CN112047718A - Powder formula and preparation process of prescription porcelain - Google Patents

Powder formula and preparation process of prescription porcelain Download PDF

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Publication number
CN112047718A
CN112047718A CN202010904085.1A CN202010904085A CN112047718A CN 112047718 A CN112047718 A CN 112047718A CN 202010904085 A CN202010904085 A CN 202010904085A CN 112047718 A CN112047718 A CN 112047718A
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Prior art keywords
prescription
porcelain
blank
stone mineral
plant ash
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CN202010904085.1A
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苗建长
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Individual
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Priority to CN202010904085.1A priority Critical patent/CN112047718A/en
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/02Preparing or treating the raw materials individually or as batches
    • C04B33/13Compounding ingredients
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/02Preparing or treating the raw materials individually or as batches
    • C04B33/13Compounding ingredients
    • C04B33/132Waste materials; Refuse; Residues
    • C04B33/135Combustion residues, e.g. fly ash, incineration waste
    • C04B33/1355Incineration residues
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/32Burning methods
    • C04B33/34Burning methods combined with glazing
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/50Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
    • C04B41/5022Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81Coating or impregnation
    • C04B41/85Coating or impregnation with inorganic materials
    • C04B41/86Glazes; Cold glazes
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427Silicates other than clay, e.g. water glass
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/40Metallic constituents or additives not added as binding phase
    • C04B2235/408Noble metals
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P40/00Technologies relating to the processing of minerals
    • Y02P40/60Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Dispersion Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Combustion & Propulsion (AREA)
  • Environmental & Geological Engineering (AREA)
  • Compositions Of Oxide Ceramics (AREA)

Abstract

The invention discloses a powder formula of prescription porcelain and a preparation process of the prescription porcelain. The preparation process of the prescription porcelain adopting the powder formula comprises the steps of processing stone mineral substances, mixing the materials, ball-milling to prepare a blank, preparing a blank, firing the blank, glazing the blank, and firing for the second time, wherein the glaze adopted in the glazing process is composed of 99% of a mixture of silver ore and granite and 1% of plant ash in parts by weight. The prescription porcelain prepared by the powder formula and the preparation process of the prescription porcelain contains more than 30 mineral substances, the contained mineral substances have stronger adsorbability, ion exchange property and catalytic property, are rich in various trace elements necessary for human bodies, have ecological activity of self-purification, and can be used for treating liquid contained in the prescription porcelain: for example, the components of wine or Chinese medicinal liquid which generate peculiar smell are adsorbed, so that foreign odor can be removed rapidly, and the quality of the liquid can be improved.

