CN112402304A - Shaddock leaf shower gel and preparation method thereof - Google Patents
Shaddock leaf shower gel and preparation method thereof Download PDFInfo
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- CN112402304A CN112402304A CN201910766480.5A CN201910766480A CN112402304A CN 112402304 A CN112402304 A CN 112402304A CN 201910766480 A CN201910766480 A CN 201910766480A CN 112402304 A CN112402304 A CN 112402304A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
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Abstract
The invention provides shaddock leaf shower gel which is prepared from 18-45 parts of surfactant, preferably 10-20 parts, shaddock leaf extract 5-30 parts, preferably 10-15 parts, thickener 0.1-5 parts, preferably 0.5-3 parts, preservative 0.1-2 parts, preferably 0.2-0.5 part, humectant 0.1-3 parts, preferably 0.1-1 part, natural oil 5-20 parts, preferably 8-10 parts, deionized water 50-70 parts, preferably 60-65 parts, the shower gel prepared by adding the shaddock leaf extract has faint scent after use, is not thick and strong, fine and smells, is sweet and smells, is particularly pleasant to the heart and spleen, is mild and non-irritant, has very good effect and disinfection effect, and can nourish deep skin, has the function of protecting fragile and allergic skin.
Description
Technical Field
The invention relates to the field of daily chemical industry, and in particular relates to shaddock leaf shower gel and a preparation method thereof.
Background
Along with the improvement of living standard, the shower gel gradually becomes a bath product for people. The bath lotion is in a liquid or milky state, is called bath foam and bath foam, and is a daily chemical product used for helping to clean the body when people take a bath. Various bathing articles are available on the market according to various demands of consumers. From the most original perfumed soap, bath foam with different fresh fragrances and different functions is full of precious minerals, along with the improvement of living standard, various types of bath foam with precious minerals in the market are gradually produced, and the quality and grade of the product are continuously improved so as to meet the requirements of consumption levels of different levels.
Disclosure of Invention
In order to solve the technical problems, the invention aims to provide the shaddock leaf shower gel, the preparation method and the preparation method thereof, so as to overcome the defects of the prior art.
In order to achieve the purpose, the technical scheme of the invention is as follows:
the shaddock leaf shower gel is prepared from the following raw materials in parts by mass:
18-45 parts of surfactant, preferably 10-20 parts;
5-30 parts of shaddock leaf extract, preferably 10-15 parts;
0.1-5 parts of thickening agent, preferably 0.5-3 parts;
0.1-2 parts of preservative, preferably 0.2-0.5 part;
0.1-3 parts of humectant, preferably 0.1-1 part;
5-20 parts of natural oil, preferably 8-10 parts;
50-70 parts of deionized water, preferably 60-65 parts.
Preferably, the surfactant comprises one or a mixture of more than two of sodium laureth sulfate, ammonium laureth sulfate, cocoamidopropyl betaine, potassium cocoyl glycinate, sodium lauroyl sarcosinate, sodium lauroyl glutamate, sodium lauroyl avenamide, potassium laureth phosphate, disodium laureth sulfosuccinate and sodium methylcocoyl taurate.
Preferably, the grapefruit leaf extract is in the form of a powder.
Preferably, the thickener comprises one or more of hydroxyethyl cellulose, sodium alginate and guar gum hydroxypropyl trimethyl ammonium chloride.
Preferably, the preservative comprises one or a mixture of more than two of methylisothiazolinone, ethylhexyl glycerol, clove leaf oil, methyl hydroxybenzoate and ethylparaben.
Preferably, the humectant comprises one or a mixture of two or more of glycerol, propylene glycol and 1, 3-butanediol.
Preferably, the natural oil comprises one or more of coconut oil, grape seed oil, olive oil, sunflower seed oil, rapeseed oil and shea butter.
The preparation method of the shaddock leaf shower gel comprises the following steps:
(1) cleaning fresh folium Citri Grandis with clear water for 1 time, and pulverizing into 30-120 mesh powder with ultramicro pulverizer to obtain folium Citri Grandis extract;
(2) firstly, mixing and stirring 70% of the total amount of the surfactant and the deionized water on a stirring kettle at the stirring temperature of 50-55 ℃ for 2-4min at the stirring speed of 1000-1500r/min, keeping the temperature and standing for 5-7min, adding the grapefruit leaf extract, continuously stirring, increasing the stirring temperature to 60-65 ℃, increasing the stirring speed to 2500-3000r/min, and stirring for 5-6min to obtain a mixture;
(3) stirring and cooling the prepared mixture A to 40-50 ℃, adding the rest 30% of deionized water into a stirring kettle, heating to 70 ℃, sequentially adding a humectant, a thickening agent, a preservative and natural grease under the stirring state, reducing the stirring speed to 1500-1700r/min, and stirring for 20-30min to obtain a shower gel finished product;
(4) and (4) cooling the bath cream finished product to below 40 ℃, and filling.
Compared with the prior art, the invention has the following remarkable advantages: according to the shaddock leaf shower gel and the preparation method thereof, the shower gel prepared by adding the shaddock leaf extract has faint scent, is not strong and not intense, is fine and smells once, is refreshing and smells well, is mild and non-irritating, has a very good moisturizing effect and a very good disinfecting effect, can deeply nourish the skin, and has the effect of protecting fragile and easily allergic skin.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is described in further detail below. It should be understood, however, that the description herein of specific embodiments is only intended to illustrate the invention and not to limit the scope of the invention.
Example 1
The shaddock leaf shower gel is prepared from the following raw materials in parts by mass:
the surfactant is sodium laureth sulfate, the part by mass is 10;
the mass portion of the shaddock leaf extract is 10 portions;
the thickening agent is hydroxyethyl cellulose, and the mass portion is 1 portion;
the preservative is methylisothiazolinone, and the mass portion is 0.2 portion;
the humectant is 0.2 part by mass of glycerol;
the natural oil is coconut oil, and the mass portion is 8 portions;
the mass part of the deionized water is 60 parts.
The preparation method of the shaddock leaf shower gel specifically comprises the following steps:
(1) cleaning fresh folium Citri Grandis with clear water for 1 time, and pulverizing into 30-120 mesh powder with ultramicro pulverizer to obtain folium Citri Grandis extract;
(2) firstly, mixing and stirring 70% of the total amount of sodium laureth sulfate and deionized water in a stirring kettle at the stirring temperature of 50-55 ℃, stirring for 2-4min at the stirring speed of 1000-1500r/min, keeping the temperature and standing for 5-7min, adding the grapefruit leaf extract, continuously stirring, increasing the stirring temperature to 60-65 ℃, increasing the stirring speed to 2500-3000r/min, and stirring for 5-6min to obtain a mixture;
(3) stirring and cooling the prepared mixture A to 40-50 ℃, adding the rest 30% of deionized water into a stirring kettle, heating to 70 ℃, sequentially adding glycerol, hydroxyethyl cellulose, methylisothiazolinone and coconut oil under stirring, reducing the stirring speed to 1500-1700r/min, and stirring for 20-30min to obtain a shower gel finished product;
(4) and (4) cooling the bath cream finished product to below 40 ℃, and filling.
Example 2
The shaddock leaf shower gel is prepared from the following raw materials in parts by mass:
the surfactant is a solution A obtained by mixing sodium laureth sulfate and sodium laureth sulfate according to a ratio of 1:1, and the mass part of the solution A is 15 parts;
the mass portion of the shaddock leaf extract is 12;
the thickening agent is a solution B obtained by mixing hydroxyethyl cellulose and sodium alginate according to the proportion of 1:1, and the mass part of the thickening agent is 2 parts;
the preservative is a solution C obtained by mixing methylisothiazolinone and ethylhexylglycerin according to the ratio of 1:1, and the mass part of the preservative is 0.3 part;
the humectant is 0.5 part by mass of a solution D obtained by mixing glycerol and propylene glycol according to the proportion of 1: 1;
the natural oil is a solution E obtained by mixing coconut oil and grape seed oil according to the proportion of 1:1, and the mass portion is 9 portions;
the mass portion of the deionized water is 65 portions.
The preparation method of the shaddock leaf shower gel specifically comprises the following steps:
(1) cleaning fresh folium Citri Grandis with clear water for 1 time, and pulverizing into 30-120 mesh powder with ultramicro pulverizer to obtain folium Citri Grandis extract;
(2) mixing and stirring 70% of the total amount of the solution A and the deionized water in a stirring kettle at 50-55 ℃ for 2-4min at the stirring speed of 1000-1500r/min, keeping the temperature and standing for 5-7min, adding the grapefruit leaf extract, continuously stirring, increasing the stirring temperature to 60-65 ℃, increasing the stirring speed to 2500-3000r/min, and stirring for 5-6min to obtain a mixture;
(3) stirring and cooling the prepared mixture A to 40-50 ℃, adding the rest 30% of deionized water into a stirring kettle, heating to 70 ℃, sequentially adding the solution D, the solution B, the solution C and the solution E under the stirring state, reducing the stirring speed to 1500-1700r/min, and stirring for 20-30min to obtain a shower gel finished product;
(4) and (4) cooling the bath cream finished product to below 40 ℃, and filling.
Example 3
The shaddock leaf shower gel is prepared from the following raw materials in parts by mass:
the surfactant is a solution A which is prepared by mixing 20 parts by mass of sodium laureth sulfate, ammonium laureth sulfate, cocoyl amidopropyl betaine, potassium cocoyl glycinate, sodium lauroyl sarcosinate, sodium lauroyl glutamate, sodium lauroyl avenamido acid, potassium laureth phosphate, disodium laureth sulfosuccinate and sodium methyl cocoyl taurate according to a ratio of 1: 1;
15 parts of the shaddock leaf extract;
the thickening agent is a solution B obtained by mixing hydroxyethyl cellulose, sodium alginate and guar gum hydroxypropyl trimethyl ammonium chloride according to the proportion of 1:1, and the mass portion of the thickening agent is 3 portions;
the preservative is a solution C obtained by mixing methylisothiazolinone, ethylhexyl glycerol, clove leaf oil, methyl hydroxybenzoate and ethylparaben according to the proportion of 1:1, and the mass portion of the solution C is 0.5 portion;
the humectant is a solution D obtained by mixing glycerol, propylene glycol and 1, 3-butanediol according to the proportion of 1:1, and the mass part of the solution D is 1 part;
the natural oil is a solution E obtained by mixing coconut oil, grape seed oil, olive oil, sunflower seed oil, rapeseed oil and shea butter according to the proportion of 1:1, and the mass portion of the solution E is 10 portions;
the mass portion of the deionized water is 65 portions.
The preparation method of the shaddock leaf shower gel specifically comprises the following steps:
(1) cleaning fresh folium Citri Grandis with clear water for 1 time, and pulverizing into 30-120 mesh powder with ultramicro pulverizer to obtain folium Citri Grandis extract;
(2) mixing and stirring 70% of the total amount of the solution A and the deionized water in a stirring kettle at 50-55 ℃ for 2-4min at the stirring speed of 1000-1500r/min, keeping the temperature and standing for 5-7min, adding the grapefruit leaf extract, continuously stirring, increasing the stirring temperature to 60-65 ℃, increasing the stirring speed to 2500-3000r/min, and stirring for 5-6min to obtain a mixture;
(3) stirring and cooling the prepared mixture A to 40-50 ℃, adding the rest 30% of deionized water into a stirring kettle, heating to 70 ℃, sequentially adding the solution D, the solution B, the solution C and the solution E under the stirring state, reducing the stirring speed to 1500-1700r/min, and stirring for 20-30min to obtain a shower gel finished product;
(4) and (4) cooling the bath cream finished product to below 40 ℃, and filling.
In summary, the performance tests of the shaddock leaf shower gel used in the embodiments 1 to 3 of the present invention have the following test indexes and results:
1. traits
The shower gels of examples 1-3 were jelly-like in appearance, uniform, transparent, stable, and slightly fragrant.
pH value
The pH (25 ℃) of the shower gel of examples 1 to 3 was measured to be 5.0 to 7.0 according to the measurement of the pH of the GBT13531.1-2008 cosmetic general test method.
3. Viscosity of the oil
The body washes of examples 1-3 have a viscosity (25 ℃) of more than 55000 as measured by GB-T10247-1988 viscosity test method using a rotational viscometer model NDJ-1.
4. Stability of
According to the national standard of GBT34857-2017, the shower gel of the embodiment 1-3 is sampled and packaged in a transparent cosmetic bottle, the shower gel is respectively placed under the experimental conditions of-10 ℃, 2 ℃, 25 ℃ and 45 ℃ under the illumination of a quartz lamp, the appearance, the fragrance, the pH value, the viscosity and other items are continuously tested for 45 days, and whether unfavorable phenomena such as bleeding, layering, separation, precipitation, discoloration, peculiar smell and emulsion breaking occur or not is observed, and the detection result shows that the shower gel of the embodiment 1-3 does not have the unfavorable phenomena such as bleeding, layering, separation, precipitation, discoloration, peculiar smell and emulsion breaking within 45 days, and the stability is good.
5. Irritability-stimulating property
The shower gel of examples 1-3 was sampled, and a suitable amount of the sample was applied to the back of the hand of the volunteer and observed for 30min to see if red swelling, rash, blistering, etc. occurred. The observation result shows that all testers do not have adverse symptoms within 30min, and the shower gel disclosed by the invention does not cause irritation and allergy to skin.
6. Comprehensive effect test
The shower gel of the examples 1 to 3 was used as an experimental subject, 30 volunteers were selected as trial subjects, and the test subjects were used for bathing once a day for one month continuously, and the test sheets were filled out for scoring after trial. The using effect of each item in the scoring table is 10 points in total: score 10 indicates very satisfactory; scores of 8 to 9 indicate that the comparison is satisfactory; scores 6-7 indicate that acceptance is acceptable; scores 4-6 indicate poor, scores 4 below indicate poor, and scores are as follows:
the average score of each using effect of the shower gel of the examples 1 to 3
Example 1
Outward appearance 9.8
Rich in foam 9.5
Flush velocity 9.4
After-bath freshness of 9.7
Moisture retention 9.8
Has no irritation of 9.8
Example 2
Outward appearance 9.7
Rich in foam 9.6
Flush velocity 9.2
After-bath refreshing property 9.8
Moisture retention 9.5
Has no irritation of 9.6
Example 3
Outward appearance 9.9
Rich in foam 9.5
Flush velocity 9.3
After-bath refreshing property 9.5
Moisture retention 9.6
Has no irritation of 9.8
From the above test results it follows: the shower gel disclosed by the invention has a very good using effect.
In addition, the pomelo leaf can be applied to shower gel and soap, and the pomelo leaf soap can be prepared by adding the pomelo leaf extract and the main component sodium stearate.
Finally, it should be noted that: the above embodiments are only used to illustrate the technical solution of the present invention, and not to limit the same; while the invention has been described in detail and with reference to the foregoing embodiments, it will be understood by those skilled in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some or all of the technical features may be equivalently replaced; such modifications and substitutions do not depart from the spirit and scope of the present invention, and they should be construed as being included in the following claims and description.
Claims (8)
1. The shaddock leaf shower gel is characterized by being prepared from the following raw materials in parts by mass:
18-45 parts of surfactant, preferably 10-20 parts;
5-30 parts of shaddock leaf extract, preferably 10-15 parts;
0.1-5 parts of thickening agent, preferably 0.5-3 parts;
0.1-2 parts of preservative, preferably 0.2-0.5 part;
0.1-3 parts of humectant, preferably 0.1-1 part;
5-20 parts of natural oil, preferably 8-10 parts;
50-70 parts of deionized water, preferably 60-65 parts.
2. The shaddock leaf shower gel and the preparation method thereof as claimed in claim 1, wherein the shaddock leaf shower gel is characterized in that: the surfactant comprises one or a mixture of more than two of sodium laureth sulfate, ammonium laureth sulfate, cocoyl amidopropyl betaine, potassium cocoyl glycinate, sodium lauroyl sarcosinate, sodium lauroyl glutamate, sodium lauroyl avenamide, potassium laureth phosphate, disodium laureth sulfosuccinate and sodium methyl cocoyl taurate.
3. The shaddock leaf shower gel and the preparation method thereof as claimed in claim 1, wherein the shaddock leaf shower gel is characterized in that: the folium Citri Grandis extract is in the form of powder.
4. The shaddock leaf shower gel and the preparation method thereof as claimed in claim 1, wherein the shaddock leaf shower gel is characterized in that: the thickener comprises one or more of hydroxyethyl cellulose, sodium alginate and guar gum hydroxypropyl trimethyl ammonium chloride.
5. The shaddock leaf shower gel and the preparation method thereof as claimed in claim 1, wherein the shaddock leaf shower gel is characterized in that: the preservative comprises one or a mixture of more than two of methylisothiazolinone, ethylhexyl glycerol, clove leaf oil, methylparaben and ethylparaben.
6. The shaddock leaf shower gel and the preparation method thereof as claimed in claim 1, wherein the shaddock leaf shower gel is characterized in that: the humectant comprises one or a mixture of more than two of glycerol, propylene glycol and 1, 3-butanediol.
7. The shaddock leaf shower gel and the preparation method thereof as claimed in claim 1, wherein the shaddock leaf shower gel is characterized in that: the natural oil comprises one or more of coconut oil, grape seed oil, olive oil, sunflower seed oil, rapeseed oil and shea butter.
8. The preparation method of the shaddock leaf shower gel as claimed in any one of claims 1 to 7, comprising the steps of:
(1) cleaning fresh folium Citri Grandis with clear water for 1 time, and pulverizing into 30-120 mesh powder with ultramicro pulverizer to obtain folium Citri Grandis extract;
(2) firstly, mixing and stirring 70% of the total amount of the surfactant and the deionized water on a stirring kettle at the stirring temperature of 50-55 ℃ for 2-4min at the stirring speed of 1000-1500r/min, keeping the temperature and standing for 5-7min, adding the grapefruit leaf extract, continuously stirring, increasing the stirring temperature to 60-65 ℃, increasing the stirring speed to 2500-3000r/min, and stirring for 5-6min to obtain a mixture;
(3) stirring and cooling the prepared mixture A to 40-50 ℃, adding the rest 30% of deionized water into a stirring kettle, heating to 70 ℃, sequentially adding a humectant, a thickening agent, a preservative and natural grease under the stirring state, reducing the stirring speed to 1500-1700r/min, and stirring for 20-30min to obtain a shower gel finished product;
and (4) cooling the bath cream finished product to below 40 ℃, and filling.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910766480.5A CN112402304A (en) | 2019-08-20 | 2019-08-20 | Shaddock leaf shower gel and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910766480.5A CN112402304A (en) | 2019-08-20 | 2019-08-20 | Shaddock leaf shower gel and preparation method thereof |
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| CN112402304A true CN112402304A (en) | 2021-02-26 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113171331A (en) * | 2021-05-14 | 2021-07-27 | 广州锦同生物科技有限公司 | Ice crystal amino acid shower gel and preparation method thereof |
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| CN113171331A (en) * | 2021-05-14 | 2021-07-27 | 广州锦同生物科技有限公司 | Ice crystal amino acid shower gel and preparation method thereof |
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Application publication date: 20210226 |