CN111982619A

CN111982619A - Efficient distillation plant for drug detection

Info

Publication number: CN111982619A
Application number: CN202010718795.5A
Authority: CN
Inventors: 洪峰
Original assignee: Hubei Jidengfeng Biotechnology Co ltd
Current assignee: Hubei Jidengfeng Biotechnology Co ltd
Priority date: 2020-07-23
Filing date: 2020-07-23
Publication date: 2020-11-24

Abstract

The invention discloses an efficient distillation device for medicine detection, which comprises a distillation tank, wherein feed inlets are formed in the left side and the right side of the top of the distillation tank, a first motor is fixedly arranged in the center of the bottom of the distillation tank, the output end of the first motor is coaxially connected with a stirrer positioned at the bottom of an inner cavity of the distillation tank, a heater is arranged at the bottom of the inner cavity of the distillation tank, a distillation hopper is arranged at the top of the inner cavity of the distillation tank, and a cooling interlayer is arranged in the inner cavity of the distillation hopper. The invention relates to the technical field of medicine distillation equipment, and provides a high-efficiency distillation device for medicine detection.

Description

Efficient distillation plant for drug detection

Technical Field

The invention relates to the technical field of medicine distillation equipment, in particular to a high-efficiency distillation device for medicine detection.

Background

Distillation is a thermodynamic separation process that utilizes the difference in boiling points of components in a mixed liquid or liquid-solid system to vaporize lower boiling components and recondense to separate the entire component in a unit operation, and distillation is a combination of both vaporization and condensation unit operations.

Distillation is one of the common methods for medicine detection, the existing distillation device has the problem of slow distillation speed, and separated liquid is easily adsorbed on the inner wall of the device and can only automatically slide down under the action of the gravity of the device, and the collection and separation of the liquid are slow.

Disclosure of Invention

Technical problem to be solved

Aiming at the defects of the prior art, the invention provides the high-efficiency distillation device for medicine detection, and solves the problems of long time consumption and low efficiency of the conventional distillation device.

(II) technical scheme

In order to achieve the purpose, the invention provides the following technical scheme: the utility model provides an efficient distillation plant for drug detection, includes a retort, the top left and right sides of retort all is provided with the feed inlet, the bottom central authorities of retort have set firmly first motor, the output of first motor and the agitator coaxial coupling that is located retort inner chamber bottom, the inner chamber bottom of retort is provided with the heater.

The top of retort inner chamber is provided with the distillation fill, the inner chamber of distillation fill is provided with the cooling intermediate layer, the cooling intermediate layer all pegs graft in the left and right sides and have cold water to advance pipe and cold water exit tube, the cold water advances the top of pipe and cold water exit tube and all runs through outside the top of retort.

The central authorities at retort top have set firmly the second motor, the output of second motor and the pivot coaxial coupling that is located retort inner chamber top, install first clear water brush and second clear water brush in the pivot respectively, and first clear water brush and second clear water brush all can contact with the inner wall of distilling fill.

The bottom fixedly connected with drain pipe of distilling hopper, a lateral wall of retort has set firmly the condensing box, the condensing box embeds there is the condenser pipe, the top and the bottom of drain pipe of condenser pipe are connected, the bottom of condenser pipe extends to outside the bottom of condensing box, the top of condensing box is pegged graft and is had the cold air duct, be provided with first ooff valve on the cold air duct.

The bottom of retort has set firmly the supporting leg, the bottom of retort is provided with row material pipe, it is provided with the second ooff valve on the material pipe to arrange.

Preferably, the stirrer comprises spiral stirring blades at the upper side and the lower side and a stirring fork positioned in the middle.

Preferably, the top of the stirrer is fixedly connected with an anti-sticking brush which can be contacted with the inner wall of the distillation tank.

Preferably, the inner cavity of the distillation bucket is provided with a heat insulation layer.

Preferably, the condensation pipe is a serpentine pipe.

Preferably, the bottom of the distillation tank is in the shape of a "W".

(III) advantageous effects

The invention provides a high-efficiency distillation device for medicine detection. The method has the following beneficial effects:

this efficient distillation plant for medicine detects through setting up rabbling mechanism, can accelerate distillation process greatly, promotes the composition quickly separating in the medicinal material to accelerate whole distillation process, through setting up clear water mechanism, can clear up the cooling liquid of distilling, make originally adsorb the liquid in the distiller inside discharge fast, accelerated the row's of distilled liquid material process, thereby improved distillation efficiency.

