CN112246201A - Double-beam double-channel photo-thermal catalytic reaction equipment - Google Patents
Double-beam double-channel photo-thermal catalytic reaction equipment Download PDFInfo
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- CN112246201A CN112246201A CN202010992241.4A CN202010992241A CN112246201A CN 112246201 A CN112246201 A CN 112246201A CN 202010992241 A CN202010992241 A CN 202010992241A CN 112246201 A CN112246201 A CN 112246201A
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- 238000006555 catalytic reaction Methods 0.000 title claims abstract description 23
- 239000010453 quartz Substances 0.000 claims abstract description 43
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 43
- 229910000831 Steel Inorganic materials 0.000 claims abstract description 38
- 239000010959 steel Substances 0.000 claims abstract description 38
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 21
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 21
- 239000001301 oxygen Substances 0.000 claims abstract description 21
- 239000012528 membrane Substances 0.000 claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 238000001816 cooling Methods 0.000 claims description 4
- 229910052736 halogen Inorganic materials 0.000 claims description 3
- 150000002367 halogens Chemical class 0.000 claims description 3
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 claims description 3
- 229910052753 mercury Inorganic materials 0.000 claims description 3
- 229910052724 xenon Inorganic materials 0.000 claims description 3
- FHNFHKCVQCLJFQ-UHFFFAOYSA-N xenon atom Chemical compound [Xe] FHNFHKCVQCLJFQ-UHFFFAOYSA-N 0.000 claims description 3
- 239000007789 gas Substances 0.000 claims 5
- 229910052684 Cerium Inorganic materials 0.000 claims 1
- GWXLDORMOJMVQZ-UHFFFAOYSA-N cerium Chemical compound [Ce] GWXLDORMOJMVQZ-UHFFFAOYSA-N 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 abstract description 25
- 238000000926 separation method Methods 0.000 abstract description 10
- 238000012546 transfer Methods 0.000 abstract description 5
- 230000002195 synergetic effect Effects 0.000 abstract description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 3
- 230000003197 catalytic effect Effects 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 230000001699 photocatalysis Effects 0.000 description 3
- 230000008901 benefit Effects 0.000 description 2
- 229910000420 cerium oxide Inorganic materials 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- BMMGVYCKOGBVEV-UHFFFAOYSA-N oxo(oxoceriooxy)cerium Chemical compound [Ce]=O.O=[Ce]=O BMMGVYCKOGBVEV-UHFFFAOYSA-N 0.000 description 2
- 230000032683 aging Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 230000019771 cognition Effects 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 230000005281 excited state Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 230000002779 inactivation Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 230000037361 pathway Effects 0.000 description 1
- 230000029553 photosynthesis Effects 0.000 description 1
- 238000010672 photosynthesis Methods 0.000 description 1
- 231100000572 poisoning Toxicity 0.000 description 1
- 230000000607 poisoning effect Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
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- 239000000126 substance Substances 0.000 description 1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
- B01J19/122—Incoherent waves
- B01J19/123—Ultra-violet light
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
- B01J19/122—Incoherent waves
- B01J19/127—Sunlight; Visible light
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
- B01J19/122—Incoherent waves
- B01J19/128—Infra-red light
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/32—Packing elements in the form of grids or built-up elements for forming a unit or module inside the apparatus for mass or heat transfer
Abstract
The invention discloses a double-beam double-channel photo-thermal catalytic reaction device, which comprises: the device comprises two light source parts, a steel connecting pipe and two quartz window modules; the steel connecting pipe is arranged between the two quartz window modules, and the two light source parts are respectively arranged at two sides of the two quartz window modules; the quartz window module comprises a flange joint, a quartz window plate and a plano-convex focusing mirror, the plano-convex focusing mirror is arranged in the quartz window plate, the quartz window plate is arranged in the flange joint, the flange joint is connected with the end part of the steel connecting pipe, and an oxygen carrier film is arranged in the end part of the steel connecting pipe. The invention provides double-beam double-channel photo-thermal catalytic reaction equipment which mainly comprises two light source parts, a steel connecting pipe and two quartz window modules, wherein an oxygen carrier film has oxygen transfer capacity under the irradiation of the light source parts, double reactions can be carried out in the steel connecting pipe, photo-thermal synergistic complete reactions are realized, the product separation is simple, and the separation cost is effectively reduced.
