CN111920722A - Production process of wolfberry facial mask - Google Patents
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/60—Sugars; Derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
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Abstract
The invention relates to the technical field of mask preparation, in particular to a wolfberry mask production process, which specifically comprises the following steps: weighing the following components in parts by weight: 0.05-0.1 part of ethylene diamine tetraacetic acid disodium salt, 2-8 parts of propylene glycol, 10-30 parts of medlar extract, 2-6 parts of glycerol, 1-4 parts of butanediol, 0.03-0.12 part of methyl ester, 2-10 parts of oat gum, 0.5-2 parts of trehalose, 0.01-0.03 part of essence, 0.02-0.1 part of pigment, 0.1-0.2 part of solubilizer and 60-130 parts of water; putting 0.05-0.1 part of ethylene diamine tetraacetic acid disodium salt, 2-8 parts of propylene glycol, 10-30 parts of medlar extract and 60-130 parts of water into a pot, and heating; keeping the temperature and sterilizing for 20min, then discharging 1kg for later use, and cooling with cooling water; adding 2-6 parts of glycerol, 1-4 parts of butanediol, 0.03-0.12 part of methyl ester, 2-10 parts of oat gum, 0.5-2 parts of trehalose, 0.01-0.03 part of essence, 0.02-0.1 part of pigment and 0.1-0.2 part of solubilizer, adjusting the pH value to 5.5-6.5 and stirring; filtering, discharging, inspecting, keeping the temperature at 36-38 deg.C, storing for 48h, filtering again, and packaging. The invention has the beneficial effects that: the prepared facial mask has dual functions of pharmacology and nutrition.
Description
Technical Field
The invention relates to the technical field of mask preparation, in particular to a wolfberry mask production process.
Background
With the continuous development of society, people pay qualitative change to the attention to life and health, the attention degree exceeds the past in any age, the consumption of 'returning to nature' and 'green' becomes fashion, and the natural functional plant industry is confronted with unprecedented development opportunities. According to the incomplete statistics of the world health organization, the worldwide functional plant market is increased at a speed of 10-20% per year, and the American functional plant production value is increased at a speed of more than 20% per year, so that the market demand potential of the functional plant product is huge. In the face of the prevailing conditions of functional products, how to comprehensively develop and utilize functional plants, develop and develop terminal products with high added values, link up industrial links, establish industrial chains, and pull continuous healthy and rapid development of the functional plant resource industry is just the important work which needs to be developed urgently.
The medlar is a traditional Chinese medicinal material with homology of medicine and food in China, and fruits, flowers, leaves, peels and roots of the medlar can be used as medicines, so that the medlar has high nutritive value and medicinal health-care efficacy. In recent years, researches show that the pharmacological effects of the medlar in the aspects of regulating human immunity, inhibiting tumor growth, preventing and blocking cancer cell mutation and the like are related to medlar polysaccharide, betaine, beta-carotene and other components in the medlar. In addition, the medlar has various nutrient components required by human body, and the detection and analysis shows that every 100g of medlar fresh fruit contains 12g of protein, 46.3g of carbohydrate, 12.6g of dietary fiber, 19.6mg of carotene, 10.2mg of VBs, 4.5mg of nicotinic acid, 13mg of ascorbic acid, 37mg of calcium, 6.5mg of iron, 224mg of phosphorus, 41mg of magnesium, 15mg of zinc, 0.79mg of manganese and 1.67mg of selenium. In addition, clinical medicine proves that the lycium barbarum polysaccharide in the lycium barbarum has the effects of reducing blood fat, blood sugar and fatty liver, resisting fatigue, resisting aging, eliminating free radicals, inhibiting the generation of oxidized lipid and enhancing the activity of glutathione peroxidase and erythrocyte superoxide dismutase in human blood. The medlar seed oil can promote skin blood circulation, directly participate in skin metabolism, eliminate oxygen free radicals, delay aging of epidermis and dermis, strengthen skin hydration function, make skin soft and elastic, have obvious whitening effect, and have obvious fading effect on senile plaque and chloasma pigmentation; therefore, the lycium barbarum polysaccharide and the lycium barbarum seed oil have high development value as natural antioxidants.
At present, related researches on medlar development mainly take health care products as main materials, and reports that medlar polysaccharide and medlar seed oil are used as the only active ingredients for resisting oxidation, scavenging free radicals, resisting aging and resisting radiation in cosmetics are not found in the field of cosmetics. Therefore, research and development of a functional wolfberry facial mask have potential market value.