Drawings

FIG. 1 is a cross-sectional view of the structure of the present invention;

FIG. 2 is a sectional view of the distillation bucket structure of the present invention.

In the figure: 1. a distillation tank; 2. a feed inlet; 3. a first motor; 4. a stirrer; 41. a spiral stirring blade; 42. a stirring fork; 5. a heater; 6. a distillation hopper; 7. cooling the interlayer; 8. a cold water inlet pipe; 9. a cold water outlet pipe; 10. a second motor; 11. a rotating shaft; 12. a first clear water brush; 13. a second clear water brush; 14. a drain pipe; 15. a condenser tank; 16. a condenser tube; 17. a cold air pipe; 18. a first on-off valve; 19. supporting legs; 20. a discharge pipe; 21. a second on-off valve; 22. anti-sticking; 23. an insulating layer.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

As shown in fig. 1, the present invention provides a technical solution: the utility model provides an efficient distillation plant for medicine detection, including a retort 1, retort 1's bottom is "W" shape, it is located the least significant end of "W" to arrange material pipe 20, other compositions after the distillation are discharged through arranging material pipe 20, retort 1's the top left and right sides all is provided with feed inlet 2, retort 1's bottom central authorities have set firmly first motor 3, first motor 3's output and the 4 coaxial coupling of agitator that are located retort 1 inner chamber bottom, agitator 4 includes the spiral stirring leaf 41 of upper and lower both sides and is located the stirring fork 42 at middle part, the top fixedly connected with of agitator 4 can with the antiseized brush 22 of retort 1 inner wall contact, set up antiseized brush 22, can prevent that a small amount of compositions from appearing gluing on retort 1's inner wall, retort 1's inner chamber bottom is provided with heater 5.

As shown in fig. 1-2, a distillation bucket 6 is disposed at the top of the inner cavity of the distillation tank 1, a thermal insulation layer 23 is disposed in the inner cavity of the distillation bucket 6, the thermal insulation layer 23 is disposed to insulate the distillation bucket 6, and prevent the distillate from being adsorbed on the outer wall of the distillation bucket 6 and being difficult to collect due to the action of cold water on the outer side of the distillation bucket 6, the distillate is adsorbed on the inner wall of the distillation bucket 6 due to the cooling effect of cold water, a cooling interlayer 7 is disposed in the inner cavity of the distillation bucket 6, a cold water inlet pipe 8 and a cold water outlet pipe 9 are respectively inserted into the left side and the right side of the cooling interlayer 7, and the tops of the cold water inlet pipe 8 and the.

As shown in fig. 1, a second motor 10 is fixedly arranged at the center of the top of the distillation retort 1, the output end of the second motor 10 is coaxially connected with a rotating shaft 11 positioned at the top of the inner cavity of the distillation retort 1, a first clean water brush 12 and a second clean water brush 13 are respectively arranged on the rotating shaft 11, and the first clean water brush 12 and the second clean water brush 13 can be contacted with the inner wall of the distillation hopper 6.

As shown in fig. 1, the bottom fixedly connected with drain pipe 14 of distillation fill 6, a lateral wall of retort 1 has set firmly condensing box 15, condensing box 15 embeds there is condenser pipe 16, condenser pipe 16 is snakelike tubular product, the area of contact of distillate with air conditioning has been increased, condensation effect has been improved, the top of condenser pipe 16 is connected with the bottom of drain pipe 14, outside the bottom of condenser pipe 16 extended to the bottom of condensing box 15, the top of condensing box 15 is pegged graft and is had air cooling pipe 17, be provided with first ooff valve 18 on the air cooling pipe 17.

As shown in figure 1, the bottom of the distillation retort 1 is fixedly provided with a supporting leg 19, the bottom of the distillation retort 1 is provided with a discharge pipe 20, and the discharge pipe 20 is provided with a second switch valve 21.

During the use, the medicine raw materials are poured into to retort 1 in through feed inlet 2, start first motor 3 and heater 5, heat the medicine through heater 5, make some composition distillation away wherein, drive agitator 4 through first motor 3 and rotate, through spiral stirring leaf 41 and the stirring fork 42 on the agitator 4, can accelerate by the quick escape of distillation composition.

