CN111642516A - Cotton defoliation ripening composition and application thereof - Google Patents

Cotton defoliation ripening composition and application thereof Download PDF

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Publication number
CN111642516A
CN111642516A CN202010492025.3A CN202010492025A CN111642516A CN 111642516 A CN111642516 A CN 111642516A CN 202010492025 A CN202010492025 A CN 202010492025A CN 111642516 A CN111642516 A CN 111642516A
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China
Prior art keywords
weight
cotton
parts
thidiazuron
ethephon
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CN202010492025.3A
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Chinese (zh)
Inventor
任相亮
马艳
马亚杰
王丹
胡红岩
宋贤鹏
马小艳
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Institute of Cotton Research of Chinese Academy of Agricultural Sciences
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Institute of Cotton Research of Chinese Academy of Agricultural Sciences
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Priority to CN202010492025.3A priority Critical patent/CN111642516A/en
Publication of CN111642516A publication Critical patent/CN111642516A/en
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/18Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds
    • A01N57/20Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds containing acyclic or cycloaliphatic radicals
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N27/00Biocides, pest repellants or attractants, or plant growth regulators containing hydrocarbons
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/44Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
    • A01N37/48Nitro-carboxylic acids; Derivatives thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/28Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
    • A01N47/36Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the group >N—CO—N< directly attached to at least one heterocyclic ring; Thio analogues thereof

Abstract

The invention discloses a defoliation ripening composition which comprises 8-10 parts by weight of thidiazuron, 2-10 parts by weight of lactofen and 24-32 parts by weight of ethephon. The invention also discloses application of the cotton defoliation ripening composition. The defoliation ripening composition can well promote defoliation of cotton, accelerate boll opening of the cotton and improve cotton yield.

