CN112322302A - Efficient soil remediation improver and preparation method thereof - Google Patents
Efficient soil remediation improver and preparation method thereof Download PDFInfo
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Abstract
The invention discloses an efficient soil remediation improver and a preparation method thereof, belonging to the technical field of soil remediation, and the efficient soil remediation improver comprises the following raw materials in parts by weight: 60-70 parts of sepiolite powder, 15-20 parts of zeolite powder, 5-8 parts of fly ash, 6-9 parts of limestone, 3-7 parts of porphyry, 15-25 parts of organic matters, 5-8 parts of trace element replenisher, 3-5 parts of photosynthetic bacteria, 2-3 parts of bacillus megaterium, 1-2 parts of bacillus subtilis, 1-2 parts of bacillus mucilaginosus and 5-8 parts of bacillus licheniformis; according to the invention, the filtrate, the bacillus licheniformis and the zeolite powder are mixed to obtain the soil remediation and improvement auxiliary liquid, so that the residual microbial bacteria in the filtrate are fully utilized, and the waste of the microbial bacteria is avoided; according to the invention, the soil remediation and improvement auxiliary liquid is applied to the soil, the bacillus licheniformis can effectively inhibit the propagation of harmful bacteria, and then the soil remediation and improvement agent is applied to the soil, so that the propagation of the microbial bacteria is facilitated, the organic matters which are difficult to degrade in the soil are efficiently decomposed, and the fertilizer quality of the soil is improved.
Description
Technical Field
The invention relates to the technical field of soil remediation, in particular to an efficient soil remediation improver and a preparation method thereof.
Background
Soil remediation is a technical measure to restore normal function to contaminated soil. In the soil remediation industry, the existing soil remediation technologies can be more than one hundred, the common technologies can be more than ten, and the existing soil remediation technologies can be roughly divided into three methods, namely physical methods, chemical methods and biological methods. Since the 80 s in the 20 th century, many countries in the world, especially developed countries, have established and developed contaminated soil remediation and remediation programs, thus forming an emerging soil remediation industry.
The soil restoration modifier is a novel biological strain with powder property, and has the characteristics of rapid propagation, strong vitality, safety, no toxicity, high temperature resistance, no inactivation in the granulation and drying processes, long-term storage and the like; contains abundant and high-value active bacteria, and has effect of improving soil structure. The soil conditioner is composed of various probiotics, so that beneficial floras in soil are greatly increased, the diversity of soil microbial communities is restored, the air permeability is enhanced, the soil hardening problem is effectively solved, and the soil micro-ecological environment is improved.
The soil remediation improver mainly comprises the following characteristics: activating soil, improving crop survival, generating active substances such as abundant metabolites and the like, and strongly promoting root growth, root whitening, root growth and capillary root number; forming a protective film, preserving water and fertilizer, enhancing the absorption capacity of the plant root system and fundamentally improving the yield. The soil hardening condition can be effectively improved, the soil is loosened, the soil air permeability is improved, the soil volume weight is reduced, the soil microbial activity is promoted, and the soil fertilizer water permeability is enhanced; improving fertilizer efficiency, reducing cost, and secreting organic acids and other substances to dissolve compounds of calcium, phosphorus, potassium, iron phosphorus, aluminum phosphorus and the like which are not easily absorbed by crops in soil; organic matters which are not easy to decompose in the soil are decomposed, and the utilization rate of the fertilizer can be obviously improved by matching with organic fertilizer; the fertilizer consumption is reduced, and the cost is reduced; bacteriostasis, pest resistance, disease reduction and auxin and multiple enzymes secretion so as to enhance the resistance of crops to certain diseases; also inhibit the growth of other pathogenic bacteria, supplement beneficial bacteria in soil, inhibit the growth and reproduction of harmful bacteria, protect crop root systems, alleviate soil-borne diseases and reduce plant diseases. The quality is improved, the income is increased, the crop quality is improved, the original ecology of the crops is effectively recovered, and the survival rate of the crops is greatly improved.
The soil restoration improver in the prior art is prepared by directly mixing a microbial agent and an organic matter, but the content of the microbial agent loaded by a carrier is low, so that the soil restoration improver is large in dosage and general in effect; moreover, the soil to be improved often has more harmful bacteria, and the harmful bacteria are easy to compete with the microbial bacteria of the soil remediation improver, so that the effect of the soil remediation improver is reduced.
