CN111920746B - Moisturizing and repairing mask and preparation method thereof - Google Patents

Moisturizing and repairing mask and preparation method thereof Download PDF

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CN111920746B
CN111920746B CN202010581629.5A CN202010581629A CN111920746B CN 111920746 B CN111920746 B CN 111920746B CN 202010581629 A CN202010581629 A CN 202010581629A CN 111920746 B CN111920746 B CN 111920746B
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percent
water
moisturizing
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CN111920746A (en
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董朝阳
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GUANGZHOU GREEN HUMAN BIOTECHNOLOGY CO Ltd
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GUANGZHOU GREEN HUMAN BIOTECHNOLOGY CO Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31Hydrocarbons
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4993Derivatives containing from 2 to 10 oxyalkylene groups
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • A61K8/602Glycosides, e.g. rutin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/68Sphingolipids, e.g. ceramides, cerebrosides, gangliosides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/731Cellulose; Quaternized cellulose derivatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8147Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8158Homopolymers or copolymers of amides or imides, e.g. (meth) acrylamide; Compositions of derivatives of such polymers
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
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    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/981Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Cosmetics (AREA)

Abstract

The invention relates to the technical field of cosmetics, in particular to moisturizing and repairing mask liquid which comprises the following components in percentage by mass: 0.05 to 0.2 percent of allantoin, 0.05 to 0.2 percent of hydroxyethyl cellulose, 1 to 5 percent of glycerol, 0.01 to 0.05 percent of sodium hyaluronate, 2 to 10 percent of propylene glycol, 0.01 to 0.3 percent of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.01 to 0.3 percent of isohexadecane, 0.01 to 0.3 percent of polysorbate-80, and 0.05 to 0.15 percent of methylparaben; 0.05-0.5% of p-hydroxyacetophenone, 0.05-0.2% of carbomer, 0.1-2% of betaine, 0.1-2% of snow lotus extract, 0.1-3% of ginseng extract, 0.1-3% of centella asiatica extract, 0.1-3% of cubilose extract, 0.1-5% of purslane extract, 0.1-3% of raglan rhizomes leaf extract, 1.1-5% of ceramide, 0.05-0.3% of triethanolamine, 0.015% of PEG-40 hydrogenated castor oil, 0.1-2% of glycerol glucoside, 0.005% of essence, 0.1-0.5% of preservative and water. The moisturizing and repairing facial mask liquid can achieve a good moisturizing and repairing effect.

Description

Moisturizing and repairing mask and preparation method thereof
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to a moisturizing and repairing mask and a preparation method thereof.
Background
Along with the continuous improvement of the living standard of people and the continuous development of science and technology, cosmetics occupy more and more important positions in the life of people, and the development of the chemistry of the cosmetics is greatly driven.
The facial mask is a carrier of beauty care products, and the components in the facial mask permeate into the horny layer of the skin epidermis to make the skin soft and elastic. However, the moisturizing and repairing effects of the facial mask in the current market are not ideal, and the pursuit of consumers for beauty cannot be completely met, so that a facial mask with good moisturizing, moisturizing and repairing effects is urgently needed to be researched.
Disclosure of Invention
In view of the above problems, the present invention aims to provide a mask with good moisturizing and repairing effects.
In order to achieve the purpose, the invention adopts the following technical scheme:
the moisturizing and repairing mask liquid comprises the following components in percentage by mass: 0.05 to 0.2 percent of allantoin, 0.05 to 0.2 percent of hydroxyethyl cellulose, 1 to 5 percent of glycerin, 0.01 to 0.05 percent of sodium hyaluronate, 2 to 10 percent of propylene glycol, 0.01 to 0.3 percent of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.01 to 0.3 percent of isohexadecane, 800.01 to 0.3 percent of polysorbate and 0.05 to 0.15 percent of methylparaben; 0.05-0.5% of p-hydroxyacetophenone, 0.05-0.2% of carbomer, 0.1-2% of betaine, 0.1-2% of snow lotus extract, 0.1-3% of ginseng extract, 0.1-3% of centella asiatica extract, 0.1-3% of cubilose extract, 0.1-5% of purslane extract, 0.1-3% of leafy extract of rhizomes fallen to the ground, 1.1-5% of ceramide, 0.05-0.3% of triethanolamine, 0.015% of PEG-40 hydrogenated castor oil, 0.1-2% of glycerol glucoside, 0.005% of essence, 0.1-0.5% of preservative and water;
the water content is the balance to bring the total content of all components to 100%.