Description

Cotton defoliation ripening composition and application thereof
Technical Field
The invention belongs to the technical field of pesticides, relates to a pesticide composition and an application field thereof, and particularly relates to a defoliation ripening composition and an application thereof.
Background
The defoliating agent is sprayed before cotton harvesting, so that the shedding and concentrated boll opening of cotton leaves can be promoted, the impurity content of cotton is reduced, and the mechanical cotton harvesting efficiency is improved. At present, 87 cotton defoliating agent products which are approved to be registered and are in the period of validity in China are obtained, wherein 45 single agents are used, and 42 mixed agents are used. The single dose is mainly thidiazuron, and 43 doses are available; the other 2 are pyraflufen-ethyl. The mixture mainly comprises 40 thidiazuron and diuron, and the other 2 thidiazuron and ethephon are thidiazuron and ethephon respectively. Therefore, the effective components of cotton defoliant products in China are single, and new defoliant products are urgently needed to be applied to production. In the production process of cotton, cotton farmers generally use defoliating mixed agents diuron, thidiazuron and ethephon.
After the thidiazuron is absorbed by the plant, abscisic acid and ethylene can be generated by the cotton plant, so that a separation layer is formed between a leaf stalk and the cotton plant, and cotton leaves fall off automatically. The thidiazuron can also promote the nutrient components of the leaves to be transferred to young and tender cotton bolls on the upper parts of the plants, and the cotton plants cannot die, so that the multiple effects of ripening acceleration, defoliation, yield increase and quality increase are integrated. The thidiazuron can make the cotton early mature, the boll opening is relatively advanced and concentrated, the proportion of cotton before frost is increased, and the mechanical and manual harvesting is facilitated. The ethephon has good ripening acceleration effect, and can rapidly crack the cotton bolls and dry the leaves after dehydration when being used on cotton. However, the thidiazuron and diuron have higher cost, the thidiazuron has lower defoliation speed and poorer low-temperature resistance, the ethephon has good ripening effect, but the defoliation effect is poor, thereby influencing the influence of mechanical harvesting on the quality of cotton. Therefore, in the process of developing a new cotton defoliant, the dosage of thidiazuron and diuron should be reduced, and the ethephon incorporation ratio and application times should be strictly controlled.
Lactofen is a selective post-emergence herbicide, is a serious inhibitor of sensitive plant protoporphyrin oxidase, catalyzes the oxidation of protoporphyrin to protoporphyrin IX in a chlorophyll biosynthesis pathway, and is a transient metabolite, a photosensitizer which obviously causes lipid peroxidation in tissues, does not accumulate in plant tissues and is an intermediate product of a heme precursor substance and a chlorophyll early precursor substance. Under the action of herbicide, protoporphyrin IX is accumulated, the accumulated amount of protoporphyrin IX is obviously and positively correlated with the toxicity level, and the increase of protoporphyrin causes the decrease of chlorophyllide, finally causes lipid peroxidation, causes membrane damage and causes cell leakage.
In the process of deeply researching the cotton defoliation ripening composition, the inventor surprisingly discovers that the defoliation effect of cotton can be obviously improved by mixing the thidiazuron, the lactofen-diclofop-methyl and the ethephon, the dosage of the thidiazuron used alone is reduced, the defoliation effect of the thidiazuron is improved, and the ripening effect of the ethephon is promoted. In addition, the mixing of thidiazuron, lactofen and ethephon can reduce the application times, the defoliation and ripening effect of cotton can be achieved by applying the pesticide once, and the yield and the quality of the cotton cannot be influenced. Thus, the present invention has been completed through further studies.
According to the data search made by the inventor, no patent and other published data conflicting with the present invention are found.
Disclosure of Invention
In order to overcome the defects of slow defoliation speed of thidiazuron and poor ripening effect of ethephon in the background art, the invention aims to provide the cotton defoliation ripening composition which can increase the defoliation speed of thidiazuron and the ripening effect of ethephon, reduce the application times, has excellent defoliation effect of cotton, is low in medication cost and does not influence the yield and quality of cotton.
The invention also aims to provide application of the cotton defoliation ripening composition.
In order to achieve the purpose, the invention provides a defoliation ripening composition which is characterized by comprising 8-10 parts by weight of thidiazuron, 2-10 parts by weight of lactofen and 24-32 parts by weight of ethephon; the auxiliary agent in the defoliation ripening composition comprises a surfactant and/or a filler; the weight percentage of the defoliating ripening active ingredients in the composition is 25-75%.
In an embodiment of the present invention, the defoliating ripening composition may include 8 to 9 parts by weight of thidiazuron, 3 to 9 parts by weight of lactofen, and 28 to 30 parts by weight of ethephon.
In an embodiment of the present invention, the defoliating ripening composition may include 8 to 9 parts by weight of thidiazuron, 6 to 9 parts by weight of lactofen, and 28 to 30 parts by weight of ethephon.
In an embodiment of the present invention, the defoliating ripening composition may comprise 8 parts by weight thidiazuron, 9 parts by weight lactofen and 28 parts by weight ethephon.
In the embodiment of the invention, the concentration of thidiazuron applied in the defoliation ripening composition can be 120-150 g/ha, the concentration of lactofen applied can be 45-144 g/ha, the concentration of ethephon applied can be 360-480 g/ha, and the water consumption can be 450-900 l/ha, based on the amount of the active ingredients.
In an embodiment of the invention, the defoliating ripening composition may be in the form of a solution, a wettable powder, a suspension, a dispersible oil suspension or water dispersible granules.
The composition of the invention is used for defoliating and ripening cotton, namely for detaching plant leaves.
The compositions of the present invention exhibit a synergistic effect, the activity of which is more pronounced than the expected sum of the activities using the individual compounds, and the individual activities of the individual compounds.
The composition of the invention can promote defoliation of cotton, accelerate boll opening of cotton, improve cotton yield and does not affect cotton quality.
The composition of the invention promotes the absorption of the defoliation ripening composition in a low-temperature environment, and has remarkable promoting effect on defoliation and boll opening of cotton.
The composition has the advantages of small dosage, reduced application frequency and reduced environmental hazard.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail with reference to specific embodiments below.
The agents used in the following examples: thidiazuron is 80% thidiazuron wettable powder, ethephon is 40% ethephon water aqua, and lactofen is 240g/L lactofen emulsifiable concentrate.
Example 1
8 parts by weight of thidiazuron, 3 parts by weight of lactofen and 28 parts by weight of ethephon are uniformly mixed to prepare the composition suspending agent with the mass fraction of 39% (namely, in the composition suspending agent, the thidiazuron accounts for 8 wt%, the lactofen accounts for 3 wt%, and the ethephon accounts for 28 wt%).
Example 2
8 parts by weight of thidiazuron, 6 parts by weight of lactofen and 28 parts by weight of ethephon are uniformly mixed to prepare a composition suspending agent with the mass fraction of 42% (namely, in the composition suspending agent, the thidiazuron accounts for 8 wt%, the lactofen accounts for 6 wt%, and the ethephon accounts for 28 wt%).
Example 3
8 parts by weight of thidiazuron, 9 parts by weight of lactofen and 28 parts by weight of ethephon are uniformly mixed to prepare a composition suspending agent with the mass fraction of 45% (namely, in the composition suspending agent, the thidiazuron accounts for 8 wt%, the lactofen accounts for 9 wt%, and the ethephon accounts for 28 wt%).
Test example
The investigation method, the data processing and calculation method related to the test example are as follows:
the investigation method comprises the following steps: before the application, 20 cotton plant fixing hanging tags are randomly selected in the middle row of each cell, and the total number of leaves of cotton at each point of each cell is investigated on the day of application. The number of the residual leaves of each point of the plant-fixed cotton is respectively investigated 10 days and 20 days after the pesticide application, the defoliation rate of each investigation is respectively calculated, the boll opening rate of the cotton 20 days after the pesticide application is calculated, and the yield is measured during the boll opening period of the cotton.
The drug effect calculation method comprises the following steps:
Figure RE-GDA0002608308060000031
Figure RE-GDA0002608308060000032
Figure RE-GDA0002608308060000033
the results show that the defoliation rates of the cotton in the examples 1-3 are 96% and 100% respectively after the application of the stone river and the Aral in the example 3 20 days, and are higher than the defoliation rates of the single use of the thidiazuron, the mixed use of the thidiazuron and the ethephon and the mixed use of the lactofen and the ethephon. In addition, the defoliation rates of examples 1 and 2 were only 84% and 86% at the highest 20 days after application of the shihe and alaer, which was lower than that of example 3 for cotton.
TABLE 1 examples 1 to 3% defoliation rate (%) of cotton (water consumption for spraying 450L/ha)
Figure RE-GDA0002608308060000041
The results of examples 1 to 3 on the cotton yield are shown in table 2, and it can be seen from the results that the cotton yield of example 3 20 days after the application of the stone river and the alaer can reach 84% and 89%, respectively, which are higher than the cotton yield of the single use of thidiazuron, the mixed use of thidiazuron and ethephon and the mixed use of lactofen and ethephon. Similarly, the boll opening rate of example 1 and example 2 20 days after the application of the pebble and alura is only 71% and 75% at the highest, which is lower than that of example 3 for cotton.
TABLE 2 examples 1 to 3 boll opening ratio (%)
Figure RE-GDA0002608308060000051
The results of the examples 1 to 3 on the yield increase of cotton are shown in Table 3, and the yield increase of cotton after the application of the mixture to the river and the Aral in the example 3 is respectively 20% and 21%, which is higher than the yield increase of cotton with single thidiazuron, the combination of the thidiazuron and ethephon and the combination of lactofen and ethephon. Similarly, the cotton yields of examples 1 and 2 were only 15% and 16% at the highest after application to the cobra and alura, which is lower than the cotton yield of example 3.
The average temperature of the pesticide applied in the rock river region is only 15 ℃ and is lower than the average temperature (24 ℃) applied in the Alar region, but the defoliation rate, the boll opening rate and the yield increasing rate of cotton in the rock river and the Alar in the examples 1-3 are not greatly different, so the temperature does not influence defoliation, boll opening and yield of the examples. However, when thidiazuron is used alone or when thidiazuron and ethephon are mixed, the defoliation rate, boll opening and yield of cotton in the rocky river region are slightly lower than those in the Alar region due to the influence of temperature.
TABLE 3 yield increase (%) of examples 1 to 3 to cotton
Drug treatment Mass ratio of Hectare dosage (based on effective components) Stone river Alar
Thidiazuron —— 120g 9 10
Thidiazuron and ethephon 8:28 120g+420g 13 15
Lactofen and ethephon 3:28 45g+420g 0 0
Lactofen and ethephon 6:28 90g+420g 1 0
Lactofen and ethephon 9:28 135g+420g 2 2
Thidiazuron, lactofen and ethephon 8:3:28 (example 1) 120g+45g+420g 14 14
Thidiazuron, lactofen and ethephon 8:6:28 (example 2) 120g+90g+420g 15 16
Thidiazuron, lactofen and ethephon 8:9:28 (example 3) 120g+135g+420g 20 21
Clear water control —— 0 0 0
Those of ordinary skill in the art will understand that: the invention is not to be considered as limited to the specific embodiments thereof, but is to be understood as being modified in all respects, all changes and equivalents that come within the spirit and scope of the invention.

