CN112451396A - Refreshing water-in-oil type cream without silicone oil - Google Patents
Refreshing water-in-oil type cream without silicone oil Download PDFInfo
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- CN112451396A CN112451396A CN202011631204.7A CN202011631204A CN112451396A CN 112451396 A CN112451396 A CN 112451396A CN 202011631204 A CN202011631204 A CN 202011631204A CN 112451396 A CN112451396 A CN 112451396A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
- A61K8/064—Water-in-oil emulsions, e.g. Water-in-silicone emulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/39—Derivatives containing from 2 to 10 oxyalkylene groups
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/34—Free of silicones
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Abstract
The invention discloses refreshing water-in-oil type cream without silicone oil, which consists of the following components in percentage by mass: 0.5-3% of PEG-30 dipolyhydroxystearate, 0.5-3% of polyglycerol-3 diisostearate, 15-30% of isononyl isononanoate, 0.02-0.1% of disodium EDTA, 0.5-2% of sodium chloride, 0.3-0.5% of p-hydroxyacetophenone, 0.05-0.1% of ethylhexyl glycerol, 0.3-1% of 1, 2-hexanediol, 2-10% of glycerol, 2-10% of butanediol, 0.5-5% of PEG/PPG/polytetramethylene glycol-8/5/3 glycerol and the balance of water. The product prepared according to the formula of the invention has light skin feel, is not greasy and has stable performance.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to refreshing water-in-oil type cream without silicone oil.
Background
The cream is a commonly used skin care product to keep the skin from being dry, but in the using process, the water-in-oil cream has a lasting moisturizing and moisture-keeping feeling compared with the oil-in-water cream, but the cream with thick, sticky and greasy skin feeling is rejected by consumers, so that most of the existing water-in-oil skin care products use silicone oil to achieve the aim of refreshing skin feeling, the silicon pollutes the environment greatly, and the consumers have a conflict psychology on products containing silicon components.
Disclosure of Invention
Aiming at the problems in the prior art, the invention relates to a refreshing water-in-oil type cream without silicone oil.
The invention is realized by the following technical scheme:
the refreshing water-in-oil type cream without silicone oil is characterized by comprising the following components in percentage by mass: PEG-30 dipolyhydroxystearate 0.5-3%, polyglycerol-3 diisostearate 0.5-3%, isononyl isononanoate 15-30%; the phase B consists of the following components: 0.02-0.1% of EDTA disodium, 0.5-2% of sodium chloride, 0.3-0.5% of p-hydroxyacetophenone, 0.05-0.1% of ethylhexyl glycerol, 0.3-1% of 1, 2-hexanediol, 2-10% of glycerol, 2-10% of butanediol, 0.5-5% of PEG/PPG/polytetramethylene glycol-8/5/3 glycerol and the balance of water.
The refreshing water-in-oil type cream without silicone oil is characterized by comprising the following components in percentage by mass: 1-2% of PEG-30 dipolyhydroxystearate, 1-3% of polyglycerol-3 diisostearate, 18-25% of isononyl isononanoate, 0.05-0.1% of disodium EDTA (ethylene diamine tetraacetic acid), 1-2% of sodium chloride, 3-5% of p-hydroxyacetophenone, 0.05-0.07% of ethylhexyl glycerol, 0.3-0.7% of 1, 2-hexanediol, 3-5% of glycerol, 3-5% of butanediol, 1-3% of PEG/PPG/polytetramethylene glycol-8/5/3 glycerol and the balance of water.
The refreshing water-in-oil type cream without silicone oil is characterized by comprising the following components in percentage by mass: 1% of PEG-30 dipolyhydroxystearate, 2% of polyglycerol-3 diisostearate, 22% of isononyl isononanoate, 0.05% of disodium EDTA, 1.5% of sodium chloride, 0.35% of p-hydroxyacetophenone, 0.05% of ethylhexyl glycerol, 0.5% of 1, 2-hexanediol, 4% of glycerol, 4% of butanediol, 2% of PEG/PPG/polytetramethylene glycol-8/5/3 glycerol and the balance of water.
The preparation method of the refreshing water-in-oil type cream without silicone oil is characterized by comprising the following steps:
1) preparing component raw materials according to the component part ratio of the cream, and dividing the component raw materials into an A phase and a B phase; wherein the content of the first and second substances,
phase A consists of the following components: PEG-30 dipolyhydroxystearate, polyglyceryl-3 diisostearate, isononyl isononanoate;
the phase B consists of the following components: water, disodium EDTA, sodium chloride, p-hydroxyacetophenone, ethylhexyl glycerin, 1, 2-hexanediol, glycerin, butylene glycol, PEG/PPG/polytetramethylene glycol-8/5/3 glycerin;
2) respectively heating phase A and phase B to 75-80 deg.C, slowly adding phase B into phase A under homogenizing condition, stirring, and cooling.
