CN111714674B - 一种中药挥发油及其制备方法和应用 - Google Patents
一种中药挥发油及其制备方法和应用 Download PDFInfo
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Abstract
本发明属于中药技术领域,具体公开了一种中药挥发油,由以下原料制成:丁香、白芷、薄荷、藿香、益智仁、砂仁、橘皮,生姜,具体中药挥发油由以下重量份的原料制成:丁香4‑16份,薄荷8‑18份,藿香6‑14份,橘皮2‑8份,白芷3‑9份,益智仁6‑12份,砂仁2‑6份,生姜4‑10份。本发明还公开了上述中药挥发油的制备方法及应用。本发明中药挥发油以纯天然的中草药为原料,将传统中医药理论与现代提取工艺技术紧密结合,科学配伍,绿色环保、无任何毒副作用,药效时间长,效果显著。本发明的中药挥发油制备简单,操作方便,制作成本低,无污染,本发明的中药挥发油制作成空气清新贴剂可适于各类人群使用,并在一定距离的范围内实施,不会引起他人对气味的敏感反应。
Description
技术领域
本发明属于中药技术领域,具体涉及一种中药挥发油及其制备方法和应用。
背景技术
空气清新剂是很多人都非常喜欢的,可以让一个区域的空气有很好闻的气味,但是空气清新剂最明显的缺陷是它含有的成分对人体可能带来的伤害。目前市场上销售的空气清新剂种类很多,但基本上都是由***、香精等成分组成,这些物质在空气中化学分解之后产生的气体某些成分本身就是空气污染物,这其实是加剧了的污染程度,长期使用对人体会产生不良刺激。
从中医的角度来说,芳香类中药,又可以化湿、醒脾、避秽、开窍。清新的气味,能够刺激神经***的兴奋,让人神清气爽,也能清除污浊的空气,美化环境。中药挥发油主要来源于芳香类中药,具有抗炎、抗过敏、抗微生物、抗突变和抗癌、驱虫作用、酶抑制作用、对中枢神经***的作用、对呼吸***的作用等。近年来,有关挥发油抗活性报道很多。将中药挥发油的抗菌效果与空气消毒紧密结合,研制成高效、低毒、使用方便挥散型空气清新剂,具有较大的市场开发前景。
发明内容
本发明所要解决的技术问题是提供一种中药挥发油,本发明还提供该中药挥发油的制备方法,该中药挥发油制作成空气清新贴剂后不仅可以长久保持气味,还对气味距离有一定限制。
为解决上述技术问题,本发明所采取的技术方案是:
一种中药挥发油,由以下原料制成:丁香、白芷、薄荷、藿香、益智仁、砂仁、橘皮,生姜。
优选的,上述中药挥发油由以下重量份的原料制成:丁香4-16份,薄荷8-18份,藿香6-14份,橘皮2-8份,白芷3-9份,益智仁6-12份,砂仁2-6份,生姜4-10份。
优选的,上述中药挥发油由以下重量份的原料制成:丁香4份,薄荷8份,藿香6份,橘皮2份,白芷3份,益智仁6份,砂仁2份,生姜4份。
本发明还提供中药挥发油的制备方法,包括以下步骤:
(1)、按配方量分别称取丁香,薄荷,藿香,益智仁,砂仁,橘皮,生姜,低温干燥,将丁香粉碎后和其余原料混匀后采用纯化水在室温下浸润0.5h,然后采用水蒸气蒸馏法进行挥发油提取,得到多味芳香中药的混合挥发油;
(2)、按配方量称取白芷,低温干燥,然后采用乙醇回流提取多次,过滤,合并滤液,得到白芷乙醇提取液,备用;
(3)、将步骤(2)得到的混合挥发油与步骤(3)得到的白芷乙醇提取液按一定比例混合均匀加入玉米油缓释剂,混合挥发油:白芷乙醇提取液:玉米油的比例为1-2:9-18:20-30,即得中药挥发油。
