CN112540046A - Up-conversion real-time reversible dynamic synchronous testing device for ferroelectric film material - Google Patents
Up-conversion real-time reversible dynamic synchronous testing device for ferroelectric film material Download PDFInfo
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- CN112540046A CN112540046A CN202011364880.2A CN202011364880A CN112540046A CN 112540046 A CN112540046 A CN 112540046A CN 202011364880 A CN202011364880 A CN 202011364880A CN 112540046 A CN112540046 A CN 112540046A
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- ferroelectric
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/01—Arrangements or apparatus for facilitating the optical investigation
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/27—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands using photo-electric detection ; circuits for computing concentration
Abstract
The invention relates to the technical field of testing, in particular to an up-conversion real-time reversible dynamic synchronous testing device for a ferroelectric film material. The device comprises a main frame, a carrier, a light emission source, a light signal acquisition mechanism, a spectrum analyzer, a ferroelectric tester, a main controller and a display. When the ferroelectric tester starts ferroelectric testing, the main controller gives synchronous control signals to the spectrum analyzer, and the main controller starts the spectrum analyzer to collect spectrum signals. Thus, the synchronous dynamic real-time reversible testing effect is achieved.
Description
Technical Field
The invention relates to the technical field of testing, in particular to an up-conversion real-time reversible dynamic synchronous testing device for a ferroelectric film material.
Background
With the gradual exhaustion of fossil fuels and the continuous deterioration of the environment caused by the exhaustion of fossil fuels, researchers pay more attention to the development and application of solar energy. As one of important applications of solar energy, most semiconductor materials used in the solar cell do not respond in the near infrared due to large forbidden band width, which greatly hinders the improvement of the efficiency of the solar cell. To address this problem, researchers at home and abroad have tried to use rare earth ion doped up-conversion optical properties to convert near infrared light into visible light and then to absorb the visible light by semiconductor materials. So far there has been an increasing search around this idea.
The rare earth ions in the up-conversion ferroelectric film material are tightly combined with the semiconductor, so that the up-conversion ferroelectric film material is more efficient even if non-radiative energy transfer is carried out, and the non-radiative energy transfer is possible, thereby being more beneficial to the rare earth ions to transfer the energy to the semiconductor material.
Because the mechanism of regulating the up-conversion luminescence property by the ferroelectric property is not clear, the mechanism of regulating the up-conversion luminescence property by the ferroelectric property is better cleared. A ferroelectric up-conversion synchronization device is urgently needed to research the ferroelectric property, regulate up-conversion luminescence and enhance up-conversion efficiency.
Therefore, the performance research for the up-conversion ferroelectric thin film material is crucial. For the performance of the up-conversion ferroelectric thin film material, a tool capable of performing performance test on it is required.
Disclosure of Invention
The invention aims to provide an up-conversion real-time reversible dynamic synchronous testing device for a ferroelectric material.
The technical scheme adopted by the invention for solving the technical problems is as follows:
an up-conversion real-time reversible dynamic synchronous testing device for ferroelectric materials comprises:
the device comprises a main frame, wherein a carrier for bearing a sample to be detected is arranged on the main frame;
the object carrier is used for providing a carrying station of a sample to be detected;
the light emitting source is arranged in the main frame and positioned below the object carrier and provides a light source for irradiating the sample from bottom to top;
the optical signal acquisition mechanism is positioned above the carrier, corresponds to the carrier and the light emission source in position and is used for acquiring optical signals penetrating through a sample to be detected;
the optical spectrum analyzer is connected with the optical signal acquisition mechanism through an optical channel and is used for carrying out spectral analysis on the acquired optical signal;
the ferroelectric tester is connected with the sample to be tested through a lead and is used for testing the ferroelectric piezoelectric property of the sample to be tested;
the main controller is simultaneously connected with the ferroelectric tester, the spectrum analyzer and the light emission source and controls the ferroelectric tester, the spectrum analyzer and the light emission source;
and the display is connected with the main controller and is used for displaying the test results of the ferroelectric tester and the spectrum analyzer.
Preferably, the optical signal collecting mechanism comprises a collecting frame, an adjusting mechanism is arranged on the collecting frame, and a lighting lens is arranged on the adjusting mechanism.
Preferably, the test device further comprises an electrode auxiliary mechanism, wherein the electrode auxiliary mechanism is provided with an auxiliary arm and a probe arranged on the auxiliary arm, and a lead of the ferroelectric tester is connected with an electrode of the sample to be tested through the probe.
Preferably, the carrier is provided with a transparent conductive slide, the sample to be detected is arranged on the conductive slide, and the conductive slide and the sample to be detected are provided with electrodes.
Preferably, a light adjusting mechanism is disposed between the light emitting source and the object carrier, and the light adjusting mechanism includes an adjusting mechanism and an adjusting lens disposed on the adjusting mechanism.