Description
Technical Field
The invention relates to the technical field of photo-thermal reaction equipment, in particular to double-beam double-channel photo-thermal catalytic reaction equipment.
Background
The study of the excited state of electrons has been promoted by the human cognition and utilization of light, and the depth and breadth of understanding of substances have been gradually increased with the introduction of new concepts and theories regarding light. Understanding the photosynthesis in nature provides an important foundation for solar energy utilization, environmental protection, the creation of new reaction pathways, and the search for new materials, and plays an increasingly important role in high-tech fields such as new energy, new materials, new information, and the like. The application of the photo-thermal catalytic system plays an important supporting role in the development of photochemistry. The photothermal catalysis method has the most important function of improving the catalysis efficiency, promoting the reaction under various experimental conditions, and improving the production rate, so that the production efficiency and the benefit are improved.
At present, most of photo-thermal catalytic devices are single-channel reactions, and photo-thermal driving reactions are utilized for carrying out. For example, patent ZL201620142695.1 belongs to a full-automatic photocatalytic activity evaluation system, and can perform on-line testing and be used in combination with a glass reaction bottle or a reaction kettle. Patent 201610144691.1, a fiber optic photocatalytic reactor and method for converting CO2 to methanol, enhances photocatalytic CO2 reduction by increasing catalyst light utilization efficiency, improving the reactor. Although the photothermal catalysis mode improves the conversion rate, for some specific application reactions, such as a hydrogen atmosphere CO oxidation reaction, the electrode in the proton exchange membrane of the hydrogen fuel cell is very sensitive to CO, and the electrode is very easy to generate CO poisoning to cause inactivation, so that the CO removal under the hydrogen atmosphere is necessary, but the introduction of oxygen for oxidation by oxygen increases the subsequent separation and removal cost, and the patent devices have application limitations. If continuous sample injection is adopted, the problem of high separation cost is caused because the reaction is incomplete and the product is difficult to separate. Therefore, it is necessary to provide a device with photothermal catalytic effect and simultaneously realize the simultaneous performance of dual-light-speed and dual-channel reaction.
Disclosure of Invention
In this summary, concepts in a simplified form are introduced that are further described in the detailed description. This summary of the invention is not intended to identify key features or essential features of the claimed subject matter, nor is it intended to be used as an aid in determining the scope of the claimed subject matter.
To at least partially solve the above problems, the present invention provides a dual-beam dual-channel photothermal catalytic reaction apparatus comprising:
the device comprises two light source parts, a steel connecting pipe and two quartz window modules;
the steel connecting pipe is arranged between the two quartz window modules, and the two light source parts are respectively arranged on two sides of the two quartz window modules;
the quartz window module comprises a flange joint, a quartz window plate and a plano-convex focusing mirror, wherein the plano-convex focusing mirror is arranged in the quartz window plate, the quartz window plate is arranged in the flange joint, the flange joint is connected with the end part of the steel connecting pipe, and an oxygen carrier film is arranged in the end part of the steel connecting pipe.
Preferably, the steel connecting pipe is provided with a plurality of air inlet heads and a plurality of air outlet heads, and the air inlet heads and the air outlet heads are both connected with an air path.
Preferably, wherein the steel connection pipe may be connected to the quartz window module by a snap.
Preferably, the steel connecting pipe is connected with a water cooling device.
Preferably, the light source unit is a xenon lamp light source, a mercury lamp light source, a laser, or a halogen lamp.
Preferably, the light source of the light source unit is one of parallel light, convergent light, ultraviolet light, visible light, and infrared light.
Preferably, wherein the oxygen support membrane comprises a cerium oxide support membrane or a perovskite support membrane.
Compared with the prior art, the invention at least comprises the following beneficial effects:
the invention provides double-beam double-channel photo-thermal catalytic reaction equipment which mainly comprises two light source parts, a steel connecting pipe and two quartz window modules, wherein an oxygen carrier film has oxygen transfer capacity under the irradiation of the light source parts, double reactions can be carried out in the steel connecting pipe, photo-thermal synergistic complete reactions are realized, the product separation is simple, and the separation cost is effectively reduced.