Disclosure of Invention
The invention aims to solve the problems in the prior art, and the prepared wolfberry facial mask has dual functions of pharmacology and nutrition, and achieves the effects of whitening, moistening, moisturizing, smoothing skin wrinkles, delaying skin aging and the like.
In order to solve the technical problems, the technical scheme provided by the invention is as follows: a production process of a wolfberry facial mask specifically comprises the following steps: (1) weighing the following components in parts by weight: 0.05-0.1 part of ethylene diamine tetraacetic acid disodium salt, 2-8 parts of propylene glycol, 10-30 parts of medlar extract, 2-6 parts of glycerol, 1-4 parts of butanediol, 0.03-0.12 part of methyl ester, 2-10 parts of oat gum, 0.5-2 parts of trehalose, 0.01-0.03 part of essence, 0.02-0.1 part of pigment, 0.1-0.2 part of solubilizer and 60-130 parts of water;
(2) cleaning equipment and a container, and checking whether the raw materials are qualified;
(3) putting 0.05-0.1 part of disodium ethylene diamine tetraacetate, 2-8 parts of propylene glycol, 10-30 parts of medlar extract and 60-130 parts of water in the step (1) into a pot for heating;
(4) keeping the temperature and sterilizing for 20min, then discharging 1kg for later use, and cooling with cooling water;
(5) adding 2-6 parts of glycerol, 1-4 parts of butanediol, 0.03-0.12 part of methyl ester, 2-10 parts of oat gum, 0.5-2 parts of trehalose, 0.01-0.03 part of essence, 0.02-0.1 part of pigment and 0.1-0.2 part of solubilizer, adjusting the pH value to 5.5-6.5 and stirring;
(6) filtering, discharging, inspecting, keeping the temperature at 36-38 deg.C, storing for 48h, filtering again, and packaging.
Further, the preparation of the medlar extracting solution in the step (1) specifically comprises the following steps: A. adding water into fructus Lycii, homogenizing, extracting with solvent containing 80% alcohol for 2 times (1 hr each time) at solid-to-liquid ratio of 8g/ml, filtering with gauze, and mixing the filtrates to obtain filtrate I;
B. b, taking residues obtained after the ethanol extraction of the barbary wolfberry fruits in the filtrate preparation in the step A, adding 10 times of distilled water, performing reflux extraction twice for 1 hour each time, filtering, and combining the two filtrates to obtain a second filtrate;
C. and mixing the first filtrate and the second filtrate to obtain the wolfberry extracting solution.
Further, the temperature of the step (3) is increased to 78-80 ℃.
Further, the temperature in the step (4) is reduced to 45-48 ℃.
Further, the stirring speed of the step (5) is 40 rpm.
The invention has the beneficial effects that: the preparation method is simple, the conditions are controllable, and the Chinese wolfberry extract is suitable for mass production, and the added Chinese wolfberry extract is matched with each component for use, so that the mask has the dual functions of pharmacology and nutrition, and achieves the effects of whitening, moistening, moisturizing, smoothing skin wrinkles, delaying skin aging and the like.
Detailed Description
The invention is illustrated below by means of specific examples, without being restricted thereto.
An experiment for determining a preparation scheme of the medlar extracting solution comprises the following steps:
TABLE 1 orthogonal experimental design table for total flavone extraction process in wolfberry fruit
1. Orthogonal test method
Pulverizing fructus Lycii into coarse powder, mixing nine parts, heating and refluxing under orthogonal conditions to extract total flavone, filtering, mixing filtrates, calculating extraction rate, and measuring total flavone content.
2. Results and analysis of orthogonal assays
According to the results of the orthogonal test, the relevant data are respectively subjected to range difference and variance analysis, the results are shown in table 2, and the results show that: the size sequence B of extraction factors influencing the extraction rate and the content of the total flavonoids>A>C>D, visually analyzing as A2B2C3D1Analysis of variance showed that: all factors have no significant influence, and the process for determining the preferred medlar extracting solution is A2B2C3D1The solid-liquid ratio is 8g/ml, 80% ethanol is used as a solvent, reflux extraction is carried out for 2 times, each time is 1h, gauze filtration is carried out, and 2 times of filtrates are combined.
