CN111588781A - Neck and shoulder strain rehabilitation essential oil for physique of wind-cold obstructing collaterals and preparation method thereof - Google Patents

Neck and shoulder strain rehabilitation essential oil for physique of wind-cold obstructing collaterals and preparation method thereof Download PDF

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CN111588781A
CN111588781A CN202010666991.2A CN202010666991A CN111588781A CN 111588781 A CN111588781 A CN 111588781A CN 202010666991 A CN202010666991 A CN 202010666991A CN 111588781 A CN111588781 A CN 111588781A
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radix
essential oil
oil
powder
parts
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许丽璇
何斯琪
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Shenzhen Huacheng Daye Industrial Co ltd
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Shenzhen Huacheng Daye Industrial Co ltd
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Abstract

The invention discloses neck and shoulder strain rehabilitation essential oil for wind-cold collateral obstruction physique and a preparation method thereof. The massage essential oil consists of base oil, traditional Chinese medicine components and vitamin E; the base oil comprises grape seed oil, sunflower seed oil, arnica oil and sesame oil; the Chinese medicinal components comprise rhizoma Ligustici Chuanxiong, Notopterygii rhizoma, radix Angelicae Pubescentis, radix Saposhnikoviae, radix Angelicae sinensis, Notoginseng radix, radix Paeoniae alba, Glycyrrhrizae radix and herba Schizonepetae. The massage essential oil disclosed by the invention has a good effect of relieving muscle strain by combining with a proper massage manipulation, can also relieve exterior syndrome, dispel cold, expel wind, relieve exterior syndrome, remove blood stasis, activate blood circulation, relieve pain and strengthen tendons and bones, is particularly suitable for people with the constitution of blocking collaterals by wind-cold, accords with the principle of traditional Chinese medicine, and has the advantages of simple preparation process and no toxic or side effect.

Description

Neck and shoulder strain rehabilitation essential oil for physique of wind-cold obstructing collaterals and preparation method thereof
Technical Field
The invention relates to neck and shoulder strain rehabilitation essential oil for wind-cold collateral obstruction physique and a preparation method thereof, and belongs to the technical field of massage essential oil.
Background
In the theory of traditional Chinese medicine, the wind-cold arthralgia syndrome refers to the condition of wind-cold-dampness blocking the joints of bones and muscles and blocking the meridians, resulting in unsmooth circulation of qi and blood, and the common symptoms of migratory pain in joints of limbs, or heavy pain, etc., which are commonly seen in the diseases of migratory arthralgia, painful arthralgia, calendar festival, etc. Cold is yin pathogen, which mainly causes stagnation, wind-cold is clear and ascends to cause a plurality of changes, so that the pathogenic wind-cold invades the human body and blocks the joints of the meridians and collaterals, so that the qi and blood circulation is not smooth, cold pain, difficulty in bending and stretching and no fixed pain of the joints of the limbs can be seen; cold is the pathogenic yin, and the excess of yin causes cold, so the local skin is not red and not hot to touch; the blood vessels are not smooth when encountering cold, so the pain is more severe, and the qi and blood are smooth when encountering heat, so the pain is reduced; a pale-red tongue with white coating and a wiry, slow or wiry and tight pulse is the condition of cold pathogen and a superficial pulse is the condition of wind pathogen.
Neck and shoulder muscle strain is a chronic disease which is frequently seen by modern people, is a chronic and repeatedly accumulated micro injury, and is closely related to occurrence and development of cervical spondylosis. The existing methods for treating neck and shoulder muscle strain mainly comprise the following two methods: 1) by using western medicines or traditional Chinese medicines with anti-inflammatory and analgesic effects, the method mainly temporarily relieves discomfort for a while, does not have obvious effect of fundamentally relieving muscle injury, and even cannot perform typing treatment according to people with different constitutions; 2) the massage essential oil is used and assisted by massage manipulation, the method has obvious effect on relieving muscle tension and pain, has no toxic or side effect, is accepted by more people, but the components and functions of the massage essential oil in the current market are single, typing treatment can not be carried out according to different physique people, the traditional Chinese medicine is not used for dialectical treatment, and the actual use effect is relatively limited.
