CN112494343A - Preparation method of deep nourishing facial mask - Google Patents
Preparation method of deep nourishing facial mask Download PDFInfo
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- CN112494343A CN112494343A CN202011586782.3A CN202011586782A CN112494343A CN 112494343 A CN112494343 A CN 112494343A CN 202011586782 A CN202011586782 A CN 202011586782A CN 112494343 A CN112494343 A CN 112494343A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
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- A61K8/9794—Liliopsida [monocotyledons]
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/81—Preparation or application process involves irradiation
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Abstract
The invention relates to a preparation method of a deep nourishing facial mask, and belongs to the technical field of cosmetics. The moisture-keeping component is prepared by extracting aloe leaves, and simultaneously, in the technical scheme of the invention, the aloe leaves are extracted and compounded to be incapable of effectively acting on the inside of the skin, the invention adopts an effective microemulsion gel complex system as a carrier to permeate the skin structure, and lipid substances existing in the microemulsion material permeate into the horny layer of the skin and even into the dermis layer, so that the structure of the horny layer is favorably changed, the liquidity of a lipid bilayer is enhanced, and components such as phospholipid, alcohol and the like in the microemulsion gel material can more easily permeate into the horny layer, thereby enhancing the liquidity of the lipid layer in the horny layer, improving the diffusion coefficient of small molecules in the skin, effectively permeating and keeping the moisture of the skin in the using process through the adsorption and loading of the mask gel, and effectively improving the moisture-keeping performance of the mask.
Description
Technical Field
The invention relates to a preparation method of a deep nourishing facial mask, and belongs to the technical field of cosmetics.
Background
The facial mask can be divided into a base cloth facial mask and a base cloth-free facial mask according to the material. The mask without the base cloth has various types, and can be specifically divided into the following types: blending a paste facial mask, a tear-off facial mask, a cream facial mask, a fresh fruit self-made facial mask and a base cloth facial mask.
At present, more than 80 percent of the base cloth facial masks in the market are base cloth facial masks, and the facial masks take the base cloth as a carrier and achieve different beauty and skin care effects by changing carried nutrient solutions with different effects. The facial mask has the advantages of convenient use, rapid onset of drug action, and convenient application and removal. The base cloth mask has high-concentration essence, is uniformly distributed, has extremely small particles, and can quickly enter the skin through the skin, so that the nourishment of the mask is greatly improved.
Most base cloth masks use non-woven fabrics as base cloth, because it has the characteristics of comfort, softness, good water retention, good air permeability, good fit with the face, wide source and low cost. Nonwoven fabrics are of a wide variety of types and can be classified into spunlaced nonwoven fabrics, needle-punched nonwoven fabrics, and the like. Among them, due to the softness, good mechanical properties, good hydrophilicity, high porosity and the ability to carry a large amount of essence of the spunlace nonwoven fabric, the existing face film substrate is not stable enough in moisture retention of human skin due to the limitation of materials in the actual use process, and is easy to be applied more dry, so it is necessary to modify the face film substrate effectively.
Disclosure of Invention
The invention aims to provide a preparation method of a deep nourishing facial mask, which aims to solve one of the problems in the prior art.
In order to achieve the purpose, the invention provides the following technical scheme:
s1, drying rapeseed meal, grinding and sieving, collecting sieved particles, stirring and mixing the particles with deionized water, collecting mixed liquid, carrying out oil bath treatment, standing, cooling to room temperature, adding mixed modified liquid, collecting modified liquid, dropwise adding glycerol into the modified liquid according to the mass ratio of 1:10, homogenizing, collecting homogenized liquid, drying, filtering and collecting filtrate;
s2, taking a non-woven fabric mask base material, soaking the non-woven fabric mask base material into the filtrate, standing, drying and collecting a dry modified mask base material;
s3, taking collagen, mixing collagen particles with deionized water according to the mass ratio of 1:10, stirring, dialyzing and rotationally evaporating to obtain modified rotary evaporation liquid;
s4, weighing deionized water, the modified rotary-steaming liquid and phospholipid respectively, placing the weighed materials in a stirrer, stirring and mixing the materials, placing the materials in a homogenizing device, homogenizing and collecting the composite liquid; peeling aloe leaves, mixing, crushing, extracting with water, concentrating and collecting concentrated solution;
s5, respectively weighing dodecyl glucoside, the compound solution, the coconut oil acid and the concentrated solution, stirring, mixing and homogenizing to obtain a transdermal modified solution, soaking the dried modified mask base material into the breathable modified solution, soaking and performing ultraviolet sterilization to obtain the deep nourishing type mask material.
