CN112043649A - Method for preparing skin care product raw material by utilizing wine brewing waste - Google Patents

Method for preparing skin care product raw material by utilizing wine brewing waste Download PDF

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Publication number
CN112043649A
CN112043649A CN202011133935.9A CN202011133935A CN112043649A CN 112043649 A CN112043649 A CN 112043649A CN 202011133935 A CN202011133935 A CN 202011133935A CN 112043649 A CN112043649 A CN 112043649A
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wine
skin care
raw material
care product
waste
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CN202011133935.9A
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CN112043649B (en
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殷传江
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/10—General cosmetic use
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/81—Preparation or application process involves irradiation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Dermatology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a method for preparing a skin care product raw material by utilizing wine brewing waste, relating to the technical field of skin care product raw material preparation, wherein the skin care product raw material comprises the following components: the wine comprises wine lees powder, wine stock solution, grape seed oil and frosted material; the method for preparing the skin care product raw material by utilizing the wine brewing waste comprises the following steps: s1, sterilizing; s2, filtering; s3, drying; s4, squeezing or extracting; and S5, manufacturing a frosted material. According to the method for preparing the skin care product raw material by using the wine brewing waste, the wine brewing waste is used as the raw material, waste is turned into wealth, the method is green and environment-friendly, the problem of environmental pollution caused by the wine brewing waste is solved, and good economic benefit and environmental benefit are generated for the wine industry.