TABLE 2 Quadrature test results of total flavone extraction process in Lycium barbarum
3. Determination of preparation process of wolfberry fruit extract
Adding water into fructus Lycii, homogenizing, extracting with solvent containing 80% alcohol for 2 times (1 hr each time) at solid-to-liquid ratio of 8g/ml, filtering with gauze, and mixing the filtrates to obtain filtrate I; taking residue obtained after extracting fructus Lycii with alcohol, adding 10 times of distilled water, reflux-extracting for two times (1 hr each time), filtering, and mixing the two filtrates to obtain filtrate II; and mixing the first filtrate and the second filtrate to obtain the wolfberry extracting solution.
Example one
Weighing the following components in parts by weight: 0.05kg of ethylene diamine tetraacetic acid disodium salt, 2kg of propylene glycol, 10kg of medlar extract, 2kg of glycerol, 1kg of butanediol, 0.03kg of methyl ester, 2kg of oat gum, 0.5kg of trehalose, 0.01kg of essence, 0.02kg of pigment, 0.1kg of solubilizer and 60kg of water; cleaning equipment and a container, and checking whether the raw materials are qualified; putting 0.05kg of ethylene diamine tetraacetic acid disodium salt, 2kg of propylene glycol, 10kg of medlar extract and 60kg of water into a pot, and heating; keeping the temperature and sterilizing for 20min, then discharging 1kg for later use, and cooling with cooling water; adding 2kg of glycerol, 1kg of butanediol, 0.03kg of methyl ester, 2kg of oat gum, 0.5kg of trehalose, 0.01kg of essence, 0.02kg of pigment and 0.1kg of solubilizer, adjusting the pH value to 5.5-6.5 and stirring; filtering, discharging, inspecting, keeping the temperature at 36-38 deg.C, storing for 48h, filtering again, and packaging.
Example two
Weighing the following components in parts by weight: 0.08kg of ethylene diamine tetraacetic acid disodium salt, 6kg of propylene glycol, 20kg of medlar extract, 4kg of glycerol, 2kg of butanediol, 0.08kg of methyl, 6kg of oat gum, 1kg of trehalose, 0.02kg of essence, 0.06kg of pigment, 0.15kg of solubilizer and 80kg of water; cleaning equipment and a container, and checking whether the raw materials are qualified; putting 0.08kg of ethylene diamine tetraacetic acid disodium salt, 6kg of propylene glycol, 20kg of medlar extract and 80kg of water into a pot, and heating; keeping the temperature and sterilizing for 20min, then discharging 1kg for later use, and cooling with cooling water; adding 4kg of glycerin, 2kg of butanediol, 0.08kg of methyl, 6kg of oat gum, 1kg of trehalose, 0.02kg of essence, 0.06kg of pigment and 0.15kg of solubilizer, adjusting the pH value to 5.5-6.5 and stirring; filtering, discharging, inspecting, keeping the temperature at 36-38 deg.C, storing for 48h, filtering again, and packaging.
EXAMPLE III
Weighing the following components in parts by weight: 0.1kg of ethylene diamine tetraacetic acid disodium salt, 8kg of propylene glycol, 30kg of medlar extract, 6kg of glycerol, 4kg of butanediol, 0.12kg of methyl ester, 10kg of oat gum, 2kg of trehalose, 0.03kg of essence, 0.1kg of pigment, 0.2kg of solubilizer and 100kg of water; cleaning equipment and a container, and checking whether the raw materials are qualified; putting 0.1kg of ethylene diamine tetraacetic acid disodium salt, 8kg of propylene glycol, 30kg of medlar extract and 100kg of water into a pot, and heating; keeping the temperature and sterilizing for 20min, then discharging 1kg for later use, and cooling with cooling water; adding 6kg of glycerin, 4kg of butanediol, 0.12kg of methyl ester, 10kg of oat gum, 2kg of trehalose, 0.03kg of essence, 0.1kg of pigment and 0.2kg of solubilizer, adjusting the pH value to 5.5-6.5 and stirring; filtering, discharging, inspecting, keeping the temperature at 36-38 deg.C, storing for 48h, filtering again, and packaging.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (5)
1. The production process of the wolfberry facial mask is characterized by comprising the following steps: (1) weighing the following components in parts by weight: 0.05-0.1 part of ethylene diamine tetraacetic acid disodium salt, 2-8 parts of propylene glycol, 10-30 parts of medlar extract, 2-6 parts of glycerol, 1-4 parts of butanediol, 0.03-0.12 part of methyl ester, 2-10 parts of oat gum, 0.5-2 parts of trehalose, 0.01-0.03 part of essence, 0.02-0.1 part of pigment, 0.1-0.2 part of solubilizer and 60-130 parts of water;
(2) cleaning equipment and a container, and checking whether the raw materials are qualified;
(3) putting 0.05-0.1 part of disodium ethylene diamine tetraacetate, 2-8 parts of propylene glycol, 10-30 parts of medlar extract and 60-130 parts of water in the step (1) into a pot for heating;
(4) keeping the temperature and sterilizing for 20min, then discharging 1kg for later use, and cooling with cooling water;
(5) adding 2-6 parts of glycerol, 1-4 parts of butanediol, 0.03-0.12 part of methyl ester, 2-10 parts of oat gum, 0.5-2 parts of trehalose, 0.01-0.03 part of essence, 0.02-0.1 part of pigment and 0.1-0.2 part of solubilizer, adjusting the pH value to 5.5-6.5 and stirring;
(6) filtering, discharging, inspecting, keeping the temperature at 36-38 deg.C, storing for 48h, filtering again, and packaging.
