CN112386956A - A integrative equipment of oil-water separation resourceization for handling oily sewage - Google Patents

A integrative equipment of oil-water separation resourceization for handling oily sewage Download PDF

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Publication number
CN112386956A
CN112386956A CN201910765552.4A CN201910765552A CN112386956A CN 112386956 A CN112386956 A CN 112386956A CN 201910765552 A CN201910765552 A CN 201910765552A CN 112386956 A CN112386956 A CN 112386956A
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filtering
oil
water
valve
chamber
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张洪源
杨杰林
安春喜
杨情
赵萃萃
吴广恒
李璐
王雪
尚亚平
郭湘丽
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Tianjin Vocational Institute
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Tianjin Vocational Institute
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Priority to CN201910765552.4A priority Critical patent/CN112386956A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/0202Separation of non-miscible liquids by ab- or adsorption
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/12Auxiliary equipment particularly adapted for use with liquid-separating apparatus, e.g. control circuits

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  • Thermal Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Filtration Of Liquid (AREA)

Abstract

The invention discloses an oil-water separation and recycling integrated device for treating oily sewage, which comprises: the jar body, axle and 2 filtration, at a jar internal fixation and be equipped with a first baffle, the other end of axle stretches out after passing this first baffle along first baffle place plane, the axle can rotate in first baffle, 2 filtration are located filter chamber and regeneration room respectively, be formed with uncovered and axle and pass from uncovered on first baffle and every filtration relative position, filtration plug up rather than relative uncovered and with lie in this uncovered axle dress admittedly, the motor drive axle is rotatory, each filtration enters into to another 1 space through on the first baffle rather than relative uncovered from 1 space when the axle is rotatory. The invention realizes the oil-water separation of the polluted oily sewage, the separated clean water can be recycled, and the separated grease can be collected and reused.

Description

A integrative equipment of oil-water separation resourceization for handling oily sewage
Technical Field
The invention belongs to the technical field of oil-water separation, and particularly relates to oil-water separation and recycling integrated equipment for treating oily sewage.
Background
The oily sewage is mainly discharged from the petroleum exploitation and processing process, the steel smelting process and the catering industry. Because water resource protection is more and more strict, under the condition that the wastewater discharge standard is improved year by year, the treatment difficulty of the oily wastewater is more and more high, the cost is continuously increased, and even partial enterprises face the embarrassment of closing because the wastewater cannot be treated.
At present, the domestic treatment of oily sewage mainly adopts the methods of air floatation, gravity separation, flocculation, filtration and the like. The oil removal rate by air flotation and gravity separation is generally not more than 70%, the efficiency is low, and the occupied space is large. The flocculation method has poor treatment effect on free grease contained in the sewage, and a flocculating agent needs to be additionally added, and secondary filtration and separation are needed after flocculation. The filtering method has higher grease removal rate on oily sewage, but has more strict requirements on filtering materials, and different filtering materials have larger difference in filtering effect, and the common filtering materials at present comprise quartz sand, clay, walnut shells, fiber balls and the like. The quartz sand has the characteristics of high strength, high density and strong dirt carrying capacity, but the labor intensity is high when the filling material is loaded and unloaded, and the subsequent adsorption is difficult to treat. The walnut shell and fiber ball filter material has the advantages of light weight, good filtering effect and the like, and is concerned by researchers and producers. For example, the wangxoujun of Zhonghai oil in 2016 introduced the filtering effect of the modified walnut shell filtering material, and Yanyuting in Liaohe oil field in 2019 made a relevant study on the walnut shell filter. The research on the application of the modified fiber ball in the deep treatment of offshore oilfield sewage is carried out by the Tang Guangrong of the Zhonghai oil, and the research shows that the modified fiber ball has good filtering effect.
The currently reported filtering means and technologies are all to treat oily sewage as three wastes, and a lot of equipment is designed according to different fillers, for example, utility model CN208726837U, a filter with backwashing function is designed, for example, CN208120905U reports a filter convenient for sewage filtering and sterilization. CN208161112U reports a multistage fiber filter. These filters have good filtering effect, but have two disadvantages: firstly, the back washing process needs intermittent operation, namely, the back washing can be carried out only after the filtration is stopped; secondly, the filtered grease is not collected in all filtering methods of the filtering equipment. Crude oil, distillate oil, lubricating grease, edible oil and the like contained in the oily sewage are valuable resources, and if the oily sewage can be effectively recovered, the pollution can be reduced, and the energy can be saved by resource utilization.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide the oil-water separation and recycling integrated equipment for treating the oily sewage, the oil-water separation and recycling integrated equipment integrates a filter (a filter structure) and a regenerator, the filtering material is regenerated while the oily sewage is filtered, and the oil released when the filtering material is regenerated can be recycled.
The invention also aims to provide the automatic oil-water separation and recycling integrated equipment, the oil-water separation and filtering material regeneration of the automatic oil-water separation and recycling integrated equipment can be continuously operated, is automatically controlled, is efficient and convenient, and has the functions of green regeneration and waste oil recycling while enabling the filter to meet the production requirement.
The invention further aims to provide a use method of the integrated equipment for automatically controlling the oil-water separation and recycling.
The purpose of the invention is realized by the following technical scheme.