As a further improvement, the preservative is bis (hydroxymethyl) imidazolidinyl urea and iodopropynyl alcohol butyl carbamate, and the mass percent of the bis (hydroxymethyl) imidazolidinyl urea and the mass percent of the iodopropynyl alcohol butyl carbamate in the mask liquid are respectively 0.099-0.49% and 0.001-0.01%.
As a further improvement, the mask liquid consists of the following components in percentage by mass: 0.10% of allantoin, 0.10% of hydroxyethyl cellulose, 3.00% of glycerol, 0.03% of sodium hyaluronate, 5.00% of propylene glycol, 0.01% of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.11% of isohexadecane, 0.08% of polysorbate-80 and 0.12% of methylparaben; 0.10% of p-hydroxyacetophenone, 0.12% of carbomer, 1.20% of betaine, 1.00% of snow lotus herb extract, 1.50% of ginseng extract, 1.00% of centella asiatica extract, 1.60% of cubilose dolichos extract, 1.20% of purslane extract, 1.5% of extract of leaves of centella asiatica, 1.30% of ceramide, 0.11% of triethanolamine, 0.015% of PEG-40 hydrogenated castor oil, 1.6% of glycerol glucoside, 0.005% of essence, 0.12625% of preservative and water;
the water content is the balance to bring the total content of all components to 100%.
As a further improvement, the water is deionized water or purified water.
As a further improvement, the preparation method comprises the following steps:
the method comprises the following steps: adding water, allantoin and hydroxyethyl cellulose into a container, heating to 90-98 deg.C, and stirring to dissolve uniformly;
step two: cooling to 70-80 deg.C, adding glycerol and sodium hyaluronate, stirring and mixing;
step three: adding carbomer and water, and stirring and mixing uniformly;
step four: cooling to 60 deg.C, adding the mixture of propylene glycol, methyl hydroxybenzoate and p-hydroxyacetophenone which is completely dissolved by heating at 70-80 deg.C;
step five: cooling to 45 deg.C, adding betaine, herba Saussureae Involueratae extract, ginseng radix extract, herba Centellae extract, nidus Collocaliae extract, herba Portulacae extract, radix rehmanniae leaf extract, ceramide 1, triethanolamine, PEG-40 hydrogenated castor oil, glycerol glucoside, sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80, essence and antiseptic, stirring and mixing;
wherein, the water added in the step one is 6.7 to 7.5 times of the water added in the step three.
Compared with the prior art, the invention has the following beneficial effects:
1) The centella extract, the purslane extract, the cubilose extract and the ragged root leaf extract (functional components) are compounded and cooperated with each other, so that the activity of skin cells can be greatly improved; hyaluronic acid, betaine, ceramide and glycerol glucoside (moisturizing components) are compounded and cooperated with one another, so that the moisture of the skin can be greatly improved; the facial mask repairing liquid is prepared by compounding sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80, carbomer and hydroxyethyl cellulose, has a good skin-soothing effect, can enable the facial mask to be more skin-friendly, enables other substances to penetrate through the skin more easily, and is mutually compounded through the mutual cooperation of functional components, moisturizing components, components with the skin-soothing effect and other various components, so that the facial mask repairing liquid can be well applied to the surface of the skin, and a good moisturizing repairing effect is realized.
2) The components prepared by the preparation method can be stably stored for a long time, and the phenomena of facial mask liquid layering and the like can not occur after the components are placed for 2 years.
Detailed Description
The present invention will be further described with reference to the following examples.
Example 1
The moisturizing and repairing mask liquid comprises the following components in percentage by mass: 0.05 to 0.2 percent of allantoin, 0.05 to 0.2 percent of hydroxyethyl cellulose, 1 to 5 percent of glycerol, 0.01 to 0.05 percent of sodium hyaluronate, 2 to 10 percent of propylene glycol, 0.01 to 0.3 percent of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.01 to 0.3 percent of isohexadecane, 0.01 to 0.3 percent of polysorbate ester and 0.05 to 0.15 percent of methylparaben; 0.05-0.5% of p-hydroxyacetophenone, 0.05-0.2% of carbomer, 0.1-2% of betaine, 0.1-2% of snow lotus extract, 0.1-3% of ginseng extract, 0.1-3% of centella asiatica extract, 0.1-3% of cubilose extract, 0.1-5% of purslane extract, 0.1-3% of leafy extract of rhizomes of the fallen rain, 1.1-5% of ceramide, 0.05-0.3% of triethanolamine, 0.015% of PEG-40 hydrogenated castor oil, 0.1-2% of glycerol glucoside, 0.005% of essence, 0.1-0.5% of preservative and water;
the water content is the balance to bring the total content of all components to 100%.