Therefore, a high-efficiency soil remediation improver is provided to solve the above problems.
Disclosure of Invention
The invention aims to provide an efficient soil remediation improver and a preparation method thereof, and aims to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following scheme to realize the following steps: an efficient soil remediation improver comprises the following raw materials in parts by weight: 60-70 parts of sepiolite powder, 15-20 parts of zeolite powder, 5-8 parts of fly ash, 6-9 parts of limestone, 3-7 parts of porphyry, 15-25 parts of organic matters, 5-8 parts of trace element replenisher, 3-5 parts of photosynthetic bacteria, 2-3 parts of bacillus megaterium, 1-2 parts of bacillus subtilis, 1-2 parts of bacillus mucilaginosus and 5-8 parts of bacillus licheniformis.
Preferably, 64-68 parts of sepiolite powder, 16-18 parts of zeolite powder, 6-7 parts of fly ash, 7-8 parts of limestone, 4-6 parts of porphyry, 16-22 parts of organic matters, 6-7 parts of trace element replenisher, 3.5-4.5 parts of photosynthetic bacteria, 2.2-2.8 parts of bacillus megaterium, 1.2-1.8 parts of bacillus subtilis, 1.4-1.6 parts of bacillus mucilaginosus and 6-7.5 parts of bacillus licheniformis.
Preferably, the composite material comprises 65 parts of sepiolite powder, 17 parts of zeolite powder, 6.5 parts of fly ash, 7.5 parts of limestone, 5 parts of porphyry, 20 parts of organic matters, 6.5 parts of trace element replenisher, 4 parts of photosynthetic bacteria, 2.5 parts of bacillus megaterium, 1.5 parts of bacillus subtilis, 1.5 parts of bacillus mucilaginosus and 7 parts of bacillus licheniformis.
Preferably, the organic matter comprises humic acid powder, amino acid powder and straw powder, and the humic acid powder, the amino acid powder and the straw powder are mixed according to the mass ratio of 2:1: 1.
Preferably, the trace supplemental elements include iron chelate, magnesium chelate and copper chelate, and the iron chelate, the magnesium chelate and the copper chelate are mixed in a ratio of 1:2: 1.
Preferably, the content of viable bacteria of the photosynthetic bacteria is 1-3 x 108CFU/ml; the viable bacteria content of the bacillus megaterium is 1-2 multiplied by 108CFU/ml; the viable bacteria content of the bacillus subtilis is 1-4 multiplied by 108CFU/ml; the viable bacteria content of the bacillus mucilaginosus is 1-3 multiplied by 108CFU/ml; the viable bacteria content of the bacillus licheniformis is 1-5 multiplied by 108CFU/ml。
The invention also provides a preparation method of the high-efficiency soil remediation improver, the high-efficiency soil remediation improver comprises a soil remediation and improvement auxiliary liquid and a soil remediation improver, and the preparation method specifically comprises the following steps:
(1) mixing photosynthetic bacteria, bacillus megaterium, bacillus subtilis and bacillus mucilaginosus, adding sepiolite powder into the mixture to obtain a mixed solution, fixing the mixed solution in a shaking table for 2-3 hours, and filtering to obtain a filter body and a filtrate;
(2) putting the filter body, the organic matter, the trace element replenisher and water with the same mass as the organic matter into an electrothermal stirrer, stirring for 25-30min at the rotating speed of 300-500r/min, and keeping the stirring temperature at 30-35 ℃ to obtain a primary soil remediation improver;
(3) placing the primary soil remediation improver into a granulator for granulation to obtain a soil remediation improver;
(4) and (3) putting the zeolite powder, the filtrate and the bacillus licheniformis into a shaking table for fixing for 1-2h to obtain the soil remediation and improvement auxiliary liquid.
Preferably, the rotation speed of the shaking table in the step (1) is 900-.
Preferably, the rotation speed of the shaking table in the step (4) is 600-.
Preferably, the sepiolite powder in the step (1) and the zeolite powder in the step (4) are placed in a muffle furnace in advance, the temperature is kept at 380-420 ℃, the heating is continuously carried out for 4-5h, and the natural cooling is carried out.
