CN112057396A - Graphene-containing mild cleansing facial cleanser - Google Patents
Graphene-containing mild cleansing facial cleanser Download PDFInfo
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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Abstract
The invention relates to the technical field of facial cleanser, and discloses a mild cleansing facial cleanser containing graphene, which comprises the following formula components in parts by weight: 12-26 parts of honeysuckle extract, 14-26 parts of aloe extract, 12-22 parts of tea seed oil, 8-15 parts of fructus forsythiae extract, 8-12 parts of Chinese yam extract, 0.7-17 parts of graphene, 2-6 parts of coconut diethanolamide, 2-6 parts of rose extract, 1-4 parts of wild chrysanthemum extract, 5-50 parts of humectant, 0.2-12 parts of preservative and 5-10 parts of deionized water; the facial cleanser can be used for deeply cleaning skin and has no stimulation to the skin, so that adverse symptoms caused by blockage of skin pores are avoided, meanwhile, the graphene is added into the facial cleanser, the bacteriostatic effect is remarkable, the antibacterial property of the graphene comes from the sharp two-dimensional edge of the graphene, the covering effect and the oxidative stress reaction of a sheet layer cause the cell membrane of bacteria to be damaged, intracellular substances are caused to flow out, the bacteria are killed, and the problem of acne bacteria is effectively solved.
Description
Technical Field
The invention relates to the technical field of facial cleanser, and particularly relates to a mild cleansing facial cleanser containing graphene and a preparation method thereof.
Background
The face is used as a human face, the face is particularly important to keep clean, and in order to effectively clean the face and fully remove stains and grease on the face, people invent a cleaning product which is facial cleanser and is specially used for cleaning the face; the facial cleanser is a facial cleaning product for cleaning skin, and has good cleaning capacity of the soap and certain nursing capacity; facial cleanser as a facial cleanser has gradually replaced soap and is popular with consumers.
At present, most people are troubled by skin problems such as acne and the like, the skin problems undoubtedly have certain negative influence and negative emotion on the psychology and physiology of the people, and the skin problems such as the acne and the like are mainly caused by the following 3 points: firstly, with the continuous improvement of living standard and scientific and technological progress, people have no attention to diet and irregular work and rest, and skin problems such as acne, whelk, acne and the like come after each other; in recent years, the air quality is gradually deteriorated, a large amount of fine particles are suspended in the air, and contain a large amount of harmful substances such as heavy metals, microorganisms and the like, and the fine particles have small particle size and strong activity, are easy to adhere to the skin and can penetrate into pores of the skin, so that the skin is increasingly poor in the past; thirdly, in the face washing process, people cannot clean the skin completely, pores are blocked, and the skin becomes worse and worse due to accumulation in the day and month.
However, the existing facial cleanser has insignificant cleaning effect and many side effects, is difficult to effectively clean grease on skin and in pores, is particularly easy to accumulate grease and dirt in the pores, further grows bacteria, causes a series of skin problems such as acne and the like, seriously has the adverse effects of fluorescent face, red face and the like, and brings great harm to human bodies.
With the discovery that graphene has antibacterial property and good biocompatibility, the application of graphene in medicine is gradually developed; acne is mainly caused by inflammation caused by anaerobic bacteria acne bacillus, the existing method for solving acne mainly takes oil control as a main method and is supplemented with medicines, but the methods have no great effect, so that a medicine which can directly kill the acne bacillus and has no drug resistance is urgently needed; in 2010, a task group in Huangqing by the institute of physics of Chinese academy first discovers that graphene and graphene oxide have antibacterial property, and the graphene nano material has sharp edges at atomic level and can pierce the cell wall of bacteria to enable the cytoplasm of the bacteria to flow outwards; graphene also causes damage to cell membranes when it comes into contact with bacteria, and is a potential physical antibiotic, raising the hot tide of graphene in biological applications.
Disclosure of Invention
The invention aims to provide a mild cleansing facial cleanser containing graphene and a preparation method thereof.