An oil-water separation and resource integrated equipment for treating oily sewage comprises: jar body, axle and 2 filtration be equipped with a first baffle admittedly in jar internal fixation for with jar internal partitioning of body is 2 spaces: a filter chamber and a regeneration chamber; one end of the shaft is fixedly installed with a motor, the other end of the shaft penetrates through the first partition plate along the plane where the first partition plate is located and then extends out, the shaft can rotate in the first partition plate, 2 filter structures are respectively located in the filter chamber and the regeneration chamber, openings are formed in the positions, opposite to the first partition plate, of the first partition plate, the shaft penetrates through the openings, the filter structures block the openings opposite to the filter structures and are fixedly installed with the shaft located in the openings, the motor drives the shaft to rotate, and when the shaft rotates, each filter structure enters the other 1 space from 1 space through the opening, opposite to the first partition plate, of the first partition plate, so that the filter chamber and the regeneration chamber are respectively provided with 1 filter structure and the filter structures block the openings opposite to the first partition plate; an oily sewage inlet is formed in the tank wall of the filtering chamber above the filtering structure, the filtering structure located in the filtering chamber is used for filtering oily sewage in the filtering chamber, a purified water outlet is formed in the tank wall of the filtering chamber below the filtering structure, an oil overflow port is formed in the tank wall of the regeneration chamber above the filtering structure, and a cleaning water inlet is formed in the tank wall of the regeneration chamber.
In the above technical solution, 2 of the filter structures are perpendicular to the shaft.
In the above technical scheme, the cross section of the inner wall of the tank body is circular, and the cross section of each filtering structure is semicircular.
In the above technical solution, each of the filter structures is a half cylinder, and the filter structure includes: the filter plate comprises an upper filter sieve plate serving as the top surface of the semi-cylinder, a lower filter sieve plate serving as the bottom surface of the semi-cylinder and a second partition plate positioned on the plane of the side surface of the semi-cylinder, wherein a filter material is filled between the upper filter sieve plate and the lower filter sieve plate.
In the above technical scheme, the cambered surface of the filtering structure is attached to the inner wall of the tank body close to the cambered surface.
In the above technical solution, a first filling opening is formed in a wall of the tank body opposite to the filter structure, a cover is installed on the first filling opening, a second filling opening is formed in an arc surface of the semi-cylinder, and the shaft is rotated until the first filling opening is opposite to the second filling opening, so as to fill the filter material between the upper filter sieve plate and the lower filter sieve plate.
In the above technical scheme, the shaft is vertically arranged on the central point of the cross section of the inner wall of the tank body, and the shaft is fixedly installed with the second partition plates of the 2 filter structures.
In the above technical scheme, 2 filtration are located same horizontal plane and these 2 filtration are connected and are formed a cylinder, the uncovered is the same with the diameter of this jar of internal wall along jar radial ascending length of body.
In the above technical scheme, 2 filtering structures are located on different horizontal planes, and the length of the opening in the radial direction of the tank body is the same as the radius of the inner wall of the tank body.
In the technical scheme, a liquid level sensor is arranged in the regeneration chamber above the filtering structure and used for detecting the liquid height of cleaning water in the regeneration chamber.
In the above technical scheme, a pressure sensor is installed in the filtering chamber above the filtering structure and used for detecting the pressure in the filtering chamber above the filtering structure.
In the above technical solution, a first concentration detector is installed at the purified water outlet and used for detecting the concentration of oil or water in the liquid discharged from the purified water outlet.
In the technical scheme, the water purification outlet is communicated with the first discharge pipe, the oily sewage inlet is communicated with the second discharge pipe, one end of a water return pipe is communicated with the water purification outlet, the other end of the water return pipe is communicated with the oily sewage inlet, the first discharge pipe is provided with a first valve, the first discharge pipe is close to the water purification outlet, the water return pipe is provided with a second valve, the water return pipe is provided with a water pump, the second discharge pipe is provided with a third valve, and the second discharge pipe is close to the oily sewage inlet, and the water return pipe is provided with a sixth valve.
In the above technical solution, a second concentration detector is installed on the oily sewage inlet and is used for detecting the concentration of oil or water in the liquid passing through the oily sewage inlet.
In the above technical solution, a manhole is formed on the tank body.
In the above technical solution, a fourth valve is installed on the washing water inlet.
In the above technical solution, a fifth valve is installed on the oil overflow port.
In the above technical solution, the tank walls of the filter chamber and the regeneration chamber are both formed with vent holes.
Automatic integrative equipment of separation of water oil recycling includes: the oil-water separation and recycling integrated equipment comprises oil-water separation and recycling integrated equipment and a PLC, wherein the PLC controls the motor to rotate.
In the above technical solution, 2 of the filter structures are perpendicular to the shaft.
In the above technical scheme, the cross section of the inner wall of the tank body is circular, and the cross section of each filtering structure is semicircular.
In the above technical solution, each of the filter structures is a half cylinder, and the filter structure includes: the filter plate comprises an upper filter sieve plate serving as the top surface of the semi-cylinder, a lower filter sieve plate serving as the bottom surface of the semi-cylinder and a second partition plate positioned on the plane of the side surface of the semi-cylinder, wherein a filter material is filled between the upper filter sieve plate and the lower filter sieve plate.
In the above technical scheme, the cambered surface of the filtering structure is attached to the inner wall of the tank body close to the cambered surface.
In the above technical solution, a first filling opening is formed in a wall of the tank body opposite to the filter structure, a cover is installed on the first filling opening, a second filling opening is formed in an arc surface of the semi-cylinder, and the shaft is rotated until the first filling opening is opposite to the second filling opening, so as to fill the filter material between the upper filter sieve plate and the lower filter sieve plate.
In the above technical scheme, the shaft is vertically arranged on the central point of the cross section of the inner wall of the tank body, and the shaft is fixedly installed with the second partition plates of the 2 filter structures.
In the above technical scheme, 2 filtration are located same horizontal plane and these 2 filtration are connected and are formed a cylinder, the uncovered is the same with the diameter of this jar of internal wall along jar radial ascending length of body.
In the above technical scheme, 2 filtering structures are located on different horizontal planes, and the length of the opening in the radial direction of the tank body is the same as the radius of the inner wall of the tank body.
In the technical scheme, a liquid level sensor is installed in the regeneration chamber above the filtering structure and used for detecting the liquid height of cleaning water in the regeneration chamber, and the liquid height signal of the liquid level sensor is read by the PLC.
