CN112237560A - Whitening composition containing emblic leafflower fruits and application thereof - Google Patents

Whitening composition containing emblic leafflower fruits and application thereof Download PDF

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Publication number
CN112237560A
CN112237560A CN202011169548.0A CN202011169548A CN112237560A CN 112237560 A CN112237560 A CN 112237560A CN 202011169548 A CN202011169548 A CN 202011169548A CN 112237560 A CN112237560 A CN 112237560A
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Prior art keywords
whitening
emblic leafflower
whitening composition
leafflower fruit
inositol
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CN202011169548.0A
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Chinese (zh)
Inventor
孟铁刚
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Guangzhou Q Max Cosmetics Co ltd
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Guangzhou Q Max Cosmetics Co ltd
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Priority to CN202011169548.0A priority Critical patent/CN112237560A/en
Publication of CN112237560A publication Critical patent/CN112237560A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Dermatology (AREA)
  • Mycology (AREA)
  • Microbiology (AREA)
  • Botany (AREA)
  • Biotechnology (AREA)
  • Engineering & Computer Science (AREA)
  • Emergency Medicine (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a whitening composition containing emblic leafflower fruits (rich in micromolecular tannic acid) and application thereof, wherein the whitening composition containing the emblic leafflower fruits comprises the following components in percentage by weight: 0.0001-10% of emblic leafflower fruit, 0.0001-10% of inositol, 0.0001-10% of ferulic acid and the balance of water. The emblic leafflower fruit is rich in micromolecular tannic acid, and is a natural antioxidant, a safe and effective freckle removing and whitening agent. Inositol is a lipid water-soluble vitamin, has good osmosis effect, and can make the composition give full play to its effects. The composition can lighten the skin and relieve the skin at the same time, and the whitening composition is relatively mild, so that the whitening composition can be used as an active whitening component and applied to various cosmetics.