Additional advantages, objects, and features of the dual-beam, dual-channel photothermal catalytic reaction apparatus of the present invention will be set forth in part in the description which follows and in part will become apparent to those having ordinary skill in the art upon examination of the following or may be learned from practice of the invention.
Drawings
The accompanying drawings, which are included to provide a further understanding of the invention and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention and together with the description serve to explain the principles of the invention and not to limit the invention. In the drawings:
fig. 1 is a schematic structural view of a dual-beam dual-channel photothermal catalytic reaction apparatus according to the present invention.
Detailed Description
The present invention is further described in detail below with reference to the drawings and examples so that those skilled in the art can practice the invention with reference to the description.
It will be understood that terms such as "having," "including," and "comprising," as used herein, do not preclude the presence or addition of one or more other elements or groups thereof.
As shown in fig. 1, the present invention provides a dual-beam dual-channel photo-thermal catalytic reaction apparatus, comprising:
the two light source parts 1, the steel connecting pipe B and the two quartz window modules;
the steel connecting pipe B is arranged between the two quartz window modules, and the two light source parts 1 are respectively arranged at two sides of the two quartz window modules;
the quartz window module comprises a flange joint 4, a quartz window plate 5 and a plano-convex focusing mirror 6, wherein the plano-convex focusing mirror 6 is arranged in the quartz window plate 5, the quartz window plate 5 is arranged in the flange joint 4, the flange joint 4 is connected with the end part of the steel connecting pipe B, and an oxygen carrier film (not shown) is arranged in the end part of the steel connecting pipe B.
The working principle of the technical scheme is as follows: the invention provides double-beam double-channel photo-thermal catalytic reaction equipment which mainly comprises two light source parts 1, a steel connecting pipe B and two quartz window modules, wherein the two quartz window modules are divided into a quartz window module A1 at the left end and a quartz window module A2 at the right end; specifically, each of the quartz window modules a1 and a2 includes a flange joint 4, a quartz window plate 5, and a plano-convex focusing mirror 6, and the light source unit 1 is irradiated onto the oxygen carrier film through the quartz window plate 5 and the convex focusing mirror 6.
When the double-beam-channel thermocatalytic reaction device is used for reaction, the light source part 1 irradiates an oxygen carrier membrane through the plano-convex focusing lens 6, and the oxygen carrier membrane has oxygen transfer capacity under the irradiation of the light source part 1 and can perform double reaction inside the steel connecting pipe B; wherein, flange joint 4 has still designed first thermocouple e, second thermocouple f, and first thermocouple e, second thermocouple f are used for detecting the reaction temperature on the oxygen carrier membrane, are convenient for carry out temperature regulation and control.
The beneficial effects of the above technical scheme are that: through the design of the structure, the invention provides double-beam double-channel photo-thermal catalytic reaction equipment which mainly comprises two light source parts 1, a steel connecting pipe B and two quartz window modules, wherein an oxygen carrier film has oxygen transfer capacity under the irradiation of the light source parts 1, double reactions can be carried out inside the steel connecting pipe B, photo-thermal synergetic complete reactions are realized, the product separation is simple, and the separation cost is effectively reduced.
Furthermore, the steel connecting pipe is provided with a plurality of air inlet heads and a plurality of air outlet heads, and the air inlet heads and the air outlet heads are connected with an air path. The air inlets are respectively a first air inlet a and a second air inlet b, the air outlets are respectively a first air outlet c and a second air outlet d, and the first air inlet a, the second air inlet b, the first air outlet c and the second air outlet d are respectively connected with an air path, so that the recycling of the air path is realized, and the specific structure is not repeated.
Further, the steel connection pipe may be connected with the quartz window module by a clip.
Further, the steel connecting pipe is connected with a water cooling device. Specifically, a circulating water inlet i and a circulating water outlet ii are designed on the steel connecting pipe, and the circulating water inlet i and the circulating water outlet ii are connected with a water cooling device and used for reducing the reaction temperature of the steel connecting pipe B and slowing down the aging speed of a rubber ring at the joint of the steel connecting pipe B and the quartz window module.
Further, the light source unit is a xenon lamp light source, a mercury lamp light source, a laser, or a halogen lamp.