The drying treatment in the step S1 is drying for 1-2 hours at 30-35 ℃ under 50-100 kPa.
The oil bath treatment in the step S1 is a heat preservation reaction at 120-130 ℃ for 250-300S.
The drying treatment in the step S2 is drying until the water content is 25-30%.
The rotary evaporation in the step S3 is rotary evaporation treatment at 30-45 ℃, and the rotary evaporation is carried out until reaching 1/3 of the original volume of the dialysate.
The homogenizing treatment in the step S4 is carried out for 45-60 min under 10-15 MPa.
The mixing proportion of the deionized water, the modified rotary evaporation liquid and the phospholipid in the step S4 is that 55-60 parts of deionized water, 10-15 parts of modified rotary evaporation liquid and 6-8 parts of phospholipid are respectively weighed according to parts by weight.
The mixing proportion of the dodecyl glucoside, the compound liquid, the coconut oleic acid and the concentrated solution in the step S5 is as follows: respectively weighing 35-40 parts by weight of dodecyl glucoside, 80-100 parts by weight of composite liquid, 15-20 parts by weight of coconut oil acid and 25-30 parts by weight of concentrated solution.
Compared with the prior art, the invention has the beneficial effects that:
(1) the technical scheme of the invention takes the rapeseed dregs as raw materials for preparation, and because a large amount of dietary fibers contained in the rapeseed dregs generate terminal brooming in the homogenizing process to form a large amount of free hydrophilic groups such as hydroxyl, and the groups interact with other substances through acting forces such as hydrogen bonds and the like to play a role in constructing a framework, the gel material has a compact network structure;
(2) the technical scheme of the invention adopts aloe leaves to extract and prepare moisture-keeping components, and simultaneously, in the technical scheme of the invention, the aloe leaves are extracted and compounded to be incapable of effectively acting on the interior of the skin, the invention adopts an effective microemulsion gel complex system as a carrier to permeate a skin structure, and lipid substances existing in a microemulsion material permeate into the horny layer of the skin and even into the dermis layer to be beneficial to changing the structure of the horny layer and enhancing the fluidity of a lipid bilayer and promote the anti-wrinkle material to permeate into the skin, meanwhile, the microemulsion material structure permeates out, and has more gully structures on the surface of the skin, the particle size of the microemulsion material is smaller, so that the microemulsion material is more closely contacted with the surface of the skin, and therefore, components such as phospholipid, alcohol and the like in the microemulsion gel material can more easily permeate into the horny layer to enhance the fluidity of the lipid in the, the diffusion coefficient of the small molecules in the skin is improved, and the mask gel effectively permeates and keeps the skin moisture in the using process through the adsorption and loading of the mask gel, so that the moisture retention performance of the mask material is effectively improved.
Drawings
The above and/or additional aspects and advantages of the present invention will become apparent and readily appreciated from the following description of the embodiments, taken in conjunction with the accompanying drawings of which:
fig. 1 is a flowchart illustrating a method for preparing a deep nourishing mask according to an embodiment of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Taking rapeseed dregs, naturally drying, grinding, sieving with a 200-mesh sieve, collecting sieved particles, stirring and mixing with deionized water, collecting a mixed solution, placing the mixed solution at 120-130 ℃ for heat preservation reaction for 250-300 s, standing, cooling to room temperature, adding a mixed modification solution, stirring, mixing, standing for 10-15 min, collecting the modification solution, dropwise adding glycerol into the modification solution according to the mass ratio of 1:10, homogenizing at 2000-3000 r/min for 10-15 min, collecting the homogenized solution, placing the homogenized solution in a vacuum drying oven, drying at 30-35 ℃ and 50-100 kPa for 1-2 h, filtering after drying, collecting a filtrate, taking a non-woven fabric mask base material, soaking the non-woven fabric mask base material into the filtrate, standing for 6-8 h, drying until the water content is 25-30%, and collecting a dried modified mask base material; mixing collagen particles with deionized water according to a mass ratio of 1:10, stirring and mixing the collagen particles and the deionized water, keeping the temperature and stirring for 25-30 min at room temperature, collecting mixed modified liquid, placing the mixed modified liquid in a dialysis bag for dialysis treatment, collecting dialysate, placing the dialysate at 30-45 ℃ for rotary evaporation treatment, and performing rotary evaporation until the volume of the dialysate is 1/3 of the original volume to obtain modified rotary evaporation liquid; respectively weighing 55-60 parts by weight of deionized water, 10-15 parts by weight of modified rotary evaporation liquid and 6-8 parts by weight of phospholipid, placing the materials into a stirrer, stirring and mixing the materials, placing the materials into a homogenizing device, homogenizing the materials under the pressure of 10-15 MPa for 45-60 min, and collecting the composite liquid; peeling aloe leaves, mixing, crushing, extracting with water, concentrating and collecting concentrated solution; respectively weighing 35-40 parts by weight of dodecyl glucoside, 80-100 parts by weight of composite liquid, 15-20 parts by weight of coconut oil acid and 25-30 parts by weight of concentrated solution, stirring, mixing and homogenizing to prepare transdermal modified liquid; and soaking the dried modified mask base material into the breathable modified solution according to the mass ratio of 1:10, and performing soaking treatment and ultraviolet sterilization to obtain the deep nourishing mask material.