Therefore, the development of massage essential oil which has an excellent effect of relieving muscle strain and is suitable for the physique of wind-cold obstruction of collaterals is urgently needed.
Disclosure of Invention
The invention aims to provide neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstruction of collaterals and a preparation method thereof.
The technical scheme adopted by the invention is as follows:
a neck and shoulder strain rehabilitation essential oil for wind-cold collateral obstruction constitution comprises base oil, Chinese medicinal components and vitamin E; the base oil comprises grape seed oil, sunflower seed oil, arnica oil and sesame oil; the Chinese medicinal components comprise rhizoma Ligustici Chuanxiong, Notopterygii rhizoma, radix Angelicae Pubescentis, radix Saposhnikoviae, radix Angelicae sinensis, Notoginseng radix, radix Paeoniae alba, Glycyrrhrizae radix and herba Schizonepetae.
Preferably, the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstructing collaterals is prepared from the following raw materials in parts by mass: grape seed oil: 30-50 parts of a solvent; sunflower seed oil: 20-40 parts of a solvent; mountain golden car oil: 5-25 parts; sesame oil: 5-15 parts of a solvent; ligusticum wallichii: 0.5-3 parts; notopterygium root: 0.5-2 parts; radix angelicae pubescentis: 0.5-2 parts; wind prevention: 0.5-2 parts; chinese angelica: 0.5-2 parts; pseudo-ginseng: 0.5-2 parts; white peony root: 0.5-2 parts; licorice root: 0.05-1.5 parts; herba schizonepetae: 0.05-1.5 parts; vitamin E: 0.05 to 0.2 portion.
Further preferably, the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstructing collaterals is prepared from the following raw materials in parts by mass: grape seed oil: 35-45 parts of a solvent; sunflower seed oil: 25-35 parts; mountain golden car oil: 10-20 parts; sesame oil: 5-9 parts of a solvent; ligusticum wallichii: 1-3 parts; notopterygium root: 0.7-1.5 parts; radix angelicae pubescentis: 0.7-1.5 parts; wind prevention: 0.7-1.5 parts; chinese angelica: 0.7-1.5 parts; pseudo-ginseng: 0.7-1.5 parts; white peony root: 0.7-1.5 parts; licorice root: 0.3-0.7 part; herba schizonepetae: 0.3-0.7 part; vitamin E: 0.05 to 0.15 portion.
Further preferably, the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstructing collaterals is prepared from the following raw materials in parts by mass: grape seed oil: 40 parts of a mixture; sunflower seed oil: 30 parts of (1); mountain golden car oil: 15 parts of (1); sesame oil: 6 parts of (1); ligusticum wallichii: 2 parts of (1); notopterygium root: 1 part; radix angelicae pubescentis: 1 part; wind prevention: 1 part; chinese angelica: 1 part; pseudo-ginseng: 1 part; white peony root: 1 part; licorice root: 0.5 part; herba schizonepetae: 0.5 part; vitamin E: 0.1 part.
Preferably, the grape seed oil is prepared by cold-pressing and primary pressing of grape seeds.
Preferably, the sunflower seed oil is prepared by cold pressing and primary pressing of sunflower seeds.
Preferably, the arnica oil is prepared by soaking and extracting arnica.
Preferably, the sesame oil is prepared by cold-pressing and primary pressing of sesame seeds.
