CN112194700A - Preparation method of natural high-purity tea saponin with high decontamination efficiency - Google Patents
Preparation method of natural high-purity tea saponin with high decontamination efficiency Download PDFInfo
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- CN112194700A CN112194700A CN202011072610.4A CN202011072610A CN112194700A CN 112194700 A CN112194700 A CN 112194700A CN 202011072610 A CN202011072610 A CN 202011072610A CN 112194700 A CN112194700 A CN 112194700A
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- 241001122767 Theaceae Species 0.000 title claims abstract description 90
- 239000001397 quillaja saponaria molina bark Substances 0.000 title claims abstract description 74
- 229930182490 saponin Natural products 0.000 title claims abstract description 74
- 150000007949 saponins Chemical class 0.000 title claims abstract description 74
- 238000002360 preparation method Methods 0.000 title claims abstract description 50
- 238000005202 decontamination Methods 0.000 title claims abstract description 24
- 230000003588 decontaminative effect Effects 0.000 title claims abstract description 24
- 239000002994 raw material Substances 0.000 claims abstract description 24
- 238000000034 method Methods 0.000 claims abstract description 15
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000000843 powder Substances 0.000 claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000011259 mixed solution Substances 0.000 claims abstract description 8
- 239000006228 supernatant Substances 0.000 claims abstract description 8
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims abstract description 4
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 claims abstract description 4
- 238000003801 milling Methods 0.000 claims abstract description 4
- 229910052700 potassium Inorganic materials 0.000 claims abstract description 4
- 239000011591 potassium Substances 0.000 claims abstract description 4
- 239000007788 liquid Substances 0.000 claims description 67
- 230000008878 coupling Effects 0.000 claims description 51
- 238000010168 coupling process Methods 0.000 claims description 51
- 238000005859 coupling reaction Methods 0.000 claims description 51
- 230000007246 mechanism Effects 0.000 claims description 18
- 238000000605 extraction Methods 0.000 claims description 11
- 230000005540 biological transmission Effects 0.000 claims description 3
- 239000013049 sediment Substances 0.000 description 12
- 239000002244 precipitate Substances 0.000 description 8
- 239000007864 aqueous solution Substances 0.000 description 6
- 230000033001 locomotion Effects 0.000 description 6
- 230000008901 benefit Effects 0.000 description 5
- 239000012141 concentrate Substances 0.000 description 5
- 238000010586 diagram Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 238000007599 discharging Methods 0.000 description 3
- 238000005381 potential energy Methods 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 238000013459 approach Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 238000011010 flushing procedure Methods 0.000 description 2
- 238000001728 nano-filtration Methods 0.000 description 2
- 238000004321 preservation Methods 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 238000007670 refining Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000003809 water extraction Methods 0.000 description 1
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07J—STEROIDS
- C07J63/00—Steroids in which the cyclopenta(a)hydrophenanthrene skeleton has been modified by expansion of only one ring by one or two atoms
- C07J63/008—Expansion of ring D by one atom, e.g. D homo steroids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/24—Feed or discharge mechanisms for settling tanks
- B01D21/2444—Discharge mechanisms for the classified liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/24—Feed or discharge mechanisms for settling tanks
- B01D21/245—Discharge mechanisms for the sediments
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/26—Separation of sediment aided by centrifugal force or centripetal force
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H1/00—Processes for the preparation of sugar derivatives
- C07H1/06—Separation; Purification
- C07H1/08—Separation; Purification from natural products
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H15/00—Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
- C07H15/20—Carbocyclic rings
- C07H15/24—Condensed ring systems having three or more rings
- C07H15/256—Polyterpene radicals
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- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Tea And Coffee (AREA)
Abstract
The invention relates to preparation of tea saponin, in particular to a preparation method of natural high-purity tea saponin with high-efficiency decontamination. The method comprises the following steps: step one, placing the tea seed cake in a tea saponin preparation system for milling; step two, putting the powder into water to be mixed to obtain a mixed solution; step three, centrifuging the mixed solution to extract supernatant; and step four, preparing the tea saponin by using the supernatant as a raw material. The tea saponin comprises the following raw materials, by mass, 9 parts of tea saponin, 1 part of propylene glycol, 1 part of butanediol and 1 part of potassium glycyrrhetate.
