CN112094553A - Odorless wood wax oil for wiping - Google Patents
Odorless wood wax oil for wiping Download PDFInfo
- Publication number
- CN112094553A CN112094553A CN202010983064.3A CN202010983064A CN112094553A CN 112094553 A CN112094553 A CN 112094553A CN 202010983064 A CN202010983064 A CN 202010983064A CN 112094553 A CN112094553 A CN 112094553A
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- China
- Prior art keywords
- resin
- reaction kettle
- parts
- solvent
- candelilla
- Prior art date
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/06—Other polishing compositions
- C09G1/08—Other polishing compositions based on wax
- C09G1/10—Other polishing compositions based on wax based on mixtures of wax and natural or synthetic resin
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Paints Or Removers (AREA)
Abstract
The invention belongs to the technical field of furniture odor removal, and particularly discloses odorless wood wax oil which is prepared by sequentially adding a proper amount of hydrogenated solid resin, acrylic acid solid resin, candelilla resin and rosin modified resin into a reaction kettle, and then adding a small amount of alkane solvent into the reaction kettle; adjusting the temperature in the reaction kettle to 155 ℃, fully dissolving hydrogenated solid resin, acrylic acid solid resin, candelilla resin and rosin modified resin in the reaction kettle, reducing the temperature in the reaction kettle to 50 ℃, solidifying the numerical solution in the reaction kettle, finally adding an alkane solvent, a hardening wear-resistant wax auxiliary agent and a DBE solvent into the reaction kettle, uniformly stirring, standing, cooling, filtering and packaging; the cabinet body, the desk and the drawer after being wiped are completely dry, no odor residue is caused, no toxic or harmful gas is contained, no methylbenzene, dimethylbenzene, ethylbenzene, heavy metal or formaldehyde is contained, the harm of the toxic gas to human bodies is reduced, the living environment is safer and more comfortable, and the cost is low.
Description
Technical Field
The invention belongs to the technical field of furniture odor removal, and particularly relates to odorless wood-coated wax oil.
Background
The wood wax oil is a wiping agent extracted from natural plants, is suitable for surface treatment of natural materials and absorbent materials, is mainly used for surface oiling, waxing, polishing and repairing of various woods (including softwood and hardwood), and can also be used for surface treatment of composite boards, OSB boards and the like. The main materials are linseed oil, castor oil, soybean oil, carnauba wax, candelilla wax and the like. Although the formulas of various manufacturers are different, the natural vegetable oil and the vegetable wax are required to be standard configurations of a pot of excellent wood wax oil, the wood wax oil can penetrate into the interior of the wood to carry out deep moistening and maintenance on the wood, the wax can be tightly combined with wood fibers to enhance the surface hardness, and the wood is waterproof and antifouling, so that the gold combination can provide the most excellent beautifying and protecting effects on the wood.
At present, after a brand-new furniture cabinet body is manufactured, a layer of wood wax oil is generally coated on the surface of the furniture cabinet body to increase the gloss, the wear resistance and the aesthetic property of the surface of the furniture cabinet body, but the coating can generate pungent smell in construction, harm is brought to the environment and workers, and a long time is needed for volatilizing partial toxic and harmful gas after the construction is finished.
Accordingly, one skilled in the art has devised a non-odorous wood wax oil to solve the problems set forth in the background above.
Disclosure of Invention
The invention aims to provide odorless wood coating wax oil to solve the problems in the background technology.
In order to achieve the purpose, the invention adopts the following technical scheme: the odorless wood-coated wax oil is prepared from the following raw materials in parts by mass: 20-30 parts of hydrogenated solid resin, 25-35 parts of acrylic acid solid resin, 1-5 parts of candelilla resin, 2-5 parts of a hardening and wear-resistant wax auxiliary agent, 5-10 parts of DBE solvent, 15-30 parts of alkane solvent and 20-30 parts of rosin modified resin.
Preferably, the rosin modified resin is prepared from the following raw materials in parts by weight: 98 kg of primary rosin, 13 kg of glycerol, 0.2 kg of stabilizer compounded by di-tert-butyl-p-cresol and phosphite ester, and 0.6 kg of 6-tert-butyl-3-methylphenol.