The preparation method of the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstruction of collaterals comprises the following steps:
1) cleaning rhizoma Ligustici Chuanxiong, Notopterygii rhizoma, radix Angelicae Pubescentis, radix Saposhnikoviae, radix Angelicae sinensis, Notoginseng radix, radix Paeoniae alba, Glycyrrhrizae radix and herba Schizonepetae, drying and pulverizing to obtain rhizoma Ligustici Chuanxiong powder, Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Angelicae sinensis powder, Notoginseng radix powder, radix Paeoniae alba powder, Glycyrrhrizae radix powder and herba Schizonepetae powder;
2) respectively performing supercritical extraction on rhizoma Ligustici Chuanxiong powder, Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Angelicae sinensis powder, Notoginseng radix powder, radix Paeoniae alba powder and herba Schizonepetae powder to obtain rhizoma Ligustici Chuanxiong essential oil, Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Angelicae sinensis essential oil, Notoginseng radix essential oil, radix Paeoniae alba essential oil and herba Schizonepetae essential oil, and distilling Glycyrrhrizae radix powder to obtain Glycyrrhrizae radix essential oil;
3) adding grape seed oil, sunflower seed oil, arnica oil and sesame oil into a stirrer, and stirring;
4) adding rhizoma Ligustici Chuanxiong essential oil, Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Angelicae sinensis essential oil, Notoginseng radix essential oil, radix Paeoniae alba essential oil, herba Schizonepetae essential oil and Glycyrrhrizae radix essential oil into a blender, and stirring;
5) adding vitamin E into a stirrer, and stirring to obtain the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstruction of collaterals.
Preferably, the drying mode in the step 1) is natural air drying.
Preferably, the particle size of the ligusticum wallichii powder, the notopterygium root powder, the radix angelicae pubescentis powder, the radix sileris powder, the angelica sinensis powder, the panax notoginseng powder, the radix paeoniae alba powder, the liquorice powder and the schizonepeta powder in the step 1) is less than 0.5 mm.
Preferably, the supercritical extraction in step 2) is supercritical carbon dioxide fluid extraction.
Preferably, the supercritical carbon dioxide fluid extraction is carried out under the conditions of the pressure of 15-25 MPa and the temperature of 35-40 ℃.
Preferably, the rotation speed of the stirrer during stirring in the steps 3) to 5) is 1500-3000 r/min.
The invention has the beneficial effects that: the massage essential oil disclosed by the invention has a good effect of relieving muscle strain by combining with a proper massage manipulation, can also relieve exterior syndrome, dispel cold, expel wind, relieve exterior syndrome, remove blood stasis, activate blood circulation, relieve pain and strengthen tendons and bones, is particularly suitable for people with the constitution of blocking collaterals by wind-cold, accords with the principle of traditional Chinese medicine, and has the advantages of simple preparation process and no toxic or side effect.
Specifically, the method comprises the following steps:
1) the grape seed oil, the sunflower seed oil, the arnica oil and the sesame oil are compounded to be used as base oil, the grape seed oil, the sunflower seed oil and the sesame oil are rich in components such as oleic acid, unsaturated fatty acid, vitamin and the like, the arnica oil is rich in components such as thymol, sesquiterpene lactone, arnica oil, flavonoid, polysaccharide and the like, and the 4-component compounding can activate cells, promote skin metabolism and relieve inflammatory reaction of skin and muscle joints;
2) the formula is designed based on the principle of traditional Chinese medicine, and the medicine components for relieving exterior syndrome, dispelling cold, expelling wind, relieving exterior syndrome, removing blood stasis, activating blood circulation, relieving pain and strengthening muscles and bones are added, so that the functional components are various, the muscle strain relieving effect is good, and the multifunctional effects are achieved;
3) the invention mainly adopts cold pressing preliminary pressing, soaking extraction and supercritical extraction to extract the functional components, and can effectively avoid the problem of decomposition of the functional components caused by high-temperature extraction.
Detailed Description
The invention will be further explained and illustrated with reference to specific examples.
Example 1:
the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold collateral obstruction is prepared from the following raw materials in parts by mass: grape seed oil: 35 parts of (B); sunflower seed oil: 27 parts of (1); mountain golden car oil: 8 parts of a mixture; sesame oil: 10 parts of (A); ligusticum wallichii: 0.7 part; notopterygium root: 0.7 part; radix angelicae pubescentis: 0.8 part; wind prevention: 0.7 part; chinese angelica: 0.6 part; pseudo-ginseng: 0.7 part; white peony root: 0.8 part; licorice root: 0.1 part; herba schizonepetae: 0.08 part; vitamin E: 0.09 part.