The facial cleanser adopts various natural mild formulas, has an outstanding cleaning effect, can deeply clean the skin, and has no stimulation to the skin, so that adverse symptoms caused by blockage of skin pores are avoided.
In order to achieve the purpose, the invention provides the following technical scheme: the mild cleansing facial cleanser containing graphene comprises the following formula components in parts by weight:
12-26 parts of honeysuckle extract
Aloe extract 14-26 parts
12-22 parts of tea seed oil
8-15 parts of fructus forsythiae extract
8-12 parts of Chinese yam extract
0.7-17 parts of graphene
Coconut diethanolamide 2-6 weight portions
2-6 parts of rose extract
1-4 parts of wild chrysanthemum extract
5-50 parts of humectant
0.2 to 12 portions of preservative
5-10 parts of deionized water.
Preferably, the added graphene is one or two of graphene oxide and reduced graphene dispersion prepared by a modified Hummers method.
The Graphene Oxide (GO) and Reduced Graphene Oxide (RGO) dispersion liquid is prepared by the following method:
accurately weighing a certain amount of graphene oxide powder prepared by an improved Hummers method, adding the graphene oxide powder into a conical flask to prepare a graphene oxide solution with the concentration of 0.5-150 mug/mL, performing ultrasonic dispersion treatment for 30min, adding a rotor, and stirring until the solution is uniform; the steps for preparing the reduced graphene solution are the same as above, and attention needs to be paid to ultraviolet sterilization of the dispersion liquid in a clean bench.
Preferably, the graphene is:
0.5-8 parts of reduced graphene
0.2-9 parts of graphene oxide.
Preferably, a modified Hummers method is adopted to prepare graphite which is a precursor of graphene powder, and the mesh number of the graphite is 800-10000 meshes.
Preferably, the preservative is one or more of trehalose, caprylyl glycol and potassium sorbate.
Wherein: the trehalose can form a unique protective film on the cell surface, effectively protects protein molecules from being inactivated without denaturation, thereby being capable of keeping the cell activity and being an important component of moisturizing cosmetics, wherein the trehalose can play a good role in corrosion prevention and also can be a supplementary component of a skin care component; caprylyl glycol is a preservative component with good permeability and very little toxicity; potassium sorbate has a strong effect of inhibiting putrefying bacteria and mold, and is the most important preservative in the world at present because the toxicity is far lower than that of other preservatives.
Preferably, the preservative is:
0.1-10 parts of trehalose
0.1-2 parts of octyl glycol.
Preferably, the humectant is one or more of glycerol, ceramide, chitin derivatives and sorbitol.
Wherein: after the glycerin is absorbed, the water is not released any more, the dynamic moisture preservation can adjust the water according to the surrounding environment, if the water in the skin is less, the glycerin can release the absorbed water, thereby realizing the long-acting moisture preservation effect; the moisture absorption and retention performances of the chitin derivative are similar to those of hyaluronic acid, the moisture absorption amount of each gram of humectant is approximately equal to the moisture retention amount, the moisturizing effect is stable and long-acting, and the chitin derivative is suitable for being used as a daily humectant; ceramides, also known as sphingolipids, are lipids present in the skin and play an important role in the formation of the stratum corneum of the epidermis; the fatty acid has acid amide bond structure on the amino group of sphingosine, and becomes sphingoglycolipid when combined with sugar, and becomes sphingomyelin when combined with phosphorylcholine; ceramide is an intermediate metabolite of sphingolipids, and particularly plays an important role in biosynthesis, and recent researches show that when the skin is dried, desquamated and cracked and the barrier function of the skin is obviously reduced, the skin can quickly recover the moisture retention and barrier function by supplementing ceramide; sorbitol is used as a humectant for toothpaste, cosmetics, and tobacco. Is a substitute of glycerin, has milder moisture retention property and better taste, can be used together with other humectants to obtain synergistic effect, and is a humectant adjuvant with good performance.