Preferably, the preservative can be selected from bis (hydroxymethyl) imidazolidinyl urea and iodopropynyl alcohol butyl carbamate, and the mass percentage of the bis (hydroxymethyl) imidazolidinyl urea and the mass percentage of the iodopropynyl alcohol butyl carbamate in the mask liquid are respectively 0.099-0.49% and 0.001-0.01%.
Example 2
The moisturizing and repairing mask liquid comprises the following components in percentage by mass: 0.10% of allantoin, 0.10% of hydroxyethyl cellulose, 3.00% of glycerol, 0.03% of sodium hyaluronate, 5.00% of propylene glycol, 0.01% of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.11% of isohexadecane, 0.08% of polysorbate-80 and 0.12% of methylparaben; 0.10% of p-hydroxyacetophenone, 0.12% of carbomer, 1.20% of betaine, 1.00% of snow lotus herb extract, 1.50% of ginseng extract, 1.00% of centella asiatica extract, 1.60% of cubilose dolichos extract, 1.20% of purslane extract, 1.5% of extract of leaves of centella asiatica, 1.30% of ceramide, 0.11% of triethanolamine, 0.015% of PEG-40 hydrogenated castor oil, 1.6% of glycerol glucoside, 0.005% of essence, 0.12625% of preservative and water;
the water content is the balance to bring the total content of all components to 100%.
Namely, the mass percentage of water in this example is 80.07375%.
The preservative can be bis (hydroxymethyl) imidazolidinyl urea and iodopropynyl alcohol butyl carbamate, and the mass percent of the bis (hydroxymethyl) imidazolidinyl urea and the mass percent of the iodopropynyl alcohol butyl carbamate in the mask liquid are respectively 0.125% and 0.00125%, respectively.
Example 3
Compared with the example 2, the glycerol glucoside is not added into the facial mask essence, and the addition amount of the rest formula is the same as that of the example 2.
Example 4
Compared with the example 2, hyaluronic acid, betaine and ceramide are not added into the facial mask essence, and the addition amount of the rest formula is the same as that of the example 2.
Example 5
Compared to example 2, hyaluronic acid, betaine, ceramide, and glycerol glucoside were not added to the mask essence, and the remaining formulation was the same as example 2. Comparative example
Example 6
Compared with the example 2, the addition amount of the standard rooting leaf extract is not added into the facial mask essence, and the addition amount of the rest formula is the same as that of the example 2. (adding centella asiatica extract, purslane extract, and cubilose extract)
Example 7
Compared with the facial mask essence of example 2, the centella asiatica extract, the purslane extract and the cubilose extract are not added into the facial mask essence, and the addition amount of the rest formula is the same as that of the facial mask essence of example 2. (extract of leaves of Fall Raddeana Lam. Et Arn. Ex Fr.) S.F.