In the above technical solution, a pressure sensor is installed in the filtering chamber above the filtering structure, and is used for detecting the pressure in the filtering chamber above the filtering structure, and a pressure signal of the pressure sensor is read by the PLC.
In the technical scheme, the water purification export communicates with the first discharge pipe, the oily sewage import communicates with the second discharge pipe, the one end of a return pipe with the water purification export communicates, the other end of return pipe with the oily sewage import communicates install first valve on the first discharge pipe, be close to the water purification export install the second valve on the return pipe install the water pump on the return pipe install the third valve on the second discharge pipe, be close to the oily sewage import install the sixth valve on the return pipe, PLC control the opening and closing of first valve, third valve, sixth valve and second valve, PLC control the opening and closing of water pump.
In the above technical solution, a first concentration detector is installed on the purified water outlet and used for detecting the concentration of oil or water in the liquid discharged from the purified water outlet, and a concentration signal of the first concentration detector is read by the PLC.
In the above technical solution, a second concentration detector is installed on the oily sewage inlet and used for detecting the concentration of oil or water in the liquid passing through the oily sewage inlet, and a concentration signal of the second concentration detector is read by the PLC.
In the above technical solution, a fourth valve is installed on the washing water inlet, and the PLC controls the opening and closing of the fourth valve.
In the above technical solution, a fifth valve is installed on the oil overflow port, and the PLC controls the opening and closing of the fifth valve.
In the above technical solution, the method further comprises: and the PLC drives the alarm module to alarm.
In the above technical solution, the tank walls of the filter chamber and the regeneration chamber are both formed with vent holes.
In the above technical solution, a manhole is formed on the tank body.
The use method of the integrated equipment for automatically controlling the oil-water separation and recycling comprises the following steps:
the PLC is used for controlling the motor to rotate, so that 1 filtering structure is arranged in each of the filtering chamber and the regeneration chamber, cleaning water is introduced into the regeneration chamber through a cleaning water inlet, the liquid level of the cleaning water is higher than that of the filtering structure in the regeneration chamber, and the following filtering steps are repeated:
and when the filtering structure in the filtering chamber needs to be replaced, the PLC controls the motor to drive the shaft to rotate 180 degrees so as to enable the filtering chamber and the regeneration chamber to exchange the filtering structure, and the filtering structure in the regeneration chamber is soaked by cleaning water so that liquid oil in the filtering structure in the regeneration chamber is leached to the liquid level of the cleaning water in the regeneration chamber.
In the above technical solution, when the thickness of the liquid oil on the liquid level of the cleaning water in the regeneration chamber increases to a level at which the liquid oil reaches the oil overflow port, the liquid oil overflows from the oil overflow port.
In the above technical solution, a fifth valve is installed on the oil overflow port, and the PLC controls the opening and closing of the fifth valve.
In the technical scheme, a fourth valve is arranged on the washing water inlet, and when washing water needs to be introduced into the regeneration chamber through the washing water inlet, the PLC controls the fourth valve to be opened; and when the washing water is stopped being introduced into the regeneration chamber, the PLC controls the fourth valve to be closed.
In the technical scheme, the water purification export communicates with the first discharge pipe, the oily sewage import communicates with the second discharge pipe, the one end of a return pipe with the water purification export communicates, the other end of return pipe with the oily sewage import communicates install first valve on the first discharge pipe, be close to the water purification export install the second valve on the return pipe install the water pump on the return pipe install the third valve on the second discharge pipe, be close to the oily sewage import install the sixth valve on the return pipe, PLC control the opening and closing of first valve, third valve, sixth valve and second valve, PLC control the opening and closing of water pump.
In the technical scheme, in the filtering step, before the oily sewage is introduced into the filtering chamber, the PLC controls the first valve and the third valve to be opened, and the PLC controls the sixth valve and the second valve to be closed.
In the technical scheme, a liquid level sensor is installed in a regeneration chamber above a filtering structure and used for detecting the liquid height of cleaning water in the regeneration chamber, a liquid height signal of the liquid level sensor is read by a PLC (programmable logic controller), a critical liquid level value L0 is set to the PLC, the critical liquid level value L0 is higher than the height of the filtering structure in the regeneration chamber and lower than an oil overflow port (5), when cleaning water is introduced into the regeneration chamber through a cleaning water inlet, the PLC reads the liquid height signal of the liquid level sensor, and when the liquid level height of the liquid height signal reaches the critical liquid level value L0, the PLC controls a fourth valve to be closed.
In the above technical solution, the method further comprises: and when the liquid height signal of the liquid level sensor reaches a critical liquid level value L0, the PLC controls the alarm module to alarm.
In the technical scheme, a first concentration detector is arranged on the purified water outlet and used for detecting the concentration of oil or water in the liquid discharged from the purified water outlet, and a concentration signal of the first concentration detector is read by the PLC; setting a critical concentration C0 to the PLC, and when the oil concentration value obtained after the PLC reads the concentration signal of the first concentration detector is higher than the oil concentration value of the critical concentration C0, controlling the first valve and the third valve to be closed and the sixth valve, the second valve and the water pump to be opened by the PLC and judging that the filtering structure in the filtering chamber needs to be replaced; a second concentration detector is arranged on the oily sewage inlet and is used for detecting the concentration of oil or water in the liquid passing through the oily sewage inlet, and a concentration signal of the second concentration detector is read by the PLC; when the oil concentration value obtained after the PLC reads the concentration signal of the second concentration detector is smaller than the oil concentration value of the critical concentration C0, the PLC controls the first valve and the third valve to be opened and the sixth valve, the second valve and the water pump to be closed.
In the above technical solution, vent holes are formed on the tank walls of the filtering chamber and the regeneration chamber, the vent hole of the filtering chamber is opened before the filtering step, and the vent hole of the regeneration chamber is opened before the washing water is introduced into the regeneration chamber.