Description
Technical Field
The invention relates to preparation of tea saponin, in particular to a preparation method of natural high-purity tea saponin with high-efficiency decontamination.
Background
For example, the publication number CN110092810A relates to the field of compound refining methods, and the technical scheme is as follows: (1) pretreatment of raw materials: drying the raw materials, crushing and sieving to obtain raw material powder; (2) adding an organic solvent into the raw material powder obtained in the step (1), and uniformly stirring to obtain a feed liquid; (3) adjusting the temperature of the feed liquid in the step (2), and performing heat preservation pretreatment; (4) carrying out solid-liquid separation on the feed liquid obtained in the step (3) under the condition of heat preservation; (5) carrying out nanofiltration separation on the liquid obtained in the step (4), adding a solvent into the trapped liquid for dilution, and then carrying out nanofiltration process again; (6) and (5) merging the trapped liquids obtained in the step (5), and drying in vacuum to obtain the high-purity tea saponin. The method for extracting and refining the tea saponin is green in process and low in cost, obtains the high-purity tea saponin with the purity of more than 95%, and simultaneously keeps the yield of more than 90%; however, the method does not have a technical scheme for improving the preparation efficiency of the tea saponin.
Disclosure of Invention
The invention aims to provide a preparation method of natural high-purity tea saponin with high decontamination efficiency, which can improve the preparation efficiency of tea saponin.
The purpose of the invention is realized by the following technical scheme:
a preparation method of natural high-purity tea saponin with high decontamination efficiency comprises the following steps:
step one, placing the tea seed cake in a tea saponin preparation system for milling;
step two, putting the powder into water to be mixed to obtain a mixed solution;
step three, centrifuging the mixed solution to extract supernatant;
step four, preparing the tea saponin by using the supernatant as a raw material;
the preparation method of the natural high-purity tea saponin with high decontamination efficiency also comprises a preparation system of the tea saponin; tea saponin's preparation system includes mounting bracket I, the mount pad, mounting bracket II, the system platform just, the axle, motor I, hydraulic push rod and pressure head, two mount pads of left side rigid coupling of I upper end of mounting bracket, the lower extreme rigid coupling axle of system platform just, the both ends of axle are rotated respectively and are connected on two mount pads, the output shaft and the axle rigid coupling of motor I, I rigid coupling of motor is on the mount pad, II rigid couplings of mounting bracket are in the upper end of mounting bracket I, hydraulic push rod installs on mounting bracket I, hydraulic push rod's expansion end rigid coupling pressure head, the pressure head is located the system platform just above.
This preparation system of tea saponin still includes, belt conveyor, mounting bracket III, electric putter I, connecting portion I and push pedal, belt conveyor sets up in the left side of just making the platform, belt conveyor's up end is higher than just making a platform centimetre, the rear end of mounting bracket III rigid coupling in mounting bracket I upper end, I rigid coupling of electric putter is on mounting bracket III, the rear end of the expansion end rigid coupling connecting portion I of electric putter I, the front end rigid coupling push pedal of connecting portion I, the push pedal is located the positive left side of just making the platform, the push pedal is located belt conveyor's upper end.
This preparation system of tea saponin still includes splash guard I and splash guard II, splash guard I of the equal body coupling in both ends around the platform upper end of just making, splash guard II of right-hand member rigid coupling of pressure head, pressure head and push pedal can get into between two splash guards I, and the left end of splash guard II is close to the right-hand member setting of just making the platform.
The preparation system of the tea saponin further comprises a hairbrush, wherein the hairbrush is arranged at the left end of the push plate, and the lower end of the hairbrush is lower than the lower end of the push plate.