The preparation method of the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstruction of collaterals comprises the following steps:
1) cleaning rhizoma Ligustici Chuanxiong rhizome, Notopterygii rhizoma rhizome, radix Angelicae Pubescentis root, radix Saposhnikoviae root, radix Angelicae sinensis rhizome, Notoginseng radix root, radix Paeoniae alba root, Glycyrrhrizae radix rhizome and herba Schizonepetae whole plant respectively, air drying naturally and pulverizing to obtain rhizoma Ligustici Chuanxiong powder, Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Angelicae sinensis powder, Notoginseng radix powder, radix Paeoniae alba powder, Glycyrrhrizae radix powder and herba Schizonepetae powder with particle diameter less than 0.5 mm;
2) respectively extracting rhizoma Ligustici Chuanxiong powder, Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Angelicae sinensis powder, Notoginseng radix powder, radix Paeoniae alba powder and herba Schizonepetae powder with supercritical carbon dioxide fluid (pressure 20MPa, temperature 40 deg.C) to obtain rhizoma Ligustici Chuanxiong essential oil, Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Angelicae sinensis essential oil, Notoginseng radix essential oil, radix Paeoniae alba essential oil and herba Schizonepetae essential oil, and distilling Glycyrrhrizae radix powder with water to obtain Glycyrrhrizae radix essential oil;
3) adding grape seed oil, sunflower seed oil, Arnica oil and sesame oil into a stirrer, adjusting the rotation speed of the stirrer to 1800r/min, and stirring for 4 min;
4) adding rhizoma Ligustici Chuanxiong essential oil, Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Angelicae sinensis essential oil, Notoginseng radix essential oil, radix Paeoniae alba essential oil, herba Schizonepetae essential oil and Glycyrrhrizae radix essential oil into a blender, adjusting the rotation speed of the blender to 1800r/min, and stirring for 4 min;
5) adding vitamin E into a stirrer, adjusting the rotating speed of the stirrer to 1800r/min, and stirring for 5min to obtain the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstruction of collaterals.
Example 2:
the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold collateral obstruction is prepared from the following raw materials in parts by mass: grape seed oil: 41 parts of (1); sunflower seed oil: 35 parts of (B); mountain golden car oil: 10 parts of (A); sesame oil: 13 parts; ligusticum wallichii: 2.2 parts of; notopterygium root: 1.4 parts; radix angelicae pubescentis: 1.2 parts; wind prevention: 1.3 parts; chinese angelica: 1.6 parts; pseudo-ginseng: 1.6 parts; white peony root: 1.1 parts; licorice root: 1.3 parts; herba schizonepetae: 1.3 parts; vitamin E: 0.15 part.
The preparation method of the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstruction of collaterals comprises the following steps:
1) cleaning rhizoma Ligustici Chuanxiong rhizome, Notopterygii rhizoma rhizome, radix Angelicae Pubescentis root, radix Saposhnikoviae root, radix Angelicae sinensis rhizome, Notoginseng radix root, radix Paeoniae alba root, Glycyrrhrizae radix rhizome and herba Schizonepetae whole plant respectively, air drying naturally and pulverizing to obtain rhizoma Ligustici Chuanxiong powder, Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Angelicae sinensis powder, Notoginseng radix powder, radix Paeoniae alba powder, Glycyrrhrizae radix powder and herba Schizonepetae powder with particle diameter less than 0.5 mm;
2) respectively extracting rhizoma Ligustici Chuanxiong powder, Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Angelicae sinensis powder, Notoginseng radix powder, radix Paeoniae alba powder and herba Schizonepetae powder with supercritical carbon dioxide fluid (pressure 20MPa, temperature 40 deg.C) to obtain rhizoma Ligustici Chuanxiong essential oil, Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Angelicae sinensis essential oil, Notoginseng radix essential oil, radix Paeoniae alba essential oil and herba Schizonepetae essential oil, and distilling Glycyrrhrizae radix powder with water to obtain Glycyrrhrizae radix essential oil;
3) adding grape seed oil, sunflower seed oil, Arnica oil and sesame oil into a stirrer, adjusting the rotation speed of the stirrer to 1800r/min, and stirring for 4 min;
4) adding rhizoma Ligustici Chuanxiong essential oil, Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Angelicae sinensis essential oil, Notoginseng radix essential oil, radix Paeoniae alba essential oil, herba Schizonepetae essential oil and Glycyrrhrizae radix essential oil into a blender, adjusting the rotation speed of the blender to 1800r/min, and stirring for 4 min;
5) adding vitamin E into a stirrer, adjusting the rotating speed of the stirrer to 1800r/min, and stirring for 5min to obtain the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstruction of collaterals.