A preparation method of a mild cleansing facial cleanser containing graphene comprises the following steps:
accurately weighing each substance component according to the proportion of the formula;
secondly, adding the tea seed oil and the coconut diethanolamide into the jacketed kettle, and stirring at the rotating speed of 150rmp at the temperature of 40-50 ℃ until the mixture is completely dissolved;
adding the humectant (one or more of glycerin, ceramide, chitin derivatives and sorbitol), preservative (one or more of trehalose, caprylyl glycol and potassium sorbate) and deionized water, continuously stirring and keeping the temperature for 1 hour;
fourthly, slowly adding the aloe extract, the honeysuckle extract, the forsythia extract, the graphene dispersion liquid, the yam extract, the rose extract and the wild chrysanthemum extract according to the formula, controlling the pH value to be 6-6.8, and continuously stirring for 3 hours to obtain mixed emulsion; the pH value is adjusted to be neutral, so that the product is suitable for human skin, and is mild, safe and non-irritant;
placing the mixed emulsion in a homogenizer for homogenization, cooling to room temperature, placing at 28-30 ℃, sterilizing at 113-; ensuring the cleanness and sanitation of the facial cleanser.
In the preparation method of the graphene mild cleansing facial cleanser, all used equipment is disinfected in the whole preparation process, and workers must wear disinfecting dustproof clothing in the whole process.
Compared with the prior art, the invention has the following advantages:
the facial cleanser is added with various natural mild components, can be used for deeply cleaning skin and has no stimulation effect on the skin, thereby avoiding adverse symptoms caused by blockage of skin pores.
Drawings
Fig. 1 shows the graphene oxide powder added in example 1.
Fig. 2 is an SEM characterization of the graphene oxide powder added in example 1.
The key parameters are as follows: the mesh number of precursor graphite for preparing graphene is as follows: 800 meshes to 10000 meshes, and the concentration of the oxidized graphene/reduced graphene for preparing the graphene dispersion liquid is 0.5 to 150 mu g/mL.
Detailed Description
Example 1:
a preparation method of a mild cleansing facial cleanser containing graphene comprises the following steps:
accurately weighing each substance component according to the following formula proportion;
16 portions of glycerol
Honeysuckle extract 12 parts
25 parts of aloe extract
22 parts of tea seed oil
8 parts of forsythia extract
Chinese yam extract liquid 8 parts
8 parts of graphene
Coconut diethanolamide 6 parts
Rose extract 6 parts
Wild chrysanthemum flower extract 1 part
Trehalose 8 parts
1 part of octyl glycol
10 portions of deionized water
Secondly, adding the tea seed oil and the coconut diethanolamide into the jacketed kettle, and stirring at the rotating speed of 150rmp at the temperature of 40-50 ℃ until the mixture is completely dissolved;
thirdly, adding the glycerol, the trehalose, the caprylyl glycol and the deionized water according to the formula, continuously stirring and keeping the temperature for 1 hour;
fourthly, slowly adding the aloe extract, the honeysuckle extract, the forsythia extract, the graphene dispersion liquid, the yam extract, the rose extract and the wild chrysanthemum extract according to the formula, controlling the pH value to be 6-6.8, and continuously stirring for 3 hours to obtain mixed emulsion; the pH value is adjusted to be neutral, so that the product is suitable for human skin, and is mild, safe and non-irritant;
placing the mixed emulsion in a homogenizer for homogenization, cooling to room temperature, placing at 28-30 ℃, sterilizing at 113-; ensuring the cleanness and sanitation of the facial cleanser.