Description

Whitening composition containing emblic leafflower fruits and application thereof
Technical Field
The invention relates to the field of cosmetics, and particularly relates to a whitening composition and application thereof in whitening products.
Background
In recent years, cosmetics for skin whitening have been actively developed, and the whitening cosmetics have been deeply developed in terms of the cause of skin melanin, whitening mechanism, evaluation of whitening effect, selection of whitening agent, and the like. Women have a strong pursuit of whitening, and the whitening agents in the market generally comprise fruit acid, vitamin C and derivatives thereof, arbutin and the like. The single or compound cosmetic can be added into cosmetic, or used for removing horny layer, inhibiting activity of tyrosinase, or reducing melanin to whiten skin. The penetration effect of the whitening active substances is not ideal, and the use of some acids brings irritation in the process of whitening skin, so that the evaluation effect of the whitening product is unsatisfactory.
Disclosure of Invention
Aiming at the defects of the existing products in the market, the whitening composition disclosed by the invention has extremely strong oxidation resistance and effective whitening and freckle removing effects on phyllanthus emblica. Inositol is a lipid water-soluble vitamin and has excellent penetration, thereby enabling the whitening composition to exert its effects sufficiently. And the whitening composition is relatively mild, and can be used as a whitening active component and applied to various cosmetics.
Specifically, the invention provides a whitening composition containing emblic leafflower fruit, which comprises the following components in percentage by weight: 0.0001-10% of emblic leafflower fruit, 0.0001-10% of inositol, 0.0001-10% of ferulic acid and the balance of water.
In another preferred embodiment, the present invention provides a whitening composition containing emblic leafflower fruit, which comprises the following components by weight: 0.0001-10% of emblic leafflower fruit, 0.0001-10% of inositol, 0.0001-10% of ferulic acid and the balance of water.
Preferably, the purity of the emblic leafflower fruit is 80-99%.
Preferably, the emblic leafflower fruit is rich in small molecular tannic acid, is a natural antioxidant and is a safe and effective freckle removing and whitening agent.
Preferably, inositol is one of the vitamin B group and is a lipid water soluble vitamin.
Preferably, inositol has an osmotic effect, which can promote the permeation of the whitening composition.
Preferably, the purity of the ferulic acid is 80-99%.
Preferably, ferulic acid accelerates the exfoliation of the stratum corneum to improve skin spots and increase skin clarity.
In a second aspect, the present invention provides a whitening cosmetic containing emblic leafflower fruit, wherein the whitening composition cosmetic contains a whitening composition containing emblic leafflower fruit.
Preferably, the whitening cosmetic containing emblic leafflower fruits comprises 1-10% of the whitening composition.
Preferably, the whitening cosmetic containing the emblic leafflower fruits is whitening cream, whitening emulsion, whitening toner and whitening essence.
In a third aspect, the present invention provides a method for preparing a whitening cream containing a whitening composition of emblic leafflower fruit, comprising the steps of:
(1) preparing raw materials according to the proportion of the formula components;
(2) adding polyalcohol and ferulic acid into the water phase at normal temperature, stirring and dispersing uniformly, heating to 75-90 ℃, homogenizing and stirring uniformly;
(3) heating the components of the oil phase to 70-90 ℃, and uniformly stirring and dispersing;
(4) homogenizing the water phase for 30-90 seconds, adding the oil phase, continuously homogenizing for 30-90 seconds, and uniformly stirring and dispersing;
(5) and when the temperature of the material body is reduced to 30-50 ℃, adding the emblic leafflower fruit and the inositol, and uniformly stirring and dispersing to obtain the whitening cream containing the emblic leafflower fruit whitening composition.
In a fourth aspect, the present invention provides the use of a whitening composition comprising emblic leafflower fruit for the preparation of a whitening cosmetic.
Preferably, the emblic leafflower fruit has antioxidant, anti-inflammatory and spot-improving effects.
Drawings
Fig. 1 is a right-face test comparison using example 1.
Fig. 2 is a graph of the comparison results of the red-in-right region using example 1.
FIG. 3 is a graph showing the comparison of the brown areas of the left face using example 1.
FIG. 4 is a graph showing the comparison of the brown regions of the left face using example 2.
FIG. 5 is a graph showing the comparison of the brown regions of the right face using example 2.
FIG. 6 is a graph showing the comparison of the brown regions of the left face using example 3.
Detailed Description
The following is a clear and complete description of the technical solution in the embodiments of the present invention. It is obvious that the described example methods are only a part of examples of the present invention, and based on the embodiments of the present invention, those skilled in the art can obtain embodiments without creative efforts, and all embodiments are within the protection scope of the present invention. The examples, in which specific conditions are not specified, were conducted under conventional conditions or conditions recommended by the manufacturer. The reagents or instruments used are not indicated by the manufacturer, and are all commercially available products.
The emblic leafflower fruit is from natural plant fruits, is rich in micromolecular tannic acid, natural antioxidant and safe and effective freckle removing and whitening agent.
Ferulic acid can improve cuticle peeling and skin speckle, thereby improving skin transparency.
Example 1 (whitening cream)
1. Raw materials
Phase A: water (Too 100), glycerol 8%, butanediol 2%, ferulic acid 0.5%, xanthan gum 0.3%, allantoin 0.2%, sodium metabisulfite 0.2%, sodium hyaluronate 0.05%, sodium citrate 0.15%, sodium citrate 0.01%, disodium EDTA 0.01%;
phase B: caprylic/capric triglyceride 3%, polydimethylsiloxane 3%, cetostearyl alcohol, whale