Example 1
Taking rapeseed dregs, naturally drying, grinding, sieving with a 200-mesh sieve, collecting sieved particles, stirring and mixing with deionized water, collecting a mixed solution, placing the mixed solution at 120 ℃ for heat preservation reaction for 250s, standing, cooling to room temperature, adding a mixed modified solution, stirring, mixing, standing for 10min, collecting the modified solution, dropwise adding glycerol into the modified solution according to the mass ratio of 1:10, homogenizing at 2000r/min for 10min, collecting the homogenized solution, placing the homogenized solution in a vacuum drying box, drying at 30 ℃ and 50kPa for 1h, filtering after drying is finished, collecting filtrate, taking a non-woven fabric mask base material, soaking the non-woven fabric mask base material into the filtrate, standing for 6h, drying until the water content is 25%, and collecting a dried modified mask base material; mixing collagen particles with deionized water according to a mass ratio of 1:10, stirring and mixing the collagen particles and the deionized water, keeping the temperature and stirring for 25min at room temperature, collecting mixed modified liquid, placing the mixed modified liquid in a dialysis bag for dialysis treatment, collecting dialysate, placing the dialysate at 30 ℃ for rotary evaporation treatment, and performing rotary evaporation until the volume of the dialysate is 1/3 of the original volume to obtain modified rotary evaporation liquid; respectively weighing 55 parts by weight of deionized water, 10 parts by weight of modified rotary evaporation liquid and 6 parts by weight of phospholipid, placing the materials in a stirrer, stirring, mixing, placing in a homogenizing device, homogenizing under 10MPa for 45min, and collecting to obtain a composite liquid; peeling aloe leaves, mixing, crushing, extracting with water, concentrating and collecting concentrated solution; respectively weighing 35 parts of dodecyl glucoside, 80 parts of composite liquid, 15 parts of coconut oil acid and 25 parts of concentrated solution according to parts by weight, stirring, mixing and homogenizing to prepare transdermal modified liquid; and soaking the dried modified mask base material into the breathable modified solution according to the mass ratio of 1:10, and performing soaking treatment and ultraviolet sterilization to obtain the deep nourishing mask material.
Example 2
Taking rapeseed dregs, naturally drying, grinding, sieving with a 200-mesh sieve, collecting sieved particles, stirring and mixing with deionized water, collecting a mixed solution, placing the mixed solution at 125 ℃ for heat preservation reaction 275s, standing, cooling to room temperature, adding a mixed modified solution, stirring, mixing, standing for 12min, collecting the modified solution, dropwise adding glycerol into the modified solution according to the mass ratio of 1:10, homogenizing at 2750r/min for 12min, collecting the homogenized solution, placing the homogenized solution in a vacuum drying box, drying at 32 ℃ and 80kPa for 1h, filtering after drying is finished, collecting filtrate, taking a non-woven fabric mask base material, soaking the non-woven fabric mask base material into the filtrate, standing for 7h, drying until the water content is 27%, and collecting a dried modified mask base material; mixing collagen particles with deionized water according to a mass ratio of 1:10, stirring and mixing the collagen particles and the deionized water, keeping the temperature and stirring for 27min at room temperature, collecting mixed modified liquid, placing the mixed modified liquid in a dialysis bag for dialysis treatment, collecting dialysate, placing the dialysate at 37 ℃ for rotary evaporation treatment, and performing rotary evaporation to 1/3 of the original volume of the dialysate to obtain modified rotary evaporation liquid; respectively weighing 57 parts by weight of deionized water, 12 parts by weight of modified rotary evaporation liquid and 7 parts by weight of phospholipid, placing the materials in a stirrer, stirring, mixing, placing in a homogenizing device, homogenizing under 12MPa for 47min, and collecting to obtain a composite liquid; peeling aloe leaves, mixing, crushing, extracting with water, concentrating and collecting concentrated solution; respectively weighing 37 parts of dodecyl glucoside, 90 parts of composite liquid, 17 parts of coconut oil acid and 27 parts of concentrated solution according to parts by weight, stirring, mixing and homogenizing to prepare transdermal modified liquid; and soaking the dried modified mask base material into the breathable modified solution according to the mass ratio of 1:10, and performing soaking treatment and ultraviolet sterilization to obtain the deep nourishing mask material.