Preferably, the candelilla resin is a brown vegetable wax with a melting temperature of 67-71 deg.C to increase the hardness of the resin when mixed with other ingredients.
Preferably, the DBE solvent is a high-boiling environment-friendly strong solvent.
A preparation method of odorless wood-coating wax oil comprises the following steps:
s1, sequentially adding a proper amount of hydrogenated solid resin, acrylic acid solid resin, candelilla resin and rosin modified resin into a reaction kettle, and adding a small amount of alkane solvent into the reaction kettle;
s2, adjusting the temperature in the reaction kettle to 150 ℃ and 180 ℃ to fully dissolve the hydrogenated solid resin, the acrylic acid solid resin, the candelilla resin and the rosin modified resin in the reaction kettle;
s3, reducing the temperature in the reaction kettle to 50 ℃ to solidify the numerical value solution in the reaction kettle;
and S4, finally adding an alkane solvent, a hardening and wear-resistant wax auxiliary agent and a DBE solvent into the reaction kettle, uniformly stirring, standing, cooling, filtering and packaging.
Preferably, the stirring time in step S4 is 5-15 min.
The invention has the technical effects and advantages that: compared with the prior art, the wood wax oil is prepared by mixing various resins to prepare the resin solution, adding various solvents and auxiliaries to prepare the wood wax oil, and coating the wood wax oil on the furniture cabinet body, so that the wood wax oil is odorless during construction, can completely dry the cabinet body, the desk and the drawer after being wiped, does not have any odor residue, does not contain toxic and harmful gases, does not contain methylbenzene, dimethylbenzene, ethylbenzene, heavy metals and formaldehyde, reduces the harm of the toxic gases to human bodies, ensures that the living environment is safer and more comfortable, and is low in cost, simple in preparation method and wide in application range.
Detailed Description
The technical solutions in the embodiments of the present invention are clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. The specific embodiments described herein are merely illustrative of the invention and do not delimit the invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The invention provides odorless wood-smearing wax oil which is prepared from the following raw materials in parts by mass: 20 parts of hydrogenated solid resin, 25 parts of acrylic solid resin, 1 part of candelilla resin, 2 parts of a hardening and wear-resistant wax auxiliary agent, 5 parts of DBE solvent, 15 parts of alkane solvent and 20 parts of rosin modified resin.
Specifically, the rosin modified resin is prepared from the following raw materials in parts by weight: 98 kg of primary rosin, 13 kg of glycerol, 0.2 kg of stabilizer compounded by di-tert-butyl-p-cresol and phosphite ester, and 0.6 kg of 6-tert-butyl-3-methylphenol.
Specifically, candelilla resin refers to a brown vegetable wax with a melting temperature of 67 deg.C to increase the hardness of the resin when mixed with other ingredients.
Specifically, the DBE solvent is a high-boiling environment-friendly strong solvent.
A preparation method of odorless wood-coating wax oil comprises the following steps:
s1, sequentially adding a proper amount of hydrogenated solid resin, acrylic acid solid resin, candelilla resin and rosin modified resin into a reaction kettle, and adding a small amount of alkane solvent into the reaction kettle;
s2, adjusting the temperature in the reaction kettle to 150 ℃ to fully dissolve the hydrogenated solid resin, the acrylic acid solid resin, the candelilla resin and the rosin modified resin in the reaction kettle;
s3, reducing the temperature in the reaction kettle to 50 ℃ to solidify the numerical value solution in the reaction kettle;
and S4, finally adding an alkane solvent, a hardening and wear-resistant wax auxiliary agent and a DBE solvent into the reaction kettle, uniformly stirring, standing, cooling, filtering and packaging.
Specifically, the stirring time in step S4 is 5 min.
Example 2
The invention provides odorless wood-smearing wax oil which is prepared from the following raw materials in parts by mass: 22 parts of hydrogenated solid resin, 26 parts of acrylic acid solid resin, 2 parts of candelilla resin, 3 parts of a hardening and wear-resistant wax auxiliary agent, 6 parts of DBE solvent, 18 parts of alkane solvent and 22 parts of rosin modified resin.
