CN111855622B - Method for detecting ultraviolet resistance of textile - Google Patents

Method for detecting ultraviolet resistance of textile Download PDF

Info

Publication number
CN111855622B
CN111855622B CN202010784357.9A CN202010784357A CN111855622B CN 111855622 B CN111855622 B CN 111855622B CN 202010784357 A CN202010784357 A CN 202010784357A CN 111855622 B CN111855622 B CN 111855622B
Authority
CN
China
Prior art keywords
textile
ultraviolet
sample
textile sample
detecting
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN202010784357.9A
Other languages
Chinese (zh)
Other versions
CN111855622A (en
Inventor
杨荣静
何秀玲
吕晶
温馨
段冀渊
严波
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hongkou Customs Of People's Republic Of China
Shanghai Customs Mechanical And Electrical Products Testing Technology Center
Original Assignee
Hongkou Customs Of People's Republic Of China
Shanghai Customs Mechanical And Electrical Products Testing Technology Center
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hongkou Customs Of People's Republic Of China, Shanghai Customs Mechanical And Electrical Products Testing Technology Center filed Critical Hongkou Customs Of People's Republic Of China
Priority to CN202010784357.9A priority Critical patent/CN111855622B/en
Publication of CN111855622A publication Critical patent/CN111855622A/en
Application granted granted Critical
Publication of CN111855622B publication Critical patent/CN111855622B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/59Transmissivity
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/04Water-soluble compounds
    • C11D3/044Hydroxides or bases
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/37Polymers
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/39Organic or inorganic per-compounds
    • C11D3/3942Inorganic per-compounds
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/34Purifying; Cleaning
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/44Sample treatment involving radiation, e.g. heat

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Organic Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Analytical Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Molecular Biology (AREA)
  • Biomedical Technology (AREA)
  • Testing Resistance To Weather, Investigating Materials By Mechanical Methods (AREA)
  • Photometry And Measurement Of Optical Pulse Characteristics (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)

Abstract

The invention belongs to the technical field of material detection, and discloses a method for detecting ultraviolet resistance of a textile, which comprises the following steps: the textile is tiled after being treated, and detection is waited for; setting three broadband filters, and setting ultraviolet bands corresponding to the broadband filters; carrying out ultraviolet transmission test under static state and ultraviolet transmission test under dynamic state on the treated textile sample, and measuring respective transmittance of three ultraviolet bands to the textile sample by using a photoelectric detector; and respectively obtaining the transmittance of the textile sample under the static state and the dynamic state to be detected, and comprehensively comparing to obtain a comparison result and obtain the ultraviolet resistance of the textile. According to the method, the transmissivity is obtained through the light spot change, and further the ultraviolet resistance of the textile is determined; the measuring method is simple and convenient to implement, has small requirements on measuring environment, can reduce measuring cost, and has good measuring accuracy.