Example 2
A preparation method of a mild cleansing facial cleanser containing graphene comprises the following steps:
accurately weighing each substance component according to the following formula proportion;
18 portions of ceramide
8 portions of glycerol
Honeysuckle extract 12 parts
25 parts of aloe extract
22 parts of tea seed oil
8 parts of forsythia extract
Chinese yam extract liquid 8 parts
8 parts of graphene
Coconut diethanolamide 6 parts
Rose extract 6 parts
Wild chrysanthemum flower extract 1 part
4 portions of potassium sorbate
10 portions of deionized water
Secondly, adding the tea seed oil and the coconut diethanolamide into the jacketed kettle, and stirring at the rotating speed of 150rmp at the temperature of 40-50 ℃ until the mixture is completely dissolved;
adding the glycerol, the ceramide, the potassium sorbate and the deionized water according to the formula, continuously stirring and keeping the temperature for 1 hour;
fourthly, slowly adding the aloe extract, the honeysuckle extract, the forsythia extract, the graphene dispersion liquid, the yam extract, the rose extract and the wild chrysanthemum extract according to the formula, controlling the pH value to be 6-6.8, and continuously stirring for 3 hours to obtain mixed emulsion; the pH value is adjusted to be neutral, so that the product is suitable for human skin, and is mild, safe and non-irritant;
placing the mixed emulsion in a homogenizer for homogenization, cooling to room temperature, placing at 28-30 ℃, sterilizing at 113-; ensuring the cleanness and sanitation of the facial cleanser.
Example 3
A preparation method of a mild cleansing facial cleanser containing graphene comprises the following steps:
accurately weighing each substance component according to the following formula proportion;
42 parts of ceramide
Glycerin 4 parts
26 parts of honeysuckle extract
Aloe extract 14 parts
12 portions of tea seed oil
8 parts of forsythia extract
12 parts of Chinese yam extract
4 parts of graphene
Coconut diethanolamide 3 parts
Rose extract 3 parts
2 parts of wild chrysanthemum extract
Trehalose 2 parts
4 portions of potassium sorbate
0.8 part of caprylyl glycol
5 portions of deionized water
Secondly, adding the tea seed oil and the coconut diethanolamide into the jacketed kettle, and stirring at the rotating speed of 150rmp at the temperature of 40-50 ℃ until the mixture is completely dissolved;
adding the glycerol, the ceramide, the trehalose, the caprylyl glycol, the potassium sorbate and the deionized water according to the formula, continuously stirring and keeping the temperature for 1 hour;
fourthly, slowly adding the aloe extract, the honeysuckle extract, the forsythia extract, the graphene dispersion liquid, the yam extract, the rose extract and the wild chrysanthemum extract according to the formula, controlling the pH value to be 6-6.8, and continuously stirring for 3 hours to obtain mixed emulsion; the pH value is adjusted to be neutral, so that the product is suitable for human skin, and is mild, safe and non-irritant;
placing the mixed emulsion in a homogenizer for homogenization, cooling to room temperature, placing at 28-30 ℃, sterilizing at 113-; ensuring the cleanness and sanitation of the facial cleanser.
The foregoing is merely a preferred embodiment of the invention and all such equivalent alterations and permutations and derivations thereof are intended to be included within the scope of the invention.
Claims (9)
1. A mild cleansing facial cleanser containing graphene is characterized in that: the formula of the facial cleanser comprises the following components in parts by weight:
12-26 parts of honeysuckle extract
14-26 parts of aloe extract
12-22 parts of tea seed oil
8-15 parts of forsythia extract
8-12 parts of Chinese yam extract
0.7-17 parts of graphene
Coconut diethanolamide 2-6 weight portions
2-6 parts of rose extract
1-4 parts of wild chrysanthemum extract
5-50 parts of humectant
0.2 to 12 portions of preservative
5-10 parts of deionized water.
2. The mild cleansing facial milk containing graphene according to claim 1, characterized in that: the graphene is one or two of graphene oxide dispersion liquid and reduced graphene dispersion liquid prepared by adopting an improved Hummers method.
3. The mild cleansing facial milk containing graphene according to claim 2, characterized in that: the graphene contains
0.5 to 8 parts of reduced graphene,
0.2-9 parts of graphene oxide.
4. The mild cleansing facial milk containing graphene according to claim 2, characterized in that: the concentration of the graphene is 0.5-150 mu g/mL.