优选的,步骤(1)中,采用水蒸气蒸馏法提取的条件为90-100℃下提取6h。
优选的,步骤(1)和步骤(2)中低温干燥温度为30-50℃。
优选的,步骤(2)中,采用体积分数为70%-95%的乙醇回流提取2-4次,每次1-3小时。
优选的,步骤(3)中,混合挥发油:白芷乙醇提取液:玉米油的体积比为1-2:9-18:20-30。
本发明还保护上述中药挥发油在制备空气清新剂中的用途。
优选的,上述用途,将中药挥发油的制备方法中步骤(3)得到的纯中药混合挥发油喷晒在具有网格状的粘性贴纸上,制作成空气清新贴剂。
生物医学研究表明本发明所选用的几种组分具有如下功效:
薄荷,辛,凉。归肺、肝经。具有疏散风热,清利头目,利咽透疹,疏肝行气的功效。本品轻扬升浮,芳香通窍,清头目。本品主含挥发油,油中主要成分为薄荷醇、薄荷酮、异薄荷酮、薄荷脑、薄荷酯等芳香成分。本品芳香辟秽,对于改善空气质量,清新空气具有重要作用。
藿香,辛,微温。归脾、胃、肺经。具有化湿,止呕,解暑的功效。研究发现藿香含挥发油2.3%,油中主要成分为广藿香醇,另外还有丁香油酚、桂皮醛等芳香成分。本品气味芳香,具有芳香解暑之功,为芳香化湿浊要药。
艾叶,辛、苦,温。归肝、脾、肾经。温经止血,散寒调经,安胎。本品含大量挥发油,因此具有特殊的馨香味。体外实验证明,艾叶油对多肺炎球菌,甲、乙溶血型链球菌、奈瑟氏球菌有抑制作用。因此,艾叶具有可以驱蚊蝇、灭菌消毒,预防疾病等功效。
白芷,辛,温。归肺、胃、大肠经。具有解表散寒,祛风止痛,通鼻窍,燥湿止带,消肿排脓等功效。白芷水煎液对大肠杆菌、痢疾杆菌、伤寒杆菌、绿脓杆菌有一定的抑制作用。
丁香,性辛,温。归脾,胃,肺,肾经。具有温中降逆、补肾助阳的功效,用于脾胃虚寒,呃逆呕吐,食少吐泻,心腹冷痛,肾虚阳痿。丁香挥发油是丁香的主要化学成分,丁香酚是有很强的抗菌、抗真菌效果,丁香挥发油对黑曲霉、白色念珠菌、枯草芽孢杆菌的抑菌作用最强,青霉菌的抑菌作用次之。
益智仁,性辛,温。归脾、肾经。具有暖肾固精缩尿,温脾止泻摄唾。用于肾虚遗尿,小便频数,遗精白浊,脾寒泄泻,腹中寒冷。益智仁挥发油中含量较高的有香橙烯、芳樟醇、圆柚酮等。临床实验表明益智仁挥发油对大肠杆菌、金黄色葡萄球菌和绿脓杆菌均有明显的抑制作用。
砂仁,性辛,温。归脾、胃、肾经。缩砂种子含挥发油1.7~3%,主要成分为d-樟脑,一种萜烯(似柠檬烯,但非柠檬烯),d-龙脑,乙酸龙脑酯,芳樟醇,橙花叔醇。
生姜,生姜味辛,性微温。归肺、脾、胃经。具有解表散寒、温中止呕、温肺止咳、解毒的功效,含姜醇、α-姜烯、β-水芹烯、柠檬醛、芳香醇、甲基庚烯酮、壬醛、α-龙脑等,尚含辣味成分姜辣素。
橘皮,性辛,温。归肺、肝、脾、胃四经。其挥发油主要为柠檬烯,具有抑制葡萄球菌、卡他奈氏菌、溶血性嗜血杆菌的生长。
与现有技术相比,本发明的有益效果在于:
本发明除了按照传统中药除四气五味外,还根据芳香药性,将其分为芳香解表、芳香化湿、芳香温里、芳香理气以及芳香开窍药。选取纯天然芳香中药为原料,进行科学配伍。其中,以薄荷为芳香解表药,具解表透析邪;丁香为芳香温理药,具有温通经脉、缓急止痛;益智仁、艾叶、白芷具有抑菌、杀灭病毒等作用。其余为芳香化湿药,具有舒畅气机,宣化湿浊;上述诸药协同作用,共同起清新空气,提神醒脑,芳香化浊等作用。