Description

Method for detecting ultraviolet resistance of textile
Technical Field
The invention belongs to the technical field of material detection, and particularly relates to a method for detecting ultraviolet resistance of textiles.
Background
At present, the ultraviolet region in sunlight can be divided into three sections, and the region with the wavelength of 400-320 nm is called UV-A; the wavelength of 320-280 nm is called UV-B; the wavelength range of 280-200 nm is called UV-C. The UV-C wavelength is short and has been absorbed in air and cannot reach the earth's surface. Ultraviolet light accounts for about 6% of sunlight, with Sup>A greater proportion of UV-A and Sup>A lesser proportion of UV-B. UV-Sup>A penetrates under the epidermal tissue, causing the muscles to lose elasticity, the skin to be rough, and wrinkles to be formed. UV-B has the problem of causing skin cancer. Therefore, the ultraviolet-proof textile has a wide market. In the prior art, the detection technology of the ultraviolet resistance of the textile is not completely mature, the operation for detecting the ultraviolet resistance of the textile is complex, and the detection accuracy is poor.
Through the above analysis, the problems and defects existing in the prior art are as follows: in the prior art, the detection technology of the ultraviolet resistance of the textile is not completely mature, the operation for detecting the ultraviolet resistance of the textile is complex, and the detection accuracy is poor.
Disclosure of Invention
Aiming at the problems existing in the prior art, the invention provides a method for detecting the ultraviolet resistance of textiles.
The invention is realized in such a way that the method for detecting the ultraviolet resistance of the textile comprises the following steps:
firstly, adding water, a clothes detergent and a treatment auxiliary agent into the purchased textile to be tested at the temperature of 35-40 ℃, heating to 80 ℃, preserving heat for 55-60 min, cooling to below 70 ℃ for washing, overflowing for 5-7 min, and draining.
Step two, neutralizing and washing the textile; under the condition of 25-30 ℃, water is fed, acetic acid HAC is added for neutralization, the temperature is raised to 55-60 ℃, the temperature is kept for 15-20 min, water is discharged, then water is fed again, deoxidizing enzyme is added, water is discharged after 15-20 min, water is fed, and washing is performed.
Naturally airing the washed textile, and insolating for 2-3 hours in the sun; and (3) using a dust collector to collect dust on the surface of the dried textile, and removing surface impurities and floating hair.
And fourthly, trimming the textile into a square with the length of 20 multiplied by 20cm to obtain a treated textile sample, and tiling the treated textile sample to wait for detection.
And fifthly, selecting a light source close to solar spectrum distribution as a light source for ultraviolet transmission test, adhering the adhesive tape on a quartz substrate, coating the textile to be tested on the adhesive tape, transferring the textile to be tested to a drying oven for constant temperature, and then performing simulated sunlight irradiation on the textile sample to be tested, wherein the adhesive tape is transparent ventilation medical adhesive tape.
And step six, carrying out diffuse reflection spectrum test on the irradiated sample by adopting a UV integrating sphere accessory.
And seventhly, setting three broadband filters, wherein the transmission peak wavelengths of the three broadband filters are 254nm, 297nm and 315nm respectively.
And step eight, corresponding to the broadband filters, three ultraviolet bands of the corresponding ultraviolet radiation area are obtained by using the three different broadband filters, and the three ultraviolet bands are respectively 200-280 nm, 280-320 nm and 320-400 nm.
Step nine, carrying out ultraviolet transmission test on the treated textile sample under static state, and respectively irradiating the three obtained ultraviolet bands on the textile sample clung to the broadband filter plate in a form of face element light spots;
step ten, corresponding data with ultraviolet light wave bands of 280-400 nm are counted, diffuse reflection values of the ultraviolet light wave bands of 320-400 nm and the diffuse reflection values of the ultraviolet light wave bands of 290-320 nm are calculated respectively, and the respective transmittance of three ultraviolet wave bands to a textile sample under static state is measured through a photoelectric detector;
step eleven, respectively irradiating the three ultraviolet bands obtained in the step eight onto a textile sample clung to the broadband filter plate in a form of a face element light spot, and moving a light source;
step twelve, recording the moving path of the surface element light spot of the textile sample and the path and area of the surface element light spot passing through the textile sample; analyzing the record through a photoelectric detector to obtain the change condition of the face unit facula and the respective transmittance of three ultraviolet bands to the textile sample under dynamic state;