Description

Powder formula and preparation process of prescription porcelain
Technical Field
The invention relates to the technical field of ceramics, in particular to a powder formula of prescription porcelain and a preparation process thereof.
Background
The new wine obtained by fermentation and distillation must be stored for a period of time to ensure the flavor and quality of the white spirit. The white spirit storage containers are various, and comprise ceramic containers, stainless steel containers, underground wine pools paved with ceramic plates and the like. The flavor and taste of the white spirit are greatly related to the materials of the storage container, and the quality of the white spirit can be directly influenced. Not only the flavor of the white spirit is greatly related to the materials of the containers for holding and storing the white spirit, but also the drug effect of certain traditional Chinese medicine liquid can be influenced by selecting different containers.
Disclosure of Invention
Therefore, based on the background, the prescription porcelain powder formula and the preparation process can improve the taste of the white spirit and improve the drug effect.
The technical scheme of the invention is as follows:
a powder formulation of prescription porcelain comprises pug, medicinal stone mineral substance, and plant ash.
Further, the plant ash comprises 70% of pug, 29% of medicinal stone mineral substances and 1% of plant ash in parts by weight.
Further, the medical stone mineral substance is a mixture of silver ore and granite.
The invention also provides a preparation process of the prescription porcelain, which comprises the following steps:
(1) weighing the pug, the medicinal stone mineral substance and the plant ash according to the formula of any one of claims 1 to 4 for later use;
(2) processing the medicinal stone mineral weighed in the step (1);
(3) weighing a proper amount of water, adding the medical stone mineral substances and the pug processed in the step (2) into the water, mixing, and then putting into a ball mill for ball milling to prepare slurry blanks;
(4) carrying out blank drawing forming on the blank manufactured in the step (3) or manufacturing a blank into a blank by adopting a mould;
(5) baking the biscuit: firing the oxidizing flame to 300 ℃ to dry the blank in the step (4), and then heating to 900 ℃ to burn the blank into a biscuit product;
(6) glazing the biscuit: cleaning the biscuit fired in the step (5), and then sequentially adopting the processes of spraying, dipping and glaze supplementing to finish glazing, and then loading into a kiln;
(7) secondary firing: firing oxidizing flame to 300 ℃, drying the glazed biscuit, heating to 800 ℃, and then preserving heat for 5 minutes to achieve complete moisture removal; then heating to 1000 ℃, transferring the oxidizing flame to the reducing flame, keeping the temperature for reaction for 10 minutes, keeping the reducing flame heated to about 2600 ℃, and then judging whether fire is required to be turned off according to the color of the fire; before shutting down the fire, the reducing flame needs to be converted into oxidizing flame, then the combustion is continued for 1min, then the fuel is shut down, and the fire is shut down; and naturally cooling the prescription porcelain subjected to secondary firing to 100 ℃, and taking out of the kiln, wherein the product after the kiln is taken out is the prescription porcelain of the invention.
Further, the processing steps of the medical stone minerals in the step (2) are as follows:
(1) calcining the weighed medical stone mineral substances at 850-950 ℃ for a period of time, and naturally cooling;
(2) weighing a certain amount of water, adding the plant ash into the water, stirring and mixing, and then adding the calcined medical stone mineral in the step (1) into the plant ash water for soaking for two days;
(3) and (3) putting the medical stone mineral substance soaked in the step (2) into a ball mill, continuously working for 36 hours, and sieving by using a mesh sieve, wherein the mesh number of the mesh sieve is more than 800.
Further, the glaze component for glazing in the step (6) comprises a mixture of silver ore and granite and plant ash.
Further, the glaze for glazing in the step (6) is composed of 99% of a mixture of silver ore and granite and 1% of plant ash in parts by weight.
By adopting the technical scheme, the beneficial effects are as follows:
the prescription porcelain prepared by the powder formula and the preparation process of the prescription porcelain contains more than 30 mineral substances, the contained mineral substances have stronger adsorbability, ion exchange property and catalytic property, are rich in various trace elements necessary for human bodies, have ecological activity of self-purification, and can be used for treating liquid contained in the prescription porcelain: for example, the components of wine or Chinese medicinal liquid which generate peculiar smell are adsorbed, so that foreign odor can be removed rapidly, and the quality of the liquid can be improved.
