CN111631983A

CN111631983A - Softening and repairing hair care composition and application thereof

Info

Publication number: CN111631983A
Application number: CN201910156252.6A
Authority: CN
Inventors: 李丹群; 潘霞; 杨土珍
Original assignee: Guangzhou Xuzhuang Biotechnology Co ltd
Current assignee: Guangzhou Xuzhuang Biotechnology Co ltd
Priority date: 2019-03-01
Filing date: 2019-03-01
Publication date: 2020-09-08
Anticipated expiration: 2039-03-01
Also published as: CN111631983B

Abstract

The invention relates to a softening and repairing hair care composition and application thereof. The softening and repairing hair care composition comprises the following components in parts by weight: 0.01 to 5 portions of lecithin; 0.01 to 5 portions of acanthus seed oil; 0.1 to 5 portions of stearyl trimethyl ammonium chloride; 0.1 to 5 portions of stearamide propyl dimethylamine; 0.1 to 5 portions of hydrolyzed wheat protein; 0.5 to 5 portions of silicone oil. The softening and repairing hair care composition has an obvious repairing effect on damaged hair after being ironed and dyed, can solve the problems of dry hair, frizzy hair and the like, and achieves the effect of softening hair.

Description

Softening and repairing hair care composition and application thereof

Technical Field

The invention relates to the field of daily chemical products, in particular to a softening and repairing hair care composition and application thereof.

Background

The surface layer of healthy hair is covered with a natural protective film consisting of a group of complete hair scales and naturally secreted grease, and the natural protective film is easily damaged by factors such as excessive washing, sunlight solarization, popular perm and hair dyeing, so that the moisture of the cortex is lost, the nutrition of the hair is poor, and the hair becomes dry, split, frizzy and easy to break. Healthy hair is not easily repaired once it is damaged. However, although there are many kinds of hair care products on the market, the hair care products have limited effects of repairing and nourishing hair.

Disclosure of Invention

Based on the above, the invention provides a softening and repairing hair care composition and application thereof. The softening and repairing hair care composition has an obvious repairing effect on damaged hair after being ironed and dyed, can solve the problems of dry hair, frizzy hair and the like, and achieves the effect of softening hair.

The specific technical scheme is as follows:

a softening, repairing and hair-care composition comprises the following components in parts by weight:

in one embodiment, the softening and repairing hair care composition comprises the following components in parts by weight:

in one embodiment, the silicone oil comprises cyclopentadimethylsiloxane, cyclomethicone, and dimethicone.

The invention also provides application of the softening and repairing hair care composition in a hair care product.

The invention also provides a hair-developing solution.

The specific technical scheme is as follows:

the hair-developing solution is prepared from the following raw materials in percentage by weight:

2-10% of the softening and repairing hair care composition, 0.1-0.5% of hydroxyethyl cellulose, 1-2% of cetearyl alcohol, 0.5-2% of PEG-20 stearate, 15-25% of glycerol, 0.1-1% of mannan, 1-3% of propylene glycol, 0.1-0.5% of chlorphenesin, 0.1-1% of phenoxyethanol, 4-6% of a thermal inductance agent, 0.01-0.1% of menthol lactate, 0.05-0.5% of EDTA-2Na, 0.05-2% of essence, 0.01-1% of citric acid and 60-70% of water.

In one embodiment, the softening, repairing and hair care composition comprises 4% to 7% by weight of the hair lotion.

In one embodiment, the warming agent is selected from one or more of vanillyl butyl ether and ginger root extract.

The invention also provides a preparation method of the hair-growing liquid.

The specific technical scheme is as follows:

a preparation method of the hair-developing solution comprises the following steps:

preparation of the aqueous phase: mixing the hydroxyethyl cellulose and glycerol, adding water, EDTA-2Na, chlorphenesin, lecithin, mannan, stearyl trimethyl ammonium chloride and citric acid, heating to 80-88 ℃ under stirring, starting homogenizing and stirring for 5-8 minutes, and stirring at constant temperature for 10-30 minutes to obtain a water phase;

preparation of oil phase: mixing the cetostearyl alcohol, PEG-20 stearate, silicone oil, argania spinosa kernel oil and stearamidopropyl dimethylamine, heating to 75-80 ℃ under stirring, and preserving heat for 15-20 minutes to obtain an oil phase;

emulsification: mixing the oil phase and the water phase, homogenizing and emulsifying for 8-10 minutes, stirring for 10-30 minutes at constant temperature, vacuumizing, and cooling to 40-45 ℃ to obtain a mixture;

preparing at low temperature: adding the phenoxyethanol, essence, vanillyl butyl ether, ginger root extract, hydrolyzed wheat protein, menthol lactate and propylene glycol into the mixture, and uniformly stirring to obtain the essence.