Example 3
Taking rapeseed dregs, naturally drying, grinding, sieving with a 200-mesh sieve, collecting sieved particles, stirring and mixing with deionized water, collecting a mixed solution, placing the mixed solution at 130 ℃ for heat preservation reaction for 300s, standing, cooling to room temperature, adding a mixed modified solution, stirring, mixing, standing for 15min, collecting the modified solution, dropwise adding glycerol into the modified solution according to the mass ratio of 1:10, homogenizing at 3000r/min for 15min, collecting the homogenized solution, placing the homogenized solution in a vacuum drying box, drying at 35 ℃ and 100kPa for 2h, filtering after drying is finished, collecting filtrate, taking a non-woven fabric mask base material, soaking the non-woven fabric mask base material into the filtrate, standing for 8h, drying until the water content is 30%, and collecting a dried modified mask base material; mixing collagen particles with deionized water according to a mass ratio of 1:10, stirring and mixing the collagen particles and the deionized water, keeping the temperature and stirring for 30min at room temperature, collecting mixed modified liquid, placing the mixed modified liquid in a dialysis bag for dialysis treatment, collecting dialysate, placing the dialysate in a rotary evaporation treatment at 45 ℃, and performing rotary evaporation to 1/3 of the original volume of the dialysate to obtain modified rotary evaporation liquid; respectively weighing 60 parts by weight of deionized water, 15 parts by weight of modified rotary evaporation liquid and 8 parts by weight of phospholipid, placing the deionized water, the modified rotary evaporation liquid and the phospholipid into a stirrer, stirring, mixing, placing the mixture into a homogenizing device, homogenizing under 15MPa for 60min, and collecting the composite liquid; peeling aloe leaves, mixing, crushing, extracting with water, concentrating and collecting concentrated solution; respectively weighing 40 parts of dodecyl glucoside, 100 parts of composite liquid, 20 parts of coconut oil acid and 30 parts of concentrated solution according to parts by weight, stirring, mixing and homogenizing to prepare transdermal modified liquid; and soaking the dried modified mask base material into the breathable modified solution according to the mass ratio of 1:10, and performing soaking treatment and ultraviolet sterilization to obtain the deep nourishing mask material.
Example 4
Mixing collagen particles with deionized water according to a mass ratio of 1:10, stirring and mixing the collagen particles and the deionized water, keeping the temperature and stirring for 27min at room temperature, collecting mixed modified liquid, placing the mixed modified liquid in a dialysis bag for dialysis treatment, collecting dialysate, placing the dialysate at 37 ℃ for rotary evaporation treatment, and performing rotary evaporation to 1/3 of the original volume of the dialysate to obtain modified rotary evaporation liquid; respectively weighing 57 parts by weight of deionized water, 12 parts by weight of modified rotary evaporation liquid and 7 parts by weight of phospholipid, placing the materials in a stirrer, stirring, mixing, placing in a homogenizing device, homogenizing under 12MPa for 47min, and collecting to obtain a composite liquid; peeling aloe leaves, mixing, crushing, extracting with water, concentrating and collecting concentrated solution; respectively weighing 37 parts of dodecyl glucoside, 90 parts of composite liquid, 17 parts of coconut oil acid and 27 parts of concentrated solution according to parts by weight, stirring, mixing and homogenizing to prepare transdermal modified liquid; and (3) soaking the non-woven fabric mask into the breathable modified liquid according to the mass ratio of 1:10, and performing soaking treatment and ultraviolet sterilization to obtain the control mask material.
The performance tests were performed on example 1, example 2, example 3 and example 4, wherein example 4 is a control mask material prepared from a mask paper using a non-woven fabric as a substrate.
The experimental steps are as follows:
8 volunteers were tested and their moisturizing effect was measured at room temperature every 2h using a facial mask and by a skin hydration meter.