2.5% of wax stearyl glucoside, 2% of cyclopentadimethylsiloxane, 2% of isononyl isononanoate, 2% of hydrogenated polydecene, 2% of glyceryl stearate, 2% of PEG-100 stearate, 1.8% of pentaerythritol distearate, 1% of boron nitride, 0.5% of tocopherol (vitamin E),
And C phase: 0.5 percent of 1, 2-hexanediol and 0.5 percent of p-hydroxyacetophenone
Phase D comprising fructus Phyllanthi 1%, inositol 0.5%, herba Portulacae extract 1%,
Phase E: 0.03 percent of lavender essential oil
2. Preparation process
(1) Preparing raw materials according to the proportion of the formula components;
(2) adding polyalcohol and ferulic acid into a water phase at normal temperature, stirring and dispersing uniformly, heating to 75-90 ℃, homogenizing and stirring uniformly;
(3) heating the components of the oil phase to 70-90 ℃, and uniformly stirring and dispersing;
(4) homogenizing the water phase for 30-90 seconds, adding the oil phase, continuously homogenizing for 30-90 seconds, and uniformly stirring and dispersing;
(5) and when the temperature of the material body is reduced to 30-50 ℃, adding the emblic leafflower fruit and the inositol, and uniformly stirring and dispersing to obtain the whitening cream containing the emblic leafflower fruit whitening composition.
Example 2 (whitening lotion)
1. Raw materials
Phase A: water (To 100%), ammonium acryloyldimethyltaurate/VP copolymer 0.40%, butanediol 2%;
phase B: 2% of C14-22 alcohol/C12-20 alkyl glucoside, 0.8% of cetearyl alcohol/cetearyl glucoside, 5% of fruit fat of Butyrospermum PARKII (Butyrrospermum PARKII), 3% of isononyl isononanoate and 1% of polydimethylsiloxane;
and C phase: the whitening composition of the embodiment of the invention is 5%;
phase D: 0.5 percent of 1, 2-hexanediol and 0.5 percent of p-hydroxyacetophenone
Phase E: 1% of purslane (Portulaca OLERACEA) extract.
2. Preparation process
(1) Adding phase A into emulsifying pot, homogenizing for 3-5 min, heating to 85 deg.C, and stirring to dissolve completely.
(2) Adding the phase B into an oil phase pot, stirring and heating to 85 ℃, and stirring until the phase B is completely dissolved;
(3) when the A, B two phases reach the designated temperature, pumping the B phase into the A phase, stirring for 5 minutes, homogenizing for 3 minutes, preserving the temperature for 15 minutes, and then adding the C phase, stirring and cooling;
(4) cooling to below 45 ℃, sequentially adding D, E phases, and uniformly stirring to obtain the whitening emulsion containing the emblic leafflower fruit whitening composition.
Example 3 (whitening toner)
At normal temperature, adding 1% of emblic leafflower fruit, 1% of ferulic acid and 1% of inositol into water, and stirring and dissolving uniformly to obtain the whitening toner containing the emblic leafflower fruit whitening composition.
In order to make the using effect of the obtained emblic leafflower fruit whitening composition more convincing, aiming at series cosmetics for whitening skin, a special cosmetic evaluation method is adopted to evaluate and analyze the using feeling and the efficacy of the whitening composition obtained by the invention.
Example 4
The whitening effect evaluation result of the whitening cream containing the emblic leafflower fruit whitening composition is as follows:
the test method comprises the following steps:
30 subjects were drawn at random, cleansed before testing, followed by a normal skin care protocol, and thereafter were rubbed with the product of the whitening composition test. It is recommended to be used in the morning and at night respectively, and the use is adhered to for one month. During the sample testing period, the skin tester VISIA machine was used to test facial surface spots every 7 days, and the comparative test results were recorded.
The results are shown in fig. 1, below, where the surface mottle ratio of the face of the subject was significantly less than that of the blank test. The experimental result proves that the emblic leafflower fruit whitening compound has the whitening effect.
Example 5
The evaluation results of the permeation-promoting effect of inositol in the emblic leafflower fruit whitening composition are as follows:
the test method comprises the following steps:
30 subjects were drawn at random, cleansed before testing, followed by a normal skin care protocol, and thereafter were rubbed with the product of the whitening composition test. It is recommended to be used in the morning and at night respectively, and the use is adhered to for one month. During the process of testing the sample by the subject, every 7 days, the test is performed by skin test
The tester VISIA machine tests the facial surface spots and records the comparative test results. The specific results are shown in FIGS. 2 to 6 and tables 1 to 5.
Table 1 shows the comparison of the right blush area data of example 1.
Before testing After testing
Feature counting 132 134
Score value 48.908 46.012
63% 75%
Table 2 shows the comparison of the left-face brown region data using example 1.
Before testing After testing
Feature counting 273 257
Score value 17.51 13.953
Percentile 77% 87%
Table 3 shows the comparison of the left-face brown region data using example 2.
Before testing After testing
Feature counting 274 181
Score value 16.513 8.881
Percentile 80% 94%
Table 4 shows the comparison of the data using the brown region of the right face of example 2.
Before testing After testing
Feature counting 281 205
Score value 15.690 11.369
Percentile 83% 91%
Table 5 shows the comparison of the left-face brown region data using example 3.
Before testing After testing
Feature counting 333 328
Score value 29.064 26.344
Percentile 24% 40%
As can be seen from fig. 3, 4, 5, 6, the number of brown spots in the face of the subject was significantly reduced compared to the blank test. The red spot test results are shown in fig. 2, where the number of red spots on the face of the subject is significantly reduced compared to the blank test. The experimental result proves that the emblic leafflower fruit whitening compound has the function of penetration promotion. The whitening composition can fully exert the efficacy.
In summary, the present invention is only a specific embodiment, but the scope of the present invention is not limited thereto, and those skilled in the art of cosmetics can change the components within the scope of the present invention, and the present invention shall be covered thereby. Accordingly, the scope of the present invention is based on the scope of the appended claims.