Specifically, the rosin modified resin is prepared from the following raw materials in parts by weight: 98 kg of primary rosin, 13 kg of glycerol, 0.2 kg of stabilizer compounded by di-tert-butyl-p-cresol and phosphite ester, and 0.6 kg of 6-tert-butyl-3-methylphenol.
Specifically, candelilla resin refers to a brown vegetable wax with a melting temperature of 69 deg.C to increase the hardness of the resin when mixed with other ingredients.
Specifically, the DBE solvent is a high-boiling environment-friendly strong solvent.
A preparation method of odorless wood-coating wax oil comprises the following steps:
s1, sequentially adding a proper amount of hydrogenated solid resin, acrylic acid solid resin, candelilla resin and rosin modified resin into a reaction kettle, and adding a small amount of alkane solvent into the reaction kettle;
s2, adjusting the temperature in the reaction kettle to 155 ℃, and fully dissolving the hydrogenated solid resin, the acrylic acid solid resin, the candelilla resin and the rosin modified resin in the reaction kettle;
s3, reducing the temperature in the reaction kettle to 50 ℃ to solidify the numerical value solution in the reaction kettle;
and S4, finally adding an alkane solvent, a hardening and wear-resistant wax auxiliary agent and a DBE solvent into the reaction kettle, uniformly stirring, standing, cooling, filtering and packaging.
Specifically, the stirring time in step S4 is 7 min.
Example 3
The invention provides odorless wood-smearing wax oil which is prepared from the following raw materials in parts by mass: 24 parts of hydrogenated solid resin, 28 parts of acrylic solid resin, 3 parts of candelilla resin, 3 parts of a hardening and wear-resistant wax auxiliary agent, 7 parts of DBE solvent, 18 parts of alkane solvent and 24 parts of rosin modified resin.
Specifically, the rosin modified resin is prepared from the following raw materials in parts by weight: 98 kg of primary rosin, 13 kg of glycerol, 0.2 kg of stabilizer compounded by di-tert-butyl-p-cresol and phosphite ester, and 0.6 kg of 6-tert-butyl-3-methylphenol.
Specifically, candelilla resin refers to a brown vegetable wax with a melting temperature of 68 deg.C to increase the hardness of the resin when mixed with other ingredients.
Specifically, the DBE solvent is a high-boiling environment-friendly strong solvent.
A preparation method of odorless wood-coating wax oil comprises the following steps:
s1, sequentially adding a proper amount of hydrogenated solid resin, acrylic acid solid resin, candelilla resin and rosin modified resin into a reaction kettle, and adding a small amount of alkane solvent into the reaction kettle;
s2, adjusting the temperature in the reaction kettle to 160 ℃, and fully dissolving the hydrogenated solid resin, the acrylic acid solid resin, the candelilla resin and the rosin modified resin in the reaction kettle;
s3, reducing the temperature in the reaction kettle to 50 ℃ to solidify the numerical value solution in the reaction kettle;
and S4, finally adding an alkane solvent, a hardening and wear-resistant wax auxiliary agent and a DBE solvent into the reaction kettle, uniformly stirring, standing, cooling, filtering and packaging.
Specifically, the stirring time in step S4 is 10 min.
Example 4
The invention provides odorless wood-smearing wax oil which is prepared from the following raw materials in parts by mass: 28 parts of hydrogenated solid resin, 30 parts of acrylic solid resin, 4 parts of candelilla resin, 4 parts of a hardening and wear-resistant wax auxiliary agent, 8 parts of DBE solvent, 25 parts of alkane solvent and 28 parts of rosin modified resin.
Specifically, the rosin modified resin is prepared from the following raw materials in parts by weight: 98 kg of primary rosin, 13 kg of glycerol, 0.2 kg of stabilizer compounded by di-tert-butyl-p-cresol and phosphite ester, and 0.6 kg of 6-tert-butyl-3-methylphenol.
Specifically, candelilla resin is a brown vegetable wax with a melting temperature of 67-71 deg.C to increase the hardness of the resin when mixed with other ingredients.
Specifically, the DBE solvent is a high-boiling environment-friendly strong solvent.