The invention has the beneficial effects that:
according to the invention, the sepiolite is heated, so that the loose degree of the sepiolite is good at the temperature of 380-420 ℃, and the specific surface area of the sepiolite is gradually increased to the maximum, thereby being beneficial to increasing the fixed quantity of microorganism bacteria;
the sepiolite, the photosynthetic bacteria, the bacillus megaterium, the bacillus subtilis and the bacillus mucilaginosus are mixed, the sepiolite has a special structure, has zeolite water channels and holes penetrating through the whole structure and a large surface area, has strong adsorption capacity, and is easy to load microbial strains in the holes of the sepiolite;
according to the invention, the zeolite powder is added, the filtrate, the bacillus licheniformis and the zeolite powder are mixed to obtain the soil remediation and improvement auxiliary liquid, and the residual photosynthetic bacteria, bacillus megaterium, bacillus subtilis and bacillus mucilaginosus in the filtrate are fully utilized, so that the residual microbial bacteria are fixed in the zeolite, and the waste of the microbial bacteria is avoided; according to the invention, the soil remediation and improvement auxiliary liquid is applied to the soil, the bacillus licheniformis can effectively inhibit the propagation of harmful bacteria, and then the soil remediation and improvement agent is applied to the soil, so that the competition of the harmful bacteria on photosynthetic bacteria, bacillus megaterium, bacillus subtilis and bacillus mucilaginosus is reduced, the propagation of the microbial bacteria is facilitated, the organic matters which are difficult to degrade in the soil are efficiently decomposed, and the fertilizer quality of the soil is improved;
according to the invention, through a proper raw material proportion and a preparation method, the soil remediation and improvement auxiliary liquid and the soil remediation and improvement agent are respectively applied in front and at the back, and the soil improvement effect is obvious.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
An efficient soil remediation improver comprises the following raw materials in parts by weight: 65 parts of sepiolite powder, 18 parts of zeolite powder, 16 parts of organic matters, 5 parts of fly ash, 6 parts of limestone, 3 parts of porphyry, 5 parts of trace element replenisher, 3 parts of photosynthetic bacteria, 2 parts of bacillus megaterium, 1.5 parts of bacillus subtilis, 1 part of bacillus mucilaginosus and 5 parts of bacillus licheniformis.
The organic matter comprises humic acid powder, amino acid powder and straw powder, and the humic acid powder, the amino acid powder and the straw powder are mixed according to the mass ratio of 2:1: 1; the trace supplementary elements comprise chelated iron, chelated magnesium and chelated copper, and the chelated iron, the chelated magnesium and the chelated copper are mixed according to a ratio of 1:2: 1;
the content of viable bacteria of photosynthetic bacteria is 1-3 × 108CFU/ml; the viable bacteria content of Bacillus megaterium is 1-2 × 108CFU/ml; the viable bacteria content of Bacillus subtilis is 1-4 × 108CFU/ml; the viable bacteria content of Bacillus mucilaginosus is 1-3 × 108CFU/ml; the viable bacteria content of Bacillus licheniformis is 1-5 × 108CFU/ml。
The preparation method of the high-efficiency soil remediation improver comprises a soil remediation and improvement auxiliary solution and a soil remediation improver, and specifically comprises the following steps:
(1) mixing photosynthetic bacteria, bacillus megaterium, bacillus subtilis and bacillus mucilaginosus, adding sepiolite powder into the mixture to obtain a mixed solution, fixing the mixed solution in a shaking table for 2.5 hours, keeping the rotation speed of the shaking table at 900r/min, keeping the temperature at 30 ℃, and filtering to obtain a filter body and a filtrate;
(2) putting the filter body, the organic matters, the microelement replenisher, the fly ash, the limestone, the porphyry, the organic matters and other mass water into an electrothermal stirrer, stirring for 25min at a rotating speed of 330r/min, and keeping the stirring temperature at 32 ℃ to obtain a primary soil remediation improver;
(3) placing the primary soil remediation improver into a granulator for granulation to obtain a soil remediation improver;
(4) and (3) putting the zeolite powder, the filtrate and the bacillus licheniformis into a shaking table, fixing for 1.2h, wherein the rotation speed of the shaking table is 600r/min, and keeping the temperature at 35 ℃ to obtain the soil remediation and improvement auxiliary liquid.
Putting the sepiolite powder in the step (1) and the zeolite powder in the step (4) in a muffle furnace in advance, keeping the temperature at 380 ℃, continuously heating for 4h, and naturally cooling.
In this example, the soil remediation and improvement auxiliary solution was applied first, and then the soil remediation and improvement agent was applied.