Example 8
Compared with the example 2, the centella asiatica extract, the centella asiatica leaf extract and the cubilose extract are not added into the mask essence, and the addition amount of the rest formula is the same as that of the example 2. (addition of Portulaca oleracea extract)
Example 9
Compared with the example 2, the purslane extract, the rhizoctonia solani leaf extract and the cubilose yunnanensis extract are not added into the mask essence, and the addition amount of the rest formula is the same as that of the example 2. (adding centella asiatica extract)
Example 10
Compared with the example 2, the purslane extract, the ragged rooting leaf extract and the centella asiatica extract are not added into the mask essence, and the addition amount of the rest of the formula is the same as that of the example 2. (adding extract of bird's nest)
Example 11
Compared with the example 2, the purslane extract, the standard groundsel leaf extract, the centella asiatica extract and the cubilose extract are not added into the mask essence, and the addition amount of the rest formula is the same as that of the example 2. (control example without addition of functional component)
Example 12
Compared with the example 2, centella asiatica extract, purslane extract, centella asiatica leaf extract, cubilose extract, glycerol glucoside, hyaluronic acid, betaine and ceramide are not added into the mask essence, and the addition amount of the rest of the formula is the same as that of the example 2. (No addition of functional ingredients and moisture-retaining ingredients)
The preparation method of the moisturizing and repairing mask liquid disclosed by the embodiments 1-12 comprises the following steps:
the method comprises the following steps: adding water, allantoin and hydroxyethyl cellulose into a container, heating to 90-98 deg.C, and stirring to dissolve uniformly;
step two: cooling to 70-80 deg.C, adding glycerol and sodium hyaluronate, stirring and mixing; the glycerol and the sodium hyaluronate can be added into the mixture which is mixed uniformly in advance;
step three: adding carbomer and water, and stirring and mixing uniformly;
step four: cooling to 60 deg.C, adding the mixture of propylene glycol, methyl hydroxybenzoate and p-hydroxyacetophenone which is completely dissolved by heating at 70-80 deg.C;
step five: cooling to 45 deg.C, adding betaine, herba Saussureae Involueratae extract, ginseng radix extract, herba Centellae extract, nidus Collocaliae extract, herba Portulacae extract, radix rehmanniae leaf extract, ceramide 1, triethanolamine, PEG-40 hydrogenated castor oil, glycerol glucoside, sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80, essence and antiseptic, stirring and mixing;
wherein, the water added in the step one is 6.7 to 7.5 times of the water added in the step three.
Wherein, the mass of each added substance is matched with the mass percentage of each substance written in the formula.
For example, in example 2, the mass of each substance added can be as follows:
0.10 part by mass of allantoin, 0.10 part by mass of hydroxyethyl cellulose, 3.00 parts by mass of glycerol, 0.03 part by mass of sodium hyaluronate, 5.00 parts by mass of propylene glycol, 0.01 part by mass of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.11 part by mass of isohexadecane, 0.08 part by mass of polysorbate-80, and 0.12 part by mass of methylparaben; 0.10 part by mass of p-hydroxyacetophenone, 0.12 part by mass of carbomer, 1.20 parts by mass of betaine, 1.00 part by mass of snow lotus extract, 1.50 parts by mass of ginseng extract, 1.00 part by mass of centella asiatica extract, 1.60 parts by mass of cubilose extract, 1.20 parts by mass of purslane extract, 1.5 parts by mass of leafy extract of rhizomes fallen to the ground, 1.30 parts by mass of ceramide, 0.11 part by mass of triethanolamine, 0.015 part by mass of PEG-40 hydrogenated castor oil, 1.6 parts by mass of glycerol glucoside, 0.005 part by mass of essence, 0.12625 part by mass of preservative and 80.07375 parts by mass of water.
Effect testing
In the skin moisture content increase amount test, the skin moisture loss (TEWL) condition test and the skin elasticity change condition test:
the trial tests were conducted on 20 persons (10 men, 10 women, age range 20-50 years) of each example and similar product on the market, and the test results were the average of 20 skin moisture content increase, skin moisture loss and skin elasticity.
Method of using 1-time mask: the facial mask is applied on the surface of human skin for 15 minutes, and then the facial mask is taken down.
Test method after 1 use of the mask: after the mask was used for 1 hour, the moisture content of the skin, the amount of the moisture loss of the skin and the skin elasticity were measured.
Test method 7 days after using the mask: the facial mask is used 1 time every other day, and skin moisture content, skin moisture loss and skin elasticity are tested 1 hour after the facial mask is used on day 7.
Test method using mask for 13 days: the skin moisture content, skin moisture loss and skin elasticity were measured 1 time every other day and 1 hour after the mask was used on day 13.
Wherein the increase in skin moisture content is an increase in skin moisture content relative to skin moisture content before use after 1 hour or 7 days or 13 days after use of the mask, for example, the skin moisture content before use is a, and the skin moisture content after 1 hour or 7 days or 13 days after use of the mask is b, the increase in skin moisture content is (b-a) × 100%/a.
Any product could not be used 2-3 days before testing. Clean and wipe the face, and sit still in the room for at least 30min before testing;
1-12 the room temperature was 24 ℃ and the humidity 55% of the test.
The facial mask comprises facial mask essence and facial mask paper soaked with the essence, wherein the facial mask is 25g of essence per piece.