The invention also provides a steam hair mask.

The specific technical scheme is as follows:

a steam hair mask comprises a hair mask packaging material and the hair mask liquid filled in the hair mask packaging material.

Compared with the prior art, the invention has the following beneficial effects:

the softening and repairing hair care composition has an obvious repairing effect on damaged hair, can solve the problems of dry hair, split hair, frizzy hair and the like, and achieves the effect of softening hair. The argania spinosa kernel oil is rich in vitamin E, can promote hair growth, is also rich in unsaturated fatty acids such as Omega 3 and Omega 6, can be easily absorbed by hair shafts, and cystine contained in hydrolyzed wheat protein has disulfide bonds and can be covalently bonded with hair to generate a permanent conditioning effect, wherein hydrophilic groups can absorb water on the hair to achieve a moisturizing effect. Meanwhile, the lecithin can further promote the penetration of nutrient substances in the argania spinosa kernel oil and the hydrolyzed wheat protein, and has certain moisture retention and oxidation resistance effects. In addition, the cationic conditioning agent adopted by the invention is stearyl trimethyl ammonium chloride and stearamidopropyl dimethylamine, and the cationic conditioning agent can play a role of conditioning hair together with argania spinosa kernel oil, hydrolyzed wheat protein and lecithin, is favorable for being combined with electrons on the hair or in the environment, so that the antistatic capacity of the hair is improved, the bonding force with the hair is strong, the hair has very good wet combing property, dry combing property, fluffy feeling and hair plumpness, the dyed and cold-permed hair is favorably repaired, the hair damage, the hair roughness and the dryness caused by chemical treatment are improved, and the hair is smooth and easy to be treated. Meanwhile, the silicone oil can further promote the formation of a layer of uniform protective film on the hair, improve the silky feeling and the moist feeling of the hair, improve the luster and the texture of the hair and improve the ultraviolet radiation resistance.

In addition, the hair-mask liquid in the steam hair mask takes the vanillyl butyl ether and the ginger root extract as the heat sensitizer, the heat sensitizer acts on the scalp, the blood circulation of capillaries can be promoted, neurotransmitter is triggered by directly stimulating nerve endings so as to continuously generate heat sensation, and a closed heat-preserving environment is formed due to the particularity of the hair-mask packing material, so that warm steam feeling is achieved. Meanwhile, the shampoo has the effects of activating hair follicles, effectively regulating scalp environment, preventing alopecia and white hair, stimulating the growth of new hairs, inhibiting scalp itch and strengthening hair roots. Furthermore, the menthol lactate is added into the hair mask liquid, after the hair mask is taken off, the heat preservation environment is relieved, and when the hair mask liquid is washed by water, the menthol lactate can selectively stimulate a cold sensor of the scalp to generate cold reflection and cold feeling to cause vasoconstriction of skin mucous membrane, so that cool feeling is generated, heat feeling generated by steam is replaced, cold and heat balance is achieved, and the effects of cooling and relieving itching are achieved to obtain comfortable body feeling.

Drawings

FIG. 1 is a diagram showing a film packaging material;

FIG. 2 is a diagram showing the amount of the feed solution;

FIG. 3 is a view showing a state of use of the back surface of the vapor deposition film;

FIG. 4 is a front view of the steam generating membrane;

FIG. 5 is a side view of the steam generating film in use;

FIG. 6 is a comparison of damaged hair A before and after application of number 1 vapor film;

FIG. 7 is a comparison of damaged hair B before and after application of number 1 vapor film;

FIG. 8 is a comparison of damaged hair C before and after application of number 2 vapor deposition;

FIG. 9 is a comparison of damaged hair D before and after application of number 2 vapor deposition;

FIG. 10 is a comparison of damaged hair mass E before and after application of number 3 vapor film;

FIG. 11 is a comparison of damaged hair F before and after application of number 3 vapor deposition;

FIG. 12 is a comparison of damaged hair A before and after application of number 4 vapor deposition;

FIG. 13 is a comparison of damaged hair A before and after application of steam hair mask No. 5;

fig. 14 is a comparison of damaged hair A before and after application of number 6 vapor film.

Detailed Description

The following examples are provided to illustrate the softening and conditioning compositions of the present invention and their use in further detail. The present invention may be embodied in many different forms and is not limited to the embodiments described herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete.

Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terminology used in the description of the invention herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. As used herein, the term "and/or" includes any and all combinations of one or more of the associated listed items.

Table 1 shows the trade names and sources of the starting materials used in the following examples.

TABLE 1

Examples 1 to 3 and comparative examples 1 to 3

According to the formula (the formula is calculated by weight percentage) shown in the table 2, the hair-growing liquid and the steam hair-growing film are prepared, and the preparation method comprises the following steps:

preparation of the aqueous phase: firstly, adding water into an interlayer emulsifying pot for preparing a water phase, then adding hydroxyethyl cellulose into glycerol, uniformly stirring, putting into the interlayer emulsifying pot, sequentially adding EDTA-2Na, chlorphenesin, lecithin, mannan, stearyltrimethyl ammonium chloride and citric acid, introducing steam into a jacket of the interlayer emulsifying pot, heating to 80-88 ℃ under stirring, starting homogenizing and stirring for 5-8 minutes, stirring at constant temperature for 20 minutes, and stirring at 30HZ to obtain the water phase.

Preparation of oil phase: adding cetearyl alcohol, PEG-20 stearate (EMU POWER 200), cetearyl alcohol (C1618), cyclopentadimethylsiloxane, cyclomethicone, dimethicone, argania spinosa oil, stearamidopropyl dimethylamine into a jacketed kettle for preparing the oil phase, starting steam for heating, heating to 75-80 ℃ under the condition of continuous stirring, and preserving heat for 15-20 minutes to fully and uniformly dissolve the materials to obtain the oil phase for later use;

emulsification: slowly pumping the oil phase into the water phase, homogenizing and emulsifying for 8-10 min, continuously stirring at constant temperature for 20 min, vacuumizing, and cooling to 40-45 deg.C with cooling water in the interlayer emulsifying pot to obtain mixture;

preparing at low temperature: adding phenoxyethanol, essence, vanillyl butyl ether, ginger root extract, hydrolyzed wheat protein, menthol lactate and propylene glycol (the menthol lactate and the propylene glycol are premixed until completely dissolved) into the mixture, and stirring uniformly; 25HZ to obtain the hair mask liquid;

preparing a steam hair mask: and (3) storing the film-forming liquid for 2-3 days, filling the film-forming liquid into a packaging material, evaluating the quality of a product before filling, and filling the product after the quality is qualified. FIG. 1 is a display picture of a hair mask packaging material, wherein the packaging material is also connected with a non-setting adhesive, and the non-setting adhesive is easy to tear and stick, and is very firm and convenient. FIG. 2 is a diagram showing the amount of the hair mask liquid filled, which is pushed away uniformly and filled to one third of the exit opening (black line in the figure), without contacting the forehead and without uneven spreading of the hair mask liquid on the hair.

The application state of the steam hair mask is shown in fig. 3-5, when in use, the hair is cleaned with shampoo, the hair is wiped with a towel to a degree of no water dripping, then the hair is wrapped with the steam hair mask, the hair is fixed with adhesive sticker after being wrapped, then the hair is massaged with hands on the hair via the hair mask, so that the hair mask liquid can be uniformly smeared on the hair, the hair is kept stand for 15min, and after the steam hair mask is taken off, the hair mask is flushed with water and dried.

TABLE 2

Performance testing

The performance tests were performed on the hair-growth liquids and vapor hair-growth films prepared in examples 1 to 3 and comparative examples 1 to 3,

the test method is as follows:

the hair-growth liquids prepared in examples 1 to 3 and comparative examples 1 to 3 were labeled as hair-growth liquids No. 1 to No. 6, and the viscosities thereof were measured and the results are shown in Table 3.

The steam hair films prepared in examples 1 to 3 and comparative examples 1 to 3 were respectively labeled as No. 1 to 6 steam hair films, and 6 kinds of hairs damaged to different degrees were labeled as A to F damaged hair qualities, wherein the number of damaged hair qualities A was 4 tufts and the number of damaged hair qualities B to F was 1 tuft, respectively, and the No. 1 to 6 steam hair films were used on the damaged hair qualities A to F, respectively, with reference to the correspondence relationship of Table 3.

The specific test method comprises the following steps: the hair is cleaned by shampoo (quantitative), the hair is wiped by a towel to the extent of no water dripping, then the hair is coated by the hair-filming liquid (quantitative) and is uniformly coated, the hair is kept stand for 15min, then cleaned and dried, after 48h, the previous steps are repeated for 4 times, after the hair is nursed each time, the dry and wet combing performance and the antistatic property of the hair are tested by using a corresponding instrument, and the flexibility and the glossiness of the hair before and after the hair is nursed are photographed and recorded after the hair is cleaned and dried for 5 th time.