Detailed Description
The invention will be further described with reference to the following examples
Example 1: a prescription porcelain powder formula comprises 70% of pug, 29% of medical stone mineral substance and 1% of plant ash in parts by weight.
The medicinal stone mineral substance is a mixture of silver ore and granite.
The plant ash is wood ash of Funishan old pear trees.
According to the powder formula, the preparation steps of the prescription porcelain are as follows:
(1) weighing the pug, the medicinal stone mineral substance and the plant ash according to the formula of any one of claims 1 to 4 for later use;
(2) processing the medicinal stone mineral weighed in the step (1);
(3) weighing a proper amount of water, adding the medical stone mineral substances and the pug processed in the step (2) into the water, mixing, and then putting into a ball mill for ball milling to prepare slurry blanks;
(4) carrying out blank drawing forming on the blank manufactured in the step (3) or manufacturing a blank into a blank by adopting a mould;
(5) baking the biscuit: firing the oxidizing flame to 300 ℃ to dry the blank in the step (4), and then heating to 900 ℃ to burn the blank into a biscuit product;
(6) glazing the biscuit: cleaning the biscuit fired in the step (5), and then sequentially adopting the processes of spraying, dipping and glaze supplementing to finish glazing, and then loading into a kiln;
(7) secondary firing: firing oxidizing flame to 300 ℃, drying the glazed biscuit, heating to 800 ℃, and then preserving heat for 5 minutes to achieve complete moisture removal; then heating to 1000 ℃, transferring the oxidizing flame to the reducing flame, keeping the temperature for reaction for 10 minutes, keeping the reducing flame heated to about 2600 ℃, and then judging whether fire is required to be turned off according to the color of the fire; before shutting down the fire, the reducing flame needs to be converted into oxidizing flame, then the combustion is continued for 1min, then the fuel is shut down, and the fire is shut down; and naturally cooling the prescription porcelain subjected to secondary firing to 100 ℃, and taking out of the kiln, wherein the product after the kiln is taken out is the prescription porcelain of the invention.
The processing steps of the medical stone mineral in the step (2) are as follows:
(1) calcining the weighed medical stone mineral substances at 850-950 ℃ for a period of time, and naturally cooling;
(2) weighing a certain amount of water, adding the plant ash into the water, stirring and mixing, and then adding the calcined medical stone mineral in the step (1) into the plant ash water for soaking for two days;
(3) and (3) putting the medical stone mineral substance soaked in the step (2) into a ball mill, continuously working for 36 hours, and sieving by using a mesh sieve, wherein the mesh number of the mesh sieve is more than 800.
The glaze for glazing in the step (6) consists of 99% of a mixture of silver ore and granite and 1% of plant ash in parts by weight.
The prescription porcelain prepared in the embodiment contains more than 30 mineral substances, has lead content less than 0.05 (unit) and 140 times lower than the international allowable value, cadmium less than 0.001 and 500 times lower than the international allowable value, and obtains a unique food standard word number [ Yuwei food standard word (2004) No. 61 ];
through the detection of the white spirit in the prescription porcelain of the invention by Chinese agriculture university, 23 indexes of the white spirit are that the beneficial substances of the raw wine are increased, the harmful substances are reduced, and 8 harmful substances disappear in 30 minutes compared with the prescription porcelain. The conductivity is increased along with time, according to reports, the prescription porcelain can effectively remove harmful substances of the white spirit and improve the quality of the white spirit, and the practice contrast is that the white spirit achieves the peculiar effect of storing in a cellar for more than 10 years after being acted by the prescription porcelain for 30 minutes, and the white spirit is extremely sublimated, mellow, smooth and lasting in bouquet and sweet and smooth in taste. Not spicy, not explosive, not dry, and not fit to the head. After the effect, the wine quality is continuously improved and aged without rebounding and restoring.
The above description is only an embodiment of the present invention, and is not intended to limit the present invention, and all simple modifications, changes and equivalent changes made to the above embodiment according to the technical spirit of the present invention fall within the protection scope of the present technical solution.

