CN112090554B - Special high shear grinding dispersion system of graphite alkene thick liquids - Google Patents
Special high shear grinding dispersion system of graphite alkene thick liquids Download PDFInfo
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- CN112090554B CN112090554B CN202010907588.4A CN202010907588A CN112090554B CN 112090554 B CN112090554 B CN 112090554B CN 202010907588 A CN202010907588 A CN 202010907588A CN 112090554 B CN112090554 B CN 112090554B
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C19/00—Other disintegrating devices or methods
- B02C19/0056—Other disintegrating devices or methods specially adapted for specific materials not otherwise provided for
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C19/00—Other disintegrating devices or methods
- B02C19/0012—Devices for disintegrating materials by collision of these materials against a breaking surface or breaking body and/or by friction between the material particles (also for grain)
- B02C19/0018—Devices for disintegrating materials by collision of these materials against a breaking surface or breaking body and/or by friction between the material particles (also for grain) using a rotor accelerating the materials centrifugally against a circumferential breaking surface
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C25/00—Control arrangements specially adapted for crushing or disintegrating
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Abstract
The invention discloses a special high-shear grinding and dispersing system for graphene slurry, which comprises a dispersion device in a kettle, a reaction kettle device, an impeller stirring device in the kettle, a conveying device, a high-speed grinding and dispersing device and a conveying pipeline, wherein the dispersion device in the kettle and the impeller stirring device in the kettle are arranged on the reaction kettle device, the conveying device is arranged below the reaction kettle device and is connected with the reaction kettle device and the high-speed grinding and dispersing device, the conveying device conveys the slurry of the reaction kettle device into the high-speed grinding and dispersing device, and the conveying pipeline and a monitoring, detecting and adjusting device are arranged among the reaction kettle device, the conveying device and the high-speed grinding and dispersing device. The high-shear grinding dispersion system special for graphene slurry can be used for multi-dispersing and grinding to obtain various graphene slurries with good quality.
Description
Technical Field
The invention belongs to the technical field of manufacturing of general mechanical equipment, and particularly relates to a special high-shear grinding dispersion system for graphene slurry.
Background
The graphene product has wide application, and the graphene slurry can be used for preparing various graphene products, such as: graphene conductive materials, graphene heating materials, graphene powder and the like.
The application provides a special high shear grinding dispersion system of graphite alkene thick liquids for obtain various graphite alkene thick liquids.
Disclosure of Invention
The purpose of the invention is as follows: the invention aims to provide a special high-shear grinding dispersion system for graphene slurry, which has a compact process and small occupied area; the slurry can be dispersed and ground in a multiple way, and the quality of the slurry is good; the process is monitored, and the production period can be controlled according to the requirement.
The technical scheme is as follows: the utility model provides a special high shear grinding dispersion system of graphite alkene thick liquids, impeller agitating unit, conveyor, high-speed grinding dispersion devices and pipeline in dispersion devices, reation kettle device, the cauldron, the middle axle center position of reation kettle device is equipped with impeller agitating unit in the cauldron, impeller agitating unit bilateral symmetry is equipped with dispersion devices in a set of cauldron in the cauldron, the below of reation kettle device is equipped with conveyor, one side of reation kettle device is equipped with high-speed grinding dispersion devices, conveyor's input and reation kettle device are connected, conveyor's output and high-speed grinding dispersion devices are connected, pipeline locates between reation kettle device, conveyor and the high-speed grinding dispersion devices. The in-kettle dispersing device and the in-kettle impeller stirring device work in the kettle body to grind and disperse the slurry in the kettle body; the reaction kettle device, the conveying device and the high-speed grinding and dispersing device are connected and combined into a slurry circulating conveying system through a conveying pipeline, and the slurry in the kettle body is circularly conveyed and processed until the requirements are met.
Further, foretell special high shear grinding dispersion system of graphite alkene thick liquids, pipeline includes first conveyer pipe, second conveyer pipe, third conveyer pipe and locates the control on the pipeline and detect adjusting device, first duct junction reation kettle device and conveyor, second duct junction conveyor and high-speed grinding dispersion devices, third duct junction high-speed grinding dispersion devices and reation kettle device.