thirteenth, respectively obtaining the transmissivity of the textile sample under the static state detected in the ninth step and the transmissivity of the textile sample under the dynamic state detected in the eleventh step, and comprehensively comparing to obtain a comparison result;
fourteen, obtaining the comprehensive transmittance of the textile sample through the ultraviolet transmission test result of the textile sample under static and dynamic conditions; the lower the combined transmittance, the higher the uv blocking performance of the textile sample.
In the first step, the clothes washing agent consists of 6-9 parts of deionized water, 3-5 parts of a polymer system and 1-2 parts of a surfactant according to parts by weight.
Further, the polymer system includes a polyethylene glycol polymer and an ethoxylated polyethyleneimine polymer; the mass ratio of the polyethylene glycol polymer to the ethoxylated polyethyleneimine polymer is 1:2-3.
Further, the preparation method of the laundry detergent comprises the following steps:
(1) Adding a polymer system into deionized water, and fully stirring to obtain a mixture A;
(2) Adding a surfactant into deionized water, and uniformly stirring to obtain a mixture B;
(3) Mixing the mixture A and the mixture B, and transferring the mixture A and the mixture B into a stirrer for stirring;
(3) Starting a stirrer, setting the rotating speed to be 50-65 r/min, and stirring for 20-25 min to obtain a clothes detergent premix;
(4) And (3) performing ultrasonic dispersion on the clothes detergent premix, wherein the ultrasonic frequency is 30-50 kHz, and the ultrasonic time is 6-10 min, so as to obtain the clothes detergent.
In the first step, the treatment auxiliary agent consists of hydrogen peroxide, caustic soda flakes and a hydrogen peroxide activator, wherein the hydrogen peroxide in the treatment auxiliary agent is 3-5 g/l, the caustic soda flakes is 1-1.5 g/l, and the hydrogen peroxide activator is 2-3 g/l.
In the fifth step, the light source spectrum accords with the natural sunlight spectrum, the temperature of the surface of the sample is controlled to be 37 ℃, and the sample is respectively irradiated for 0 h, 0.5h, 1h, 2h, 3h and 4h.
Further, in step nine, the diameter of the face spot is 10mm.
In a tenth step, the photodetector is specifically a QE quantum light spot detector.
It is another object of the present invention to provide a computer program product stored on a computer readable medium, comprising a computer readable program for providing a user input interface for implementing the method of detecting the anti-uv performance of a textile product when executed on an electronic device.
It is another object of the present invention to provide a computer readable storage medium storing instructions that, when executed on a computer, cause the computer to perform the method for detecting the anti-uv performance of a textile.
By combining all the technical schemes, the invention has the advantages and positive effects that: according to the invention, the textile is cleaned and dried before the ultraviolet resistance of the textile is measured, so that the textile can be cleaned, the actual state of the textile after being worn and washed for multiple times is simulated, and the obtained structure of the ultraviolet resistance is more accurate; the transmissivity is obtained through the light spot change, and further, the ultraviolet resistance of the textile is determined, and the detection method is simpler and more convenient and can accurately display the ultraviolet resistance of the textile; by comprehensively analyzing the test results through static and dynamic ultraviolet resistance tests, the accuracy of the measurement results of the ultraviolet resistance of the textile can be improved. The method is simple and convenient to implement, has small requirements on the measuring environment, can reduce the measuring cost, and has good measuring accuracy.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present application, the following description will briefly explain the drawings needed in the embodiments of the present application, and it is obvious that the drawings described below are only some embodiments of the present application, and that other drawings can be obtained according to these drawings without inventive effort for a person skilled in the art.
Fig. 1 is a flowchart of a method for detecting ultraviolet resistance of a textile according to an embodiment of the present invention.
Fig. 2 is a flow chart of a method for treating a textile to obtain a treated textile sample according to an embodiment of the present invention.
Fig. 3 is a flowchart of a method for preparing a laundry detergent according to an embodiment of the present invention.
Fig. 4 is a flow chart of a method for performing ultraviolet transmission testing in a static state on a treated textile sample in accordance with an embodiment of the present invention.
Fig. 5 is a flow chart of a method for performing ultraviolet transmission testing in a static state on a treated textile sample in accordance with an embodiment of the present invention.
