CN112120971B - 一种保湿口红及其制备方法 - Google Patents
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Abstract
本发明公开了一种保湿口红，涉及化妆品技术领域。所述保湿口红，包含以下重量份的组分：聚乙烯3‑8份、小烛树蜡0.5‑3份、双‑二甘油多酰基己二酸酯‑2 5‑15份、蚕丝胶蛋白0.2‑1份、甘油辛酸酯0.2‑1份和山梨坦倍半油酸酯0.3‑1.5份。本发明提供的保湿口红具有良好吸湿和散湿性能、适应周围环境、天然调湿、改善人体皮肤营养以及防止皮肤起皱的效果。
Description
技术领域
本发明涉及一种化妆品技术领域，尤其是一种保湿口红及其制备方法。
背景技术
目前市面上常见的口红存在以下缺点：(1)膏体不够细腻，涂抹不够细滑；(2)膏体较硬，不易上妆和涂抹，不易显色，使用感差；(3)对唇部肌肤深层修护保湿不够。
发明内容
基于此，本发明的目的在于克服上述现有技术的不足之处而提供一种具有良好吸湿和散湿性能、适应周围环境、天然调湿、改善人体皮肤营养以及防止皮肤起皱的保湿口红。
为实现上述目的，本发明所采取的技术方案为：一种保湿口红，包含以下重量份的组分：聚乙烯3-8份、小烛树蜡0.5-3份、双-二甘油多酰基己二酸酯-25-15份、蚕丝胶蛋白0.2-1份、甘油辛酸酯0.2-1份和山梨坦倍半油酸酯0.3-1.5份。
本发明提供的保湿口红，采用各种组分的合理搭配组合，得到的保湿口红柔韧热稳定性好、颜料分散性佳，能够修护唇部肌肤纹理。
优选地，所述保湿口红，包含以下重量份的组分：聚乙烯6-8份、小烛树蜡1-2份、双-二甘油多酰基己二酸酯-2 8-12份、蚕丝胶蛋白0.4-0.6份、甘油辛酸酯0.7-0.9份和山梨坦倍半油酸酯0.6-1份。
更优选地，所述保湿口红，包含以下重量份的组分：聚乙烯7.8份、小烛树蜡1.5份、双-二甘油多酰基己二酸酯-2 10份、蚕丝胶蛋白0.5份、甘油辛酸酯0.8份和山梨坦倍半油酸酯0.8份。
聚乙烯可以提供高的凝固点和熔点的同时提升产品韧性；小烛树蜡属于植物来源的蜡，能显著改善产品的柔软性和热稳定性；蚕丝胶原蛋白中蚕丝蛋白质与人体皮肤角朊蛋白结构相似，两者具有极好的亲和性，能增强皮肤细胞活力和弹性，具有良好的吸湿性和保湿性。
优选地，所述保湿口红，还包含以下重量份的成分：地蜡1-8份、微晶蜡0.5-4份、二异硬脂醇苹果酸酯5-20份、苯基聚三甲基硅氧烷6-15份、季戊四醇四异硬脂酸酯8-15份、CI15850 3-12份、CI 77491 0.1-10份、十三烷醇偏苯三酸酯2-10份、棕榈酸乙基己酯2-10份、硅石3-7份、二甲基甲硅烷基化硅石0.5-2份、辛基十二醇2-15份和生育酚乙酸酯0.05-0.2份。
所述CI 15850为着色剂立索尔宝红，CI 15850是一种蓝光红色的粉末，色泽鲜艳，着色力强，在油墨中具有良好的流动性，并具有良好的稳定性；CI 77491为着色剂氧化铁红。
优选地，所述保湿口红，还包含以下重量份的成分：地蜡4-6份、微晶蜡2-4份、二异硬脂醇苹果酸酯10-15份、苯基聚三甲基硅氧烷10-15份、季戊四醇四异硬脂酸酯10-15份、CI 15850 5-7份、CI 77491 0.1-0.5份、十三烷醇偏苯三酸酯6-7份、棕榈酸乙基己酯6-7份、硅石4-6份、二甲基甲硅烷基化硅石0.5-1.5份、辛基十二醇10-12份和生育酚乙酸酯0.05-0.15份。
更优选地，所述保湿口红，还包含以下重量份的成分：地蜡5份、微晶蜡3份、二异硬脂醇苹果酸酯12份、苯基聚三甲基硅氧烷13份、季戊四醇四异硬脂酸酯12份、CI 15850 6.2份、CI 77491 0.3份、十三烷醇偏苯三酸酯6.5份、棕榈酸乙基己酯6.5份、硅石5份、二甲基甲硅烷基化硅石1份、辛基十二醇11份和生育酚乙酸酯0.1份。