Further, foretell special high shear grinding disperse system of graphite alkene thick liquids, be equipped with control detection adjusting device on first conveyer pipe, second conveyer pipe and the third conveyer pipe, the input port of first conveyer pipe is equipped with the ooff valve, the second conveyer pipe is equipped with first viewing aperture, third conveyer pipe is from upwards being equipped with second temperature probe, sample connection, second viewing aperture and de-ironing separator down in proper order, third conveyer pipe input port still is equipped with the tee bend discharge gate. The monitoring, detecting and adjusting devices can monitor, detect and adjust the slurry in the conveying pipeline in real time.
Further, foretell special high shear grinding disperse system of graphite alkene thick liquids, the reation kettle device includes kettle cover, the cauldron body, cauldron collet and cauldron support, the outer wall of cauldron leg joint, the inner chamber of cauldron collet is equipped with the cauldron body, the lower extreme of the cauldron body is equipped with the discharging pipe, discharging pipe lower extreme and first duct connections, the top of the cauldron body is equipped with the kettle cover through the screw connection, be equipped with raw materials entry, a set of first mount pad and second mount pad on the kettle cover.
Further, foretell special high shear grinding disperse system of graphite alkene thick liquids, disperse the device including first motor, shaft coupling, flange seat, axle and dispersion mechanism in the cauldron, the flange seat is equipped with upper flange board, well flange board and lower flange board, the lower flange board passes through the screw and is connected with the first mount pad of below, first motor flange passes through the screw and is connected with the upper flange board of below.
Further, foretell special high shear grinding dispersion system of graphite alkene thick liquids, dispersion mechanism from the top down is first end cover, first bearing, retaining ring, second bearing, second end cover, connecting rod, connecting plate, stator, rotor, big flat pad and cap nut in proper order, first end cover passes through the fix with screw on the well flange plate of below, the second end cover passes through the fix with screw on the lower flange plate of top, the below of lower flange plate is equipped with a set of connecting rod, the below of connecting rod is equipped with the connecting plate, lower flange plate and connecting plate pass through the connecting rod and locate the circular nut at connecting rod both ends and connect, the stator cover is located epaxially, the stator still passes through the fix with screw on the connecting plate, the rotor passes through big flat pad and the cap nut is fixed at the end of axle. The rotor rotates along with the shaft, and relative motion through stator and rotor disperses the thick liquids, two dispersion devices of dispersion device work at the different degree of depth layers of the cauldron body in the cauldron, let the thick liquids in the cauldron body all obtain abundant dispersion, and every dispersion device can the exclusive use.
Further, foretell special high shear grinding dispersion system of graphite alkene thick liquids, impeller agitating unit includes second motor, connecting axle and impeller in the cauldron, the ring flange of second motor is fixed on the second flange seat of kettle cover, the below of second motor is equipped with the connecting axle, the end of connecting axle is equipped with the impeller, the impeller is W shape, the wheel piece of the both sides of impeller matches with the inner wall of the cauldron body and follows the inner wall rotation. The impeller stirring device in the kettle can uniformly stir the mixture in the kettle body.
Further, the special high shear grinding dispersion system for graphene slurry comprises a third motor, a pump and a fixed bottom frame, wherein the third motor and the pump are fixed on the fixed bottom frame below the third motor and the pump.
Further, foretell special high shear grinding dispersion system of graphite alkene thick liquids, high-speed grinding dispersion devices includes chassis, high-speed grinding dispenser, fourth motor and temperature regulation system, high-speed grinding dispenser and fourth motor are fixed on the chassis of below, temperature regulation system is connected with the cooling loop of high-speed grinding dispenser, through the temperature of the high-speed grinding dispenser of cooling water control, the export of high-speed grinding dispenser is connected with the tee bend discharge gate of third conveyer pipe.
Further, foretell special high shear of graphite alkene thick liquids grinds dispersion system, the export of high speed grinding dispersion machine is equipped with the three-way valve, and the passageway of the same way of export is used for arranging the material all the way in inserting the cauldron, the three-way valve can control to export thick liquids and get into the cauldron body or bin outlet, temperature regulation system is equipped with a temperature control probe, the temperature of real time monitoring high speed grinding dispersion machine.