This preparation system of tea saponin still includes bushing, roller, gear and motor II, and the bushing rigid coupling is on the right side of I upper end of mounting bracket, two rollers of bushing internal rotation connection, and two roller surfacing, the shortest distance is 0.25mm between two rollers, gear of the equal rigid coupling in front end of two rollers, two gear engagement transmissions, one of them roller of motor II drive rotates, and motor II is installed on the bushing, and the bushing is located the right side below of just making the platform.
This preparation system of tea saponin still includes draws the mechanism, draws the mechanism and includes the liquid case, and the upper left side of liquid case is equipped with the opening, the opening is located under the blow-by box.
Draw mechanism still includes valve plate I and electric putter II, and valve plate I is on the liquid case from right to left sliding connection, and valve plate I is used for sealing or opens the opening, electric putter II's expansion end and the I rigid coupling of valve plate, electric putter II install on the liquid case.
This preparation system of tea saponin still includes cross, platform and base, and it is equipped with two to extract mechanism mirror symmetry, and the inner and cross rigid coupling of two liquid tanks and intercommunication, both ends all are equipped with the valve around the cross, and both ends about the platform are fixed connection respectively to two liquid tanks, and the platform rotates to be connected on the base, is equipped with the motor in the base, the motor is used for driving platform to rotate.
Draw mechanism still includes valve plate II, connecting portion and electric putter III, and valve plate II is kept away from cross pipe department by back to preceding sliding connection at the liquid case, and valve plate II can be with two appearance chambeies of liquid incasement portion isolated, and connecting portion one end rigid coupling is on valve plate II, and the other end rigid coupling of connecting portion is in electric putter III's expansion end, and electric putter III rigid couplings are in the outer end of liquid case.
The tea saponin comprises the following raw materials, by mass, 9 parts of tea saponin, 1 part of propylene glycol, 1 part of butanediol and 1 part of potassium glycyrrhetate.
The preparation system of the natural high-purity tea saponin with high decontamination efficiency has the beneficial effects that:
utilize centrifugal force to concentrate the precipitate in the inside outside of liquid case, start electric putter III and drive II forward movements of valve plate and completely cut off the precipitate in one side that the cross was kept away from to the liquid case, then open the valve that the cross is located the rear side and discharge the clear liquid and collect, open the valve that the cross is located the front side after finishing discharging, then utilize electric putter III to drive II backward movements of valve plate no longer the separation precipitate, utilize the gravitational potential energy of liquid this moment to do benefit to and drive the precipitate and move right and discharge through the cross. The method is convenient for rapidly preparing a large amount of aqueous solution containing tea saponin, and the aqueous solution is taken as a raw material to extract the tea saponin by a water extraction and alcohol precipitation method or biological fermentation.
Drawings
The invention is described in further detail below with reference to the accompanying drawings and specific embodiments.
FIG. 1 is a schematic diagram showing the overall structure of a system for preparing natural high-purity tea saponin with high decontamination efficiency according to the present invention;
FIG. 2 is a partial schematic view of the first embodiment of the present invention;
FIG. 3 is a second partial schematic structural view of the present invention;
FIG. 4 is a third schematic view of a portion of the present invention;
FIG. 5 is a fourth schematic view of a portion of the present invention;
FIG. 6 is a schematic diagram of a portion of the present invention;
FIG. 7 is a schematic diagram six of a portion of the present invention;
fig. 8 is a schematic diagram seven of a partial structure of the present invention.
In the figure: a belt conveyor 1; the mounting frame I2; a mounting seat 201; a mounting rack II 202; a mounting rack III 203; a primary manufacturing station 3; a shaft 301; a motor I302; a splash shield I303; a hydraulic push rod 4; a ram 401; a splash plate II 402; an electric push rod I5; a connecting part I501; a push plate 502; a brush 503; a leakage box 6; a roller 601; a gear 602; a motor II 603; an extraction mechanism 7 a; a liquid tank 7; a valve plate I701; an electric push rod II 702; a valve plate II 703; a connecting portion 704; an electric push rod III 705; a cross pipe 8; a platform 9; a base 901.