A preparation method of odorless wood-coating wax oil comprises the following steps:
s1, sequentially adding a proper amount of hydrogenated solid resin, acrylic acid solid resin, candelilla resin and rosin modified resin into a reaction kettle, and adding a small amount of alkane solvent into the reaction kettle;
s2, adjusting the temperature in the reaction kettle to 170 ℃ to fully dissolve the hydrogenated solid resin, the acrylic acid solid resin, the candelilla resin and the rosin modified resin in the reaction kettle;
s3, reducing the temperature in the reaction kettle to 50 ℃ to solidify the numerical value solution in the reaction kettle;
and S4, finally adding an alkane solvent, a hardening and wear-resistant wax auxiliary agent and a DBE solvent into the reaction kettle, uniformly stirring, standing, cooling, filtering and packaging.
Specifically, the stirring time in step S4 is 13 min.
Example 5
The invention provides odorless wood-smearing wax oil which is prepared from the following raw materials in parts by mass: 30 parts of hydrogenated solid resin, 35 parts of acrylic solid resin, 5 parts of candelilla resin, 5 parts of a hardening and wear-resistant wax auxiliary agent, 10 parts of DBE solvent, 30 parts of alkane solvent and 30 parts of rosin modified resin.
Specifically, the rosin modified resin is prepared from the following raw materials in parts by weight: 98 kg of primary rosin, 13 kg of glycerol, 0.2 kg of stabilizer compounded by di-tert-butyl-p-cresol and phosphite ester, and 0.6 kg of 6-tert-butyl-3-methylphenol.
Specifically, candelilla resin refers to a brown vegetable wax with a melting temperature of 71 deg.C to increase the hardness of the resin when mixed with other ingredients.
Specifically, the DBE solvent is a high-boiling environment-friendly strong solvent.
A preparation method of odorless wood-coating wax oil comprises the following steps:
s1, sequentially adding a proper amount of hydrogenated solid resin, acrylic acid solid resin, candelilla resin and rosin modified resin into a reaction kettle, and adding a small amount of alkane solvent into the reaction kettle;
s2, adjusting the temperature in the reaction kettle to 180 ℃ to fully dissolve the hydrogenated solid resin, the acrylic acid solid resin, the candelilla resin and the rosin modified resin in the reaction kettle;
s3, reducing the temperature in the reaction kettle to 50 ℃ to solidify the numerical value solution in the reaction kettle;
and S4, finally adding an alkane solvent, a hardening and wear-resistant wax auxiliary agent and a DBE solvent into the reaction kettle, uniformly stirring, standing, cooling, filtering and packaging.
Specifically, the stirring time in step S4 is 15 min.
The working principle and the using process of the invention are as follows: adding a proper amount of hydrogenated solid resin, acrylic acid solid resin, candelilla resin and rosin modified resin into a reaction kettle in sequence, and adding a small amount of alkane solvent into the reaction kettle; adjusting the temperature in the reaction kettle to 155 ℃, fully dissolving hydrogenated solid resin, acrylic acid solid resin, candelilla resin and rosin modified resin in the reaction kettle, reducing the temperature in the reaction kettle to 50 ℃, solidifying the numerical solution in the reaction kettle, finally adding an alkane solvent, a hardening wear-resistant wax auxiliary agent and a DBE solvent into the reaction kettle, uniformly stirring, standing, cooling, filtering and packaging; the coating is coated on the furniture cabinet body, has no smell during construction, can completely dry the cabinet body, the desk and the drawer after being wiped, has no smell residue, contains no toxic and harmful gas, and does not contain methylbenzene, dimethylbenzene, ethylbenzene, heavy metal and formaldehyde, reduces the harm of the toxic gas to human bodies, ensures that the living environment is safer and more comfortable, and has low cost, simple preparation method and wide application range.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation. The phrase "comprising a defined element does not exclude the presence of other identical elements in the process, method, article, or apparatus that comprises the element.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments or portions thereof without departing from the spirit and scope of the invention.
Claims (6)
1. An odorless wood coating wax oil is characterized in that: the material is prepared from the following raw materials in parts by mass: 20-30 parts of hydrogenated solid resin, 25-35 parts of acrylic acid solid resin, 1-5 parts of candelilla resin, 2-5 parts of a hardening and wear-resistant wax auxiliary agent, 5-10 parts of DBE solvent, 15-30 parts of alkane solvent and 20-30 parts of rosin modified resin.