本发明中药挥发油以纯天然的中草药为原料,将传统中医药理论与现代提取工艺技术紧密结合,科学配伍,绿色环保、无任何毒副作用,药效时间长,效果显著,制作成空气清新贴剂后,不仅可以清新空气,而且还可提神醒脑,增加人体免疫力等作用。本发明的中药挥发油制备简单,操作方便,制作成本低,无污染,本发明的中药挥发油制作成空气清新贴剂可适于各类人群使用,并在一定距离的范围内实施,不会引起他人对气味的敏感反应。
附图说明
图1为本发明纯中药挥发油空气清新贴的除臭效果作用曲线;
图2为本发明纯中药挥发油空气清新贴的除菌效果作用曲线。
具体实施方式
为了使本领域技术人员更好地理解本发明的技术方案能予以实施,下面结合具体实施例对本发明作进一步说明,但不应理解为本发明的限制。下面实例中未注明具体条件的实验方法,均按照本领域的常规方法和条件进行。
实施例1
一种中药挥发油,由以下重量份原料制成:
丁香4份,薄荷8份,藿香6份,橘皮2份,白芷3份,益智仁6份,砂仁2份,生姜4份。
所述的制备方法包括以下步骤:
制备时,分别称取丁香、薄荷、藿香、益智仁、砂仁、橘皮,生姜,35℃低温干燥,将丁香粉碎后和其余原料混匀后采用纯化水在室温下浸润0.5h,然后采用水蒸气蒸馏法进行挥发油提取,得到多味芳香中药的混合挥发油:再按配方量称取白芷,低温干燥,然后采用75%乙醇按照白芷和75%乙醇的质量体积比为1毫克:5毫升回流提取2次,每次2h,过滤,合并滤液,得到白芷乙醇提取液,备用。混合挥发油与白芷乙醇提取液加入玉米油缓释剂按体积比为1:9:20混合均匀,即得中药挥发油。将中药挥发油,喷涂到具有网格状的粘性贴纸上,即得本产品。
实施例2
一种中药挥发油,由以下重量份原料制成:
丁香6份,薄荷8份,藿香8份,橘皮4份,白芷6份,益智仁6份,砂仁2份,生姜6份。
所述的制备方法包括以下步骤:
制备时,分别称取丁香、薄荷、藿香、益智仁、砂仁、橘皮,生姜,40℃低温干燥,将丁香粉碎后和其余原料混匀后采用纯化水在室温下浸润0.5h,然后采用水蒸气蒸馏法进行挥发油提取,得到多味芳香中药的混合挥发油:再按配方量称取白芷,低温干燥,然后采用85%乙醇按照白芷和85%乙醇的质量体积比为1毫克:5毫升回流提取2次,每次2h,过滤,合并滤液,得到白芷乙醇提取液,备用。混合挥发油与白芷乙醇提取液加入玉米油缓释剂按体积比为1:10:25混合均匀,即得中药挥发油。将中药挥发油,喷涂到具有网格状的粘性贴纸上,即得产品。
实施例3
一种局部释放纯中药挥发油的空气清新贴剂,由以下重量份原料制成:
丁香8份,薄荷12份,藿香10份,橘皮4份,白芷5份,益智仁6份,砂仁2份,生姜6份。
所述的制备方法包括以下步骤:
制备时,首先分别取丁香、薄荷、藿香、益智仁、砂仁、橘皮,生姜,45℃低温干燥,将丁香粉碎后和其余原料混匀后采用纯化水在室温下浸润0.5h,然后采用水蒸气蒸馏法进行挥发油提取,得到多味芳香中药的混合挥发油:再按配方量称取白芷,低温干燥,然后采用95%乙醇按照白芷和95%乙醇的质量体积比为1毫克:5毫升回流提取2次,每次2h,过滤,合并滤液,得到白芷乙醇提取液,备用。混合挥发油与白芷乙醇提取液加入玉米油缓释剂按体积比为2:15:30混合均匀,即得中药挥发油。将中药挥发油,喷涂到贴剂上,即得产品。
一、制作成的空气清新贴剂的具体应用如下:
应用例1:将纯中药空气清新贴张贴在口罩外部,改善口罩内的异味和杀菌作用。
应用例2:将纯中药空气清新贴张贴在肩胛衣物处,可以自然挥发,改善口鼻附近环境的气味和杀菌作用。