In the above technical solution, a pressure sensor is installed in the filtering chamber above the filtering structure and used for detecting the pressure in the filtering chamber above the filtering structure, a pressure signal of the pressure sensor is read by the PLC, a critical pressure P0 is set to the PLC, and when the pressure value of the pressure signal of the pressure sensor read by the PLC is greater than the critical pressure P0, the PLC determines that the filtering structure in the filtering chamber needs to be replaced.
The invention has the following beneficial effects:
the invention realizes the oil-water separation of the polluted oily sewage, the separated clean water can be recycled, and the separated grease (liquid oil) can be collected and reused. Because the filtering material is a renewable filtering material and can be recycled, three wastes are not generated, and zero emission and resource utilization of the oily sewage are realized.
Drawings
Fig. 1 is a front view of an oil-water separation and recycling integrated apparatus (automatic control oil-water separation and recycling integrated apparatus) according to the present invention;
fig. 2 is a front view of the integrated oil-water separation and recycling apparatus (integrated automatic oil-water separation and recycling apparatus) according to the present invention;
FIG. 3 is a top view (with shaft mounting) of 2 of the filter structures of FIG. 1;
FIG. 4 is a top view of 1 filter structure (mounted with a shaft);
FIG. 5 is a side view of the first separator plate of FIG. 1;
FIG. 6 is a side view of the first separator plate of FIG. 2;
FIG. 7 shows water samples before and after being treated by the integrated oil-water separation and recycling device.
Wherein, 1: jar body, 2: shaft, 3: first separator, 4: oily sewage inlet, 5: oil overflow port, 6: manhole, 7: first filling opening, 8: purified water outlet, 9: return pipe, 10: water pump, 11: washing water inlet, 12: motor, 13: bearing, 14: upper filter sieve plate, 15: lower filter screen deck, 16: third valve, 17: first valve, 18: second valve, 19: sixth valve, 20: fifth valve, 21: fourth valve, 22: filter material, 23: second separator, 24: second discharge pipe, 25: first discharge pipe, 26: and (4) a vent.
Detailed Description
The technical scheme of the invention is further explained by combining specific examples.
In the following examples, the level sensor is of type HM21F, the pressure sensor is of type AK-2088, and the first and second concentration detectors are both of type DHP-485. The PLC is of the type AX3U-80 MT.
Example 1
An oil-water separation and resource integrated equipment for treating oily sewage comprises: jar body 1, axle 2 and 2 filtration, at 1 internal fixation of jar body and be equipped with a first baffle 3 for with 1 internal partitioning of jar body 2 spaces: a filter chamber and a regeneration chamber; one end of the shaft 2 is fixedly installed with a motor 12, the other end of the shaft passes through the first clapboard 3 along the plane of the first clapboard 3 and then extends out and is provided with a bearing 13 (or the bearing 13 is not required), the shaft 2 can rotate in the first clapboard 3, 2 filtering structures are respectively positioned in the filtering chamber and the regeneration chamber, wherein, the position that is opposite to each filtering structure on the first clapboard 3 is formed with an opening and the shaft 2 passes through the opening, one end of the filtering structure stretches into the opening and is fixedly installed with the shaft 2 positioned in the opening (one end of the filtering structure stretches into the opening to block the opening), the motor 12 drives the shaft 2 to rotate, when the shaft 2 rotates, each filtering structure enters into the other 1 space from 1 space through the opening opposite to the filtering structure on the first clapboard 3 and the filtering structure blocks the opening opposite to the filtering structure, so that 1 filtering structure is respectively arranged in the filtering chamber and the regeneration chamber; an oily sewage inlet 4 is formed on the tank wall of the filtering chamber above the filtering structure, the filtering structure positioned in the filtering chamber is used for filtering the oily sewage in the filtering chamber, a purified water outlet 8 is formed on the tank wall of the filtering chamber below the filtering structure, an oil overflow port 5 is formed on the tank wall of the regenerating chamber above the filtering structure, a cleaning water inlet 11 is formed on the tank wall of the regenerating chamber, and preferably, the cleaning water inlet 11 is positioned below the filtering structure in the regenerating chamber.
Example 2
On the basis of example 1, 2 filter structures are perpendicular to the axis 2. The cross section of the inner wall of the tank body 1 is circular, and the cross section of each filter structure is semicircular, as shown in fig. 4. Every filtration is a half cylinder, and the filtration includes: an upper filter sieve plate 14 as a top surface of the semi-cylinder, a lower filter sieve plate 15 as a bottom surface of the semi-cylinder, and a second partition plate 23 (the arc surface of the filter structure may be a closed surface or an open surface) located on a plane of a side surface of the semi-cylinder, a plurality of small holes are formed on each of the upper filter sieve plate 14 and the lower filter sieve plate 15, a filter material 22 is filled between the upper filter sieve plate 14 and the lower filter sieve plate 15, and the filter material 22 is a material capable of releasing oil adsorbed by the filter material by soaking, for example: the filter material 22 may be a fiber ball filter packing (patent publication No. CN 109453562A). The cambered surface of the filtering structure is attached to the inner wall of the tank body 1 close to the cambered surface. Preferably, the edges of the upper filtering sieve plate 14 and the lower filtering sieve plate 15, which are in contact with the inner wall of the tank body 1, are respectively and fixedly provided with a soft sealing material for improving the sealing effect between the edge of the filtering structure and the inner wall of the tank body 1, and the filtering effect of the filtering structure can be improved after the sealing effect is improved.
A first filling opening 7 is formed on the tank wall of the tank body 1 opposite to the filtering structure, the first filling opening 7 is preferably located on the tank wall of the regeneration chamber, a cover body is installed on the first filling opening 7, a second filling opening (when the cambered surface of the filtering structure is an open surface, the open surface is the second filling opening) is formed on the cambered surface of the semi-cylinder, and the rotating shaft 2 is opposite to the first filling opening 7 and the second filling opening and is used for filling the filtering material 22 between the upper filtering sieve plate 14 and the lower filtering sieve plate 15.