Further, the light source of the light source unit may be one of parallel light, convergent light, ultraviolet light, visible light, and infrared light. Specifically, the user may select any suitable light source for the reaction.
Further, the oxygen support membrane comprises a cerium oxide support membrane or a perovskite support membrane.
Compared with the prior art, the invention at least comprises the following beneficial effects:
the invention provides double-beam double-channel photo-thermal catalytic reaction equipment which mainly comprises two light source parts, a steel connecting pipe and two quartz window modules, wherein an oxygen carrier film has oxygen transfer capacity under the irradiation of the light source parts, double reactions can be carried out in the steel connecting pipe, photo-thermal synergistic complete reactions are realized, the product separation is simple, and the separation cost is effectively reduced.
In the description of the present invention, it is to be understood that the terms "central," "longitudinal," "lateral," "length," "width," "thickness," "upper," "lower," "front," "rear," "left," "right," "vertical," "horizontal," "top," "bottom," "inner," "outer," "clockwise," "counterclockwise," "axial," "radial," "circumferential," and the like are used in the orientations and positional relationships indicated in the drawings for convenience in describing the invention and to simplify the description, and are not intended to indicate or imply that the referenced devices or elements must have a particular orientation, be constructed and operated in a particular orientation, and are therefore not to be considered limiting of the invention.
In the present invention, unless otherwise expressly stated or limited, the terms "mounted," "connected," "secured," and the like are to be construed broadly and can, for example, be fixedly connected, detachably connected, or integrally formed; may be mechanically coupled, may be electrically coupled or may be in communication with each other; they may be directly connected or indirectly connected through intervening media, or they may be connected internally or in any other suitable relationship, unless expressly stated otherwise. The specific meanings of the above terms in the present invention can be understood by those skilled in the art according to specific situations.
While embodiments of the invention have been disclosed above, it is not limited to the applications set forth in the description and the embodiments, which are fully applicable in various fields of endeavor to which the invention pertains, and further modifications may readily be made by those skilled in the art, it being understood that the invention is not limited to the details shown and described herein without departing from the general concept defined by the appended claims and their equivalents.
Claims (7)
1. A dual-beam dual-channel photothermal catalytic reaction apparatus, comprising:
the device comprises two light source parts, a steel connecting pipe and two quartz window modules;
the steel connecting pipe is arranged between the two quartz window modules, and the two light source parts are respectively arranged on two sides of the two quartz window modules;
the quartz window module comprises a flange joint, a quartz window plate and a plano-convex focusing mirror, wherein the plano-convex focusing mirror is arranged in the quartz window plate, the quartz window plate is arranged in the flange joint, the flange joint is connected with the end part of the steel connecting pipe, and an oxygen carrier film is arranged in the end part of the steel connecting pipe.
2. The dual-beam dual-channel photothermal catalytic reaction device according to claim 1, wherein the steel connecting pipe is provided with a plurality of gas inlets and a plurality of gas outlets, and the gas inlets and the gas outlets are connected with a gas circuit.
3. The dual-beam dual-channel photothermal catalytic reaction device according to claim 1, wherein the steel connecting tube can be connected to the quartz window module by a snap.
4. The dual-beam dual-channel photothermal catalytic reaction device according to claim 1, wherein a water cooling device is connected to the steel connecting pipe.
5. The dual-beam dual-channel photothermal catalytic reaction apparatus according to claim 1, wherein the light source portion is a xenon lamp light source, a mercury lamp light source, a laser, or a halogen lamp.
6. The dual-beam dual-channel photo-thermal catalytic reaction apparatus according to claim 1, wherein the light source of the light source part is one of parallel light, convergent light, ultraviolet light, visible light and infrared light.
7. The dual-beam, dual-channel photothermal catalytic reaction device of claim 1, wherein the oxygen-carrying membrane comprises a cerium oxide-carrying membrane or a perovskite-carrying membrane.
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CN202010992241.4A CN112246201A (en) | 2020-09-21 | 2020-09-21 | Double-beam double-channel photo-thermal catalytic reaction equipment |
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CN202010992241.4A CN112246201A (en) | 2020-09-21 | 2020-09-21 | Double-beam double-channel photo-thermal catalytic reaction equipment |
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