应用例3:将纯中药空气清新贴张贴在台式电脑屏幕,自然恢复可以改善面部所处近距离空气异味和杀菌作用。
应用例4:将纯中药空气清新贴张贴在手机背部,随身携带,遇臭气环境,可拿起改善鼻息异味和杀菌作用。
应用例5:将纯中药空气清新贴张贴在车内方向盘中心,改善司机鼻息异味和杀菌作用。
二、将制作成的空气清新贴剂进行效果实验
1、检测方法
(1)通过在室温下暴露于密闭空间中挥发油的散发时间,来测试贴剂的持久效果。用气体检测管测定,将空气清新贴剂放置在60×60×60cm的有机玻璃箱中进行,分别在放置前和放置后6、12、18、24h取样,以测定箱内丁香、白芷、薄荷、藿香、益智仁在挥发油中的占比,结果如表1所示。
(a):样品(丁香、白芷、薄荷、藿香、益智仁占总量的50%)(持续时间6小时);
(b):样品(丁香、白芷、薄荷、藿香、益智仁占总量的65%)(持续时间12小时);
(c):样品(丁香、白芷、薄荷、藿香、益智仁占总量的80%),(持续时间18小时);
(d):样品(丁香、白芷、薄荷、藿香、益智仁占总量的85%),(持续时间24小时)。
表1纯中药挥发油空气清新贴剂持久效果评价表
实验时间/小时 | 丁香、白芷、薄荷、藿香、益智仁占总量(%) |
6 | 50 |
12 | 65 |
18 | 80 |
24 | 85 |
(2)除臭效果评价
选取NH3和H2S臭气为代表,臭气浓度用气体检测管测定,除臭效果评价在60×60×60cm的有机玻璃箱中进行。将空气清新贴剂放置有机玻璃箱内,分别在放置前和放置后1、3、5、7、10min取样,以测定箱内臭气浓度,计算消除率,结果如表2所示。
表2除臭效果评价表
由表2和图1可知,本发明纯中药挥发油空气清新贴能够有效地消除NH3和H2S,作用20min后,消除率趋于稳定,NH3和H2S的消除率分别达到93.5%和95.7%。
采用实施例1的纯中药挥发油空气清新贴的考察方法,对实施例2和3制备的纯中药挥发油空气清新贴进行除臭效果评价,实验表明:实施例2和纯中药挥发油空气清新贴能够有效地消除NH3和H2S,作用20min后,消除率趋于稳定,NH3和H2S的消除率分别达到91.2%和92.4%;实施例2和纯中药挥发油空气清新贴能够有效地消除NH3和H2S,作用20min后,消除率趋于稳定,NH3和H2S的消除率分别达到94.6%和93.8%。
(3)除菌效果评价
以密闭的有机玻璃箱作为实验场所,用平板沉降法测定空气细菌总数。在60×60×60cm的有机玻璃箱的待测纯中药空气清新贴剂,以75%的酒精作为对照组进行比较,分别在5、15、30min测定空气细菌总数。结果如表2所示。
表3除菌效果评价表
由表3和图2可知,本纯中药挥发油空气清新贴剂能够有效除菌,作用5min后除菌率能够迅速到达63.3%;作用10min后,除菌率趋于稳定;作用20min后,除菌率达到90.8%,各阶段的除菌率均高于对照组。
采用实施例1的纯中药挥发油空气清新贴剂的考察方法,对实施例2-3制备的纯中药挥发油空气清新贴剂进行除菌效果评价,实验结果表明,实施例2的纯中药挥发油空气清新贴剂作用5min后除菌效果能够达到65.5%;作用15min后,除菌率趋于稳定;作用时间30min后,除菌率达到91.2%。实施例3的纯中药挥发油空气清新贴剂作用5min后除菌效果能够达到68.9%;作用15min后,除菌率趋于稳定;作用时间30min后,除菌率达到94.1%,且实施例2-3的纯中药挥发油空气清新贴剂在各阶段的除菌率均高于对照组。