Description

Method for preparing skin care product raw material by utilizing wine brewing waste
Technical Field
The invention relates to the technical field of skin care product raw material preparation, in particular to a method for preparing skin care product raw materials by utilizing wine brewing wastes.
Background
The waste from wine brewing is the leftover produced in wine brewing process in wine factory, and consists of mainly liquid un-separated wine, yeast, grape seed, grape peel and pulp, grape stalk, organic acid, etc. these matters are usually precipitated in wine brewing and ageing process. The leftovers are mostly discarded as garbage in China, environmental pollution and soil acidification are caused, only a small part of leftovers are used as fuel and fertilizer or used as feed, and the utilization efficiency is low.
The wine brewing waste contains a plurality of functional components which can be used for skin care products, such as: saccharides, resveratrol, organic acids, amino acids, tannic acid, proanthocyanidins, quercetin, vitamins, minerals, and grapeseed oil.
At present, a method for preparing skin care product raw materials by utilizing wine brewing wastes does not exist.
Disclosure of Invention
Aiming at the defects in the prior art, the invention provides a method for preparing a skin care product raw material by utilizing wine brewing wastes.
The skin care product comprises the following raw materials: the wine comprises wine lees powder, wine stock solution, grape seed oil and frosted material. The method for preparing the skin care product raw material by utilizing the wine brewing waste comprises the following steps: s1, sterilization: uniformly pouring the fermented grape wine waste into a sterilization tray until the thickness is 15-18cm, sterilizing to obtain sterilized fermented grape wine waste, adding caprylyl hydroximic acid and p-hydroxyacetophenone, uniformly stirring to obtain a mixture A, and charging nitrogen, sealing and storing for later use; s2, filtering: performing pressure filtration on the mixture A to obtain separated liquid wine and solid wine lees, and filtering the liquid wine by adopting a polymer filtering membrane to obtain a clear wine stock solution; s3, drying: drying the solid wine lees, separating grape seeds from the dried solid wine lees by a vibrating screen to obtain dried and deseeded solid wine lees, crushing and screening to obtain wine lees powder; s4, squeezing or extracting: carrying out low-temperature squeezing or carbon dioxide supercritical extraction on the grape seeds separated in the step S3 to obtain grape seed oil and solid substances; s5, manufacturing a frosted material: and (4) crushing the solid substance prepared in the step (S4), and sieving to prepare the frosted material.
Preferably, in step S1, the mass ratio of the sterilized wine brewing waste to the caprylyl hydroxamic acid is 100: 0.05-0.1.
Preferably, in step S1, the mass ratio of the sterilized brewing waste of wine to the p-hydroxyacetophenone is 1: 0.2-0.5.
Preferably, in step S1, the sterilization is electron beam sterilization.
Preferably, in step S2, the polymeric filtration membrane is a 0.2um cross-flow membrane.
Preferably, in step S3, the sieving is 40-60 mesh sieving.
Preferably, in step S3, the drying is performed until the moisture content is less than or equal to 5%.
The invention also aims to protect the skin care product raw material prepared by the method for preparing the skin care product raw material by utilizing the wine brewing waste.
The invention also aims to protect the application of the skin care product raw material prepared by the method for preparing the skin care product raw material by utilizing the wine brewing waste in preparing the skin care product. Wherein the skin care product comprises a smearing facial mask, a facial mask solution and a scrub cream.
The invention has the beneficial effects that:
(1) according to the method for preparing the skin care product raw material by using the wine brewing waste, the wine brewing waste is used as the raw material, waste is turned into wealth, the method is green and environment-friendly, the problem of environmental pollution caused by the wine brewing waste is solved, and good economic benefit and environmental benefit are generated for the wine industry.
(2) The method for preparing the skin care product raw material by utilizing the wine brewing waste provided by the invention has the advantages of easily available raw materials, low cost, simple operation and stable technology, can prepare various skin care product raw materials such as wine lees powder, wine stock solution, grape seed oil, frosted material and the like from the wine brewing waste, and has great commercial value.
Detailed Description
Hereinafter, embodiments of the present invention will be described in detail. The following examples are only for illustrating the technical solutions of the present invention more clearly, and therefore are only examples, and the protection scope of the present invention is not limited thereby.
It is to be noted that, unless otherwise specified, technical or scientific terms used herein shall have the ordinary meaning as understood by those skilled in the art to which the invention pertains.
Example 1
A method for preparing skin care product raw materials by utilizing wine brewing wastes comprises the following steps: the wine comprises wine lees powder, wine stock solution, grape seed oil and frosted material.
The method for preparing the skin care product raw material by utilizing the wine brewing waste comprises the following steps:
s1, sterilization: uniformly pouring the fermented grape wine brewing waste into a sterilization tray until the thickness is 15-18cm, performing electron beam sterilization to obtain sterilized fermented grape wine brewing waste, adding caprylyl hydroximic acid and p-hydroxyacetophenone, uniformly stirring to obtain a mixture A, and filling nitrogen to seal and store for later use;
s2, filtering: performing pressure filtration on the mixture A to obtain separated liquid wine and solid wine lees, and filtering the liquid wine by adopting a polymer filtering membrane to obtain a clear wine stock solution;
s3, drying: drying the solid wine lees, separating grape seeds from the dried solid wine lees by a vibrating screen to obtain dried and deseeded solid wine lees, crushing and screening to obtain wine lees powder;
s4, squeezing or extracting: carrying out low-temperature squeezing or carbon dioxide supercritical extraction on the grape seeds separated in the step S3 to obtain grape seed oil and solid substances;
s5, manufacturing a frosted material: and (4) crushing the solid substance prepared in the step (S4), and sieving to prepare the frosted material.
In step S1, the mass ratio of the sterilized wine brewing waste to the caprylyl hydroxamic acid is 100: 0.1; the mass ratio of the sterilized wine brewing waste to the p-hydroxyacetophenone is 1: 0.5.
In step S2, the polymer filtration membrane is a 0.2um cross-flow membrane.
In step S3, the sieving is 60 mesh sieving.
In step S3, the drying is carried out until the moisture is less than or equal to 5%.
Wherein, the yield of the prepared skin care product raw materials is respectively as follows: 5-10% of wine lees powder, 75-85% of wine stock solution, 2-5% of grape seed oil and 5-10% of ground material.
Example 2
The skin care product raw materials prepared in the embodiment 1 are used for preparing the grape vinasse mud film, and the grape vinasse mud film comprises the following raw material components in percentage by mass: 0.5% of hydroxyethyl cellulose, 0.5% of dextrin, 2.5% of wine lees powder, 8.0% of glycerol, 0.1% of EDTA disodium, 0.05% of caprylyl hydroximic acid, 0.3% of p-hydroxyacetophenone, 25% of wine stock solution and the balance of deionized water.
The preparation method of the grape vinasse mud membrane comprises the following steps: uniformly dispersing hydroxyethyl cellulose and dextrin in glycerol, stirring uniformly, adding into deionized water, adding EDTA disodium, caprylyl hydroximic acid and p-hydroxyacetophenone, heating to 80-85 ℃, uniformly stirring, keeping the temperature for 10 minutes, cooling to 40 ℃, adding the wine stock solution and the wine lees powder, and stirring uniformly to obtain the wine lees mud film.
Example 3
The skin care product raw material prepared in the embodiment 1 is used for preparing the wine mask liquid, and the wine mask liquid comprises the following raw material components in percentage by mass: 4.0% of glycerol, 3.0% of 1, 3-butanediol, 0.5% of D-panthenol, 0.3% of xanthan gum, 0.1% of sodium hyaluronate, 1.0% of betaine, 0.05% of disodium EDTA, 0.05% of caprylyl hydroximic acid, 0.3% of p-hydroxyacetophenone, 30% of wine stock solution and the balance of deionized water.
The preparation method of the wine mask liquid comprises the following steps: uniformly dispersing xanthan gum and sodium hyaluronate in glycerol, uniformly stirring, adding the mixture into deionized water, adding 1, 3-butanediol, D-panthenol, betaine, EDTA disodium, caprylyl hydroximic acid and p-hydroxyacetophenone, heating to 80-85 ℃, uniformly stirring, keeping the temperature for 10 minutes, cooling to 40 ℃, adding a wine stock solution, and uniformly stirring to obtain the wine mask solution.
Example 4
The skin care product raw materials prepared in the embodiment 1 are used for preparing the wine scrub cream, and the wine scrub cream comprises the following raw material components in percentage by mass:
4.0% of glycerol, 3.0% of 1, 3-butanediol, 0.5% of D-panthenol, 0.2% of carbomer, 0.05% of sodium hyaluronate, 1.0% of betaine, 0.05% of disodium EDTA, 0.2% of methylparaben, 0.3% of phenoxyethanol, 2.0% of polyglycerol-10 stearate, 2.5% of monoglyceride SE, 1.5% of PEG-100 stearate, 2.0% of cetostearyl alcohol, 15% of grape seed oil, 3.0% of shea butter, 1.0% of tocopherol acetate, 2.0% of polydimethylsiloxane, 10.0% of wine stock solution, 5.0% of ground material, 0.2% of triethanolamine and the balance of deionized water.
The preparation method of the grape wine scrub cream comprises the following steps: adding glycerol, 1, 3-butanediol, D-panthenol, carbomer, sodium hyaluronate, betaine, disodium EDTA, methylparaben and phenoxyethanol into deionized water, heating to 80-85 deg.C, stirring, and keeping the temperature for 10 min to obtain water phase mixture; adding monoglyceride SE, PEG-100 stearate, cetearyl alcohol, grapeseed oil, shea butter, tocopheryl acetate and polydimethylsiloxane into polyglycerol-10 stearate, heating to 80-85 deg.C, and stirring to obtain oil phase mixture; adding the frosting material and triethanolamine into the wine stock solution, stirring, heating to 40 deg.C, adding the water phase mixture and the oil phase mixture, and stirring to obtain wine frosting cream.
Finally, it should be noted that: the above embodiments are only used to illustrate the technical solution of the present invention, and not to limit the same; while the invention has been described in detail and with reference to the foregoing embodiments, it will be understood by those skilled in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some or all of the technical features may be equivalently replaced; such modifications and substitutions do not depart from the spirit and scope of the present invention, and they should be construed as being included in the following claims and description.

Claims (9)

1. A method for preparing skin care product raw materials by utilizing wine brewing wastes is characterized by comprising the following steps: the skin care product comprises the following raw materials: the wine comprises wine lees powder, wine stock solution, grape seed oil and frosted material; the method for preparing the skin care product raw material by utilizing the wine brewing waste comprises the following steps: s1, sterilization: uniformly pouring the fermented grape wine waste into a sterilization tray until the thickness is 15-18cm, sterilizing to obtain sterilized fermented grape wine waste, adding caprylyl hydroximic acid and p-hydroxyacetophenone, uniformly stirring to obtain a mixture A, and charging nitrogen, sealing and storing for later use; s2, filtering: performing pressure filtration on the mixture A to obtain separated liquid wine and solid wine lees, and filtering the liquid wine by adopting a polymer filtering membrane to obtain a clear wine stock solution; s3, drying: drying the solid wine lees, separating grape seeds from the dried solid wine lees by a vibrating screen to obtain dried and deseeded solid wine lees, crushing and screening to obtain wine lees powder; s4, squeezing or extracting: carrying out low-temperature squeezing or carbon dioxide supercritical extraction on the grape seeds separated in the step S3 to obtain grape seed oil and solid substances; s5, manufacturing a frosted material: and (4) crushing the solid substance prepared in the step (S4), and sieving to prepare the frosted material.
2. The method for preparing skin care raw material by using the wine brewing waste as claimed in claim 1, wherein the method comprises the following steps: in step S1, the mass ratio of the sterilized wine brewing waste to the caprylyl hydroxamic acid is 100: 0.05-0.1.
3. The method for preparing skin care raw material by using the wine brewing waste as claimed in claim 1, wherein the method comprises the following steps: in step S1, the mass ratio of the sterilized wine brewing waste to the p-hydroxyacetophenone is 1: 0.2-0.5.
4. The method for preparing skin care raw material by using the wine brewing waste as claimed in claim 1, wherein the method comprises the following steps: in step S1, the sterilization is electron beam sterilization.
5. The method for preparing skin care raw material by using the wine brewing waste as claimed in claim 1, wherein the method comprises the following steps: in step S2, the polymer filtration membrane is a 0.2um cross-flow membrane.
6. The method for preparing skin care raw material by using the wine brewing waste as claimed in claim 1, wherein the method comprises the following steps: in step S3, the sieving is 40-60 mesh sieving.
7. The method for preparing skin care raw material by using the wine brewing waste as claimed in claim 1, wherein the method comprises the following steps: in step S3, the drying is carried out until the moisture is less than or equal to 5%.
8. A skin care raw material obtained by the method of any one of claims 1 to 7.
9. Use of a skin care product material prepared by the method of any one of claims 1 to 7 for preparing a skin care product, wherein: the skin care product comprises a smearing facial mask, a facial mask liquid and a scrub cream.
CN202011133935.9A 2020-10-21 2020-10-21 Method for preparing skin care product raw material by utilizing wine brewing waste Active CN112043649B (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102366371A (en) * 2011-10-25 2012-03-07 西北农林科技大学 Patched grape pip facial mask and preparation method thereof
CN107619738A (en) * 2017-11-09 2018-01-23 赵秉莳 Shower grape wine
CN108210432A (en) * 2017-12-28 2018-06-29 河南健特生物科技集团有限公司 Scrub cream containing brown sugar and chamomile Ultramicro-powder and preparation method thereof
CN111714420A (en) * 2020-06-19 2020-09-29 秦皇岛慧爱医药有限公司 Traditional Chinese medicine scrub cream for removing wrinkles and reducing pores and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102366371A (en) * 2011-10-25 2012-03-07 西北农林科技大学 Patched grape pip facial mask and preparation method thereof
CN107619738A (en) * 2017-11-09 2018-01-23 赵秉莳 Shower grape wine
CN108210432A (en) * 2017-12-28 2018-06-29 河南健特生物科技集团有限公司 Scrub cream containing brown sugar and chamomile Ultramicro-powder and preparation method thereof
CN111714420A (en) * 2020-06-19 2020-09-29 秦皇岛慧爱医药有限公司 Traditional Chinese medicine scrub cream for removing wrinkles and reducing pores and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
王霄倩: "《葡萄皮渣的营养价值及综合利用》", 《中国农学通报》 *

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