Example 2
An efficient soil remediation improver comprises the following raw materials in parts by weight: 63 parts of sepiolite powder, 16 parts of zeolite powder, 6 parts of fly ash, 7 parts of limestone, 4 parts of porphyry, 15 parts of organic matters, 6 parts of trace element replenisher, 3.5 parts of photosynthetic bacteria, 2.2 parts of bacillus megaterium, 1.2 parts of bacillus subtilis, 1.4 parts of bacillus mucilaginosus and 5 parts of bacillus licheniformis.
The organic matter comprises humic acid powder, amino acid powder and straw powder, and the humic acid powder, the amino acid powder and the straw powder are mixed according to the mass ratio of 2:1: 1; the trace supplementary elements comprise chelated iron, chelated magnesium and chelated copper, and the chelated iron, the chelated magnesium and the chelated copper are mixed according to a ratio of 1:2: 1;
the content of viable bacteria of photosynthetic bacteria is 1-3 × 108CFU/ml; the viable bacteria content of Bacillus megaterium is 1-2 × 108CFU/ml; the viable bacteria content of Bacillus subtilis is 1-4 × 108CFU/ml; the viable bacteria content of Bacillus mucilaginosus is 1-3 × 108CFU/ml; the viable bacteria content of Bacillus licheniformis is 1-5 × 108CFU/ml。
The preparation method of the high-efficiency soil remediation improver comprises a soil remediation and improvement auxiliary solution and a soil remediation improver, and specifically comprises the following steps:
(1) mixing photosynthetic bacteria, bacillus megaterium, bacillus subtilis and bacillus mucilaginosus, adding sepiolite powder into the mixture to obtain a mixed solution, fixing the mixed solution in a shaking table for 2 hours, keeping the rotation speed of the shaking table at 950r/min, keeping the temperature at 33 ℃, and filtering to obtain a filter body and a filtrate;
(2) putting the filter body, the organic matters, the microelement replenisher, the fly ash, the limestone, the porphyry, the organic matters and other mass water into an electrothermal stirrer, stirring for 28min at the rotating speed of 400r/min, and keeping the stirring temperature at 32 ℃ to obtain a primary soil remediation improver;
(3) placing the primary soil remediation improver into a granulator for granulation to obtain a soil remediation improver;
(4) and (3) putting the zeolite powder, the filtrate and the bacillus licheniformis into a shaking table, fixing for 1h, keeping the rotation speed of the shaking table at 650r/min and the temperature at 38 ℃ to obtain the soil remediation and improvement auxiliary liquid.
Putting the sepiolite powder in the step (1) and the zeolite powder in the step (4) in a muffle furnace in advance, keeping the temperature at 400 ℃, continuously heating for 4.2h, and naturally cooling.
In this example, the soil remediation and improvement auxiliary solution was applied first, and then the soil remediation and improvement agent was applied.
Example 3
An efficient soil remediation improver comprises the following raw materials in parts by weight: 65 parts of sepiolite powder, 17 parts of zeolite powder, 6.5 parts of fly ash, 7.5 parts of limestone, 5 parts of porphyry, 20 parts of organic matters, 6.5 parts of trace element replenisher, 4 parts of photosynthetic bacteria, 2.5 parts of bacillus megaterium, 1.5 parts of bacillus subtilis, 1.5 parts of bacillus mucilaginosus and 7 parts of bacillus licheniformis.
The organic matter comprises humic acid powder, amino acid powder and straw powder, and the humic acid powder, the amino acid powder and the straw powder are mixed according to the mass ratio of 2:1: 1; the trace supplementary elements comprise chelated iron, chelated magnesium and chelated copper, and the chelated iron, the chelated magnesium and the chelated copper are mixed according to a ratio of 1:2: 1;
the content of viable bacteria of photosynthetic bacteria is 1-3 × 108CFU/ml; the viable bacteria content of Bacillus megaterium is 1-2 × 108CFU/ml; the viable bacteria content of Bacillus subtilis is 1-4 × 108CFU/ml; the viable bacteria content of Bacillus mucilaginosus is 1-3 × 108CFU/ml; the viable bacteria content of Bacillus licheniformis is 1-5 × 108CFU/ml。
The preparation method of the high-efficiency soil remediation improver comprises a soil remediation and improvement auxiliary solution and a soil remediation improver, and specifically comprises the following steps:
(1) mixing photosynthetic bacteria, bacillus megaterium, bacillus subtilis and bacillus mucilaginosus, adding sepiolite powder into the mixture to obtain a mixed solution, fixing the mixed solution in a shaking table for 2 hours, keeping the rotation speed of the shaking table at 950r/min, keeping the temperature at 33 ℃, and filtering to obtain a filter body and a filtrate;
(2) putting the filter body, the organic matters, the microelement replenisher, the fly ash, the limestone, the porphyry, the organic matters and other mass water into an electrothermal stirrer, stirring for 28min at the rotating speed of 300r/min, and keeping the stirring temperature at 30 ℃ to obtain a primary soil remediation improver;
(3) placing the primary soil remediation improver into a granulator for granulation to obtain a soil remediation improver;
(4) and (3) putting the zeolite powder, the filtrate and the bacillus licheniformis into a shaking table, fixing for 1.3h, wherein the rotation speed of the shaking table is 700r/min, and keeping the temperature at 38 ℃ to obtain the soil remediation and improvement auxiliary liquid.