Claims (10)

1. The whitening composition containing the emblic leafflower fruits is characterized by comprising the following components in percentage by weight: 0.0001-10% of emblic leafflower fruit, 0.0001-10% of inositol, 0.0001-10% of ferulic acid and the balance of water.
2. The whitening composition containing the emblic leafflower fruits is characterized by comprising the following components in percentage by weight: 0.0001-10% of emblic leafflower fruit, 0.0001-10% of inositol, 0.0001-10% of ferulic acid and the balance of water.
3. The whitening composition according to claim 1, wherein the purity of the emblic leafflower fruit is 80 to 99%.
4. The whitening composition according to claim 1, wherein the inositol is a lipid water-soluble vitamin.
5. The whitening composition containing emblic leafflower fruit according to claim 1, wherein the ferulic acid has a purity of 80 to 99%.
6. A whitening cosmetic composition containing Emblica officinalis, characterized in that the whitening cosmetic composition contains the Emblica officinalis-containing whitening composition according to any one of claims 1 to 5.
7. The whitening cosmetic containing emblic leafflower fruit according to claim 6, comprising 1 to 10% of the whitening composition.
8. A method for preparing a whitening cream containing the whitening composition of Emblica officinalis according to any one of claims 1 to 5, comprising the steps of:
(1) preparing raw materials according to the proportion of the formula components;
(2) adding polyalcohol and ferulic acid into the water phase at normal temperature, stirring and dispersing uniformly, heating to 75-90 ℃, homogenizing and stirring uniformly;
(3) heating the components of the oil phase to 70-90 ℃, and uniformly stirring and dispersing;
(4) homogenizing the water phase for 30-90 seconds, adding the oil phase, continuously homogenizing for 30-90 seconds, and uniformly stirring and dispersing;
(5) and when the temperature of the material body is reduced to 30-50 ℃, adding the emblic leafflower fruit and the inositol, and uniformly stirring and dispersing to obtain the whitening cream containing the emblic leafflower fruit whitening composition.
9. Use of the whitening composition containing emblic leafflower fruit according to any one of claims 1 to 5 for preparing a whitening cosmetic.
10. Use of the whitening composition containing emblic leafflower fruits according to claim 9 for preparing whitening cosmetics, wherein the emblic leafflower fruits are antioxidant and anti-inflammatory.
CN202011169548.0A 2020-10-28 2020-10-28 Whitening composition containing emblic leafflower fruits and application thereof Pending CN112237560A (en)

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CN202011169548.0A CN112237560A (en) 2020-10-28 2020-10-28 Whitening composition containing emblic leafflower fruits and application thereof

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114748389A (en) * 2022-04-29 2022-07-15 彭氏(惠州)实业发展有限公司 Essence water and preparation method thereof
CN115399478A (en) * 2022-08-19 2022-11-29 何直源 Beautifying and whitening composition and whitening health product

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114748389A (en) * 2022-04-29 2022-07-15 彭氏(惠州)实业发展有限公司 Essence water and preparation method thereof
CN114748389B (en) * 2022-04-29 2024-03-22 彭氏(惠州)实业发展有限公司 Essence liquid and preparation method thereof
CN115399478A (en) * 2022-08-19 2022-11-29 何直源 Beautifying and whitening composition and whitening health product

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Application publication date: 20210119