Detailed Description
In the description of the present invention, it is to be understood that the terms "center", "longitudinal", "lateral", "up", "down", "front", "back", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", and the like, indicate orientations or positional relationships based on those shown in the drawings, and are used only for convenience in describing the present invention and for simplicity in description, and do not indicate or imply that the referenced devices or elements must have a particular orientation, be constructed and operated in a particular orientation, and thus, are not to be construed as limiting the present invention.
The present invention will be described in further detail with reference to the accompanying drawings.
The first embodiment is as follows:
as shown in the figure, the preparation system of natural high-purity tea saponin with high decontamination efficiency comprises the following steps:
step one, placing the tea seed cake in a tea saponin preparation system for milling;
step two, putting the powder into water to be mixed to obtain a mixed solution;
step three, centrifuging the mixed solution to extract supernatant;
step four, preparing the tea saponin by using the supernatant as a raw material;
the preparation method of the natural high-purity tea saponin with high decontamination efficiency also comprises a preparation system of the tea saponin; tea saponin's preparation system includes mounting bracket I2, mount pad 201, mounting bracket II 202, system platform 3 just, axle 301, motor I302, hydraulic push rod 4 and pressure head 401, two mount pads 201 of left side rigid coupling of mounting bracket I2 upper end, the lower extreme rigid coupling axle 301 of system platform 3 just, the both ends of axle 301 are rotated respectively and are connected on two mount pads 201, the output shaft and the axle 301 rigid coupling of motor I302, I302 rigid coupling of motor is on mount pad 201, II 202 rigid couplings of mounting bracket are in the upper end of mounting bracket I2, hydraulic push rod 4 installs on mounting bracket I2, the expansion end rigid coupling pressure head 401 of hydraulic push rod 4, pressure head 401 is located system platform 3 just over. Place the tea-seed cake on primary system platform 3, start hydraulic rod 4, utilize hydraulic rod 4 to drive pressure head 401 and crush the tea-seed cake. The starter motor I302, the output shaft of motor I302 drives and just makes 3 rotations of platform, emptys the dried tea cake after will crushing, and the dried tea cake after the crushing does benefit to the solid extraction of liquid.
The second embodiment is as follows:
as shown in the figure, this preparation system of tea saponin still includes, belt conveyor 1, mounting bracket iii 203, electric putter i 5, connecting portion i 501 and push pedal 502, belt conveyor 1 sets up in the left side of just making platform 3, belt conveyor 1's up end is higher than just making platform 3 centimetres, the rear end of mounting bracket iii 203 rigid coupling in mounting bracket i 2 upper end, electric putter i 5 rigid coupling is on mounting bracket iii 203, the rear end of the I501 of movable end rigid coupling connecting portion of electric putter i 5, the front end rigid coupling push pedal 502 of connecting portion i 501, push pedal 502 is located the positive left side of just making platform 3, push pedal 502 is located belt conveyor 1's upper end. Utilize belt conveyor 1 to constantly transport the tea-seed cake to just left side of primary system platform 3, start electric putter I5, electric putter I5 drives push pedal 502 and moves right and promote the tea-seed cake and remove and fall into primary system platform 3. To facilitate pipelining.
The third concrete implementation mode:
as shown in the figure, this preparation system of tea saponin still includes splash shield I303 and splash shield II 402, the splash shield I303 of homogeneous body coupling in both ends around the primary system platform 3 upper end, and pressure head 401's right-hand member rigid coupling splash shield II 402, pressure head 401 and push pedal 502 can get into between two splash shields I303, and the left end of splash shield II 402 is close to the right-hand member setting of primary system platform 3. Splashplate I303 shelters from around primary system platform 3 position, and splashplate II 402 shelters from the right-hand position of primary system platform 3, and push pedal 502 shelters from the left position of primary system platform 3, and then when crushing tea-seed cake, the raw materials can not splash four times, and then concentrates on waiting to empty on primary system platform 3 and does not cause the waste of raw materials.
The fourth concrete implementation mode:
as shown in the figure, the tea saponin preparation system further comprises a brush 503, the brush 503 is arranged at the left end of the push plate 502, and the lower end of the brush 503 is lower than the lower end of the push plate 502. The brush 503 can take place to extrude crooked along with push pedal 502 side-to-side movement on belt conveyor 1, and when push pedal 502 and brush 503 were located belt conveyor 1's right side, brush 503 reset through material self nature, because of the tea cake on primary platform 3, primary platform 3 is less than belt conveyor 1, and push pedal 502 has the clearance with primary platform 3's upper end, and brush 503 is used for sheltering from when crushing the tea cake through the raw materials that the clearance splashes, also can replace push pedal 502 to promote the median of tea cake crushing to the position on primary platform 3. Crushing the dried tea cakes to obtain a primary raw material.
The fifth concrete implementation mode:
as shown in the figure, this preparation system of tea saponin still includes bushing 6, roller 601, gear 602 and motor II 603, bushing 6 rigid coupling is on the right side of I2 upper end of mounting bracket, bushing 6 internal rotation connects two rollers 601, two rollers 601 surfacing, the shortest distance is 0.25mm between two rollers 601, gear 602 of equal rigid coupling of front end of two rollers 601, two gear 602 meshing transmissions, motor II 603 drives one of them roller 601 and rotates, motor II 603 is installed on bushing 6, bushing 6 is located the right side below of primary system platform 3. Primary table 3 clockwise rotation 45 degrees left and right will tentatively raw materials fall between two rollers 601, because of through the crushing, the crushed aggregates can get into between the little two rollers 601 in clearance, make roller 601 surfacing not have sunken to the powder that the diameter is less than 0.25mm of the crushing acquisition of preliminary raw materials once more, should divide the material and need not to sieve and can directly drop into aquatic preparation aqueous solution.
The sixth specific implementation mode:
as shown in the figure, the preparation system of the tea saponin further comprises an extraction mechanism 7a, the extraction mechanism 7a comprises a liquid tank 7, and an opening is arranged at the upper left of the liquid tank 7 and is positioned right below the leakage tank 6. The liquid tank 7 is filled with water through the opening, and powder can directly fall into the liquid tank 7 to be mixed with water to prepare an aqueous solution.
The seventh embodiment:
as shown in the figure, the extraction mechanism 7a further comprises a valve plate I701 and an electric push rod II 702, the valve plate I701 is connected to the liquid tank 7 in a sliding mode from right to left, the valve plate I701 is used for closing or opening the opening, the movable end of the electric push rod II 702 is fixedly connected with the valve plate I701, and the electric push rod II 702 is installed on the liquid tank 7.
The specific implementation mode is eight:
as shown in the figure, the preparation system of the tea saponin further comprises a cross pipe 8, a platform 9 and a base 901, wherein two extraction mechanisms 7a are arranged in mirror symmetry, the inner ends of the two liquid tanks 7 are fixedly connected and communicated with the cross pipe 8, valves are arranged at the front end and the rear end of the cross pipe 8, the two liquid tanks 7 are respectively and fixedly connected at the left end and the right end of the platform 9, the platform 9 is rotatably connected onto the base 901, and a motor is arranged in the base 901 and used for driving the platform 9 to rotate. The motor is started, the motor is utilized to drive the platform 9 to rotate, the platform 9 drives the two extraction mechanisms 7a to rotate, and the precipitates in the two liquid tanks 7 are concentrated to the outer sides of the inner parts of the two liquid tanks 7 by utilizing centrifugal force, so that the precipitates are separated and gathered. The sediment gradually falls from the outer side of the liquid tank 7 to the bottom half of the liquid tank 7 far away from the cross pipe 8. At the moment, the valve of the cross pipe 8 on the rear side is opened, clear liquid is discharged, after the liquid level approaches to the sediment, the valve on the rear side is closed, the valve of the cross pipe 8 on the front side is opened, the sediment is discharged, the sediment can be flushed out while the liquid tank 7 is flushed by water through the opening, and the sediment is gathered at the opening, so that the sediment can be directly flushed towards the cross pipe 8 during flushing.