Putting the sepiolite powder in the step (1) and the zeolite powder in the step (4) in a muffle furnace in advance, keeping the temperature at 400 ℃, continuously heating for 4.5h, and naturally cooling.
In this example, the soil remediation and improvement auxiliary solution was applied first, and then the soil remediation and improvement agent was applied.
Example 4
An efficient soil remediation improver comprises the following raw materials in parts by weight: 68 parts of sepiolite powder, 18 parts of zeolite powder, 8 parts of fly ash, 9 parts of limestone, 7 parts of porphyry, 22 parts of organic matters, 7 parts of trace element replenisher, 4.5 parts of photosynthetic bacteria, 2.5 parts of bacillus megaterium, 1.5 parts of bacillus subtilis, 1.5 parts of bacillus mucilaginosus and 7.5 parts of bacillus licheniformis.
The organic matter comprises humic acid powder, amino acid powder and straw powder, and the humic acid powder, the amino acid powder and the straw powder are mixed according to the mass ratio of 2:1: 1; the trace supplementary elements comprise chelated iron, chelated magnesium and chelated copper, and the chelated iron, the chelated magnesium and the chelated copper are mixed according to a ratio of 1:2: 1;
the content of viable bacteria of photosynthetic bacteria is 1-3 × 108CFU/ml; the viable bacteria content of Bacillus megaterium is 1-2 × 108CFU/ml; the viable bacteria content of Bacillus subtilis is 1-4 × 108CFU/ml; the viable bacteria content of Bacillus mucilaginosus is 1-3 × 108CFU/ml; the viable bacteria content of Bacillus licheniformis is 1-5 × 108CFU/ml。
The preparation method of the high-efficiency soil remediation improver comprises a soil remediation and improvement auxiliary solution and a soil remediation improver, and specifically comprises the following steps:
(1) mixing photosynthetic bacteria, bacillus megaterium, bacillus subtilis and bacillus mucilaginosus, adding sepiolite powder into the mixture to obtain a mixed solution, fixing the mixed solution in a shaking table for 2.6 hours, keeping the rotation speed of the shaking table at 980r/min, keeping the temperature at 33 ℃, and filtering to obtain a filter body and a filtrate;
(2) putting the filter body, the organic matters, the microelement replenisher, the fly ash, the limestone, the porphyry, the organic matters and other mass water into an electrothermal stirrer, stirring for 28min at the rotating speed of 500r/min, and keeping the stirring temperature at 35 ℃ to obtain a primary soil remediation improver;
(3) placing the primary soil remediation improver into a granulator for granulation to obtain a soil remediation improver;
(4) and (3) putting the zeolite powder, the filtrate and the bacillus licheniformis into a shaking table, fixing for 2h, wherein the rotation speed of the shaking table is 750r/min, and keeping the temperature at 38 ℃ to obtain the soil remediation and improvement auxiliary liquid.
Putting the sepiolite powder in the step (1) and the zeolite powder in the step (4) in a muffle furnace in advance, keeping the temperature at 400 ℃, continuously heating for 4.8h, and naturally cooling.
In this example, the soil remediation and improvement auxiliary solution was applied first, and then the soil remediation and improvement agent was applied.