Example 3:
the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold collateral obstruction is prepared from the following raw materials in parts by mass: grape seed oil: 40 parts of a mixture; sunflower seed oil: 30 parts of (1); mountain golden car oil: 15 parts of (1); sesame oil: 6 parts of (1); ligusticum wallichii: 2 parts of (1); notopterygium root: 1 part; radix angelicae pubescentis: 1 part; wind prevention: 1 part; chinese angelica: 1 part; pseudo-ginseng: 1 part; white peony root: 1 part; licorice root: 0.5 part; herba schizonepetae: 0.5 part; vitamin E: 0.1 part.
The preparation method of the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstruction of collaterals comprises the following steps:
1) cleaning rhizoma Ligustici Chuanxiong rhizome, Notopterygii rhizoma rhizome, radix Angelicae Pubescentis root, radix Saposhnikoviae root, radix Angelicae sinensis rhizome, Notoginseng radix root, radix Paeoniae alba root, Glycyrrhrizae radix rhizome and herba Schizonepetae whole plant respectively, air drying naturally and pulverizing to obtain rhizoma Ligustici Chuanxiong powder, Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Angelicae sinensis powder, Notoginseng radix powder, radix Paeoniae alba powder, Glycyrrhrizae radix powder and herba Schizonepetae powder with particle diameter less than 0.5 mm;
2) respectively extracting rhizoma Ligustici Chuanxiong powder, Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Angelicae sinensis powder, Notoginseng radix powder, radix Paeoniae alba powder and herba Schizonepetae powder with supercritical carbon dioxide fluid (pressure 20MPa, temperature 40 deg.C) to obtain rhizoma Ligustici Chuanxiong essential oil, Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Angelicae sinensis essential oil, Notoginseng radix essential oil, radix Paeoniae alba essential oil and herba Schizonepetae essential oil, and distilling Glycyrrhrizae radix powder with water to obtain Glycyrrhrizae radix essential oil;
3) adding grape seed oil, sunflower seed oil, Arnica oil and sesame oil into a stirrer, adjusting the rotation speed of the stirrer to 1800r/min, and stirring for 4 min;
4) adding rhizoma Ligustici Chuanxiong essential oil, Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Angelicae sinensis essential oil, Notoginseng radix essential oil, radix Paeoniae alba essential oil, herba Schizonepetae essential oil and Glycyrrhrizae radix essential oil into a blender, adjusting the rotation speed of the blender to 1800r/min, and stirring for 4 min;
5) adding vitamin E into a stirrer, adjusting the rotating speed of the stirrer to 1800r/min, and stirring for 5min to obtain the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstruction of collaterals.
Example 4:
the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold collateral obstruction is prepared from the following raw materials in parts by mass: grape seed oil: 37 parts of; sunflower seed oil: 31 parts of (B); mountain golden car oil: 11 parts of (1); sesame oil: 9 parts of (1); ligusticum wallichii: 1.1 parts; notopterygium root: 0.7 part; radix angelicae pubescentis: 0.9 part; wind prevention: 1 part; chinese angelica: 1 part; pseudo-ginseng: 1.1 parts; white peony root: 0.6 part; licorice root: 0.1 part; herba schizonepetae: 0.06 part; vitamin E: 0.1 part.