1. Skin moisture content increase amount test
The moisture content of the skin was measured by a Cotomer MPA6 host machine of the German CK company and a skin moisture content Cornemeter CM825 test probe, and the increase of the moisture content of the skin is shown in Table 1.
TABLE 1
Figure BDA0002552516580000061
The product prepared by the invention has good moisturizing effect on skin. Meanwhile, the hyaluronic acid, the betaine, the ceramide and the glycerol glucoside are added for compounding, so that the water replenishing effect is good, and the substances generate a synergistic effect.
In addition, the functional components, the soothing components and the moisturizing components are compounded with other substances, so that the moisturizing effect is good.
1.2 skin Water loss (TEWL) Condition testing
The skin water loss condition of the facial mask of the invention in different time is tested by adopting a skin water loss Tewameter TM300 probe and a skin water loss TEWL test method, and the experimental result is shown in a table 2.
TABLE 2
Article item Average value of skin water loss (g/square meter. H)
Pre-use testing 14.7
Test after 7 days using the product of example 1 13.9-14.5
13 days after testing using the product of example 1 13.4-13.8
7 days after testing using the product of example 2 14.1
13 days after testing using the product of example 2 13.6
The use of the facial mask of the invention can ensure that the skin protective layer becomes more complete, the longer the use time is, the less the skin moisture loss is, the more complete the skin protective layer is and the better the moisturizing effect is.
1.3 measurement of skin elasticity Change
The skin elasticity was tested using a skin elasticity test probe Reviscometer RV600 using the instrument, meter MPA580, and the results are shown in table 3.
The skin elasticity probe was used to test different parts of the face on both sides, and 4 test values were read, the average of which was taken as experimental test data.
TABLE 3
Article item Average value of skin elasticity test (Ur/Uf)
Pre-use testing 0.63
Test after 7 days using the product of example 1 0.63-0.66
13 days after testing using the product of example 1 0.65-0.70
Test after 7 days using the product of example 2 0.65
13 days after testing using the product of example 2 0.68
7 days after testing using the product of example 12 0.63
13 days after testing using the product of example 12 0.63
The test data is gradually increased, which shows that the skin elasticity is better improved by continuously using the facial mask.
Meanwhile, the functional components, the components with the relieving effect, the moisturizing components and other substances are compounded, so that the skin elasticity is greatly improved, and the repairing effect is good.
1.4 Effect of active substances on cell Activity
The MTT method was used to examine the effect of the example serum on the relative viability of cells, and the results are shown in Table 4.
TABLE 4
Figure BDA0002552516580000071
Figure BDA0002552516580000081
Table 4 shows that the centella asiatica extract, the centella asiatica leaf extract, the cubilose extract and the purslane extract are compounded, and when the product is applied, the product has a good effect of improving cell activity, and when the mask is applied, the skin elasticity can be well improved, and damaged cells of the skin can be repaired.
Meanwhile, the sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80, carbomer and hydroxyethyl cellulose are not added, so that various substances cannot be fused together, and the facial mask essence cannot be prepared at all.
In the present invention, an extract of snow lotus (SAUSSUREA INVOLUCRATA), an extract of GINSENG (GINSENG), an extract of CENTELLA ASIATICA (CENTELLA ASIATICA), an extract of cubilose, an extract of purslane (PORTULACA OLERACEA), and an extract of leaves of kalanchoepensis (kalanchoepinata) can be purchased from the market, and other components can be purchased from the market.
The snow lotus herb EXTRACT is available from Shanghai Gajia leaf industry Co., ltd under the name of SAUSSUREA INVOLUTA EXTRACT.
Ginseng EXTRACT having the English name PANAX GINSENG EXTRACT is available from Shanghai Gajia leaf industries, inc.
CENTELLA ASIATICA EXTRACT, known by the INCI name CENTELLA ASIATICA EXTRACT, is available from noran biotechnology, guangzhou.
The EXTRACT of bird's NEST in the rain, having the INCI name SWIFTLET NEST EXTRACT, is available from guangzhou reputable chemical technology ltd.
The purslane EXTRACT is available from Noro, guangzhou Biotech, inc. under the name Portulaca Oleracea EXTRACT, inc.
EXTRACT of leaves of Kalanchoe (Kalanchoepensis) is available from Kalanchoe Pinnata LEAF EXTRACT, guangzhou, inc., under the name of KAlanchoe Pinnata LEAF EXTRACT.