Example 5
An efficient soil remediation improver comprises the following raw materials in parts by weight: 70 parts of sepiolite powder, 20 parts of zeolite powder, 18 parts of zeolite powder, 7 parts of fly ash, 8 parts of limestone, 6 parts of porphyria, 25 parts of organic matters, 8 parts of trace element replenisher, 5 parts of photosynthetic bacteria, 3 parts of bacillus megaterium, 2 parts of bacillus subtilis, 2 parts of bacillus mucilaginosus and 8 parts of bacillus licheniformis.
The organic matter comprises humic acid powder, amino acid powder and straw powder, and the humic acid powder, the amino acid powder and the straw powder are mixed according to the mass ratio of 2:1: 1; the trace supplementary elements comprise chelated iron, chelated magnesium and chelated copper, and the chelated iron, the chelated magnesium and the chelated copper are mixed according to a ratio of 1:2: 1;
the content of viable bacteria of photosynthetic bacteria is 1-3 × 108CFU/ml; the viable bacteria content of Bacillus megaterium is 1-2 × 108CFU/ml;The viable bacteria content of Bacillus subtilis is 1-4 × 108CFU/ml; the viable bacteria content of Bacillus mucilaginosus is 1-3 × 108CFU/ml; the viable bacteria content of Bacillus licheniformis is 1-5 × 108CFU/ml。
The preparation method of the high-efficiency soil remediation improver comprises a soil remediation and improvement auxiliary solution and a soil remediation improver, and specifically comprises the following steps:
(1) mixing photosynthetic bacteria, bacillus megaterium, bacillus subtilis and bacillus mucilaginosus, adding sepiolite powder into the mixture to obtain a mixed solution, fixing the mixed solution in a shaking table for 3 hours, keeping the rotation speed of the shaking table at 1000r/min, keeping the temperature at 35 ℃, and filtering to obtain a filter body and a filtrate;
(2) putting the filter body, the organic matters, the microelement replenisher, the fly ash, the limestone, the porphyry, the organic matters and other mass water into an electrothermal stirrer, stirring for 28min at the rotating speed of 450r/min, and keeping the stirring temperature at 32 ℃ to obtain a primary soil remediation improver;
(3) placing the primary soil remediation improver into a granulator for granulation to obtain a soil remediation improver;
(4) and (3) putting the zeolite powder, the filtrate and the bacillus licheniformis into a shaking table, fixing for 1.8h, wherein the rotation speed of the shaking table is 800r/min, and keeping the temperature at 40 ℃ to obtain the soil remediation and improvement auxiliary liquid.
Putting the sepiolite powder in the step (1) and the zeolite powder in the step (4) in a muffle furnace in advance, keeping the temperature at 420 ℃, continuously heating for 5h, and naturally cooling.
In this example, the soil remediation and improvement auxiliary solution was applied first, and then the soil remediation and improvement agent was applied.
Comparative example
An efficient soil remediation improver comprises the following raw materials in parts by weight: 65 parts of sepiolite powder, 6.5 parts of fly ash, 7.5 parts of limestone, 5 parts of porphyry, 20 parts of organic matters, 6.5 parts of trace element replenisher, 4 parts of photosynthetic bacteria, 2.5 parts of bacillus megaterium, 1.5 parts of bacillus subtilis, 1.5 parts of bacillus mucilaginosus and 7 parts of bacillus licheniformis.
The organic matter comprises humic acid powder, amino acid powder and straw powder, and the humic acid powder, the amino acid powder and the straw powder are mixed according to the mass ratio of 2:1: 1; the trace supplementary elements comprise chelated iron, chelated magnesium and chelated copper, and the chelated iron, the chelated magnesium and the chelated copper are mixed according to a ratio of 1:2: 1;
the content of viable bacteria of photosynthetic bacteria is 1-3 × 108CFU/ml; the viable bacteria content of Bacillus megaterium is 1-2 × 108CFU/ml; the viable bacteria content of Bacillus subtilis is 1-4 × 108CFU/ml; the viable bacteria content of Bacillus mucilaginosus is 1-3 × 108CFU/ml; the viable bacteria content of Bacillus licheniformis is 1-5 × 108CFU/ml。
The preparation method of the high-efficiency soil remediation improver specifically comprises the following steps:
(1) mixing photosynthetic bacteria, bacillus megaterium, bacillus subtilis, bacillus mucilaginosus and bacillus licheniformis, adding sepiolite powder into the mixture to obtain a mixed solution, placing the mixed solution into a shaking table to be fixed for 2 hours, keeping the rotation speed of the shaking table at 950r/min, keeping the temperature at 33 ℃, and filtering to obtain a filter body;
(2) putting the filter body, the organic matters, the microelement replenisher, the fly ash, the limestone, the porphyry, the organic matters and other mass water into an electrothermal stirrer, stirring for 28min at the rotating speed of 300r/min, and keeping the stirring temperature at 30 ℃ to obtain a primary soil remediation improver;
(3) and (4) putting the primary soil remediation improver into a granulator for granulation to obtain the soil remediation improver.