The shaft 2 is vertically arranged on the central point of the cross section of the inner wall of the tank body 1, and the shaft 2 and the second partition plates 23 of the 2 filter structures are fixedly arranged.
A liquid level sensor is arranged in the regeneration chamber above the filtering structure and used for detecting the liquid height of cleaning water in the regeneration chamber and preventing the cleaning water from overflowing to the oil overflow port due to overhigh liquid level.
And a pressure sensor is arranged in the filtering chamber above the filtering structure and used for detecting the pressure in the filtering chamber above the filtering structure and preventing the pressure in the filtering chamber from exceeding a set value.
A first concentration detector is installed on the purified water outlet 8 for detecting the concentration of oil or water in the liquid discharged from the purified water outlet 8.
The water purification outlet 8 is communicated with a first discharge pipe 25, the oily sewage inlet 4 is communicated with a second discharge pipe 24, one end of a water return pipe 9 is communicated with the water purification outlet 8, the other end of the water return pipe 9 is communicated with the oily sewage inlet 4, a first valve 17 is installed on the first discharge pipe 25, a second valve 18 is installed on the water return pipe 9 close to the water purification outlet 8, a water pump 10 is installed on the water return pipe 9, a third valve 16 is installed on the second discharge pipe 24, and a sixth valve 19 is installed on the water return pipe 9 close to the oily sewage inlet 4.
A second concentration detector is mounted on the oily sewage inlet 4 and is used for detecting the concentration of oil or water in the liquid passing through the oily sewage inlet 4.
Manholes 6 are formed in the tank body 1, 2 as shown in fig. 1, and are respectively located at opposite sides of the tank body 1.
A fourth valve 21 is installed at the washing water inlet 11.
A fifth valve 20 is installed at the oil overflow port 5.
Vents 26 are formed in the tank walls of both the filtration and regeneration chambers.
Example 3
As shown in fig. 1 and 3, on the basis of embodiment 2, 2 filtering structures are located on the same horizontal plane and the 2 filtering structures are connected to form a cylinder, the length of the opening along the radial direction of the tank body 1 is the same as the diameter of the inner wall of the tank body 1, and the first partition plate is shown in fig. 5. The shaft 2 passes through the opening and is located at the center line of the opening. The size of the opening in the first partition is the same as the size of the plane on which the filter structure is located.
Example 4
As shown in figure 2, on the basis of the embodiment 2, 2 filtering structures are positioned at different horizontal planes, the length of an opening along the radial direction of a tank body 1 is the same as the radius of the inner wall of the tank body 1, and a first clapboard is shown in figure 6. Half of the shaft 2 (divided in the radial direction of the shaft 2 to form 2 "shaft halves") passes through the opening. The size of the opening on the first partition board is half of the plane of the side face of the filtering structure.
Example 5
Automatic integrative equipment of separation of water oil recycling includes: in the embodiment 1, the integrated equipment for separating and recycling agricultural oil from water and the PLC control the motor 12 to rotate.
Example 6
On the basis of example 5, 2 filter structures are perpendicular to the axis 2.
The cross section of the inner wall of the tank body 1 is circular, and the cross section of each filtering structure is semicircular.
Every filtration is a half cylinder, and the filtration includes: an upper filter sieve plate 14 as a top surface of the semi-cylinder, a lower filter sieve plate 15 as a bottom surface of the semi-cylinder, and a second partition plate 23 (the arc surface of the filter structure may be a closed surface or an open surface) located on a plane of a side surface of the semi-cylinder, wherein a plurality of small holes are formed on each of the upper filter sieve plate 14 and the lower filter sieve plate 15, a filter material 22 is filled between the upper filter sieve plate 14 and the lower filter sieve plate 15, and the filter material 22 may be a fiber ball filter filler (patent publication No. CN 109453562A).
The cambered surface of the filtering structure is attached to the inner wall of the tank body 1 close to the cambered surface. Preferably, the edges of the upper filtering sieve plate 14 and the lower filtering sieve plate 15, which are in contact with the inner wall of the tank body 1, are respectively and fixedly provided with a soft sealing material for improving the sealing effect between the edge of the filtering structure and the inner wall of the tank body 1, and further improving the filtering effect of the filtering structure.
A first filling opening 7 is formed on the tank wall of the tank body 1 opposite to the filtering structure, the first filling opening 7 is preferably positioned on the tank wall of the regeneration chamber, a cover body is arranged on the first filling opening 7, a second filling opening (when the cambered surface of the filtering structure is an open surface, the open surface is the second filling opening) is formed on the cambered surface of the semi-cylinder, and the rotating shaft 2 is opposite to the first filling opening 7 and the second filling opening and is used for filling the filtering material 22 between the upper filtering sieve plate 14 and the lower filtering sieve plate 15.
The shaft 2 is vertically arranged on the central point of the cross section of the inner wall of the tank body 1, and the shaft 2 and the second partition plates 23 of the 2 filter structures are fixedly arranged.
Install level sensor in the regeneration room of filtration top for detect the indoor liquid height who washs water of regeneration, prevent that the liquid level is too high to lead to wasing water to overflow to oil overflow mouth, level sensor's liquid height signal is read by PLC.
And a pressure sensor is arranged in the filtering chamber above the filtering structure and used for detecting the pressure when the filtering chamber above the filtering structure is filled with oily sewage, so that the pressure in the filtering chamber is prevented from exceeding a set value, and a pressure signal of the pressure sensor is read by a PLC (programmable logic controller).