微晶蜡是以支链为主的烃蜡混合物，为配方提供优异的结晶性和稳定的结构；二异硬脂醇苹果酸酯是具有轻质柔软的肤感高折光率油脂，滑而不腻，有效改善产品黏腻性和亮度；硅石是球状内孔型微球体，使产品有丝滑质感和滑度，提高颜料的上色率；二甲基甲硅烷基化硅石属于气相二氧化硅，有效增稠体系的同时能形成三维网状结构稳定体系。
同时，本发明还提供了上述保湿口红的制备方法，包括如下步骤：
(1)将聚乙烯、小烛树蜡、地蜡、微晶蜡、二异硬脂醇苹果酸酯、双-二甘油多酰基己二酸酯-2、苯基聚三甲基硅氧烷13和季戊四醇四异硬脂酸酯加入乳化锅，搅拌加热至完全溶解，得到混合液A；
(2)将混合液A降温后加入CI 15850、CI 77491、十三烷醇偏苯三酸酯和棕榈酸乙基己酯，进行均质至分散完全，得到混合液B；
(3)向混合液B中加入硅石和二甲基甲硅烷基化硅石，搅拌至分散完全，得到混合液C；
(4)向混合液C中加入混合均匀的蚕丝胶蛋白、山梨坦倍半油酸酯和辛基十二醇，进行搅拌，继续加入甘油辛酸酯和生育酚乙酸酯，搅拌后出料备用。
优选地，所述步骤(1)中，搅拌的速率为100-200r/min，加热的温度为80-85℃。
优选地，所述步骤(2)中，混合液A降温至75-80℃，均质的速率为7000-8000r/min。
优选地，所述步骤(3)中，搅拌的速率为100-200r/min；所述步骤(4)中，搅拌的速率为50-100r/min，搅拌的时间为15-20min。
相对于现有技术，本发明的有益效果为：(1)产品柔韧热稳定性好；(2)颜料分散性佳，涂抹柔顺均匀；(3)膏体柔软顺滑好上妆，色泽浓郁，使用感好；(4)良好的吸湿性和持久保湿性能，能够修护唇部肌肤纹理。
具体实施方式
为更好的说明本发明的目的、技术方案和优点，下面将结合具体实施例对本发明作进一步说明。
本申请设置实施例1-9，具体实施例1-5的重量份选择如表1所示，具体实施例6-9的重量份选择如表2所示，具体实施例6-9的其余重量份与实施例3相同
表1实施例1-5各组分的重量份选择
表2实施例6-9各组分的重量份选择
| 组分 | 实施例6 | 实施例7 | 实施例8 | 实施例9 |
| 聚乙烯 | 3 | 6 | 7 | 8 |
| 小烛树蜡 | 0.5 | 1 | 2 | 3 |
| 双-二甘油多酰基己二酸酯-2 | 5 | 8 | 12 | 15 |
| 蚕丝胶蛋白 | 0.2 | 0.4 | 0.6 | 1 |
| 甘油辛酸酯 | 0.2 | 0.7 | 0.9 | 1 |
| 山梨坦倍半油酸酯 | 0.3 | 0.6 | 1 | 1.5 |
本申请还提供对比例1-7，其中，对比例1-7的重量份选择如表3所示，其余组分及重量份与实施例3完全相同：
表3对比例1-7的重量份选择
本发明提供了上述保湿口红的制备方法，包括如下步骤：
(1)将聚乙烯、小烛树蜡、地蜡、微晶蜡、二异硬脂醇苹果酸酯、双-二甘油多酰基己二酸酯-2、苯基聚三甲基硅氧烷13和季戊四醇四异硬脂酸酯加入乳化锅，搅拌加热至完全溶解，得到混合液A；
(2)将混合液A降温后加入CI 15850、CI 77491、十三烷醇偏苯三酸酯和棕榈酸乙基己酯，进行均质至分散完全，得到混合液B；
(3)向混合液B中加入硅石和二甲基甲硅烷基化硅石，搅拌至分散完全，得到混合液C；
(4)向混合液C中加入混合均匀的蚕丝胶蛋白、山梨坦倍半油酸酯和辛基十二醇，进行搅拌，继续加入甘油辛酸酯和生育酚乙酸酯，搅拌后出料备用。
效果分析
试验例1合格性测试
以QBT 1977-2004作为参照标准，检验实施例中口红的卫生指标是否合格，
卫生指标如表4所示：
表4卫生指标
测试结果如表5所示
表5实施例1-9测试结果
由表4和表5可知，本发明实施例提供的口红均符合卫生标准。