5. The mild cleansing facial milk containing graphene according to claim 2, characterized in that: the graphene is used for preparing a precursor of graphene oxide powder, namely graphite, by adopting an improved Hummers method, and the mesh number of the graphite is 800-10000 meshes.
6. The mild cleansing facial milk containing graphene according to claim 1, characterized in that: the preservative is one or more of trehalose, caprylyl glycol and potassium sorbate.
7. The mild cleansing facial milk containing graphene according to claim 6, characterized in that: the preservative comprises
0.1 to 10 portions of trehalose,
0.1-2 parts of octyl glycol.
8. The mild cleansing facial milk containing graphene according to claim 1, characterized in that: the humectant is one or more of glycerol, ceramide, chitin derivatives and sorbitol.
9. A preparation method of a mild cleansing facial cleanser containing graphene is characterized by comprising the following steps:
step 1: accurately weighing each substance component according to the proportion of the formula;
step 2: adding the tea seed oil and the coconut diethanolamide into the jacketed kettle, and stirring at 40-50 deg.C at 150rmp until completely dissolving;
and step 3: adding the humectant (one or more of glycerol, ceramide, chitin derivative and sorbitol), antiseptic (one or more of trehalose, caprylyl glycol and potassium sorbate) and deionized water, stirring and keeping the temperature for 1 h;
and 4, step 4: slowly adding the aloe extract, the honeysuckle extract, the forsythia extract, the graphene dispersion liquid, the yam extract, the rose extract and the wild chrysanthemum extract according to the formula, controlling the pH value to be 6-6.8, and continuously stirring for 3 hours to obtain mixed emulsion; the pH value is adjusted to be neutral, so that the product is suitable for human skin, and is mild, safe and non-irritant;
and 5: and (3) homogenizing the mixed emulsion in a homogenizer, cooling to room temperature, sterilizing at 28-30 ℃ and 113-115MPa for 18-30min under ultrahigh pressure to obtain the graphene mild and clean facial cleanser.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114455575A (en) * | 2022-01-28 | 2022-05-10 | 中安新材料(深圳)有限公司 | Graphene and preparation method and application thereof |
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| CN104591173A (en) * | 2015-01-24 | 2015-05-06 | 南昌航空大学 | Method for preparing graphene by reducing graphene oxide based on camellia oleifera extract |
| CN105902426A (en) * | 2016-04-20 | 2016-08-31 | 李兵 | Gentle facial cleanser specially used for moisturization |
| CN105997572A (en) * | 2016-05-19 | 2016-10-12 | 曾新民 | Cleansing milk containing nano graphene and preparation method thereof |
| CN109394637A (en) * | 2017-08-18 | 2019-03-01 | 荆晓东 | Clean facial cleanser |
| CN110151627A (en) * | 2019-06-20 | 2019-08-23 | 苏州米颜生物科技有限公司 | A kind of graphene-based clean facial cleanser |
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2020
- 2020-09-11 CN CN202010956178.9A patent/CN112057396A/en not_active Withdrawn
Patent Citations (5)
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|---|---|---|---|---|
| CN104591173A (en) * | 2015-01-24 | 2015-05-06 | 南昌航空大学 | Method for preparing graphene by reducing graphene oxide based on camellia oleifera extract |
| CN105902426A (en) * | 2016-04-20 | 2016-08-31 | 李兵 | Gentle facial cleanser specially used for moisturization |
| CN105997572A (en) * | 2016-05-19 | 2016-10-12 | 曾新民 | Cleansing milk containing nano graphene and preparation method thereof |
| CN109394637A (en) * | 2017-08-18 | 2019-03-01 | 荆晓东 | Clean facial cleanser |
| CN110151627A (en) * | 2019-06-20 | 2019-08-23 | 苏州米颜生物科技有限公司 | A kind of graphene-based clean facial cleanser |
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Cited By (1)
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| CN114455575A (en) * | 2022-01-28 | 2022-05-10 | 中安新材料(深圳)有限公司 | Graphene and preparation method and application thereof |
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Application publication date: 20201211 |