The water purification outlet 8 is communicated with a first discharge pipe 25, the oily sewage inlet 4 is communicated with a second discharge pipe 24, one end of a water return pipe 9 is communicated with the water purification outlet 8, the other end of the water return pipe 9 is communicated with the oily sewage inlet 4, a first valve 17 is installed on the first discharge pipe 25, a second valve 18 is installed on the water return pipe 9 close to the water purification outlet 8, a water pump 10 is installed on the water return pipe 9, a third valve 16 is installed on the second discharge pipe 24, a sixth valve 19 is installed on the water return pipe 9 close to the oily sewage inlet 4, the PLC controls the opening and closing of the first valve 17, the third valve 16, the sixth valve 19 and the second valve 18, and the PLC controls the opening and closing of the water pump 10.
A first concentration detector is installed on the purified water outlet 8 for detecting the concentration of oil or water in the liquid discharged from the purified water outlet 8, and a concentration signal of the first concentration detector is read by the PLC.
A second concentration detector is installed on the oily sewage inlet 4 and is used for detecting the concentration of oil or water in the liquid passing through the oily sewage inlet 4, and a concentration signal of the second concentration detector is read by the PLC.
A fourth valve 21 is installed at the washing water inlet 11, and the PLC controls the opening and closing of the fourth valve 21.
A fifth valve 20 is installed on the oil overflow port 5, and the PLC controls the opening and closing of the fifth valve 20.
Further comprising: the PLC drives the alarm module to alarm, and the alarm module can give an audible and visual alarm and display related reasons when giving an alarm.
Vents 26 are formed in the tank walls of both the filtration and regeneration chambers.
A manhole 6, 2 as shown in fig. 1, is formed in the tank body 1.
Example 7
As shown in figure 1, on the basis of embodiment 6, 2 filtering structures are positioned on the same horizontal plane and the 2 filtering structures are connected to form a cylinder, the length of an opening along the radial direction of the tank body 1 is the same as the diameter of the inner wall of the tank body 1, as shown in figure 1, and a first partition plate is shown in figure 5. The shaft 2 passes through the opening and is located at the center line of the opening. The size of the opening in the first partition is the same as the size of the plane on which the filter structure is located.
Example 8
As shown in figure 2, on the basis of the embodiment 6, 2 filtering structures are positioned at different horizontal planes, the length of an opening along the radial direction of the tank body 1 is the same as the radius of the inner wall of the tank body 1, as shown in figure 2, and a first baffle plate is shown in figure 6. Half of the shaft 2 (divided in the radial direction of the shaft 2 to form 2 "shaft halves") passes through the opening. The size of the opening on the first partition board is half of the plane of the side face of the filtering structure.
Example 9
The use method of the integrated equipment for automatically controlling oil-water separation and recycling in the embodiment 5 comprises the following steps:
the PLC is used for controlling the motor 12 to rotate, so that 1 filtering structure is respectively arranged in the filtering chamber and the regeneration chamber, cleaning water is introduced into the regeneration chamber through the cleaning water inlet 11, the liquid level of the cleaning water is higher than that of the filtering structure in the regeneration chamber, and the following filtering steps are repeated:
oily sewage is introduced into the filtering chamber through the oily sewage inlet 4, the oily sewage is filtered into pure water after passing through the filtering structure and is discharged from the pure water outlet 8, when the filtering structure in the filtering chamber needs to be replaced, the PLC control motor 12 rotates 180 degrees by the driving shaft 2, so that the filtering chamber and the regeneration chamber exchange the filtering structure, the filtering structure in the regeneration chamber is soaked by cleaning water, liquid oil in the filtering structure in the regeneration chamber is leached to the liquid level of the cleaning water in the regeneration chamber, and the filtering capacity of the filtering structure is recovered.
Although the second partition plate fixedly arranged in the filter structure can isolate the liquid in the filter chamber and the regeneration chamber, a small amount of purified water still enters the regeneration chamber through the filter material in the filter structure during the rotation of the filter structure, and tests show that the regeneration process of the regeneration chamber is not influenced.
Example 10
On the basis of example 9, when the thickness of the liquid oil on the surface of the washing water in the regeneration chamber increases to the level of the liquid oil reaching the oil overflow port 5, the liquid oil overflows from the oil overflow port 5.
A fifth valve 20 is installed on the oil overflow port 5, and the PLC controls the opening and closing of the fifth valve 20.
A fourth valve 21 is installed on the washing water inlet 11, and when washing water needs to be introduced into the regeneration chamber through the washing water inlet 11, the PLC controls the fourth valve 21 to be opened; when the washing water is stopped to be introduced into the regeneration chamber, the PLC controls the fourth valve 21 to be closed.
The water purification outlet 8 is communicated with a first discharge pipe 25, the oily sewage inlet 4 is communicated with a second discharge pipe 24, one end of a water return pipe 9 is communicated with the water purification outlet 8, the other end of the water return pipe 9 is communicated with the oily sewage inlet 4, a first valve 17 is installed on the first discharge pipe 25, a second valve 18 is installed on the water return pipe 9 close to the water purification outlet 8, a water pump 10 is installed on the water return pipe 9, a third valve 16 is installed on the second discharge pipe 24, a sixth valve 19 is installed on the water return pipe 9 close to the oily sewage inlet 4, the PLC controls the opening and closing of the first valve 17, the third valve 16, the sixth valve 19 and the second valve 18, and the PLC controls the opening and closing of the water pump 10.
In the filtering step, before the oily sewage is introduced into the filtering chamber, the PLC controls the first valve 17 and the third valve 16 to be opened, and the PLC controls the sixth valve 19 and the second valve 18 to be closed (at the moment, the water pump 10 is closed).
Install level sensor in the regeneration chamber of filtration top, a liquid height for detecting the indoor liquid height who washs water of regeneration, level sensor's liquid height signal is read by PLC, set for a critical level value L0 to PLC, critical level value L0 is higher than the indoor filtration of regeneration's height and is less than oil overflow mouth 5, when washing water import 11 to the indoor access of regeneration through wasing water, PLC reads liquid level sensor's liquid height signal once at every interval 0.1 ~ 10s, when the liquid level height of liquid height signal reaches critical level value L0 2 times in succession, PLC control fourth valve 21 closes.