通过上述效果评价,证明了本发明纯中药挥发油空气清新贴剂无毒副作用,能有效抑菌抗病毒,气味芳香、持续时长良好。
需要说明的是,本发明权利要求书中涉及数值范围时,应理解为每个数值范围的两个端点以及两个端点之间任何一个数值均可选用,由于采用的步骤方法与实施例相同,为了防止赘述,本发明的描述了优选的实施例,尽管已描述了本发明的优选实施例,但本领域内的技术人员一旦得知了基本创造性概念,则可对这些实施例作出另外的变更和修改。所以,所附权利要求意欲解释为包括优选实施例以及落入本发明范围的所有变更和修改。
显然,本领域的技术人员可以对本发明进行各种改动和变型而不脱离本发明的精神和范围。这样,倘若本发明的这些修改和变型属于本发明权利要求及其等同技术的范围之内,则本发明也意图包含这些改动和变型在内。
Claims (7)
1.一种中药挥发油,其特征在于,由以下原料制成:丁香4-16份,薄荷8-18份,藿香6-14份,橘皮2-8份,白芷3-9份,益智仁6-12份,砂仁2-6份,生姜4-10份;
制备方法,其特征在于,包括以下步骤:
(1)、按配方量分别称取丁香,薄荷,藿香,益智仁,砂仁,橘皮,生姜,低温干燥,将丁香粉碎后和其余原料混匀,采用纯化水在室温下浸润,然后采用水蒸气蒸馏法进行挥发油提取,得到多味芳香中药的混合挥发油;
(2)、按配方量称取白芷,低温干燥,然后采用乙醇回流提取多次,过滤,合并滤液,得到白芷乙醇提取液,备用;
(3)、将步骤(2)得到的混合挥发油与步骤(3)得到的白芷乙醇提取液按一定比例混合均匀加入玉米油缓释剂,即得中药挥发油;
其中,混合挥发油:白芷乙醇提取液:玉米油缓释剂的体积比为1-2:9-18:20-30。
2.根据权利要求1所述的中药挥发油,其特征在于,中药挥发油由以下重量份的原料制成:丁香4份,薄荷8份,藿香6份,橘皮2份,白芷3份,益智仁6份,砂仁2份,生姜4份。
3.根据权利要求1-2任意一项所述的中药挥发油的制备方法,其特征在于,包括以下步骤:
(1)、按配方量分别称取丁香,薄荷,藿香,益智仁,砂仁,橘皮,生姜,低温干燥,将丁香粉碎后和其余原料混匀,采用纯化水在室温下浸润,然后采用水蒸气蒸馏法进行挥发油提取,得到多味芳香中药的混合挥发油;
(2)、按配方量称取白芷,低温干燥,然后采用乙醇回流提取多次,过滤,合并滤液,得到白芷乙醇提取液,备用;
(3)、将步骤(2)得到的混合挥发油与步骤(3)得到的白芷乙醇提取液按一定比例混合均匀加入玉米油缓释剂,即得中药挥发油;
其中,混合挥发油:白芷乙醇提取液:玉米油缓释剂的体积比为1-2:9-18:20-30。
4.根据权利要求3所述的中药挥发油的制备方法,其特征在于,步骤(1)中,采用水蒸气蒸馏法提取的条件为90-100℃下提取6h。
5.根据权利要求3所述的中药挥发油的制备方法,其特征在于,步骤(1)和步骤(2)中低温干燥温度为30-50℃。
6.根据权利要求3所述的中药挥发油的制备方法,其特征在于,步骤(2)中,采用体积分数为70%-95%的乙醇回流提取2-4次,每次1-3小时。
7.权利要求1-2任意一项所述的中药挥发油在制备空气清新剂中的用途,其中,将步骤(3)得到的中药挥发油喷晒在具有网格状的粘性贴纸上,制作成空气清新贴剂。
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