试验例2稳定性及保湿性测试
参照标准为QBT 1977-2004，针对相关原材料是添加比例在此口红配方里的实验效果和相关材料对口红的各项参数的影响，结果如表6所示，其中顺滑细腻度效果由好到差为：非常好>较好>一般>较差。
表6实施例1-9和对比例1-7的效果分析结果
由表6可知，实施例-9提供的口红，稳定性均很好，可以通过高低温稳定性测试；由对比例1、4、5、7可知，聚乙烯的量对口红的稳定性有很大影响，聚乙烯重量份为两份时，口红的高温稳定性测试不能通过；对比例2、3表明，仅含双-二甘油多酰基己二酸酯-2或仅含蚕丝胶蛋白时，顺滑细腻度均一般，仅能保湿3-4小时，对比例4、5、6、7的结果表明，双-二甘油多酰基己二酸酯-2、蚕丝胶蛋白以及聚乙烯间存在协同增效的作用。
最后所应当说明的是，以上实施例仅用以说明本发明的技术方案而非对本发明保护范围的限制，尽管参照较佳实施例对本发明作了详细说明，本领域的普通技术人员应当理解，可以对本发明的技术方案进行修改或者等同替换，而不脱离本发明技术方案的实质和范围。
Claims (6)
1.一种保湿口红，其特征在于，包含以下重量份的组分：聚乙烯6-8份、小烛树蜡1-2份、双-二甘油多酰基己二酸酯-2 8-12份、蚕丝胶蛋白0.4-0.6份、甘油辛酸酯0.7-0.9份、山梨坦倍半油酸酯0.6-1份、地蜡4-6份、微晶蜡2-4份、二异硬脂醇苹果酸酯10-15份、苯基聚三甲基硅氧烷10-15份、季戊四醇四异硬脂酸酯10-15份、CI 15850 5-7份、CI 77491 0.1-0.5份、十三烷醇偏苯三酸酯6-7份、棕榈酸乙基己酯6-7份、硅石4-6份、二甲基甲硅烷基化硅石0.5-1.5份、辛基十二醇10-12份和生育酚乙酸酯0.05-0.15份。
2.如权利要求1所述的保湿口红，其特征在于，包含以下重量份的组分：聚乙烯7.8份、小烛树蜡1.5份、双-二甘油多酰基己二酸酯-2 10份、蚕丝胶蛋白0.5份、甘油辛酸酯0.8份、山梨坦倍半油酸酯0.8份、地蜡5份、微晶蜡3份、二异硬脂醇苹果酸酯12份、苯基聚三甲基硅氧烷13份、季戊四醇四异硬脂酸酯12份、CI 15850 6.2份、CI 77491 0.3份、十三烷醇偏苯三酸酯6.5份、棕榈酸乙基己酯6.5份、硅石5份、二甲基甲硅烷基化硅石1份、辛基十二醇11份和生育酚乙酸酯0.1份。
3.一种如权利要求1-2任一项所述的保湿口红的制备方法，其特征在于，包括如下步骤：
（1）将聚乙烯、小烛树蜡、地蜡、微晶蜡、二异硬脂醇苹果酸酯、双-二甘油多酰基己二酸酯-2、苯基聚三甲基硅氧烷和季戊四醇四异硬脂酸酯加入乳化锅，搅拌加热至完全溶解，得到混合液A；
（2）将混合液A降温后加入CI 15850、CI 77491、十三烷醇偏苯三酸酯和棕榈酸乙基己酯，进行均质至分散完全，得到混合液B；
（3）向混合液B中加入硅石和二甲基甲硅烷基化硅石，搅拌至分散完全，得到混合液C；
（4）向混合液C中加入混合均匀的蚕丝胶蛋白、山梨坦倍半油酸酯和辛基十二醇，进行搅拌，继续加入甘油辛酸酯和生育酚乙酸酯，搅拌后出料备用。
4.如权利要求3所述的保湿口红的制备方法，其特征在于，所述步骤（1）中，搅拌的速率为100-200 r/min，加热的温度为80-85 ℃。
5.如权利要求3所述的保湿口红的制备方法，其特征在于，所述步骤（2）中，将混合液A降温至75-80 ℃，均质的速率为7000-8000 r/min。
6.如权利要求3所述的保湿口红的制备方法，其特征在于，所述步骤（3）中，搅拌的速率为100-200 r/min；所述步骤（4）中，搅拌的速率为50-100 r/min，搅拌的时间为15-20 min。
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