The technical scheme shows that the invention has the following beneficial effects:
1. the high-shear grinding dispersion system special for graphene slurry is compact in process, can implement multiple dispersing and grinding according to slurry requirements, monitors and adjusts slurry in each stage, and produces various high-quality graphene slurries.
2. The high-shear grinding dispersion system special for graphene slurry is suitable for preparing graphene heating film slurry.
3. The high-shear grinding dispersion system special for graphene slurry is suitable for preparing graphene conductive slurry.
4. The high-shear grinding dispersion system special for graphene slurry is a key system for preparing graphene powder.
Drawings
Fig. 1 is a schematic structural diagram of a special high shear grinding and dispersing system for graphene slurry according to the present invention;
fig. 2 is a schematic structural diagram of a reaction kettle device of the special high-shear grinding and dispersing system for graphene slurry according to the present invention;
fig. 3 is a schematic structural diagram of a dispersing device in a kettle of the high shear grinding and dispersing system special for graphene slurry according to the present invention;
fig. 4 is a schematic partial structural diagram of a reactor dispersing device of the dedicated high shear grinding dispersing system for graphene slurry according to the present invention;
fig. 5 is a schematic structural diagram of an impeller stirring device in a kettle of the special high shear grinding and dispersing system for graphene slurry according to the present invention;
fig. 6 is a schematic structural diagram of a conveying device of the graphene slurry dedicated high shear grinding and dispersing system according to the present invention;
fig. 7 is a schematic structural diagram of a high-speed grinding and dispersing device and a conveying pipeline of the special high-shear grinding and dispersing system for graphene slurry according to the present invention;
in the figure: 1 in-kettle dispersing device, 11 first motor, 12 coupler, 13 flange seat, 131 upper flange plate, 132 middle flange plate, 133 lower flange plate, 14 shaft, 15 connecting rod, 16 connecting plate, 17 stator, 18 rotor, 19 first end cover, 20 first bearing, 21 retainer ring, 22 second bearing, 23 second end cover, 24 large flat pad, 25 cover-shaped nut, 2 reaction kettle device, 21 kettle cover, 211 raw material inlet, 212 first flange seat, 213 second flange seat, 22 kettle body, 221 discharge pipe, 23 kettle bottom support, 24 kettle support, 3 kettle middle impeller stirring device, 31 second motor, 32 connecting shaft, 33 impeller, 4 conveying device, 41 third motor, 42 pump, 43 fixed bottom support, 5 high-speed grinding dispersing device, 51 bottom support, 52 high-speed grinding dispersing machine, 53 fourth motor, 54 temperature regulating system, 541 first temperature control probe, 6 conveying pipeline, 61 first conveying pipe, 611 switch valve, 62 second delivery pipe, 621 first inspection hole, 63 third delivery pipe, 631 second temperature control probe, 632 sampling hole, 633 second inspection hole, 634 de-ironing separator, 635 three-way discharge hole.
Detailed Description
The invention is further elucidated with reference to the drawings and the embodiments.
Reference will now be made in detail to embodiments of the present invention, examples of which are illustrated in the accompanying drawings, wherein like reference numerals refer to the same or similar elements or elements having the same or similar functions throughout. The embodiments described below with reference to the drawings are illustrative and intended to be illustrative of the invention and are not to be construed as limiting the invention.
In the description of the present invention, it is to be understood that the terms "center", "longitudinal", "lateral", "length", "width", "thickness", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "clockwise", "counterclockwise", and the like, indicate orientations and positional relationships based on those shown in the drawings, and are used only for convenience of description and simplicity of description, and do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus, are not to be considered as limiting the present invention.
Furthermore, the terms "first", "second" and "first" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance or implicitly indicating the number of technical features indicated. Thus, a feature defined as "first" or "second" may explicitly or implicitly include one or more of that feature. In the description of the present invention, unless otherwise specified, "a plurality" means two or more unless explicitly defined otherwise.
In the present invention, unless otherwise explicitly stated or limited, the terms "mounted," "connected," "fixed," and the like are to be construed broadly and may, for example, be fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood by those skilled in the art according to specific situations.