The specific implementation method nine:
as shown in the figure, the extraction mechanism 7a further comprises a valve plate ii 703, a connecting portion 704 and an electric push rod iii 705, the valve plate ii 703 is connected to the liquid tank 7 from back to front in a sliding manner and is far away from the cross pipe 8, the valve plate ii 703 can isolate the inside of the liquid tank 7 into two cavities, one end of the connecting portion 704 is fixedly connected to the valve plate ii 703, the other end of the connecting portion 704 is fixedly connected to the movable end of the electric push rod iii 705, and the electric push rod iii 705 is fixedly connected to the outer end of the liquid tank 7. Electric putter III 705 can install the battery on liquid case 7, utilize the battery to supply power to electric putter III 705, when utilizing centrifugal force deposit to concentrate on the inside outside of liquid case 7, start electric putter III 705 and drive II 703 of valve plate and move forward and completely cut off the deposit in one side that cross 8 was kept away from to liquid case 7, then open the valve that cross 8 was located the rear side and discharge clear solution and collect, open the valve that cross 8 was located the front side after finishing discharging, then utilize III 705 of electric putter to drive II 703 of valve plate backward motion and no longer separate the deposit, the gravitational potential energy of utilizing liquid this moment does benefit to and drives the deposit and moves right and discharges through cross 8.
The detailed implementation mode is ten:
as shown in the figure, the tea saponin comprises 9 parts of tea saponin, 1 part of propylene glycol, 1 part of butanediol and 1 part of potassium glycyrrhetate by mass. The natural high-purity tea saponin with high decontamination efficiency has moisturizing and anti-inflammatory effects.
The invention relates to a preparation system of natural high-purity tea saponin with high-efficiency decontamination, which has the working principle that:
place the tea-seed cake on primary system platform 3, start hydraulic rod 4, utilize hydraulic rod 4 to drive pressure head 401 and crush the tea-seed cake. The starter motor I302, the output shaft of motor I302 drives and just makes 3 rotations of platform, emptys the dried tea cake after will crushing, and the dried tea cake after the crushing does benefit to the solid extraction of liquid. Utilize belt conveyor 1 to constantly transport the tea-seed cake to just left side of primary system platform 3, start electric putter I5, electric putter I5 drives push pedal 502 and moves right and promote the tea-seed cake and remove and fall into primary system platform 3. To facilitate pipelining. Splashplate I303 shelters from around primary system platform 3 position, and splashplate II 402 shelters from the right-hand position of primary system platform 3, and push pedal 502 shelters from the left position of primary system platform 3, and then when crushing tea-seed cake, the raw materials can not splash four times, and then concentrates on waiting to empty on primary system platform 3 and does not cause the waste of raw materials. The brush 503 can take place to extrude crooked along with push pedal 502 side-to-side movement on belt conveyor 1, and when push pedal 502 and brush 503 were located belt conveyor 1's right side, brush 503 reset through material self nature, because of the tea cake on primary platform 3, primary platform 3 is less than belt conveyor 1, and push pedal 502 has the clearance with primary platform 3's upper end, and brush 503 is used for sheltering from when crushing the tea cake through the raw materials that the clearance splashes, also can replace push pedal 502 to promote the median of tea cake crushing to the position on primary platform 3. Crushing the dried tea cakes to obtain a primary raw material. Primary table 3 clockwise rotation 45 degrees left and right will tentatively raw materials fall between two rollers 601, because of through the crushing, the crushed aggregates can get into between the little two rollers 601 in clearance, make roller 601 surfacing not have sunken to the powder that the diameter is less than 0.25mm of the crushing acquisition of preliminary raw materials once more, should divide the material and need not to sieve and can directly drop into aquatic preparation aqueous solution. The liquid tank 7 is filled with water through the opening, and powder can directly fall into the liquid tank 7 to be mixed with water to prepare an aqueous solution. The motor is started, the motor is utilized to drive the platform 9 