Further comprising: and when the liquid height signal of the liquid level sensor reaches a critical liquid level value L0, the PLC controls the alarm module to alarm.
A first concentration detector is arranged on the purified water outlet 8 and used for detecting the concentration of oil or water in the liquid discharged from the purified water outlet 8, and a concentration signal of the first concentration detector is read by the PLC; and setting a critical concentration C0 to the PLC, and when the oil concentration value obtained after the PLC continuously reads the concentration signal of the first concentration detector for 1-5 times is higher than the oil concentration value of the critical concentration C0, controlling the first valve 17 and the third valve 16 to be closed and the sixth valve 19, the second valve 18 and the water pump 10 to be opened by the PLC, and judging that the filtering structure in the filtering chamber needs to be replaced. The PLC reads the concentration signal of the first concentration detector once every 0.1-30 s. The first valve 17 and the third valve 16 are closed and the sixth valve 19, the second valve 18 and the water pump 10 are opened, so that the liquid passing through the filtering structure can be conveyed back to the upper part of the filtering structure and filtered (i.e. internally circulated) again.
A second concentration detector is arranged on the oily sewage inlet 4 and is used for detecting the concentration of oil or water in the liquid passing through the oily sewage inlet 4, and a concentration signal of the second concentration detector is read by the PLC; and when the oil concentration value obtained after the PLC continuously reads the concentration signal of the second concentration detector for 1-5 times is less than the oil concentration value of the critical concentration C0, the PLC controls the first valve 17 and the third valve 16 to be opened and the sixth valve 19, the second valve 18 and the water pump 10 to be closed. The PLC reads the concentration signal of the second concentration detector once every 0.1-30 s.
The tank walls of the filter chamber and the regeneration chamber are formed with vent holes 26, and before the filtration step, the vent hole 26 of the filter chamber is opened, and before the washing water is introduced into the regeneration chamber, the vent hole 26 of the regeneration chamber is opened.
Install pressure sensor in the filter chamber of filter structure top for detect the pressure in the filter chamber of filter structure top, pressure sensor's pressure signal is read by PLC, sets for a critical pressure P0 to PLC, and when PLC reads pressure value of pressure sensor's pressure signal 1 ~ 5 times in succession and is greater than critical pressure P0, PLC judges that the filter structure in the filter chamber needs to be changed. The PLC reads the pressure signal of the pressure sensor at intervals of 0.1-30.
For an oily sewage treatment example of a certain section of an oil refinery, according to the incoming water condition and the process requirements, firstly setting a critical concentration value C0 through a PLC (programmable logic controller) and setting the critical concentration value C0 to be 5 mg/L; setting the critical pressure P0 at 0.35MPa and the liquid level critical value L0 at 1.0 m; the PLC is set to read the values of the first concentration detector and the second concentration detector every 3 s. Oily sewage is introduced into the filtering chamber through the oily sewage inlet 4, the second concentration detector detects that the oil content of the oily sewage fluctuates within a small range of 46-53 mg/L, the oily sewage becomes clear purified water after passing through the filtering structure, and the first concentration detector detects that the oil content of the purified water passing through the purified water outlet 8 is 1-1.5 mg/L (the detection result fluctuates within a small range of 1-1.5 mg/L). When the PLC reads that the concentration of the first concentration detector is greater than 5.0mg/L for 3 times continuously, the first concentration detector detects that the value is 5.1mg/L after the oil-water separation and recycling integrated equipment is operated for 22 hours continuously, the PLC controls the first valve 17 and the third valve 16 to be closed and the sixth valve 19, the second valve 18 and the water pump 10 to be opened for internal circulation, meanwhile, the PLC controls the motor 12 to rotate 180 degrees through the driving shaft 2, so that the filtering chamber and the regeneration chamber exchange a filtering structure, namely a new filtering structure (a filtering structure which does not adsorb oil) rotates into the filtering chamber, the filtering structure which adsorbs the oil rotates into the regeneration chamber and soaks in the regeneration chamber, and the liquid oil in the filtering structure in the regeneration chamber can be leached to the liquid level of cleaning water in the regeneration chamber through soaking. When the filtering chamber and the regeneration chamber exchange the filtering structure, the second concentration detector quickly detects that the concentration value is less than 5.0 mg/L; when the PLC reads the concentration signal of the second concentration detector for 3 times continuously, the concentration signal is less than 5.0mg/L, the PLC controls the first valve 17 and the third valve 16 to be opened, and the sixth valve 19, the second valve 18 and the water pump 10 to be closed. The process completes an automatic replacement cycle for the oil-water separation and recycling integrated equipment. After the above process was carried out 10 times, 30kg of the regenerated oil was collected from the oil overflow port. In fig. 7, the left bottle contains oily sewage to be inputted to the oily sewage inlet, and the right bottle contains clean water to be discharged from the clean water outlet.
The invention has been described in an illustrative manner, and it is to be understood that any simple variations, modifications or other equivalent changes which can be made by one skilled in the art without departing from the spirit of the invention fall within the scope of the invention.