The specific method for the dry and wet combing property and the antistatic property of the hair comprises the following steps:

1. dry and wet combing test method for hair: the combing performance of the hair is judged by measuring the resistance and the change condition of the resistance in the process of combing the hair by the mechanical comb under the dry state and the wet state of the hair.

2. Method for testing the antistatic properties of hair: the potential of the hair was measured using a vibration volume type potentiometer. The voltage applied to the hair strands after treatment with the hair care product is much lower, sometimes half or one third lower, than to the hair strands treated with shampoo alone.

The results of the experiment are shown in table 3 and fig. 6 to 14. Wherein, FIG. 6 is a comparison of the damaged hair A before and after application of No. 1 vapor film; FIG. 7 is a comparison of damaged hair B before and after application of number 1 vapor film; FIG. 8 is a comparison of damaged hair C before and after application of number 2 vapor deposition; FIG. 9 is a comparison of damaged hair D before and after application of number 2 vapor deposition; FIG. 10 is a comparison of damaged hair mass E before and after application of number 3 vapor film; FIG. 11 is a comparison of damaged hair F before and after application of number 3 vapor deposition; FIG. 12 is a comparison of damaged hair A before and after application of number 4 vapor deposition; FIG. 13 is a comparison of damaged hair A before and after application of steam hair mask No. 5; fig. 14 is a comparison of damaged hair A before and after application of number 6 vapor film.

TABLE 3

It can be seen from table 3 and fig. 6 to 14 that the vapor hair mask of examples 1 to 3 can significantly improve the damaged hair quality, and when used, the hair mask has warm "vapor" feeling, and when washed with water, the hair mask also has cool feeling and comfortable feeling. After a period of time of nursing, the damaged hair quality of the original dry hair and the frizzy hair becomes smoother, more flexible, glossy, high in hairline fullness, and good in dry-wet combing property and antistatic property. Among them, the effect of the No. 1 steam film is most remarkable. The hair spray prepared in comparative examples 1 to 3, however, had relatively weak gloss, combing property and softening effect although the damaged hair quality, which was dry and frizzy, was repaired after the same conditioning steps and conditioning time as in examples 1 to 3.

The technical features of the embodiments described above may be arbitrarily combined, and for the sake of brevity, all possible combinations of the technical features in the embodiments described above are not described, but should be considered as being within the scope of the present specification as long as there is no contradiction between the combinations of the technical features.

The above-mentioned embodiments only express several embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the present invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present patent shall be subject to the appended claims.

Claims

1. The softening and repairing hair care composition is characterized by comprising the following components in parts by weight:

2. the softening, repairing and hair care composition according to claim 1, which comprises the following components in parts by weight:

3. the softening, repairing and hair care composition according to claim 2, which comprises the following components in parts by weight:

4. the softening and conditioning hair care composition according to any one of claims 1 to 3, wherein the silicone oil comprises cyclopentadimethylsiloxane, cyclomethicone and dimethicone.

5. Use of a softening and restoring hair care composition according to any one of claims 1 to 4 in a hair care product.

6. The hair-growing liquid is characterized by being prepared from the following raw materials in percentage by weight:

the compliant repair hair care composition of any of claims 1-4, 2% -10%, hydroxyethyl cellulose 0.1% -0.5%, cetearyl alcohol 1% -2%, PEG-20 stearate 0.5% -2%, glycerin 15% -25%, mannan 0.1% -1%, propylene glycol 1% -3%, chlorphenesin 0.1% -0.5%, phenoxyethanol 0.1% -1%, a thermal sensate 4% -6%, menthol lactate 0.01% -0.1%, EDTA-2Na 0.05% -0.5%, citric acid 0.01% -1%, and water 60% -70%.

7. The hair spray solution of claim 6, wherein the softening and repairing hair care composition is present in an amount of 4% to 7% by weight of the hair spray solution.

8. The hair spray solution of claim 6 or 7, wherein the thermogenic agent is selected from one or more of vanillyl butyl ether and ginger root extract.

9. A method of preparing the hair casting solution according to any one of claims 6 to 8, comprising the steps of:

10. A steam hair mask, which is characterized by comprising a hair mask packaging material and the hair mask liquid of any one of claims 6-8 filled in the hair mask packaging material.