to rotate, the platform 9 drives the two extraction mechanisms 7a to rotate, and the precipitates in the two liquid tanks 7 are concentrated to the outer sides of the inner parts of the two liquid tanks 7 by utilizing centrifugal force, so that the precipitates are separated and gathered. The sediment gradually falls from the outer side of the liquid tank 7 to the bottom half of the liquid tank 7 far away from the cross pipe 8. At the moment, the valve of the cross pipe 8 on the rear side is opened, clear liquid is discharged, after the liquid level approaches to the sediment, the valve on the rear side is closed, the valve of the cross pipe 8 on the front side is opened, the sediment is discharged, the sediment can be flushed out while the liquid tank 7 is flushed by water through the opening, and the sediment is gathered at the opening, so that the sediment can be directly flushed towards the cross pipe 8 during flushing. Electric putter III 705 can install the battery on liquid case 7, utilize the battery to supply power to electric putter III 705, when utilizing centrifugal force deposit to concentrate on the inside outside of liquid case 7, start electric putter III 705 and drive II 703 of valve plate and move forward and completely cut off the deposit in one side that cross 8 was kept away from to liquid case 7, then open the valve that cross 8 was located the rear side and discharge clear solution and collect, open the valve that cross 8 was located the front side after finishing discharging, then utilize III 705 of electric putter to drive II 703 of valve plate backward motion and no longer separate the deposit, the gravitational potential energy of utilizing liquid this moment does benefit to and drives the deposit and moves right and discharges through cross 8.
It is to be understood that the above description is not intended to limit the present invention, and the present invention is not limited to the above examples, and that various changes, modifications, additions and substitutions which are within the spirit and scope of the present invention and which may be made by those skilled in the art are also within the scope of the present invention.
Claims (10)
1. A preparation method of natural high-purity tea saponin with high decontamination efficiency is characterized by comprising the following steps:
step one, placing the tea seed cake in a tea saponin preparation system for milling;
step two, putting the powder into water to be mixed to obtain a mixed solution;
step three, centrifuging the mixed solution to extract supernatant;
step four, preparing the tea saponin by using the supernatant as a raw material;
the preparation method of the natural high-purity tea saponin with high decontamination efficiency also comprises a preparation system of the tea saponin; tea saponin's preparation system includes mounting bracket I (2), mount pad (201), mounting bracket II (202), just system platform (3), axle (301), motor I (302), hydraulic push rod (4) and pressure head (401), two mount pads (201) of left side rigid coupling of mounting bracket I (2) upper end, just system platform (3) lower end rigid coupling axle (301), the both ends of axle (301) are rotated respectively and are connected on two mount pads (201), the output shaft and axle (301) rigid coupling of motor I (302), motor I (302) rigid coupling is on mount pad (201), mounting bracket II (202) rigid coupling is in the upper end of mounting bracket I (2), hydraulic push rod (4) are installed on mounting bracket I (2), the expansion end rigid coupling pressure head (401) of hydraulic push rod (4), pressure head (401) are located just over just system platform (3).
2. The preparation method of natural high-purity tea saponin with high decontamination efficiency as claimed in claim 1, is characterized in that: this preparation system of tea saponin still includes, belt conveyor (1), mounting bracket III (203), electric putter I (5), connecting portion I (501) and push pedal (502), belt conveyor (1) sets up the left side at primary system platform (3), the up end of belt conveyor (1) is higher than primary system platform (3) one centimetre, mounting bracket III (203) rigid coupling is in the rear end of mounting bracket I (2) upper end, electric putter I (5) rigid coupling is on mounting bracket III (203), the rear end of the expansion end rigid coupling connecting portion I (501) of electric putter I (5), the front end rigid coupling push pedal (502) of connecting portion I (501), push pedal (502) are located the positive left side of primary system platform (3), push pedal (502) are located the upper end of belt conveyor (1).