And (2) putting the sepiolite powder in the step (1) in a muffle furnace in advance, keeping the temperature at 400 ℃, continuously heating for 4.5h, and naturally cooling.
The present comparative example is based on example 3, and the zeolite powder and the filtrate are discarded, and the bacillus licheniformis is directly mixed with the sepiolite powder, and the soil remediation improver of the comparative example is applied to the soil.
Result detection
1. The test method comprises the following steps: selecting soil with soil heavy metals exceeding the standard for planting rice in the past year, dividing into 7 blocks, and normally applying fertilizers, wherein 5 blocks adopt the soil repair improvement auxiliary liquid and the soil repair amendment in the embodiments 1-5, the total amount of the soil repair improvement auxiliary liquid and the soil repair amendment is applied according to 80kg per mu, and the soil repair improvement auxiliary liquid accounts for 10 kg; one of the soil remediation conditioners is applied by 80kg per mu by adopting the soil remediation conditioner in the comparative example; the other block is only applied with common fertilizer (nitrogen-potassium compound fertilizer), the fertilizing amount and the management measures of each group are the same, and the yield increase rate is calculated by taking the rice yield with the same area in the past year as a reference. Specific detection results are shown in table 1.
TABLE 1 yield increase
Group of | Rice yield increase/% |
Example 1 | 17.8 |
Example 2 | 17.3 |
Example 3 | 18.5 |
Example 4 | 18.4 |
Example 5 | 17.9 |
Comparative example | 15.9 |
Control group | 0.9 |
2. The test method comprises the following steps: selecting 7 land plots polluted by heavy metal, detecting that the average value of the total arsenic content of 7 land plots is 180mg/kg, the average value of the total chromium content is 520mg/kg, the average value of the total mercury content is 15mg/kg, and a control group is not treated, wherein 5 land plots adopt the soil remediation and improvement auxiliary liquid and the soil remediation improver in the embodiments 1-5, the total amount of the soil remediation and improvement auxiliary liquid and the soil remediation improver is broadcast according to 80kg per mu, the soil remediation and improvement auxiliary liquid accounts for 10kg, the remaining land plot adopts the soil remediation improver in the comparative example, the soil remediation improver is broadcast according to 80kg per mu, and the total arsenic, total chromium and total mercury content of 7 soil plots are sampled and analyzed after one year. Specific detection results are shown in table 2.
TABLE 2 heavy metal content
In summary, as can be seen from table 1, the average yield increase rate of the rice in examples 1 to 5 reaches 17.98%, and the yield increase rate of the rice in the comparative example reaches 15.9%, which indicates that the soil remediation improver is obviously improved on the soil, meanwhile, the comparative example only applies the soil remediation improver, and the example applies the soil remediation improver after applying the soil remediation improver auxiliary solution on the soil in advance, which is improved by 2.08% compared with the comparative example, which indicates that the application of the soil remediation auxiliary solution is beneficial to the propagation of beneficial microorganisms, efficiently decomposes the refractory organic matters in the soil, and improves the fertilizer quality of the soil;
as can be seen from Table 2, the soil remediation improver has a high heavy metal removal rate, and can further improve the heavy metal removal rate by being supplemented with the soil remediation improver auxiliary liquid, so that the soil improvement effect is good.
In the description herein, references to the description of "one embodiment," "an example," "a specific example" or the like are intended to mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the invention. In this specification, the schematic representations of the terms used above do not necessarily refer to the same embodiment or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.
The preferred embodiments of the invention disclosed above are intended to be illustrative only. The preferred embodiments are not exhaustive and do not limit the method of making a high strength caliper seal to the specific embodiments described. Obviously, many modifications and variations are possible in light of the above teaching. The embodiments were chosen and described in order to best explain the principles of the invention and the practical application, to thereby enable others skilled in the art to best utilize the invention. The invention is limited only by the claims and their full scope and equivalents.