5. The method for preparing refreshing water-in-oil cream free of silicone oil according to claim 4, wherein the homogenization speed in step 2) is 5000-5500rpm and the homogenization time is 3-5 minutes.
The preparation method of the refreshing water-in-oil type cream without silicone oil is characterized in that the cooling is carried out to below 38 ℃ by stirring in the step 2).
The formula of the invention adopts non-silicone oil and grease which are green and pollution-free to the environment and an emulsifier, and has better skin-friendly effect, the viscosity stability of the water-in-oil type cream can be obviously improved by adding PEG/PPG/polytetramethylene glycol-8/5/3 glycerin water-soluble moisturizing oil into the water-in-oil type cream, and the prepared cream has stable performance and good rheological property, and has light and non-greasy skin feel by taking PEG-30 dipolyhydroxystearate and polyglycerol-3 diisostearate as an emulsification system.
Detailed Description
The present invention will be described in further detail with reference to specific examples to better understand the technical solution.
Example 1
A refreshing water-in-oil type cream without silicone oil comprises the following components in percentage by mass: 1% of PEG-30 dipolyhydroxystearate, 2% of polyglycerol-3 diisostearate, 22% of isononyl isononanoate, 0.05% of disodium EDTA, 1.5% of sodium chloride, 0.35% of p-hydroxyacetophenone, 0.05% of ethylhexyl glycerol, 0.5% of 1, 2-hexanediol, 4% of glycerol, 4% of butanediol, 2% of PEG/PPG/polytetramethylene glycol-8/5/3 glycerol and 62.55% of water.
Wherein, PEG-30 dipolyhydroxystearate, polyglycerol-3 diisostearate and isononyl isononanoate form phase A, namely an oil phase; water, EDTA disodium, sodium chloride, p-hydroxyacetophenone, ethylhexyl glycerin, 1, 2-hexanediol, glycerin, butanediol, PEG/PPG/polytetramethylene glycol-8/5/3 glycerin form a phase B, namely a water phase.
The preparation method comprises the following steps: respectively heating the oil phase and the water phase with the formula amount to 75-80 ℃, slowly adding the water phase into the oil phase under the condition of the homogenization speed of 5000-5500rpm, homogenizing for 3-5 minutes, and stirring and cooling to below 38 ℃ to obtain the water-in-oil type cream without the silicone oil.
After trial, 100% of the users of the cream prepared in the embodiment show that the cream has light and non-greasy skin after use; and under the conditions of normal temperature, 45 ℃, 4 ℃ and-18 ℃, the stability is good, and oil and water are not layered.
Comparative example 1
A water-in-oil type cream comprises the following components in percentage by mass: cetyl PEG/PPG-10/1 polydimethylsiloxane 3%, isononyl isononanoate 22%, disodium EDTA 0.05%, sodium chloride 1.5%, p-hydroxyacetophenone 0.35%, ethylhexylglycerin 0.05%, 1, 2-hexanediol 0.5%, glycerin 4%, butylene glycol 4%, PEG/PPG/polytetramethylene glycol-8/5/3 glycerin 2%, water 62.55%.
The preparation method is the same as example 1.
Comparative example 2
A water-in-oil type cream comprises the following components in percentage by mass: 3% of PEG-10 polydimethylsiloxane, 22% of isononyl isononanoate, 0.05% of EDTA disodium, 1.5% of sodium chloride, 0.35% of p-hydroxyacetophenone, 0.05% of ethylhexyl glycerol, 0.5% of 1, 2-hexanediol, 4% of glycerol, 4% of butanediol, 2% of PEG/PPG/polytetramethylene glycol-8/5/3 glycerol and 62.55% of water.
The preparation method is the same as example 1.
Both comparative example 1 and comparative example 2 above were alternatives to the emulsifier, comparative example 1 replacing PEG-30 dipolyhydroxystearate and polyglycerol-3 diisostearate with cetyl PEG/PPG-10/1 polydimethylsiloxane, which is the silicon-containing emulsifier, and comparative example 2 replacing PEG-30 dipolyhydroxystearate and polyglycerol-3 diisostearate with PEG-10 polydimethylsiloxane, which is the silicon-containing emulsifier, to prepare the cream. In the actual use process of the two products prepared by the comparative example, all the users reflect heavy sticky skin feel, and in the stability test, the delamination instability state appears after 1-2 times of freeze thawing.
Comparative example 3
A refreshing water-in-oil type cream without silicone oil comprises the following components in percentage by mass: PEG-30 dipolyhydroxystearate 1%, polyglycerol-3 diisostearate 2%, caprylic/capric triglyceride 22%, disodium EDTA 0.05%, sodium chloride 1.5%, p-hydroxyacetophenone 0.35%, ethylhexylglycerin 0.05%, 1, 2-hexanediol 0.5%, glycerin 4%, butanediol 4%, PEG/PPG/polytetramethylene glycol-8/5/3 glycerin 2%, water 62.55%.
The preparation method is the same as example 1.
Comparative example 4
A refreshing water-in-oil type cream without silicone oil comprises the following components in percentage by mass: PEG-30 dipolyhydroxystearate 1%, polyglycerol-3 diisostearate 2%, ethylhexyl palmitate 22%, disodium EDTA 0.05%, sodium chloride 1.5%, p-hydroxyacetophenone 0.35%, ethylhexyl glycerol 0.05%, 1, 2-hexanediol 0.5%, glycerol 4%, butanediol 4%, PEG/PPG/polytetramethylene glycol-8/5/3 glycerol 2%, water 62.55%.
The preparation method is the same as example 1.
Comparative example 5
A refreshing water-in-oil type cream without silicone oil comprises the following components in percentage by mass: PEG-30 dipolyhydroxystearate 1%, polyglycerol-3 diisostearate 2%, ethylhexyl palmitate 22%, disodium EDTA 0.05%, sodium chloride 1.5%, p-hydroxyacetophenone 0.35%, ethylhexyl glycerol 0.05%, 1, 2-hexanediol 0.5%, glycerol 4%, butanediol 4%, PEG/PPG/polytetramethylene glycol-8/5/3 glycerol 2%, water 62.55%.
The preparation method is the same as example 1.
In comparative examples 3 to 5, representative oils and fats were selected: and carrying out a comparison test on caprylic/capric triglyceride, ethylhexyl palmitate and mineral oil, wherein the results of the tests show that the products prepared by the three formulas are in a layered unstable state after being frozen and thawed for 1-2 times in a stability test.
Comparative example 6
A refreshing water-in-oil type cream without silicone oil comprises the following components in percentage by mass: 1% of PEG-30 dipolyhydroxystearate, 2% of polyglycerol-3 diisostearate, 22% of isononyl isononanoate, 0.05% of disodium EDTA, 1.5% of sodium chloride, 0.35% of p-hydroxyacetophenone, 0.05% of ethylhexyl glycerol, 0.5% of 1, 2-hexanediol, 4% of glycerol, 4% of butanediol and 64.55% of water.
The preparation method is the same as example 1.
This example differs from the comparative example only in that the formulation does not contain the co-stabilizer PEG/PPG/polytetramethylene glycol-8/5/3 glycerol, and the product obtained is tested for stability and the results show that: the delamination and instability state appears after 1-2 times of freeze thawing, and the delamination and oil yielding phenomenon appears after one month observation at normal temperature, 4 ℃ and 45 ℃.
The examples and the comparative examples show that the skin feel and the stability of the product prepared according to the formula of the water-in-oil type cream are superior to those of the comparative examples, the water-soluble moisturizing oil of PEG/PPG/polytetramethylene glycol-8/5/3 glycerin is added into the water-in-oil type cream, the viscosity stability of the water-in-oil type cream can be obviously improved, and the prepared cream has stable performance and good rheological property; the skin-friendly cream uses PEG-30 dipolyhydroxystearate and polyglycerol-3 diisostearate as an emulsifying system, and has light and non-greasy skin feel.
Claims (6)
1. The refreshing water-in-oil type cream without silicone oil is characterized by comprising the following components in percentage by mass: PEG-30 dipolyhydroxystearate 0.5-3%, polyglycerol-3 diisostearate 0.5-3%, isononyl isononanoate 15-30%; the phase B consists of the following components: 0.02-0.1% of EDTA disodium, 0.5-2% of sodium chloride, 0.3-0.5% of p-hydroxyacetophenone, 0.05-0.1% of ethylhexyl glycerol, 0.3-1% of 1, 2-hexanediol, 2-10% of glycerol, 2-10% of butanediol, 0.5-5% of PEG/PPG/polytetramethylene glycol-8/5/3 glycerol and the balance of water.
2. The refreshing water-in-oil cream free of silicone oil according to claim 1, characterized in that the mass percentages of the components are: 1-2% of PEG-30 dipolyhydroxystearate, 1-3% of polyglycerol-3 diisostearate, 18-25% of isononyl isononanoate, 0.05-0.1% of disodium EDTA (ethylene diamine tetraacetic acid), 1-2% of sodium chloride, 3-5% of p-hydroxyacetophenone, 0.05-0.07% of ethylhexyl glycerol, 0.3-0.7% of 1, 2-hexanediol, 3-5% of glycerol, 3-5% of butanediol, 1-3% of PEG/PPG/polytetramethylene glycol-8/5/3 glycerol and the balance of water.
3. The refreshing water-in-oil cream free of silicone oil according to claim 1 or 2, characterized in that the mass percentages of the components are: PEG-30 dipolyhydroxystearate 1%, polyglycerol-3 diisostearate 2%, isononyl isononanoate 22%, disodium EDTA/0.05%, sodium chloride 1.5%, p-hydroxyacetophenone 0.35%, ethylhexylglycerin 0.05%, 1, 2-hexanediol 0.5%, glycerin 4%, butanediol 4%, PEG/PPG/polytetramethylene glycol-8/5/3 glycerin 2%, water 62.5%.
4. A method for preparing a refreshing water-in-oil cream free of silicone oil according to any one of claims 1 to 3, characterized by comprising the steps of:
1) preparing component raw materials according to the component part ratio of the cream, and dividing the component raw materials into an A phase and a B phase; wherein the content of the first and second substances,
phase A consists of the following components: PEG-30 dipolyhydroxystearate, polyglyceryl-3 diisostearate, isononyl isononanoate;
the phase B consists of the following components: water, disodium EDTA, sodium chloride, p-hydroxyacetophenone, ethylhexyl glycerin, 1, 2-hexanediol, glycerin, butylene glycol, PEG/PPG/polytetramethylene glycol-8/5/3 glycerin;
2) respectively heating phase A and phase B to 75-80 deg.C, slowly adding phase B into phase A under homogenizing condition, stirring, and cooling.
5. The method for preparing refreshing water-in-oil cream free of silicone oil according to claim 4, wherein the homogenization speed in step 2) is 5000-5500rpm and the homogenization time is 3-5 minutes.
6. The method for preparing refreshing water-in-oil cream free of silicone oil according to claim 4, wherein the cooling under stirring in step 2) is carried out to below 38 ℃.
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| CN202011631204.7A CN112451396B (en) | 2020-12-31 | 2020-12-31 | Refreshing water-in-oil type cream without silicone oil |
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| CN202011631204.7A CN112451396B (en) | 2020-12-31 | 2020-12-31 | Refreshing water-in-oil type cream without silicone oil |
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| CN112451396B CN112451396B (en) | 2022-07-29 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114632031A (en) * | 2022-03-17 | 2022-06-17 | 彭氏(惠州)实业发展有限公司 | Water-out cream with milk texture |
| CN115737461A (en) * | 2022-12-15 | 2023-03-07 | 诺斯贝尔化妆品股份有限公司 | Ion-rich cream and preparation method thereof |
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2020
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Patent Citations (5)
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| CN106726708A (en) * | 2017-02-22 | 2017-05-31 | 广州市聚吉科绿色化学共性技术研究院有限公司 | A kind of waterproof BB frosts |
| CN108283584A (en) * | 2018-03-31 | 2018-07-17 | 佛山娇芙生物科技有限公司 | It is a kind of that there is the foundation emulsion for well holding adornment |
| CN109172410A (en) * | 2018-11-17 | 2019-01-11 | 长沙浩然医疗科技有限公司 | A kind of foundation emulsion and preparation method thereof that antibiotic property is good |
| CN111904891A (en) * | 2019-05-08 | 2020-11-10 | 西安博鸿生物技术有限公司 | Water-in-oil composition |
| CN111096912A (en) * | 2020-02-14 | 2020-05-05 | 广州艾蓓生物科技有限公司 | Bicontinuous phase type eye and lip makeup remover and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114632031A (en) * | 2022-03-17 | 2022-06-17 | 彭氏(惠州)实业发展有限公司 | Water-out cream with milk texture |
| CN115737461A (en) * | 2022-12-15 | 2023-03-07 | 诺斯贝尔化妆品股份有限公司 | Ion-rich cream and preparation method thereof |
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| CN112451396B (en) | 2022-07-29 |
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