3. The method for preparing natural high-purity tea saponin with high decontamination efficiency according to claim 2, is characterized in that: this preparation system of tea saponin still includes splash guard I (303) and splash guard II (402), splash guard I (303) of equal body coupling in both ends around primary system platform (3) upper end, splash guard II (402) of right-hand member rigid coupling of pressure head (401), pressure head (401) and push pedal (502) can get into between two splash guards I (303), and the left end of splash guard II (402) is close to the right-hand member setting of primary system platform (3).
4. The preparation method of natural high-purity tea saponin with high decontamination efficiency as claimed in claim 3, is characterized in that: the preparation system of the tea saponin also comprises a hairbrush (503), the left end of the push plate (502) is provided with the hairbrush (503), and the lower end of the hairbrush (503) is lower than the lower end of the push plate (502).
5. The method for preparing natural high-purity tea saponin with high decontamination efficiency according to claim 4, is characterized in that: this preparation system of tea saponin still includes hourglass case (6), roller (601), gear (602) and motor II (603), hourglass case (6) rigid coupling is on the right side of mounting bracket I (2) upper end, two roller (601) of hourglass case (6) internal rotation connection, two roller (601) surfacing, the shortest distance is 0.25mm between two roller (601), gear (602) of the equal rigid coupling of front end of two roller (601), two gear (602) meshing transmission, one of them roller (601) of motor II (603) drive rotate, install on hourglass case (6) motor II (603), hourglass case (6) are located the right side below of primary system platform (3).
6. The method for preparing natural high-purity tea saponin with high decontamination efficiency according to claim 5, is characterized in that: this preparation system of tea saponin still includes draws mechanism (7a), draws mechanism (7a) including liquid case (7), and the upper left side of liquid case (7) is equipped with the opening, the opening is located under hourglass case (6).
7. The method for preparing natural high-purity tea saponin with high decontamination efficiency according to claim 6, is characterized in that: the extraction mechanism (7a) further comprises a valve plate I (701) and an electric push rod II (702), the valve plate I (701) is connected to the liquid tank (7) in a sliding mode from right to left, the valve plate I (701) is used for closing or opening the opening, the movable end of the electric push rod II (702) is fixedly connected with the valve plate I (701), and the electric push rod II (702) is installed on the liquid tank (7).
8. The method for preparing natural high-purity tea saponin with high decontamination efficiency according to claim 7, is characterized in that: this preparation system of tea saponin still includes cross (8), platform (9) and base (901), draws mechanism (7a) mirror symmetry to be equipped with two, the inner and cross (8) rigid coupling and the intercommunication of two liquid case (7), both ends all are equipped with the valve around cross (8), both ends about platform (9) are fixed connection respectively in two liquid case (7), platform (9) rotate to be connected on base (901), be equipped with the motor in base (901), the motor is used for drive platform (9) to rotate.
9. The method for preparing natural high-purity tea saponin with high decontamination efficiency according to claim 8, is characterized in that: draw mechanism (7a) and still include valve plate II (703), connecting portion (704) and electric putter III (705), valve plate II (703) are kept away from cross (8) department by back to preceding sliding connection in liquid case (7), valve plate II (703) can be with inside isolated two chambeies that become of liquid case (7), connecting portion (704) one end rigid coupling is on valve plate II (703), the other end rigid coupling of connecting portion (704) is at the expansion end of electric putter III (705), electric putter III (705) rigid coupling is in the outer end of liquid case (7).
10. The tea saponin prepared by the preparation method of natural high-purity tea saponin with high decontamination efficiency according to claim 9 is characterized in that: the tea saponin comprises the following raw materials, by mass, 9 parts of tea saponin, 1 part of propylene glycol, 1 part of butanediol and 1 part of potassium glycyrrhetate.
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