Claims (10)
1. The efficient soil remediation improver is characterized by comprising the following raw materials in parts by weight: 60-70 parts of sepiolite powder, 15-20 parts of zeolite powder, 5-8 parts of fly ash, 6-9 parts of limestone, 3-7 parts of porphyry, 15-25 parts of organic matters, 5-8 parts of trace element replenisher, 3-5 parts of photosynthetic bacteria, 2-3 parts of bacillus megaterium, 1-2 parts of bacillus subtilis, 1-2 parts of bacillus mucilaginosus and 5-8 parts of bacillus licheniformis.
2. The efficient soil remediation improver as claimed in claim 1, wherein the efficient soil remediation improver comprises 64-68 parts of sepiolite powder, 16-18 parts of zeolite powder, 6-7 parts of fly ash, 7-8 parts of limestone, 4-6 parts of porphyria, 16-22 parts of organic matters, 6-7 parts of trace element supplements, 3.5-4.5 parts of photosynthetic bacteria, 2.2-2.8 parts of bacillus megaterium, 1.2-1.8 parts of bacillus subtilis, 1.4-1.6 parts of bacillus mucilaginosus and 6-7.5 parts of bacillus licheniformis.
3. The high-efficiency soil remediation improver as claimed in claim 2, wherein the improver comprises 65 parts of sepiolite powder, 17 parts of zeolite powder, 6.5 parts of fly ash, 7.5 parts of limestone, 5 parts of porphyria, 20 parts of organic matter, 6.5 parts of a trace element supplement, 4 parts of photosynthetic bacteria, 2.5 parts of bacillus megaterium, 1.5 parts of bacillus subtilis, 1.5 parts of bacillus mucilaginosus and 7 parts of bacillus licheniformis.
4. The efficient soil remediation improver as claimed in claim 1, wherein the organic matter comprises humic acid powder, amino acid powder and straw powder, and the humic acid powder, the amino acid powder and the straw powder are mixed in a mass ratio of 2:1: 1.
5. The high-efficiency soil remediation improver according to claim 1, wherein the trace supplemental elements comprise iron chelate, magnesium chelate and copper chelate, and the iron chelate, the magnesium chelate and the copper chelate are mixed in a ratio of 1:2: 1.
6. The high-efficiency soil remediation improver as claimed in claim 1, wherein the viable bacteria content of the photosynthetic bacteria is 1-3 x 108CFU/ml; the viable bacteria content of the bacillus megaterium is 1-2 multiplied by 108CFU/ml; the viable bacteria content of the bacillus subtilis is 1-4 multiplied by 108CFU/ml; the viable bacteria content of the bacillus mucilaginosus is 1-3 multiplied by 108CFU/ml; the viable bacteria content of the bacillus licheniformis is 1-5 multiplied by 108CFU/ml。
7. The preparation method of the high-efficiency soil remediation improver as claimed in any one of claims 1 to 6, wherein the high-efficiency soil remediation improver comprises a soil remediation and improvement auxiliary liquid and a soil remediation improver, and the preparation method comprises the following steps:
(1) mixing photosynthetic bacteria, bacillus megaterium, bacillus subtilis and bacillus mucilaginosus, adding sepiolite powder into the mixture to obtain a mixed solution, fixing the mixed solution in a shaking table for 2-3 hours, and filtering to obtain a filter body and a filtrate;
(2) putting the filter body, the organic matters, the microelement replenisher, the fly ash, the limestone, the bentonite, the organic matters and other mass water into an electrothermal stirrer, stirring for 25-30min at the rotating speed of 300-;
(3) placing the primary soil remediation improver into a granulator for granulation to obtain a soil remediation improver;
(4) and (3) putting the zeolite powder, the filtrate and the bacillus licheniformis into a shaking table for fixing for 1-2h to obtain the soil remediation and improvement auxiliary liquid.
8. The method for preparing a high efficiency soil remediation improver as claimed in claim 7, wherein the rotation speed of the rocking platforms in step (1) is 900-.
9. The method for preparing a high efficiency soil remediation improver as claimed in claim 7, wherein the rotation speed of the rocking platforms in step (4) is 600-800r/min, and the temperature is maintained at 35-40 ℃.
10. The method for preparing a high efficiency soil remediation improver as claimed in claim 7, wherein the sepiolite powder in step (1) and the zeolite powder in step (4) are placed in a muffle furnace in advance, kept at a temperature of 380 ℃ and 420 ℃, heated for 4-5h and naturally cooled.
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