Detailed Description
The present invention will be described in further detail with reference to the following examples in order to make the objects, technical solutions and advantages of the present invention more apparent. It should be understood that the specific embodiments described herein are for purposes of illustration only and are not intended to limit the scope of the invention.
Aiming at the problems existing in the prior art, the invention provides a method for detecting the ultraviolet resistance of textiles, and the invention is described in detail below with reference to the accompanying drawings.
As shown in fig. 1, the method for detecting the ultraviolet resistance of the textile according to the embodiment of the invention comprises the following steps:
s101, treating the textile to obtain a treated textile sample, and tiling the treated textile sample for detection.
S102, setting three broadband filters, wherein the transmission peak wavelengths of the three broadband filters are 254nm, 297nm and 315nm respectively.
S103, corresponding to the broadband filter, setting ultraviolet bands, wherein the three ultraviolet bands are respectively 200-280 nm, 280-320 nm and 320-400 nm.
S104, carrying out ultraviolet transmission test on the treated textile sample under static state, and measuring the respective transmittance of three ultraviolet bands on the textile sample by using a photoelectric detector.
S105, carrying out ultraviolet transmission test on the treated textile sample under dynamic state, and measuring the respective transmittance of three ultraviolet bands on the textile sample through a photoelectric detector.
S106, respectively obtaining the transmittance of the textile sample under the static state detected in the step S104 and the transmittance of the textile sample under the dynamic state detected in the step S105, and comprehensively comparing to obtain a comparison result.
S107, obtaining the ultraviolet resistance of the textile by analyzing the comparison result.
As shown in fig. 2, in step S101 provided in the embodiment of the present invention, a method for treating a textile to obtain a treated textile sample includes the following steps:
s201, adding water, a clothes detergent and a treatment auxiliary agent into the purchased textile to be tested at the temperature of 35-40 ℃, heating to 80 ℃, preserving heat for 55-60 min, cooling to below 70 ℃ for washing, overflowing for 5-7 min, and draining.
S202, neutralizing and washing textiles; under the condition of 25-30 ℃, water is fed, acetic acid HAC is added for neutralization, the temperature is raised to 55-60 ℃, the temperature is kept for 15-20 min, water is discharged, then water is fed again, deoxidizing enzyme is added, water is discharged after 15-20 min, water is fed, and washing is performed.
S203, naturally airing the washed textile, and insolating for 2-3 hours in the sun; and (3) using a dust collector to collect dust on the surface of the dried textile, and removing surface impurities and floating hair.
S204, trimming the textile into a square with the length of 20 multiplied by 20cm to obtain a treated textile sample, and tiling the treated textile sample to wait for detection.
In the step S101 provided by the embodiment of the invention, the treatment auxiliary agent consists of hydrogen peroxide, caustic soda flakes and a hydrogen peroxide activator, wherein the hydrogen peroxide in the treatment auxiliary agent is 3-5 g/l, the caustic soda flakes is 1-1.5 g/l, and the hydrogen peroxide activator is 2-3 g/l.
In the step S101 provided by the embodiment of the invention, the clothes washing agent consists of 6-9 parts of deionized water, 3-5 parts of a polymer system and 1-2 parts of a surfactant according to parts by weight.
The polymer system provided by the embodiment of the invention comprises a polyethylene glycol polymer and an ethoxylated polyethyleneimine polymer; the mass ratio of the polyethylene glycol polymer to the ethoxylated polyethyleneimine polymer is 1:2-3.
As shown in fig. 3, the method for preparing the laundry detergent provided by the embodiment of the invention comprises the following steps:
and S301, adding a polymer system into deionized water, and fully stirring to obtain a mixture A.
S302, adding a surfactant into deionized water, and uniformly stirring to obtain a mixture B.
And S303, mixing the mixture A and the mixture B, and transferring the mixture A and the mixture B into a stirrer for stirring.
S304, starting the stirrer, setting the rotating speed to be 50r/min, and stirring to obtain the clothes detergent premix.
S305, performing ultrasonic dispersion on the clothes detergent premix, wherein the ultrasonic frequency is 30-50 kHz, and the ultrasonic time is 6-10 min, so as to obtain the clothes detergent.
As shown in fig. 4, in step S104 provided in the embodiment of the present invention, the method for performing ultraviolet transmission test on the treated textile sample under static state includes the following steps:
s401, selecting a light source, selecting the light source close to solar spectrum distribution as the light source for ultraviolet transmission test, and performing simulated sunlight irradiation on the textile sample to be tested.
S402, for the irradiated sample, performing diffuse reflection spectrum test by adopting a UV integrating sphere accessory.
S403, setting three broadband filters, wherein the transmission peak wavelengths of the three broadband filters are 254nm, 297nm and 315nm respectively.
S404, corresponding to the broadband filters, three ultraviolet bands of the corresponding ultraviolet radiation region are obtained by using the three different broadband filters, and the three ultraviolet bands are respectively 200-280 nm, 280-320 nm and 320-400 nm.
S405, carrying out ultraviolet transmission test on the treated textile sample under static state, and respectively irradiating the three obtained ultraviolet bands on the textile sample which is tightly attached to the broadband filter in the form of face element light spots.
S406, corresponding data with ultraviolet light wave bands of 280-400 nm are counted, and diffuse reflection values of 320-400 nm and 290-320 nm of the ultraviolet light wave bands are calculated respectively.
And S407, measuring the respective transmittance of the textile sample in the static state by three ultraviolet bands through a photoelectric detector, and recording the surface element light spots passing through the textile sample.
In the step S401 provided by the embodiment of the invention, the light source spectrum accords with the natural sunlight spectrum, the temperature of the surface of the sample is controlled to be 37 ℃, and the sample is respectively irradiated for 0 h, 0.5h, 1h, 2h, 3h and 4h.
In step S405 provided in the embodiment of the present invention, the diameter of the binning light spot is 10mm.
As shown in fig. 5, in step S105 provided in the embodiment of the present invention, a method for performing ultraviolet transmission test on a processed textile sample under static state includes:
s501, selecting a light source, and selecting the light source close to solar spectrum distribution as the light source for ultraviolet transmission test.
S502, three ultraviolet bands of the corresponding ultraviolet radiation areas are obtained by using the three different broadband filters.
And S503, respectively irradiating the three obtained ultraviolet bands on the textile sample clung to the broadband filter plate in the form of a face element light spot, and moving the light source.
S504, the moving path of the surface element light spot of the textile sample and the path and area of the surface element light spot passing through the textile sample are recorded.
S505, analysis of the record is provided, and the change condition of the face unit light spot is obtained.
In step S105 provided by the embodiment of the present invention, the photodetector is specifically a QE quantum light spot detector.
In step S105 provided in the embodiment of the present invention, the method for obtaining the ultraviolet protection performance of the textile by analyzing the comparison result specifically includes: obtaining the comprehensive transmittance of the textile sample through the ultraviolet transmission test results of the textile sample under static and dynamic conditions; the lower the combined transmittance, the higher the uv blocking performance of the textile sample.
In the above embodiments, it may be implemented in whole or in part by software, hardware, firmware, or any combination thereof. When used in whole or in part, is implemented in the form of a computer program product comprising one or more computer instructions. When loaded or executed on a computer, produces a flow or function in accordance with embodiments of the present invention, in whole or in part. The computer may be a general purpose computer, a special purpose computer, a computer network, or other programmable apparatus. The computer instructions may be stored in a computer-readable storage medium or transmitted from one computer-readable storage medium to another computer-readable storage medium, for example, the computer instructions may be transmitted from one website, computer, server, or data center to another website, computer, server, or data center by a wired (e.g., coaxial cable, fiber optic, digital Subscriber Line (DSL), or wireless (e.g., infrared, wireless, microwave, etc.) means. The computer readable storage medium may be any available medium that can be accessed by a computer or a data storage device such as a server, data center, etc. that contains an integration of one or more available media. The usable medium may be a magnetic medium (e.g., floppy Disk, hard Disk, magnetic tape), an optical medium (e.g., DVD), or a semiconductor medium (e.g., solid State Disk (SSD)), etc.
While the invention has been described with respect to what is presently considered to be the most practical and preferred embodiments, it is to be understood that the invention is not limited to the disclosed embodiments, but on the contrary, is intended to cover various modifications, equivalents, and alternatives falling within the spirit and scope of the invention.