The essence can be selected from facial mask essence purchased in the market, flower fragrance essence, such as chamomile essence sold by Yunya spice Co., ltd in Jiangmen city, and other essence.
The technical solutions provided by the embodiments of the present invention are described in detail above, and the principles and embodiments of the present invention are explained herein by using specific examples, and the descriptions of the embodiments are only used to help understanding the principles of the embodiments of the present invention; meanwhile, for a person skilled in the art, according to the embodiments of the present invention, there may be variations in the specific implementation manners and application ranges, and in summary, the content of the present description should not be construed as a limitation to the present invention.

Claims (4)

1. The moisturizing and repairing mask liquid is characterized by comprising the following components in percentage by mass: 0.05 to 0.2 percent of allantoin, 0.05 to 0.2 percent of hydroxyethyl cellulose, 1 to 5 percent of glycerol, 0.01 to 0.05 percent of sodium hyaluronate, 2 to 10 percent of propylene glycol, 0.01 to 0.3 percent of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.01 to 0.3 percent of isohexadecane, 0.01 to 0.3 percent of polysorbate-80, and 0.05 to 0.15 percent of methylparaben; 0.05-0.5% of p-hydroxyacetophenone, 0.05-0.2% of carbomer, 0.1-2% of betaine, 0.1-2% of snow lotus extract, 0.1-3% of ginseng extract, 0.1-3% of centella asiatica extract, 0.1-3% of cubilose extract, 0.1-5% of purslane extract, 0.1-3% of leafy extract of rhizomes of the fallen rain, 1.1-5% of ceramide, 0.05-0.3% of triethanolamine, 0.015% of PEG-40 hydrogenated castor oil, 0.1-2% of glycerol glucoside, 0.005% of essence, 0.1-0.5% of preservative and water;
the water content is the balance which enables the total content of all the components to reach 100%;
the preservative is bis (hydroxymethyl) imidazolidinyl urea and iodopropynyl alcohol butyl carbamate, and the mass percent of the bis (hydroxymethyl) imidazolidinyl urea and the mass percent of the iodopropynyl alcohol butyl carbamate in the mask liquid are respectively 0.099-0.49% and 0.001-0.01%.
2. The moisturizing repairing mask solution according to claim 1, wherein the mask solution consists of the following components in percentage by mass: 0.10% of allantoin, 0.10% of hydroxyethyl cellulose, 3.00% of glycerol, 0.03% of sodium hyaluronate, 5.00% of propylene glycol, 0.01% of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.11% of isohexadecane, 0.08% of polysorbate-80 and 0.12% of methylparaben; 0.10% of p-hydroxyacetophenone, 0.12% of carbomer, 1.20% of betaine, 1.00% of snow lotus herb extract, 1.50% of ginseng extract, 1.00% of centella asiatica extract, 1.60% of cubilose dolichos extract, 1.20% of purslane extract, 1.5% of extract of leaves of centella asiatica, 1.30% of ceramide, 0.11% of triethanolamine, 0.015% of PEG-40 hydrogenated castor oil, 1.6% of glycerol glucoside, 0.005% of essence, 0.12625% of preservative and water;
the water content is the balance to bring the total content of all components to 100%.
3. The moisturizing repair mask solution of claim 1, wherein the water is deionized or purified water.
4. The preparation method of the moisturizing and repairing mask liquid is characterized by comprising the following steps:
the method comprises the following steps: adding water, allantoin and hydroxyethyl cellulose into a container, heating to 90-98 deg.C, and stirring to dissolve uniformly;
step two: cooling to 70-80 deg.C, adding glycerol and sodium hyaluronate, stirring and mixing;
step three: adding carbomer and water, and stirring and mixing uniformly;
step four: cooling to 60 deg.C, adding the mixture of propylene glycol, methyl hydroxybenzoate and p-hydroxyacetophenone which is completely dissolved by heating at 70-80 deg.C;
step five: cooling to 45 deg.C, adding betaine, herba Saussureae Involueratae extract, ginseng radix extract, herba Centellae extract, nidus Collocaliae extract, herba Portulacae extract, radix rehmanniae leaf extract, ceramide 1, triethanolamine, PEG-40 hydrogenated castor oil, glycerol glucoside, sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80, essence and antiseptic, stirring and mixing;
wherein, the water added in the step one is 6.7 to 7.5 times of the water added in the step three.
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