In the present invention, unless expressly stated or limited otherwise, the recitation of a first feature "on" or "under" a second feature may include the recitation of the first and second features being in direct contact, and may also include the recitation that the first and second features are not in direct contact, but are in contact via another feature between them. Also, the first feature being "on," "above" and "over" the second feature includes the first feature being directly on and obliquely above the second feature, or merely indicating that the first feature is at a higher level than the second feature. A first feature being "under," "below," and "beneath" a second feature includes the first feature being directly under and obliquely below the second feature, or simply meaning that the first feature is at a lesser elevation than the second feature.
Example 1
As shown in fig. 1-7, the high shear grinding and dispersing system special for graphene slurry of the present invention comprises a dispersion device 1 in a kettle, a reaction kettle device 2, an impeller stirring device 3 in a kettle, a conveying device 4, a high speed grinding and dispersing device 5 and a conveying pipeline 6, a middle shaft center position of the reaction kettle device 2 is provided with a kettle-in impeller stirring device 3, a group of kettle-in dispersing devices 1 are symmetrically arranged at two sides of the kettle-in impeller stirring device 3, a conveying device 4 is arranged below the reaction kettle device 2, a high-speed grinding and dispersing device 5 is arranged on one side of the reaction kettle device 1, the input end of the conveying device 4 is connected with the reaction kettle device 2, the output end of the conveying device 4 is connected with the high-speed grinding and dispersing device 5, the conveying pipeline 6 is arranged among the reaction kettle device 2, the conveying device 4 and the high-speed grinding and dispersing device 5. The in-kettle dispersing device 1 and the in-kettle impeller stirring device 3 work in the kettle body 22 to grind and disperse the slurry in the kettle body 22; the reaction kettle device 2, the conveying device 4 and the high-speed grinding and dispersing device 5 are connected and combined into a slurry circulating conveying system through a conveying pipeline 6, and the slurry in the kettle body 22 is circularly conveyed and processed until the requirements are met.
Example 2
As shown in fig. 1-7, the high shear grinding and dispersing system special for graphene slurry of the present invention comprises a dispersion device 1 in a kettle, a reaction kettle device 2, an impeller stirring device 3 in a kettle, a conveying device 4, a high speed grinding and dispersing device 5 and a conveying pipeline 6, a middle shaft center position of the reaction kettle device 2 is provided with a kettle-in impeller stirring device 3, a group of kettle-in dispersing devices 1 are symmetrically arranged at two sides of the kettle-in impeller stirring device 3, a conveying device 4 is arranged below the reaction kettle device 2, a high-speed grinding and dispersing device 5 is arranged on one side of the reaction kettle device 1, the input end of the conveying device 4 is connected with the reaction kettle device 2, the output end of the conveying device 4 is connected with the high-speed grinding and dispersing device 5, the conveying pipeline 6 is arranged among the reaction kettle device 2, the conveying device 4 and the high-speed grinding and dispersing device 5. The in-kettle dispersing device 1 and the in-kettle impeller stirring device 3 work in the kettle body 22 to grind and disperse the slurry in the kettle body 22; the reaction kettle device 2, the conveying device 4 and the high-speed grinding and dispersing device 5 are connected and combined through a conveying pipeline 6 to form a slurry circulating conveying system, and the slurry in the kettle body 22 is circularly conveyed and processed until the requirement is met.
Be equipped with the control on first conveyer pipe 61, second conveyer pipe 62 and the third conveyer pipe 63 and detect adjusting device, the input port of first conveyer pipe 61 is equipped with ooff valve 611, second conveyer pipe 62 is equipped with first viewing aperture 621, third conveyer pipe 63 from the bottom up is equipped with second temperature probe 631, sample connection 632, second viewing aperture 633 and de-ironing separator 634 in proper order, third conveyer pipe 63 input port still is equipped with tee bend discharge gate 635. The monitoring, detecting and adjusting devices can be used for monitoring, detecting and adjusting the slurry in the conveying pipeline 6 in real time.