Claims (7)

1. The powder formula of the prescription porcelain is characterized by comprising pug, medicinal stone mineral substances and plant ash.
2. The powder formulation of a prescription porcelain according to claim 1, characterized in that it consists of 70% of pug, 29% of medical stone mineral and 1% of plant ash by weight.
3. The powder formulation of a prescription porcelain according to claim 1, wherein the medical stone mineral is a mixture of silver ore and granite.
4. The preparation process of the prescription porcelain is characterized by comprising the following steps:
(1) weighing pug, medicinal stone mineral substances and plant ash according to the formula of any one of claims 1 to 3 for later use;
(2) processing the medicinal stone mineral weighed in the step (1);
(3) weighing a proper amount of water, adding the medical stone mineral substances and the pug processed in the step (2) into the water, mixing, and then putting into a ball mill for ball milling to prepare slurry blanks;
(4) carrying out blank drawing forming on the blank manufactured in the step (3) or manufacturing a blank into a blank by adopting a mould;
(5) baking the biscuit: firing the oxidizing flame to 300 ℃ to dry the blank in the step (4), and then heating to 900 ℃ to burn the blank into a biscuit product;
(6) glazing the biscuit: cleaning the biscuit fired in the step (5), and then sequentially adopting the processes of spraying, dipping and glaze supplementing to finish glazing, and then loading into a kiln;
(7) secondary firing: firing oxidizing flame to 300 ℃, drying the glazed biscuit, heating to 800 ℃, and then preserving heat for 5 minutes to achieve complete moisture removal; then heating to 1000 ℃, transferring the oxidizing flame to the reducing flame, keeping the temperature for reaction for 10 minutes, keeping the reducing flame heated to about 2600 ℃, and then judging whether fire is required to be turned off according to the color of the fire; before shutting down the fire, the reducing flame needs to be converted into oxidizing flame, then the combustion is continued for 1min, then the fuel is shut down, and the fire is shut down; and naturally cooling the prescription porcelain subjected to secondary firing to 100 ℃, and taking out of the kiln, wherein the product after the kiln is taken out is the prescription porcelain of the invention.
5. The preparation process of the prescription porcelain according to claim 4, wherein the processing steps of the medical stone mineral in the step (2) are as follows:
(1) calcining the weighed medical stone mineral substances at 850-950 ℃ for a period of time, and naturally cooling;
(2) weighing a certain amount of water, adding the plant ash into the water, stirring and mixing, and then adding the calcined medical stone mineral in the step (1) into the plant ash water for soaking for two days;
(3) and (3) putting the medical stone mineral substance soaked in the step (2) into a ball mill, continuously working for 36 hours, and sieving by using a mesh sieve, wherein the mesh number of the mesh sieve is more than 800.
6. The process for preparing a prescription porcelain according to claim 4, wherein the glaze component for glazing in step (6) comprises a mixture of silver ore and granite, plant ash.
7. The process for preparing a prescription porcelain according to claim 6, wherein the glaze for glazing in step (6) consists of 99% by weight of a mixture of silver ore and granite, and 1% by weight of plant ash.
CN202010904085.1A 2020-09-01 2020-09-01 Powder formula and preparation process of prescription porcelain Pending CN112047718A (en)

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Application Number Priority Date Filing Date Title
CN202010904085.1A CN112047718A (en) 2020-09-01 2020-09-01 Powder formula and preparation process of prescription porcelain

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CN112047718A true CN112047718A (en) 2020-12-08

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2016082400A1 (en) * 2014-11-25 2016-06-02 福建省佳美集团公司 Surface glaze of lead-free tableware ceramic and preparation method thereof
CN107226718A (en) * 2017-05-30 2017-10-03 刘新乐 Pottery health-promotion kettle and preparation method thereof
CN108727005A (en) * 2018-07-04 2018-11-02 福建省德化县荣华陶瓷有限公司 A kind of preparation method of no oil smoke health ceramic pot
CN110642614A (en) * 2019-09-25 2020-01-03 张军召 Jun porcelain formed by demolding and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2016082400A1 (en) * 2014-11-25 2016-06-02 福建省佳美集团公司 Surface glaze of lead-free tableware ceramic and preparation method thereof
CN107226718A (en) * 2017-05-30 2017-10-03 刘新乐 Pottery health-promotion kettle and preparation method thereof
CN108727005A (en) * 2018-07-04 2018-11-02 福建省德化县荣华陶瓷有限公司 A kind of preparation method of no oil smoke health ceramic pot
CN110642614A (en) * 2019-09-25 2020-01-03 张军召 Jun porcelain formed by demolding and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
创意中原网: "工艺品设计篇之钧瓷养生壶", 《HTTP://WWW.IDEAHN.COM/PRODUCT/CRAFT/5656.HTML》 *

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