2. The wolfberry facial mask production process according to claim 1, which is characterized in that: the preparation of the medlar extracting solution in the step (1) specifically comprises the following steps: A. adding water into fructus Lycii, homogenizing, extracting with solvent containing 80% alcohol for 2 times (1 hr each time) at solid-to-liquid ratio of 8g/ml, filtering with gauze, and mixing the filtrates to obtain filtrate I;
B. b, taking residues obtained after the ethanol extraction of the barbary wolfberry fruits in the filtrate preparation in the step A, adding 10 times of distilled water, performing reflux extraction twice for 1 hour each time, filtering, and combining the two filtrates to obtain a second filtrate;
C. and mixing the first filtrate and the second filtrate to obtain the wolfberry extracting solution.
3. The wolfberry facial mask production process according to claim 1, which is characterized in that: and (4) heating the temperature in the step (3) to 78-80 ℃.
4. The wolfberry facial mask production process according to claim 1, which is characterized in that: and (4) cooling to 45-48 ℃.
5. The wolfberry facial mask production process according to claim 1, which is characterized in that: the stirring speed of the step (5) is 40 rpm.
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101040713A (en) * | 2007-04-27 | 2007-09-26 | 乔泓程 | Health-care food having functions of oxidation resisting and immunity improving |
| CN102659741A (en) * | 2012-04-27 | 2012-09-12 | 宁夏大学 | Method for extracting and preparing active ingredients of Ningxia wolfberries |
| CN102824473A (en) * | 2012-09-17 | 2012-12-19 | 青海红鼎生物工程有限公司 | Lycium ruthenicum murr total flavonoid extract and preparation method thereof |
| CN107440981A (en) * | 2017-09-27 | 2017-12-08 | 海南利南生物科技有限公司 | A kind of matrimony vine facial mask and preparation method thereof |
| AU2020101467A4 (en) * | 2020-07-24 | 2020-08-27 | Institute Of Wolfberry Engineering Technology, Ningxia Academy Of Agriculture And Forestry Sciences | Preparation method of lycium ruthenicum murr spray powder capsule |
-
2020
- 2020-09-08 CN CN202010934055.5A patent/CN111920722A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101040713A (en) * | 2007-04-27 | 2007-09-26 | 乔泓程 | Health-care food having functions of oxidation resisting and immunity improving |
| CN102659741A (en) * | 2012-04-27 | 2012-09-12 | 宁夏大学 | Method for extracting and preparing active ingredients of Ningxia wolfberries |
| CN102824473A (en) * | 2012-09-17 | 2012-12-19 | 青海红鼎生物工程有限公司 | Lycium ruthenicum murr total flavonoid extract and preparation method thereof |
| CN107440981A (en) * | 2017-09-27 | 2017-12-08 | 海南利南生物科技有限公司 | A kind of matrimony vine facial mask and preparation method thereof |
| AU2020101467A4 (en) * | 2020-07-24 | 2020-08-27 | Institute Of Wolfberry Engineering Technology, Ningxia Academy Of Agriculture And Forestry Sciences | Preparation method of lycium ruthenicum murr spray powder capsule |
Non-Patent Citations (1)
| Title |
|---|
| 贡长生编: "《现代工业化学概论》", 湖北科学技术出版社 * |
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Application publication date: 20201113 |