The reaction kettle device 2 comprises a kettle cover 21, a kettle body 22, a kettle bottom support 23 and a kettle support 24, the outer wall of the kettle bottom support 23 is connected with the kettle support 24, the inner cavity of the kettle bottom support 23 is provided with the kettle body 22, the lower end of the kettle body 22 is provided with a discharge pipe 221, the lower end of the discharge pipe 221 is connected with a first conveying pipe 61, the kettle cover 21 connected with a screw is arranged above the kettle body 22, and a raw material inlet 211, a first mounting seat 212 and a second mounting seat 213 are arranged on the kettle cover 21.
The dispersion device 1 in the kettle comprises a first motor 11, a coupler 12, a flange seat 13, a shaft 14 and a dispersion mechanism, wherein the flange seat 13 is provided with an upper flange plate 131, a middle flange plate 132 and a lower flange plate 133, the lower flange plate 133 is connected with a first mounting seat 212 below through screws, and the flange of the first motor 11 is connected with the upper flange plate 131 below through screws.
The dispersing mechanism comprises a first end cover 19, a first bearing 20, a retainer ring 21, a second bearing 22, a second end cover 23, a connecting rod 15, a connecting plate 16, a stator 17, a rotor 18, a large flat gasket 24 and a cap nut 25 from top to bottom in sequence, the first end cover 19 is fixed on a middle flange plate 132 below through screws, the second end cover 23 is fixed on a lower flange plate 133 above through screws, a group of connecting rods 15 are arranged below the lower flange plate 133, the connecting plate 16 is arranged below the connecting rod 15, the lower flange plate 133 and the connecting plate 16 are connected with round nuts arranged at two ends of the connecting rod 15 through the connecting rod 15, the stator 17 is sleeved on a shaft, the stator 17 is further fixed on the connecting plate 16 through screws, and the connecting plate 18 is fixed at the tail end of the shaft 14 through the large flat gasket 24 and the cap nut 25. The dispersion mechanism rotor 18 rotates along with the rotation of the shaft 14, slurry is dispersed through the relative motion of the stator 17 and the rotor 18, two dispersion devices of the dispersion device 1 in the kettle work at different depth layers in the kettle body 22, the slurry in the kettle body 22 is fully dispersed, and each dispersion device can be used independently.
The conveying device 4 comprises a third motor 41, a pump 42 and a fixed chassis 43, wherein the third motor 41 and the pump 42 are fixed on the lower fixed chassis 43.
The high-speed grinding and dispersing device 5 comprises a base frame 51, a high-speed grinding and dispersing machine 52, a fourth motor 53 and a temperature adjusting system 54, wherein the high-speed grinding and dispersing machine 52 and the fourth motor 53 are fixed on the base frame 51 below, the temperature adjusting system 54 is connected with a cooling loop of the high-speed grinding and dispersing machine 52, the temperature of the high-speed grinding and dispersing machine 52 is controlled by cooling water, and an outlet of the high-speed grinding and dispersing machine 52 is connected with a three-way discharge port 635 of a third conveying pipe 63.
The export of high-speed grinding dispenser 52 is equipped with the three-way valve, and the passageway of the same way of export is connected in the cauldron, is used for the row material all the way, the three-way valve can control export thick liquids and get into the cauldron body 22 or discharge through the bin outlet, temperature regulation system 54 is equipped with first control by temperature change probe 541, the high-speed temperature that grinds dispenser 52 of real time monitoring.