Claims (9)

1. The method for detecting the ultraviolet resistance of the textile is characterized by comprising the following steps of:
firstly, adding water, a clothes detergent and a treatment auxiliary agent into the purchased textile to be tested at the temperature of 35-40 ℃, heating to 80 ℃, preserving heat for 55-60 min, cooling to below 70 ℃ for washing, overflowing for 5-7 min, and draining;
step two, neutralizing and washing the textile; adding water at 25-30 ℃, adding acetic acid HAC for neutralization, heating to 55-60 ℃, preserving heat for 15-20 min, draining water, adding deoxidizing enzyme, draining water after 15-20 min, adding water, and washing;
naturally airing the washed textile, and insolating for 2-3 hours in the sun; dust is collected on the surface of the dried textile by using a dust collector, and surface impurities and floating hair are removed;
fourthly, trimming the textile into a square with the length of 20 multiplied by 20cm to obtain a treated textile sample, tiling the treated textile sample, and waiting for detection;
selecting a light source close to solar spectrum distribution as a light source for ultraviolet transmission test, adhering an adhesive tape on a quartz substrate, coating a textile to be tested on the adhesive tape, transferring the textile to be tested to a drying oven for constant temperature, and then performing simulated sunlight irradiation on a textile sample to be tested, wherein the adhesive tape is a transparent ventilation medical adhesive tape;
step six, for the irradiated sample, firstly adopting a UV integrating sphere accessory to perform diffuse reflection spectrum test;
step seven, three broadband filters are set, and the transmission peak wavelengths of the three broadband filters are 254nm, 297nm and 315nm respectively;
step eight, corresponding to the broadband filters, three ultraviolet bands of the corresponding ultraviolet radiation area are obtained by using the three different broadband filters, and the three ultraviolet bands are respectively 200-280 nm, 280-320 nm and 320-400 nm;
step nine, carrying out ultraviolet transmission test on the treated textile sample under static state, and respectively irradiating the three obtained ultraviolet bands on the textile sample clung to the broadband filter plate in a form of face element light spots;
step ten, corresponding data with ultraviolet light wave bands of 280-400 nm are counted, diffuse reflection values of the ultraviolet light wave bands of 320-400 nm and the diffuse reflection values of the ultraviolet light wave bands of 290-320 nm are calculated respectively, and the respective transmittance of three ultraviolet wave bands to a textile sample under static state is measured through a photoelectric detector;
step eleven, respectively irradiating the three ultraviolet bands obtained in the step eight onto a textile sample clung to the broadband filter plate in a form of a face element light spot, and moving a light source;
step twelve, recording the moving path of the surface element light spot of the textile sample and the path and area of the surface element light spot passing through the textile sample; analyzing the record through a photoelectric detector to obtain the change condition of the face unit facula and the respective transmittance of three ultraviolet bands to the textile sample under dynamic state;
thirteenth, respectively obtaining the transmissivity of the textile sample under the static state detected in the ninth step and the transmissivity of the textile sample under the dynamic state detected in the eleventh step, and comprehensively comparing to obtain a comparison result;