The liquid of distillation out is absorbed through distillation fill 6, the distillate adsorbs on the lateral wall of distillation fill 6, advance pipe 8 through cold water and let in cold water, cold water is after the distillate cooling, rethread cold water exit tube 9 discharges, form circulation cold water supply in proper order, ensure the condensation effect, start second motor 10, it rotates to drive pivot 11, thereby drive first clear water brush 12 and second clear water brush 13 and rotate, thereby will adsorb the distillate on distillation fill 6 lateral wall and fall, make it discharge to the condenser pipe 16 in the condensate tank 15 through drain pipe 14, continuously input cold air in condensate tank 15 through air conditioning pipe 17, after cold air and condenser pipe 16 contact, further accelerate the discharge of distillate.

To sum up, this efficient distillation plant for medicine detection through setting up rabbling mechanism, can accelerate the distillation process greatly, promotes the composition quickly separating in the medicinal material to accelerate whole distillation process, through setting up clear water mechanism, can clear up the cooling liquid of distilling, make originally adsorb the liquid quick discharge in the distiller inside, accelerated the row's of distilled liquid material process, thereby improved distillation efficiency.

It should be noted that the electrical components shown in this document are all electrically connected to an external master controller and 220V mains, and the master controller may be a conventional known device such as a computer for controlling, and the control principle, internal structure, and control switching manner of the device are conventional means in the prior art, and are directly referred to herein without further description. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims

1. The utility model provides an efficient medicine distillation plant for detection which characterized in that: the device comprises a distillation tank (1), wherein feed inlets (2) are formed in the left side and the right side of the top of the distillation tank (1), a first motor (3) is fixedly arranged in the center of the bottom of the distillation tank (1), the output end of the first motor (3) is coaxially connected with a stirrer (4) positioned at the bottom of an inner cavity of the distillation tank (1), and a heater (5) is arranged at the bottom of the inner cavity of the distillation tank (1);

a distillation hopper (6) is arranged at the top of the inner cavity of the distillation tank (1), a cooling interlayer (7) is arranged in the inner cavity of the distillation hopper (6), a cold water inlet pipe (8) and a cold water outlet pipe (9) are respectively inserted into the left side and the right side of the cooling interlayer (7), and the tops of the cold water inlet pipe (8) and the cold water outlet pipe (9) penetrate through the outside of the top of the distillation tank (1);

a second motor (10) is fixedly arranged at the center of the top of the distillation tank (1), the output end of the second motor (10) is coaxially connected with a rotating shaft (11) positioned at the top of an inner cavity of the distillation tank (1), a first clear water brush (12) and a second clear water brush (13) are respectively arranged on the rotating shaft (11), and the first clear water brush (12) and the second clear water brush (13) can be in contact with the inner wall of the distillation hopper (6);

the bottom of the distillation bucket (6) is fixedly connected with a drain pipe (14), a condensation box (15) is fixedly arranged on one side wall of the distillation tank (1), a condensation pipe (16) is arranged in the condensation box (15), the top of the condensation pipe (16) is connected with the bottom of the drain pipe (14), the bottom of the condensation pipe (16) extends out of the bottom of the condensation box (15), a cold air pipe (17) is inserted into the top of the condensation box (15), and a first switch valve (18) is arranged on the cold air pipe (17);

the bottom of distillation retort (1) has set firmly supporting leg (19), the bottom of distillation retort (1) is provided with row material pipe (20), be provided with second ooff valve (21) on row material pipe (20).

2. A high efficiency distillation apparatus for drug testing as defined in claim 1, wherein: the stirrer (4) comprises spiral stirring blades (41) on the upper side and the lower side and a stirring fork (42) positioned in the middle.

3. A high efficiency distillation apparatus for drug testing as defined in claim 1, wherein: the top of the stirrer (4) is fixedly connected with an anti-sticking brush (22) which can be contacted with the inner wall of the distillation retort (1).

4. A high efficiency distillation apparatus for drug testing as defined in claim 1, wherein: and a heat insulation layer (23) is arranged in the inner cavity of the distillation hopper (6).

5. A high efficiency distillation apparatus for drug testing as defined in claim 1, wherein: the condensation pipe (16) is a coiled pipe.

6. A high efficiency distillation apparatus for drug testing as defined in claim 1, wherein: the bottom of the distillation tank (1) is W-shaped.