The working principle of the special high-shear grinding dispersion system for graphene slurry provided by the invention is as follows:
1) before the high-speed grinding disperser 52 starts working, cooling water is introduced into a cooling system of the high-speed grinding disperser for controlling the temperature of the high-speed grinding disperser;
2) closing an input valve of the pump 42 and a three-way valve of an outlet of the high-speed grinding dispersion machine 52, and putting raw materials into the kettle from a raw material inlet 211 of the kettle cover 21, wherein the raw materials comprise raw material graphite and different additives in proportion;
3) starting a first motor 11 of the dispersing device 1 in the kettle and a second motor 31 of the impeller stirring device 3 in the kettle to disperse and mix the graphite raw material and the additive;
4) starting a third motor 41 of the conveying device 4, starting a fourth motor 53 of the high-speed grinding and dispersing device 5, opening a switch valve 611 at the bottom of the kettle, and transmitting the mixed materials in the kettle body 22 to an input port of the high-speed grinding and dispersing machine 52 through a pump 42, wherein the mixed materials are further ground and dispersed in the high-speed grinding and dispersing machine 52;
5) opening a three-way valve at the outlet of the high-speed grinding disperser 52 to enable the mixed raw materials to flow into the kettle body 22, conveying the raw materials to the high-speed grinding disperser 52 by the pump 42 after the raw materials are dispersed and stirred in the kettle body 22, opening a discharge port in the three-way valve at the outlet of the high-speed grinding disperser 52 to discharge the slurry after the ground and dispersed slurry meets the requirements, and finishing the preparation of the slurry, wherein different additives are used for preparing graphene slurries with different properties;
6) in the preparation process, if the mixed raw material is found to be unsuitable to flow into the next device or be discharged through the first observation port 621, the second observation port 633 or the sampling port 632, the kettle bottom switch valve 611 or the outlet of the three-way valve of the high-speed grinding disperser 52 can be selected to be closed until the state of the mixed raw material obtained through the observation port and the sampling port meets the requirement, and the mixed raw material can flow into the next device or be discharged. Thus, various devices can be optimally utilized to produce a slurry of good quality.
The above description is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, several modifications can be made without departing from the principle of the present invention, and these modifications should also be regarded as the protection scope of the present invention.
Claims (6)
1. The utility model provides a special high shear grinding disperse system of graphite alkene thick liquids which characterized in that: comprises a dispersing device (1) in a kettle, a reaction kettle device (2), a impeller stirring device (3) in the kettle, a conveying device (4), a high-speed grinding dispersing device (5) and a conveying pipeline (6), wherein the middle axle center position of the reaction kettle device (2) is provided with the impeller stirring device (3) in the kettle, two sides of the impeller stirring device (3) in the kettle are symmetrically provided with a group of dispersing devices (1) in the kettle, two dispersing devices of the dispersing devices (1) in the kettle work at different depth layers in a kettle body (22), the conveying device (4) is arranged below the reaction kettle device (2), one side of the reaction kettle device (2) is provided with the high-speed grinding dispersing device (5), the input end of the conveying device (4) is connected with the reaction kettle device (2), the output end of the conveying device (4) is connected with the high-speed grinding dispersing device (5), the conveying pipeline (6) is arranged among the reaction kettle device (2), the conveying device (4) and the high-speed grinding and dispersing device (5) and comprises a first conveying pipe (61), a second conveying pipe (62) and a third conveying pipe (63), the first conveying pipe (61) is connected with the reaction kettle device (2) and the conveying device (4), the second conveying pipe (62) is connected with the conveying device (4) and the high-speed grinding and dispersing device (5), and the third conveying pipe (63) is connected with the high-speed grinding and dispersing device (5) and the reaction kettle device (2); the device is characterized in that monitoring, detecting and adjusting devices are arranged on the first conveying pipe (61), the second conveying pipe (62) and the third conveying pipe (63), a switch valve (611) is arranged at an input port of the first conveying pipe (61), a first observation port (621) is arranged on the second conveying pipe (62), a second temperature probe (631), a sampling port (632), a second observation port (633) and an iron remover (634) are sequentially arranged on the third conveying pipe (63) from bottom to top, and a three-way discharge port (635) is further arranged at an input port of the third conveying pipe (63); high-speed grinding dispersion devices (5) are including chassis (51), high-speed grinding dispersion machine (52), fourth motor (53) and temperature regulation system (54), high-speed grinding dispersion machine (52) and fourth motor (53) are fixed on chassis (51) of below, the export of high-speed grinding dispersion machine (52) is equipped with the three-way valve to be connected with tee bend discharge gate (635) of third conveyer pipe (63), temperature regulation system (54) are connected with the cooling loop of high-speed grinding dispersion machine (52), be equipped with first temperature control probe (541) on temperature regulation system (54).