fourteen, obtaining the comprehensive transmittance of the textile sample through the ultraviolet transmission test result of the textile sample under static and dynamic conditions; the lower the overall transmittance, the higher the uv blocking performance of the textile sample;
in the first step, the clothes washing agent consists of 6-9 parts of deionized water, 3-5 parts of a polymer system and 1-2 parts of a surfactant according to parts by weight.
2. The method for detecting the anti-ultraviolet performance of a textile according to claim 1, wherein the polymer system comprises a polyethylene glycol polymer and an ethoxylated polyethyleneimine polymer; the mass ratio of the polyethylene glycol polymer to the ethoxylated polyethyleneimine polymer is 1:2-3.
3. The method for detecting ultraviolet resistance of textiles according to claim 1, wherein the method for preparing the laundry detergent comprises the following steps:
(1) Adding a polymer system into deionized water, and fully stirring to obtain a mixture A;
(2) Adding a surfactant into deionized water, and uniformly stirring to obtain a mixture B;
(3) Mixing the mixture A and the mixture B, and transferring the mixture A and the mixture B into a stirrer for stirring;
(3) Starting a stirrer, setting the rotating speed to be 50-65 r/min, and stirring for 20-25 min to obtain a clothes detergent premix;
(4) And (3) performing ultrasonic dispersion on the clothes detergent premix, wherein the ultrasonic frequency is 30-50 kHz, and the ultrasonic time is 6-10 min, so as to obtain the clothes detergent.
4. The method for detecting the ultraviolet resistance of the textile according to claim 1, wherein in the first step, the treatment auxiliary agent consists of hydrogen peroxide, caustic soda flakes and a hydrogen peroxide activator, wherein the hydrogen peroxide in the treatment auxiliary agent is 3-5 g/l, the caustic soda flakes is 1-1.5 g/l, and the hydrogen peroxide activator is 2-3 g/l.
5. The method for detecting ultraviolet resistance of textiles according to claim 1, wherein in the fifth step, the light source spectrum accords with the natural sunlight spectrum, the temperature of the surface of the sample is controlled to be 37 ℃, and the sample is irradiated for 0, 0.5h, 1h, 2h, 3h and 4h respectively.
6. The method for detecting ultraviolet resistance of textiles according to claim 1, wherein in step nine, the diameter of said face spot is 10mm.
7. The method for detecting ultraviolet resistance of textiles according to claim 1, wherein in the step ten, the photodetector is specifically a QE quantum light spot detector.
8. A computer program product stored on a computer readable medium, comprising a computer readable program for providing a user input interface for implementing a method of detecting anti-uv performance of a textile product according to any one of claims 1 to 7 when executed on an electronic device.
9. A computer readable storage medium storing instructions that when run on a computer cause the computer to perform the method of detecting the anti-uv performance of a textile product according to any one of claims 1 to 7.
CN202010784357.9A 2020-08-06 2020-08-06 Method for detecting ultraviolet resistance of textile Active CN111855622B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202010784357.9A CN111855622B (en) 2020-08-06 2020-08-06 Method for detecting ultraviolet resistance of textile