The invention has the beneficial effects that: the device has simple structure, and can dynamically and reversibly detect the regulation and control of the ferroelectric effect on the up-conversion luminescence property and dynamically regulate and control the conversion efficiency of the ferroelectric film in real time.
Drawings
Fig. 1 shows the overall structure of the invention.
Fig. 2 shows a partial structural schematic diagram of the present invention.
Fig. 3 is a schematic diagram showing the structure of the conductive slide carrying sample according to the present invention.
In the figure: the device comprises a main frame 1, a carrier 2, a light emission source 3, a light signal acquisition mechanism 4, a spectrum analyzer 5, a ferroelectric tester 6, a main controller 7, a display 8, an acquisition frame 9, an adjusting mechanism 10, a lighting lens 11, an electrode auxiliary mechanism 12, an auxiliary arm 13, a probe 14, a conductive slide glass 15, an electrode 16, a dimming mechanism 17, an adjusting lens 18 and a microscope mechanism 19.
Detailed Description
Further refinements will now be made on the basis of the representative embodiment shown in the figures. It should be understood that the following description is not intended to limit the embodiments to one preferred embodiment. On the contrary, it is intended to cover alternatives, modifications, and equivalents as may be included within the spirit and scope of the embodiments as defined by the appended claims. Although these embodiments are described in sufficient detail to enable those skilled in the art to practice the embodiments, it is to be understood that these examples are not limiting, such that other examples may be used and that corresponding modifications may be made without departing from the spirit and scope of the embodiments.
Specifically, referring to fig. 1, fig. 2 and fig. 3, fig. 1-fig. 2 show an apparatus for testing the upconversion real-time reversible dynamic synchronization of ferroelectric materials, which includes a main frame, a carrier, a light emitting source, an optical signal collecting mechanism, a spectrum analyzer, a ferroelectric tester, a main controller and a display.
Specifically, the structure and the interrelation of each part are as follows:
the main frame is provided with a carrier for bearing a sample to be detected.
The object carrying frame provides an object carrying station for a sample to be measured, a transparent conductive slide is arranged on the object carrying station of the object carrying frame, as shown in fig. 3, the sample to be measured is arranged on the conductive slide in a thin film manner, and electrodes are arranged on the conductive slide and the sample to be measured.
And the light emitting source is arranged in the main frame and positioned below the object carrier and provides a light source for irradiating the sample from bottom to top.
The optical signal acquisition mechanism is positioned above the carrier, corresponds to the carrier and the light emission source in position and is used for acquiring optical signals penetrating through a sample to be detected; the optical signal acquisition mechanism comprises an acquisition frame, an adjusting mechanism is arranged on the acquisition frame, and a lighting lens is arranged on the adjusting mechanism.
The spectrum analyzer is connected with the optical signal acquisition mechanism through an optical channel and is used for performing spectrum analysis on the acquired optical signal.
The ferroelectric tester is connected with the sample to be tested through a lead and is used for testing the ferroelectric piezoelectric property of the sample to be tested; and an electrode auxiliary mechanism is also arranged in a matching way, the electrode auxiliary mechanism is provided with an auxiliary arm and a probe arranged on the auxiliary arm, and a lead of the ferroelectric tester is connected with an electrode of a sample to be tested through the probe. Meanwhile, a microscope mechanism is arranged at the position of the sample to be detected and used for observing the electrode matching condition of the probe on the sample.
The main controller is simultaneously connected with the ferroelectric tester, the spectrum analyzer and the light emission source and controls the ferroelectric tester, the spectrum analyzer and the light emission source; the main controller is used for controlling the synchronization of the ferroelectric tester and the spectrum analyzer, and the performance test of the ferroelectric film material of the sample to be tested is carried out by controlling the synchronization of the ferroelectric tester and the spectrum analyzer.
And the display is connected with the main controller and is used for displaying the test results of the ferroelectric tester and the spectrum analyzer.
A light adjusting mechanism is arranged between the light emitting source and the object carrier and comprises an adjusting mechanism and an adjusting lens arranged on the adjusting mechanism.
Firstly, preparing an up-conversion ferroelectric film on a light-transmitting conductive slide, and then preparing corresponding electrodes on the film and the conductive slide; the electrodes were connected by a ferroelectric tester. Meanwhile, the optical signal acquisition mechanism is matched and corresponds to the sample to be measured on the carrier and is connected with the spectrometer.
The spectrometer is a CCD spectrum tester, and the spectrum information of the spectrometer can be dynamically displayed in real time. The ferroelectric test is a reversible process, so that the relationship between the ferroelectric effect and the up-conversion luminescence performance can be dynamically and reversibly tested in real time.
In order to achieve the effect of synchronous dynamic reversible real-time test. The master controller is used for carrying out coordinated control on the spectrum analyzer and the ferroelectric tester. Therefore, the aim of coordinating the test and dynamically testing the reversibility in real time is achieved.
Specifically, when the ferroelectric tester starts the ferroelectric test, the master controller gives synchronous control signals to the spectrum analyzer, and the master controller starts the spectrum analyzer to collect spectrum signals. Thus, the synchronous dynamic real-time reversible testing effect is achieved.
For purposes of explanation, specific nomenclature is used in the above description to provide a thorough understanding of the described embodiments. It will be apparent to those skilled in the art that certain modifications, combinations, and variations can be made in light of the above teachings.
Claims (5)
1. The utility model provides a ferroelectric material's real-time reversible dynamic synchronization testing arrangement of up-conversion which characterized in that: the method comprises the following steps:
the device comprises a main frame, wherein a carrier for bearing a sample to be detected is arranged on the main frame;
the object carrier is used for providing a carrying station of a sample to be detected;
the light emitting source is arranged in the main frame and positioned below the object carrier and provides a light source for irradiating the sample from bottom to top;
the optical signal acquisition mechanism is positioned above the carrier, corresponds to the carrier and the light emission source in position and is used for acquiring optical signals penetrating through a sample to be detected;
the optical spectrum analyzer is connected with the optical signal acquisition mechanism through an optical channel and is used for carrying out spectral analysis on the acquired optical signal;
the ferroelectric tester is connected with the sample to be tested through a lead and is used for testing the ferroelectric piezoelectric property of the sample to be tested;
the main controller is simultaneously connected with the ferroelectric tester, the spectrum analyzer and the light emission source and controls the ferroelectric tester, the spectrum analyzer and the light emission source;
and the display is connected with the main controller and is used for displaying the test results of the ferroelectric tester and the spectrum analyzer.
2. The device for testing the up-conversion real-time reversible dynamic synchronization of ferroelectric thin film material according to claim 1, wherein: the optical signal acquisition mechanism comprises an acquisition frame, an adjusting mechanism is arranged on the acquisition frame, and a lighting lens is arranged on the adjusting mechanism.
3. The device for testing the up-conversion real-time reversible dynamic synchronization of ferroelectric thin film material according to claim 2, wherein: the ferroelectric tester also comprises an electrode auxiliary mechanism, wherein the electrode auxiliary mechanism is provided with an auxiliary arm and a probe arranged on the auxiliary arm, and a lead of the ferroelectric tester is connected with an electrode of a sample to be tested through the probe.
4. The device for testing the up-conversion real-time reversible dynamic synchronization of ferroelectric thin film material according to claim 2, wherein: the object carrier is provided with a transparent conductive slide, the sample to be detected is arranged on the conductive slide, and the conductive slide and the sample to be detected are provided with electrodes.
5. The device for testing the up-conversion real-time reversible dynamic synchronization of ferroelectric thin film material according to claim 2, wherein: a light adjusting mechanism is arranged between the light emitting source and the object carrier and comprises an adjusting mechanism and an adjusting lens arranged on the adjusting mechanism.
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CN109950403A (en) * | 2019-03-29 | 2019-06-28 | 中国科学院上海技术物理研究所 | A kind of the two-dimensional material PN junction photodetector and preparation method of the regulation of ferroelectricity field |
CN111089851A (en) * | 2019-12-31 | 2020-05-01 | 洛阳师范学院 | Magneto-optical testing device |
CN111458315A (en) * | 2020-04-21 | 2020-07-28 | 中国科学院福建物质结构研究所 | Spectral detection device and method for ferroelectric crystal structure |
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2020
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Patent Citations (10)
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JP2003297828A (en) * | 2002-04-01 | 2003-10-17 | Seiko Epson Corp | Method and apparatus for forming ferroelectric film |
US20080019648A1 (en) * | 2005-08-01 | 2008-01-24 | California Institute Of Technology | Ferroelectric nanophotonic materials and devices |
CN102735628A (en) * | 2012-06-21 | 2012-10-17 | 南京邮电大学 | Real-time dynamic absorption spectrum test method |
CN204556740U (en) * | 2014-12-30 | 2015-08-12 | 同济大学 | A kind of Electrical Characteristics and breakdown characteristics real-time testing system |
CN105895718A (en) * | 2016-06-22 | 2016-08-24 | 内蒙古大学 | Ferroelectric thin film photovoltaic effect regulation method, ferroelectric thin film and solar photovoltaic cell |
CN206638407U (en) * | 2017-04-14 | 2017-11-14 | 广州标旗电子科技有限公司 | A kind of distributed spectroanalysis instrument |
CN109884346A (en) * | 2019-03-10 | 2019-06-14 | 复旦大学 | A kind of ferroelectric film is macro/microstructure and electric property combined test system |
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