The elastic modulus of the left and right cheeks of the volunteer was measured in advance, and then the cosmetics prepared according to the present invention and the control group were used on the right face to measure the plasticity and elasticity, and then the average value was calculated. For the measurement, the volunteers were arranged in a room at a temperature of 23 ℃ and a humidity of 50% for 15 minutes in order to maintain the skin state stably.
Specific test results are shown in table 1.
TABLE 1 comparison of Properties
(1) Comparing the examples 1, 2, 3 and 4, the water retention performance of the example 4 is significantly reduced, because the mask paper material prepared by performing composite modification on rapeseed meal gel is adopted in the technical scheme of the invention, because the effective microemulsion gel complex system is adopted as the carrier to permeate the skin structure, the lipid substance existing in the microemulsion material permeates into the stratum corneum of the skin and even into the dermis, the structure of the stratum corneum is favorably changed, the fluidity of the lipid bilayer is enhanced, and the anti-wrinkle material is promoted to permeate into the skin, meanwhile, the microemulsion material structure permeates out, the skin surface has more 'gully' structures, the smaller the particle size of the microemulsion material is, the closer the contact with the skin surface is, so that the components such as phospholipid, alcohol and the like in the microemulsion gel material can permeate into the stratum corneum more easily, therefore, the fluidity of lipid layers in the stratum corneum is enhanced, the diffusion coefficient of small molecules in the skin is improved, and the mask gel effectively permeates and keeps skin moisture in the using process through the adsorption and loading of the mask gel, so that the water retention performance of the mask material is effectively improved.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Claims (8)
1. A preparation method of a deep nourishing facial mask is characterized by comprising the following specific preparation steps:
s1, drying rapeseed meal, grinding and sieving, collecting sieved particles, stirring and mixing the particles with deionized water, collecting mixed liquid, carrying out oil bath treatment, standing, cooling to room temperature, adding mixed modified liquid, collecting modified liquid, dropwise adding glycerol into the modified liquid according to the mass ratio of 1:10, homogenizing, collecting homogenized liquid, drying, filtering and collecting filtrate;
s2, taking a non-woven fabric mask base material, soaking the non-woven fabric mask base material into the filtrate, standing, drying and collecting a dry modified mask base material;
s3, taking collagen, mixing collagen particles with deionized water according to the mass ratio of 1:10, stirring, dialyzing and rotationally evaporating to obtain modified rotary evaporation liquid;
s4, weighing deionized water, the modified rotary-steaming liquid and phospholipid respectively, placing the weighed materials in a stirrer, stirring and mixing the materials, placing the materials in a homogenizing device, homogenizing and collecting the composite liquid; peeling aloe leaves, mixing, crushing, extracting with water, concentrating and collecting concentrated solution;
s5, respectively weighing dodecyl glucoside, the compound solution, the coconut oil acid and the concentrated solution, stirring, mixing and homogenizing to obtain a transdermal modified solution, soaking the dried modified mask base material into the breathable modified solution, soaking and performing ultraviolet sterilization to obtain the deep nourishing type mask material.
2. The method of claim 1, wherein the drying step S1 is carried out at 30-35 deg.C under 50-100 kPa for 1-2 h.
3. The method for preparing a deep nourishing facial mask as claimed in claim 1, wherein the oil bath treatment of step S1 is a 120-130 ℃ heat preservation reaction for 250-300S.
4. The method for preparing a deep nourishing facial mask as claimed in claim 1, wherein the drying process of step S2 is drying to a moisture content of 25-30%.
5. The method of claim 1, wherein the rotary evaporation in step S3 is performed at 30-45 deg.C until reaching 1/3 of the original volume of dialysate.
6. The method of claim 1, wherein the homogenizing treatment in step S4 is performed under 10-15 MPa for 45-60 min.
7. The method for preparing a deep nourishing facial mask according to claim 1, wherein the deionized water, the modified rotary evaporation liquid and the phospholipid are mixed in the proportion of 55-60 parts by weight, 10-15 parts by weight and 6-8 parts by weight respectively according to the step S4.
8. The method for preparing a deep nourishing facial mask as claimed in claim 1, wherein the mixing ratio of the dodecyl glycoside, the complex liquid, the coconut oil acid and the concentrated solution in step S5 is: respectively weighing 35-40 parts by weight of dodecyl glucoside, 80-100 parts by weight of composite liquid, 15-20 parts by weight of coconut oil acid and 25-30 parts by weight of concentrated solution.
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Cited By (1)
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| CN113648229A (en) * | 2021-09-02 | 2021-11-16 | 苏州优薇孚智能科技有限公司 | Double-layer moisturizing type crystalline mask and using method thereof |
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