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202010784357.9A CN111855622B (en) 2020-08-06 2020-08-06 Method for detecting ultraviolet resistance of textile

Publications (2)

Publication Number Publication Date
CN111855622A CN111855622A (en) 2020-10-30
CN111855622B true CN111855622B (en) 2023-05-16

Family

ID=72972608

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202010784357.9A Active CN111855622B (en) 2020-08-06 2020-08-06 Method for detecting ultraviolet resistance of textile

Country Status (1)

Country Link
CN (1) CN111855622B (en)

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1442902A (en) * 1973-05-21 1976-07-14 Deering Milliken Res Corp Method of detecting defects and composition therefor
CN1385689A (en) * 2001-05-15 2002-12-18 华南师范大学 Method for testing ultraviolet resistance of fabric
CN105421018A (en) * 2015-11-30 2016-03-23 宁波广源纺织品有限公司 Dyeing pre-treatment energy-saving method of cotton textiles
CN110186876A (en) * 2019-05-29 2019-08-30 广西柳州慧蓝科技有限公司 A kind of textile UV resistance method for testing performance
CN209471049U (en) * 2018-12-24 2019-10-08 苏州强合智能制造有限公司 A kind of ultraviolet resistance of fabric automatic testing equipment

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5006958B2 (en) * 2010-09-17 2012-08-22 株式会社 資生堂 Ultraviolet ray protection effect evaluation method, evaluation apparatus, evaluation program, and recording medium on which the program is recorded

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1442902A (en) * 1973-05-21 1976-07-14 Deering Milliken Res Corp Method of detecting defects and composition therefor
CN1385689A (en) * 2001-05-15 2002-12-18 华南师范大学 Method for testing ultraviolet resistance of fabric
CN105421018A (en) * 2015-11-30 2016-03-23 宁波广源纺织品有限公司 Dyeing pre-treatment energy-saving method of cotton textiles
CN209471049U (en) * 2018-12-24 2019-10-08 苏州强合智能制造有限公司 A kind of ultraviolet resistance of fabric automatic testing equipment
CN110186876A (en) * 2019-05-29 2019-08-30 广西柳州慧蓝科技有限公司 A kind of textile UV resistance method for testing performance

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
乌拉草纤维素纳米晶的制备及其对棉织物抗紫外线功能整理;杨雪等;《毛纺科技》;20200516(第05期);全文 *
周启澄等.植物源防紫外线整理剂的制备.《中国传统植物染料现代研发与生态纺织技术》.2015,第142-144页. *

Also Published As

Publication number Publication date
CN111855622A (en) 2020-10-30

Similar Documents

Publication Publication Date Title
Pan et al. Towards understanding KOH conditioning of amidoxime-based polymer adsorbents for sequestering uranium from seawater
CN110004717B (en) Multifunctional polyester fabric and preparation method thereof
Hou et al. Preparation and UV-protective properties of functional cellulose fabrics based on reactive azobenzene Schiff base derivative
CN111855622B (en) Method for detecting ultraviolet resistance of textile
Periolatto et al. Low temperature dyeing of wool fabric by acid dye after UV irradiation
CN104531039A (en) Preparation method of polyurethane pressure-sensitive adhesive composition and polyurethane protective film
CN103528998B (en) Coated photovoltaic glass light transmittance detection method
JP2008111834A (en) Method and device for evaluating ultraviolet radiation protective effect
CN106381680A (en) Method for scouring and bleaching cotton fabric in gaseous phase by utilizing ozone
Iqbal et al. Effect of the factors affecting high-performance p-aramid fibre dyeing and their optimization
CN111721710A (en) Method for calibrating silicon nanowire sensor by light
CN116147764A (en) Device and method for calibrating illuminance and testing sensitivity
CN102590101A (en) Method for detecting photocatalytic capacity of ultraviolet photocatalytic material
CN103744141A (en) Polyvinyl alcohol polarizing membrane and preparation method thereof
Xia et al. A new method for measuring cross-link density in ethylene vinyl acetate-based encapsulant
CN116249361A (en) Manufacturing method of X-ray detector
Gawęda et al. Surface and in-depth structural changes in nuclear graphite irradiated with noble gases described with Raman imaging
Piccolo et al. Combined radiation and temperature effects on Brillouin scattering based sensing with ge-doped optical fibers
Bedolla et al. Oxidation of ultralene and paraffin due to radiation damage after exposure to soft X-rays probed by FTIR microspectroscopy and X-ray fluorescence
DE102015200648A1 (en) Method for determining the degree of crosslinking of a polyethylene compound
CN112557287A (en) Anti-ultraviolet research method for knitted single jersey nano zinc oxide sol
CN112300719A (en) Masking tape
Bait et al. Synthesis, characterization, and dyeing performance of UV protective mono azo acid dyes based on 4-hydroxybenzophenone
CN110312924A (en) Aridity sensor
Sharma et al. Development of a quantitative assessment method for self cleaning by photocatalytic degradation of stains on cotton

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant