magnetic ball outside, all be connected with a plurality of high absorbent fibres on the lateral wall all around of hot melt bag, it is a plurality of fibrous outer end that high absorbent fibres all runs through effervescent disintegration layer, high absorbent fibres in proper order and extends to the hot melt bag outside, is equipped with the effervescent disintegration layer of meeting water disintegration and releasing gas in the interlayer inside that glass microballon formed, and the in-process that the temperature promoted gradually in S3, hot melt bag is not totally dissolved when the temperature first-class is promoted, and effervescent disintegration layer is disintegrated by high absorbent fibres water guide, after producing gas, is favorable to promoting glass microballon outwards to jump out.
It is further, a plurality of all install the agitator in the stirred tank, the embedded magnet core of installing of establishing of agitator in S3 sets up the magnet core on the agitator, and the high temperature resistant granule of hot melt can move in the emulsion along with the agitator to effectively enlarged the home range of a plurality of high temperature resistant granules of hot melt, made glass bead can distribute in the emulsion comparatively evenly, and after the inside glass bead of hot melt bag releases completely, the agitator can also play the magnetic absorption recovery effect to a plurality of magnetic balls.
3. Advantageous effects
Compared with the prior art, the invention has the advantages that:
(1) according to the scheme, the modified polyether amine, the epoxy resin, the modified polypropylene resin and the polysorbate are added into the emulsifier formula, so that the hydrophilicity, the stability, the solubility and the viscosity of the emulsifier are enhanced to a certain degree, meanwhile, the high-temperature-resistant material is added into the emulsifier formula, is subjected to high-temperature hot melting diffusion and is uniformly distributed in the emulsifier, the thermal stability of the emulsifier is effectively improved, the emulsifier is suitable for being used in high-temperature industries, oil-phase fiber bundles are uniformly distributed in the emulsifier, are of a net-like structure and have net-like porous gaps, the emulsifier is easy to disperse and form in emulsification work, a large amount of foam is generated to form emulsion, the emulsification effect of the emulsifier in a high-temperature environment is effectively improved, and the application range of the emulsifier is expanded.
(2) The oil phase is formed by mixing glycerol and vegetable oil, the vegetable oil is stearic acid and oleic acid, the mass ratio of the glycerol to the vegetable oil is 2:1, the water phase is pure water, the glycerol is used as a moisturizing filler of the emulsifier, and the vegetable oil is matched to form the oil phase, so that the physical and chemical properties and the stability of the emulsifier are effectively improved.
(3) The oil phase fiber bundle adopts a fiber mesh bag formed by combining aluminum silicate fibers, glass fibers and carbon fibers, the mass ratio of the aluminum silicate fibers, the glass fibers and the carbon fibers is 1:2:1, the fiber mesh bag comprises a hollow outer bag shell, a plurality of fiber wires are distributed on the peripheral side wall of the hollow outer bag shell, the hollow outer bag shell is made of the aluminum silicate fibers, the plurality of fiber wires are made of the carbon fibers, a plurality of fiber balls are filled in the hollow outer bag shell, the fiber balls are made of the glass fibers, the outer diameter of each fiber ball is far larger than the gap distance between every two adjacent fiber wires, the mesh bag structure formed by the hollow outer bag shell and the fiber wires is easy to foam during the stirring process of the emulsion, and the plurality of fiber balls filled in the hollow outer bag shell, and the emulsion is shaken in the hollow outer capsule shell in the stirring process along with the emulsion, so that the emulsion effect on the emulsion is further enhanced.
(4) The outer diameter of the hollow outer capsule shell is 2-5mm, and the diameter of the hollow outer capsule shell is set to be 1 in a certain specification range, so that under the effect of promoting emulsification, the influence of the fiber mesh capsule on the use of the emulsifier due to larger particle size is effectively avoided.
(5) The high-temperature resistant material adopts hot-melt high-temperature resistant granules with a spherical structure, the hot-melt high-temperature resistant granules comprise hot-melt capsules positioned on the outer side, a plurality of glass beads are filled in the hollow outer capsule shells, the glass beads have the advantages of light weight, low heat conduction, higher strength, good chemical stability and the like, the surfaces of the glass beads have oleophylic and hydrophobic properties through special treatment, the glass beads are very easy to disperse in an organic material system, after the hot-melt high-temperature resistant granules are placed in a stirring kettle, the hot-melt capsules positioned on the outer side are heated and fused under a certain temperature condition, and a plurality of glass beads in the hot-melt high-temperature resistant granules are released, and the glass beads are dispersed in the emulsion, so that.
(6) The hollow outer capsule shell is made of hot melt resin, the magnetic ball is embedded in the hollow outer capsule shell, an air overflow layer is filled between the magnetic ball and the glass beads, the air overflow layer comprises an effervescent disintegration layer fixedly coated on the outer side of the magnetic ball, a plurality of high water-absorbing fibers are connected to the peripheral side wall of the hot melt capsule, the outer ends of the high water-absorbing fibers sequentially penetrate through the effervescent disintegration layer, the high water-absorbing fibers extend to the outer side of the hot melt capsule, the effervescent disintegration layer capable of being disintegrated and released when meeting water is arranged in the interlayer formed by the glass beads, the temperature is gradually increased in S3, the hot melt capsule is not completely dissolved when the temperature is initially increased, the effervescent disintegration layer is decomposed by the high water-absorbing fibers, and after gas is generated, the glass beads are favorably pushed to jump outwards.
(7) All install the agitator in a plurality of stirred tanks, the magnet core is installed to the embedded magnet core of establishing of agitator in S3, set up the magnet core on the agitator, the high temperature resistant granule of hot melt can be along with the agitator motion in the emulsion to effectively enlarged the home range of a plurality of high temperature resistant granules of hot melt, make glass bead can distribute in the emulsion comparatively evenly, and after the inside glass bead of hot melt bag releases completely, the agitator can also play the magnetic recovery effect to a plurality of magnetism balls.
Drawings
FIG. 1 is a process flow diagram of the present invention;
FIG. 2 is a diagram illustrating the state of the present invention in S3;
FIG. 3 is a schematic view of the structure at a fibrous web bladder of the present invention;
FIG. 4 is a schematic view of the interior of the hot melt refractory granule of the present invention;
FIG. 5 is a schematic view of the hot-melt high-temperature resistant granules of the present invention during hot-melt diffusion;
FIG. 6 is a schematic view showing the state before and after the hot-melt diffusion of the hot-melt high temperature resistant granules of the present invention.
The reference numbers in the figures illustrate:
1 fiber mesh capsule, 101 hollow outer capsule shell, 102 fiber filament, 103 fiber ball, 2 hot melt high temperature resistant granule, 201 hot melt capsule, 202 magnetic ball, 203 effervescent disintegration layer, 204 high water absorption fiber, 205 glass bead.
Detailed Description
The drawings in the embodiments of the invention will be combined; the technical scheme in the embodiment of the invention is clearly and completely described; obviously; the described embodiments are only some of the embodiments of the invention; but not all embodiments, are based on the embodiments of the invention; all other embodiments obtained by a person skilled in the art without making any inventive step; all fall within the scope of protection of the present invention.
In the description of the present invention, it should be noted that the terms "upper", "lower", "inner", "outer", "top/bottom", and the like indicate orientations or positional relationships based on those shown in the drawings, and are only for convenience of description and simplification of description, but do not indicate or imply that the referred device or element must have a specific orientation, be constructed in a specific orientation, and be operated, and thus should not be construed as limiting the present invention. Furthermore, the terms "first" and "second" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.
In the description of the present invention, it should be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "disposed," "sleeved/connected," "connected," and the like are to be construed broadly, e.g., "connected," which may be fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art.
Example 1:
referring to fig. 1, the high-temperature resistant easily dispersible emulsifier comprises the following components in parts by mass: 15-20 parts of oil phase, 20-30 parts of water phase, 10-15 parts of oil phase fiber cluster, 2-5 parts of modified polyether amine, 30-45 parts of epoxy resin, 10-15 parts of modified polypropylene resin, 7-10 parts of polysorbate, 5-10 parts of sodium alginate and 5-8 parts of high-temperature resistant material, wherein the preparation method comprises the following steps:
s1, placing the oil phase, the modified polyether amine, the epoxy resin and the polysorbate in a stirring kettle, stirring for 1-1.5h at the high temperature of 100-120 ℃, cooling to 50-70 ℃, adding the oil phase fiber cluster, keeping the temperature, and stirring for 0.5-1h to obtain a mixture A;
s2, placing the water phase, the modified polypropylene resin and the sodium alginate in a stirring kettle, and stirring for 0.5-1h at the temperature of 30-50 ℃ to obtain a mixture B;
s3, adding the mixture B into the mixture A, slowly raising the temperature to 80-100 ℃, finally adding the high-temperature resistant material, stirring for 1-1.2h, and carrying out high-temperature hot melting diffusion on the high-temperature resistant material to obtain the high-temperature resistant easily-dispersible emulsifier.
Wherein the oil phase is prepared by mixing glycerol and vegetable oil, the vegetable oil is stearic acid and oleic acid, the mass ratio of the glycerol to the vegetable oil is 2:1, and the water phase is pure water.
Referring to fig. 2-3, the oil phase fiber bundle adopts a fiber mesh bag 1 formed by combining aluminum silicate fibers, glass fibers and carbon fibers, the mass ratio of the aluminum silicate fibers, the glass fibers and the carbon fibers is 1:2:1, the fiber mesh bag 1 comprises a hollow outer bag shell 101, a plurality of fiber threads 102 are distributed on the peripheral side wall of the hollow outer bag shell 101, the hollow outer bag shell 101 is made of the aluminum silicate fibers, and the plurality of fiber threads 102 are made of the carbon fibers.
The hollow outer capsule shell 101 is filled with a plurality of fiber balls 103, the fiber balls 103 are made of glass fiber, the outer diameter of the fiber balls 103 is far larger than the gap distance between two adjacent fiber wires 102, so that the fiber balls 103 can be always positioned in the hollow structure formed by the hollow outer capsule shell 101 and the plurality of fiber yarns 102, the net-bag structure formed by the hollow outer capsule shell 101 and the fiber yarns 102 is easy to diffuse and foam the emulsion in the stirring process, and the plurality of fiber balls 103 filled in the hollow outer capsule shell 101, the hollow outer capsule shell 101 is shaken in the stirring process along with the emulsion, so as to further enhance the emulsion effect on the emulsion, the outer diameter of the hollow outer capsule shell 101 is 2-5mm, the fiber mesh capsule 1 is set in a certain specification range, under the action of promoting emulsification, the influence of the fiber net bag 1 on industrial use of the emulsifier due to larger particle size is effectively avoided.
Referring to fig. 2 and fig. 4-6, the high temperature resistant material is a hot-melt high temperature resistant granule 2 with a spherical structure, the hot-melt high temperature resistant granule 2 includes a hot-melt capsule 201 located at the outer side, the hollow outer capsule shell 101 is filled with a plurality of glass beads 205, the glass beads 205 have the advantages of light weight, low thermal conductivity, high strength, good chemical stability, and the like, the surface of the hot-melt high temperature resistant granule has oleophilic and hydrophobic properties through special treatment, and is very easy to disperse in an organic material system, after the hot-melt high temperature resistant granule 2 is placed in a stirring kettle, the hot-melt capsule 201 located at the outer side is heated and fused under a certain temperature condition, and the plurality of glass beads 205 inside the hot-melt high temperature resistant granule are released, and the plurality of glass beads 205 are dispersed in an emulsion, which is beneficial to improving the.
It is to be supplemented here that the hollow outer capsule shell 101 is made of a hot-melt resin, the hot-melt temperature of the hot-melt resin is within a range of 75-80 ℃, the magnetic ball 202 is embedded inside the hollow outer capsule shell 101, an air overflow layer is filled between the magnetic ball 202 and the glass bead 205, the air overflow layer comprises an effervescent disintegration layer 203 fixedly coated outside the magnetic ball 202, the peripheral side wall of the hot-melt capsule 201 is connected with a plurality of high water-absorbing fibers 204, the outer ends of the plurality of high water-absorbing fibers 204 sequentially penetrate through the effervescent disintegration layer 203 and the high water-absorbing fibers 204 and extend to the outside of the hot-melt capsule 201, the effervescent disintegration layer 203 which is disintegrated with water and releases air is arranged inside the interlayer formed by the glass bead 205, in S3, when the temperature does not refer to the pyrolysis temperature of the hot-melt capsule 201, the hot-melt capsule 201 is not dissolved, the effervescent disintegration layer 203 is disintegrated by the high water-absorbing fibers 204 to generate air, and when the hot-melt capsule 201, the stored gas is beneficial to pushing the glass beads 205 to overflow outwards, and further enhances the dispersion effect of the plurality of glass beads 205 in the emulsion.
In addition, it should be further noted that all install the agitator in a plurality of stirred tanks, the magnet core is installed to the embedded magnet core that establishes of agitator in S3, set up the magnet core on the agitator, hot melt high temperature resistant granule 2 can move in the emulsion along with the agitator to effectively enlarged a plurality of hot melt high temperature resistant granule 2' S home range, make glass bead 205 can comparatively evenly distribute in the emulsion, and after the inside glass bead 205 complete release of hot melt bag 201, the agitator can also play the magnetic absorption recovery effect to a plurality of magnetic balls 202.
According to the scheme, the modified polyether amine, the epoxy resin, the modified polypropylene resin and the polysorbate are added into the emulsifier formula, so that the hydrophilicity, the stability, the solubility and the viscosity of the emulsifier are enhanced to a certain degree, meanwhile, the high-temperature-resistant material is added into the emulsifier formula, is subjected to high-temperature hot melting diffusion and is uniformly distributed in the emulsifier, so that the thermal stability of the emulsifier is effectively improved, oil-phase fiber bundles are uniformly distributed in the emulsifier, are in a net-like structure and have net-like porous gaps, so that the emulsifier is easy to disperse and form in the emulsification work, a large amount of foam is generated and forms an emulsion, the emulsification effect of the emulsifier in a high-temperature environment is effectively improved, and the application range of the emulsifier is expanded.
The components used in the present invention are all standard components or components known to those skilled in the art, and the structure and principle thereof can be known to those skilled in the art through technical manuals or through routine experiments.
The above; but are merely preferred embodiments of the invention; the scope of the invention is not limited thereto; any person skilled in the art is within the technical scope of the present disclosure; the technical scheme and the improved concept of the invention are equally replaced or changed; are intended to be covered by the scope of the present invention.

Claims (10)

1. A high-temperature-resistant easy-to-disperse emulsifier is characterized in that: the adhesive comprises the following components in parts by mass: 15-20 parts of oil phase, 20-30 parts of water phase, 10-15 parts of oil phase fiber cluster, 2-5 parts of modified polyether amine, 30-45 parts of epoxy resin, 10-15 parts of modified polypropylene resin, 7-10 parts of polysorbate, 5-10 parts of sodium alginate and 5-8 parts of high-temperature resistant material, wherein the preparation method comprises the following steps:
s1, placing the oil phase, the modified polyether amine, the epoxy resin and the polysorbate in a stirring kettle, stirring for 1-1.5h at the high temperature of 100-120 ℃, cooling to 50-70 ℃, adding the oil phase fiber cluster, keeping the temperature, and stirring for 0.5-1h to obtain a mixture A;
s2, placing the water phase, the modified polypropylene resin and the sodium alginate in a stirring kettle, and stirring for 0.5-1h at the temperature of 30-50 ℃ to obtain a mixture B;
s3, adding the mixture B into the mixture A, slowly raising the temperature to 80-100 ℃, finally adding the high-temperature resistant material, stirring for 1-1.2h, and carrying out high-temperature hot melting diffusion on the high-temperature resistant material to obtain the high-temperature resistant easily-dispersible emulsifier.