Claims (7)

1. The defoliation ripening composition is characterized by comprising 8-10 parts by weight of thidiazuron, 2-10 parts by weight of lactofen and 24-32 parts by weight of ethephon; the auxiliary agent in the defoliation ripening composition comprises a surfactant and/or a filler; the weight percentage of the defoliation ripening active ingredients in the composition is 25-75%.
2. The defoliating and ripening composition of claim 1, wherein the defoliating and ripening composition comprises 8 to 9 parts by weight thidiazuron, 3 to 9 parts by weight lactofen and 28 to 30 parts by weight ethephon.
3. The defoliating and ripening composition of claim 1, wherein the defoliating and ripening composition comprises 8 to 9 parts by weight thidiazuron, 6 to 9 parts by weight lactofen and 28 to 30 parts by weight ethephon.
4. A defoliating and ripening composition according to claim 1, wherein said defoliating and ripening composition comprises 8 parts by weight thidiazuron, 9 parts by weight lactofen and 28 parts by weight ethephon.
5. The defoliation and ripening composition according to claim 1, wherein the concentration of thidiazuron applied in the defoliation and ripening composition is 120-150 g/ha, the concentration of lactofen applied is 45-144 g/ha, the concentration of ethephon applied is 360-480 g/ha, and the amount of water used is 450-900 l/ha.
6. A defoliating and ripening composition according to claim 1, wherein said defoliating and ripening composition is in the form of a solution, a wettable powder, a suspension, a dispersible oil suspension or water dispersible granules.
7. The defoliating and ripening composition of claim 1, wherein said defoliating and ripening composition is used for defoliating and ripening cotton.
CN202010492025.3A 2020-06-03 2020-06-03 Cotton defoliation ripening composition and application thereof Pending CN111642516A (en)

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