Claims (10)

1. The utility model provides an integrative equipment of water oil separating resourceization for handling oily sewage which characterized in that includes: jar body (1), axle (2) and 2 filtration be equipped with a first baffle (3) in jar body (1) internal fixation for with jar body (1) internal partitioning becomes 2 spaces: a filter chamber and a regeneration chamber; one end of shaft (2) is fixed with a motor (12), and the other end is followed stretch out after first baffle (3) place plane passes this first baffle (3), axle (2) are in can rotate in first baffle (3), 2 filtration is located respectively in filter chamber and regeneration chamber, wherein first baffle (3) and every be formed with uncovered just on the position that filtration is relative axle (2) are followed uncovered is passed, filtration plug up rather than relative uncovered and with be located this uncovered axle (2) are fixed admittedly, motor (12) drive axle (2) are rotatory, each when axle (2) are rotatory each filtration plug up rather than relative on first baffle (3) uncovered from 1 the space gets into to 1 in addition the space, so that filtration chamber and regeneration chamber respectively are provided with 1 filtration and filtration plug up rather than relative uncovered 1 filtration (ii) a An oily sewage inlet (4) is formed in the tank wall of the filtering chamber above the filtering structure, the filtering structure located in the filtering chamber is used for filtering oily sewage in the filtering chamber, a purified water outlet (8) is formed in the tank wall of the filtering chamber below the filtering structure, an oil overflow port (5) is formed in the tank wall of the regeneration chamber above the filtering structure, and a cleaning water inlet (11) is formed in the tank wall of the regeneration chamber.
2. The integrated equipment for oil-water separation and resource utilization according to claim 1, wherein 2 of the filter structures are perpendicular to the shaft (2); the cross section of the inner wall of the tank body (1) is circular, and the cross section of each filtering structure is semicircular; each said filter structure is a semi-cylinder, said filter structure comprising: an upper filtering sieve plate (14) as the top surface of the semi-cylinder, a lower filtering sieve plate (15) as the bottom surface of the semi-cylinder and a second clapboard (23) positioned on the plane of the side surface of the semi-cylinder, wherein a filtering material (22) is filled between the upper filtering sieve plate (14) and the lower filtering sieve plate (15); the cambered surface of the filtering structure is attached to the inner wall of the tank body (1) close to the cambered surface.
3. The integrated equipment for separating and recycling oil and water as claimed in claim 2, wherein a first filling opening (7) is formed on the wall of the tank body (1) opposite to the filtering structure, a cover body is installed on the first filling opening (7), a second filling opening is formed on the arc surface of the semi-cylinder, and the shaft (2) is rotated until the first filling opening (7) is opposite to the second filling opening, so that the filtering material (22) is filled between the upper filtering sieve plate (14) and the lower filtering sieve plate (15).
4. The oil-water separation and resource utilization integrated equipment as claimed in claim 3, wherein the shaft (2) is vertically arranged on the central point of the cross section of the inner wall of the tank body (1), and the shaft (2) and the second partition plates (23) of the 2 filter structures are fixedly arranged.
5. The oil-water separation and resource utilization integrated equipment as claimed in claim 4, wherein 2 filtering structures are located on the same horizontal plane and the 2 filtering structures are connected to form a cylinder, and the length of the opening along the radial direction of the tank body (1) is the same as the diameter of the inner wall of the tank body (1).
6. The oil-water separation and resource utilization integrated equipment as claimed in claim 4, wherein 2 filtering structures are positioned on different horizontal planes, and the length of the opening along the radial direction of the tank body (1) is the same as the radius of the inner wall of the tank body (1).
7. The integrated oil-water separation and resource utilization device of claim 5 or 6, wherein a liquid level sensor is installed in the regeneration chamber above the filtering structure and used for detecting the liquid level of cleaning water in the regeneration chamber; and a pressure sensor is arranged in the filtering chamber above the filtering structure and used for detecting the pressure in the filtering chamber above the filtering structure.
8. The integrated equipment for oil-water separation and resource utilization according to claim 7, wherein a first concentration detector is installed at the clean water outlet (8) for detecting the concentration of oil or water in the liquid discharged from the clean water outlet (8).
9. The integrated equipment for oil-water separation and resource utilization as claimed in claim 8, wherein the clean water outlet (8) is communicated with a first discharge pipe (25), the oily sewage inlet (4) is communicated with a second discharge pipe (24), one end of a return pipe (9) is communicated with the clean water outlet (8), the other end of the water return pipe (9) is communicated with the oily sewage inlet (4), a first valve (17) is arranged on the first discharge pipe (25), a second valve (18) is arranged on the water return pipe (9) close to the purified water outlet (8), a water pump (10) is arranged on the water return pipe (9), a third valve (16) is arranged on the second discharge pipe (24), and a sixth valve (19) is arranged on the water return pipe (9) close to the oily sewage inlet (4).
10. The integrated equipment for oil-water separation and resource utilization according to claim 9, wherein a second concentration detector is installed on the oily sewage inlet (4) for detecting the concentration of oil or water in the liquid passing through the oily sewage inlet (4); a manhole (6) is formed on the tank body (1); a fourth valve (21) is arranged on the washing water inlet (11); a fifth valve (20) is arranged on the oil overflow port (5); and air vents (26) are formed on the tank walls of the filter chamber and the regeneration chamber.
CN201910765552.4A 2019-08-19 2019-08-19 A integrative equipment of oil-water separation resourceization for handling oily sewage Pending CN112386956A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
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CN112386954A (en) * 2019-08-19 2021-02-23 天津市职业大学 Automatic integrative equipment of separation of water from oil recycling
CN114455669A (en) * 2022-01-13 2022-05-10 上海工程技术大学 Engineering oil removing device based on modified magnetic particles

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CN210933902U (en) * 2019-08-19 2020-07-07 天津市职业大学 Automatic control oil-water separation recycling integrated equipment capable of continuously working
CN112386954A (en) * 2019-08-19 2021-02-23 天津市职业大学 Automatic integrative equipment of separation of water from oil recycling

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CN106745499A (en) * 2015-11-25 2017-05-31 成都德善能科技有限公司 A kind of biconvex dielectric layer sewage disposal oil water separator
CN108187368A (en) * 2018-01-22 2018-06-22 哈尔滨工业大学 A kind of three station-rotary type oily-water seperating equipments and method
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CN112386954A (en) * 2019-08-19 2021-02-23 天津市职业大学 Automatic integrative equipment of separation of water from oil recycling
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CN114455669A (en) * 2022-01-13 2022-05-10 上海工程技术大学 Engineering oil removing device based on modified magnetic particles

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