2. An odorless wood smearing wax oil as claimed in claim 1, wherein: the rosin modified resin is prepared from the following raw materials in parts by weight: 98 kg of primary rosin, 13 kg of glycerol, 0.2 kg of stabilizer compounded by di-tert-butyl-p-cresol and phosphite ester, and 0.6 kg of 6-tert-butyl-3-methylphenol.
3. An odorless wood smearing wax oil as claimed in claim 1, wherein: the candelilla resin is a brown vegetable wax, the melting temperature is 67-71 ℃, and the candelilla resin is used for increasing the hardness of the resin and other components when the candelilla resin is mixed.
4. An odorless wood smearing wax oil as claimed in claim 1, wherein: the DBE solvent is a high-boiling-point environment-friendly strong solvent.
5. A method of preparing an odorless wood wipe wax oil according to any one of claims 1 to 4, wherein: the method comprises the following steps:
s1, sequentially adding a proper amount of hydrogenated solid resin, acrylic acid solid resin, candelilla resin and rosin modified resin into a reaction kettle, and adding a small amount of alkane solvent into the reaction kettle;
s2, adjusting the temperature in the reaction kettle to 150 ℃ and 180 ℃ to fully dissolve the hydrogenated solid resin, the acrylic acid solid resin, the candelilla resin and the rosin modified resin in the reaction kettle;
s3, reducing the temperature in the reaction kettle to 50 ℃ to solidify the numerical value solution in the reaction kettle;
and S4, finally adding an alkane solvent, a hardening and wear-resistant wax auxiliary agent and a DBE solvent into the reaction kettle, uniformly stirring, standing, cooling, filtering and packaging.
6. The method of claim 5, wherein the step of preparing the odorless wood wax oil comprises the steps of: in step S4, the stirring time is 5-15 min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010983064.3A CN112094553A (en) | 2020-09-18 | 2020-09-18 | Odorless wood wax oil for wiping |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010983064.3A CN112094553A (en) | 2020-09-18 | 2020-09-18 | Odorless wood wax oil for wiping |
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| Publication Number | Publication Date |
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| CN112094553A true CN112094553A (en) | 2020-12-18 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202010983064.3A Withdrawn CN112094553A (en) | 2020-09-18 | 2020-09-18 | Odorless wood wax oil for wiping |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5120355A (en) * | 1990-04-07 | 1992-06-09 | Nippon Oil Co., Ltd. | Water-repellent composition |
| CN102993981A (en) * | 2012-11-30 | 2013-03-27 | 浙江鑫松树脂有限公司 | Colorless rosin modified resin and production method thereof |
| CN109679423A (en) * | 2019-01-22 | 2019-04-26 | 重庆环绿明珠新材料科技有限公司 | A kind of aqueous wood wax oil and preparation method thereof |
| CN110591559A (en) * | 2019-10-17 | 2019-12-20 | 刘杰 | Wear-resistant waterproof wood wax oil and preparation method thereof |
| CN111534227A (en) * | 2020-05-09 | 2020-08-14 | 惠州市坤洋实业有限公司 | Environment-friendly wax oil applied to wooden furniture |
-
2020
- 2020-09-18 CN CN202010983064.3A patent/CN112094553A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5120355A (en) * | 1990-04-07 | 1992-06-09 | Nippon Oil Co., Ltd. | Water-repellent composition |
| CN102993981A (en) * | 2012-11-30 | 2013-03-27 | 浙江鑫松树脂有限公司 | Colorless rosin modified resin and production method thereof |
| CN109679423A (en) * | 2019-01-22 | 2019-04-26 | 重庆环绿明珠新材料科技有限公司 | A kind of aqueous wood wax oil and preparation method thereof |
| CN110591559A (en) * | 2019-10-17 | 2019-12-20 | 刘杰 | Wear-resistant waterproof wood wax oil and preparation method thereof |
| CN111534227A (en) * | 2020-05-09 | 2020-08-14 | 惠州市坤洋实业有限公司 | Environment-friendly wax oil applied to wooden furniture |
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Application publication date: 20201218 |