2. The graphene slurry dedicated high shear grinding dispersion system according to claim 1, wherein: the reaction kettle device (2) comprises a kettle cover (21), a kettle body (22), a kettle bottom support (23) and a kettle support (24), wherein the kettle support (24) is connected with the outer wall of the kettle bottom support (23), the inner cavity of the kettle bottom support (13) is provided with the kettle body (22), the lower end of the kettle body (22) is provided with a discharging pipe (221), the lower end of the discharging pipe (221) is connected with a first conveying pipe (61), the kettle cover (21) connected through a screw is arranged above the kettle body (22), and a raw material inlet (211), a group of first mounting seats (212) and a second mounting seat (213) are arranged on the kettle cover (21).
3. The graphene slurry dedicated high shear grinding dispersion system according to claim 1, wherein: dispersing device (1) includes first motor (11), shaft coupling (12), flange seat (13), axle (14) and dispersion mechanism in the cauldron, flange seat (13) are equipped with flange board (131), well flange board (132) and lower flange board (133), lower flange board (133) are connected through screw and first mount pad (212) of below, first motor (11) flange is connected through screw and upper flange board (131) of below.
4. The graphene slurry dedicated high shear grinding dispersion system according to claim 3, wherein: the dispersing mechanism comprises a first end cover (19), a first bearing (20), a retainer ring (21), a second bearing (22), a second end cover (23), a connecting rod (15), a connecting plate (16), a stator (17), a rotor (18), a large flat pad (24) and a cap nut (25) from top to bottom in sequence, wherein the first end cover (19) is fixed on a middle flange plate (132) below through screws, the second end cover (23) is fixed on a lower flange plate (133) above through screws, a group of connecting rods (15) are arranged below the lower flange plate (133), the connecting plate (16) is arranged below the connecting rod (15), the lower flange plate (133) and the connecting plate (16) are connected with round nuts arranged at two ends of the connecting rod (15) through the connecting rod (15), the stator (17) is sleeved on the shaft (14), and the stator (17) is further fixed on the connecting plate (16) through screws, the rotor (18) is secured to the end of the shaft (14) by a large flat washer (24) and a cap nut (25).
5. The graphene slurry dedicated high shear grinding dispersion system according to claim 1, wherein: impeller agitating unit (3) include second motor (31), connecting axle (32) and impeller (33) in the cauldron, the ring flange of second motor (31) is fixed on second flange seat (213) of kettle cover (21), the below of second motor (31) is equipped with connecting axle (32), the end of connecting axle (32) is equipped with impeller (33).
6. The graphene slurry dedicated high shear grinding dispersion system according to claim 1, wherein: the conveying device (4) comprises a third motor (41), a pump (42) and a fixed chassis (43), wherein the third motor (41) and the pump (42) are fixed on the fixed chassis (43) below.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010907588.4A CN112090554B (en) | 2020-09-02 | 2020-09-02 | Special high shear grinding dispersion system of graphite alkene thick liquids |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010907588.4A CN112090554B (en) | 2020-09-02 | 2020-09-02 | Special high shear grinding dispersion system of graphite alkene thick liquids |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN112090554A CN112090554A (en) | 2020-12-18 |
| CN112090554B true CN112090554B (en) | 2022-07-22 |
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| CN202010907588.4A Active CN112090554B (en) | 2020-09-02 | 2020-09-02 | Special high shear grinding dispersion system of graphite alkene thick liquids |
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| CN104785348A (en) * | 2015-04-26 | 2015-07-22 | 潘阿海 | High-shearing and accurate-grinding complete equipment |
| CN204973901U (en) * | 2015-09-14 | 2016-01-20 | 福建亚亨动力科技集团有限公司 | Lead acid battery colloid electrolyte stirring processingequipment |
| CN205517398U (en) * | 2016-04-22 | 2016-08-31 | 无锡嘉联电子材料有限公司 | Biax stirred tank for epoxy resin compound |
| CN207307647U (en) * | 2017-10-10 | 2018-05-04 | 合肥新万成环保科技有限公司 | Band machine envelope high shearing mixing emulsor |
| CN207786526U (en) * | 2017-12-22 | 2018-08-31 | 河南硅宝能源科技有限公司 | A kind of high speed dispersor automatic water inflow device |
| CN208097857U (en) * | 2018-03-01 | 2018-11-16 | 山东宇龙高分子科技有限公司 | A kind of middle high viscosity material stirring Scattered Kettle |
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