2. The high temperature resistant easy dispersible emulsifier according to claim 1, characterized in that: the oil phase is formed by mixing glycerol and vegetable oil, the vegetable oil is stearic acid and oleic acid, the mass ratio of the glycerol to the vegetable oil is 2:1, and the water phase is pure water.
3. The high temperature resistant easy dispersible emulsifier according to claim 1, characterized in that: the oil phase fiber bundle adopts a fiber mesh bag (1) formed by combining aluminum silicate fibers, glass fibers and carbon fibers, and the mass ratio of the aluminum silicate fibers to the glass fibers to the carbon fibers is 1:2: 1.
4. The high temperature resistant easy dispersible emulsifier according to claim 3, characterized in that: the fiber mesh bag (1) comprises a hollow outer bag shell (101), a plurality of fiber yarns (102) are distributed on the peripheral side wall of the hollow outer bag shell (101), the hollow outer bag shell (101) is made of aluminum silicate fibers, and the fiber yarns (102) are made of carbon fibers.
5. The high temperature resistant easy dispersible emulsifier according to claim 4, characterized in that: the hollow outer capsule shell (101) is filled with a plurality of fiber balls (103), the fiber balls (103) are made of glass fibers, and the outer diameter of each fiber ball (103) is far larger than the gap distance between every two adjacent fiber wires (102).
6. The high temperature resistant easy dispersible emulsifier according to claim 5, characterized in that: the outer diameter of the hollow outer capsule shell (101) is 2-5 mm.
7. The high temperature resistant easy dispersible emulsifier according to claim 1, characterized in that: the high-temperature resistant material is hot-melt high-temperature resistant granules (2) with a spherical structure, the hot-melt high-temperature resistant granules (2) comprise hot-melt capsules (201) located on the outer side, and a plurality of glass beads (205) are filled in the hollow outer capsule shell (101).
8. The high temperature resistant easy dispersible emulsifier according to claim 7, characterized in that: the hollow capsule shell (101) is made of hot-melt resin, a magnetic ball (202) is embedded in the hollow capsule shell (101), and an air overflow layer is filled between the magnetic ball (202) and the glass beads (205).
9. The high temperature resistant easy dispersible emulsifier according to claim 8, characterized in that: the gas overflow layer comprises an effervescent disintegration layer (203) fixedly wrapped on the outer side of the magnetic ball (202), the side walls of the periphery of the hot melt capsule (201) are connected with a plurality of high water absorption fibers (204), and the outer ends of the high water absorption fibers (204) sequentially penetrate through the effervescent disintegration layer (203) and the high water absorption fibers (204) and extend to the outer side of the hot melt capsule (201).
10. The high temperature resistant easy dispersible emulsifier according to claim 9, characterized by: all install the agitator in a plurality of in the stirred tank, the embedded magnet core that installs of agitator in S3.
CN202011536776.7A 2020-12-23 2020-12-23 High-temperature-resistant easy-to-disperse emulsifier and preparation method thereof Pending CN112675779A (en)

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CN113322120A (en) * 2021-06-29 2021-08-31 江苏品和石油科技有限公司 Production and preparation method of annealing cleaning volatile auxiliary for aluminum alloy strip rolling oil
CN113337901A (en) * 2021-08-06 2021-09-03 杨俊波 Preparation process of tensile polyester fiber industrial yarn
CN113338041A (en) * 2021-06-29 2021-09-03 江苏品和石油科技有限公司 Production and preparation method of novel emulsifier for spinning oil
CN114702851A (en) * 2022-01-28 2022-07-05 上海派拉纶生物技术股份有限公司 High-temperature-resistant promoter

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