The preparation method of the massage essential oil for the wind-cold arthralgia type physique comprises the following steps:
1) cleaning rhizoma Ligustici Chuanxiong rhizome, Notopterygii rhizoma rhizome, radix Angelicae Pubescentis root, radix Saposhnikoviae root, radix Angelicae sinensis rhizome, Notoginseng radix root, radix Paeoniae alba root, Glycyrrhrizae radix rhizome and herba Schizonepetae whole plant respectively, air drying naturally and pulverizing to obtain rhizoma Ligustici Chuanxiong powder, Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Angelicae sinensis powder, Notoginseng radix powder, radix Paeoniae alba powder, Glycyrrhrizae radix powder and herba Schizonepetae powder with particle diameter less than 0.5 mm;
2) respectively extracting rhizoma Ligustici Chuanxiong powder, Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Angelicae sinensis powder, Notoginseng radix powder, radix Paeoniae alba powder and herba Schizonepetae powder with supercritical carbon dioxide fluid (pressure 20MPa, temperature 40 deg.C) to obtain rhizoma Ligustici Chuanxiong essential oil, Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Angelicae sinensis essential oil, Notoginseng radix essential oil, radix Paeoniae alba essential oil and herba Schizonepetae essential oil, and distilling Glycyrrhrizae radix powder with water to obtain Glycyrrhrizae radix essential oil;
3) adding grape seed oil, sunflower seed oil, Arnica oil and sesame oil into a stirrer, adjusting the rotation speed of the stirrer to 1800r/min, and stirring for 4 min;
4) adding rhizoma Ligustici Chuanxiong essential oil, Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Angelicae sinensis essential oil, Notoginseng radix essential oil, radix Paeoniae alba essential oil, herba Schizonepetae essential oil and Glycyrrhrizae radix essential oil into a blender, adjusting the rotation speed of the blender to 1800r/min, and stirring for 4 min;
5) adding vitamin E into a stirrer, adjusting the rotating speed of the stirrer to 1800r/min, and stirring for 5min to obtain the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstruction of collaterals.
Example 5:
the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold collateral obstruction is prepared from the following raw materials in parts by mass: grape seed oil: 39 parts of a mixture; sunflower seed oil: 37 parts of; mountain golden car oil: 8 parts of a mixture; sesame oil: 12 parts of (1); ligusticum wallichii: 2.8 parts; notopterygium root: 1.7 parts; radix angelicae pubescentis: 1.6 parts; wind prevention: 1.1 parts; chinese angelica: 0.9 part; pseudo-ginseng: 1.4 parts; white peony root: 1.9 parts; licorice root: 0.9 part; herba schizonepetae: 1.4 parts; vitamin E: 0.13 part.
The preparation method of the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstruction of collaterals comprises the following steps:
1) cleaning rhizoma Ligustici Chuanxiong rhizome, Notopterygii rhizoma rhizome, radix Angelicae Pubescentis root, radix Saposhnikoviae root, radix Angelicae sinensis rhizome, Notoginseng radix root, radix Paeoniae alba root, Glycyrrhrizae radix rhizome and herba Schizonepetae whole plant respectively, air drying naturally and pulverizing to obtain rhizoma Ligustici Chuanxiong powder, Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Angelicae sinensis powder, Notoginseng radix powder, radix Paeoniae alba powder, Glycyrrhrizae radix powder and herba Schizonepetae powder with particle diameter less than 0.5 mm;
2) respectively extracting rhizoma Ligustici Chuanxiong powder, Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Angelicae sinensis powder, Notoginseng radix powder, radix Paeoniae alba powder and herba Schizonepetae powder with supercritical carbon dioxide fluid (pressure 20MPa, temperature 40 deg.C) to obtain rhizoma Ligustici Chuanxiong essential oil, Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Angelicae sinensis essential oil, Notoginseng radix essential oil, radix Paeoniae alba essential oil and herba Schizonepetae essential oil, and distilling Glycyrrhrizae radix powder with water to obtain Glycyrrhrizae radix essential oil;
3) adding grape seed oil, sunflower seed oil, Arnica oil and sesame oil into a stirrer, adjusting the rotation speed of the stirrer to 1800r/min, and stirring for 4 min;
4) adding rhizoma Ligustici Chuanxiong essential oil, Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Angelicae sinensis essential oil, Notoginseng radix essential oil, radix Paeoniae alba essential oil, herba Schizonepetae essential oil and Glycyrrhrizae radix essential oil into a blender, adjusting the rotation speed of the blender to 1800r/min, and stirring for 4 min;
5) adding vitamin E into a stirrer, adjusting the rotating speed of the stirrer to 1800r/min, and stirring for 5min to obtain the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstruction of collaterals.
Comparative example 1:
the massage essential oil is prepared from the following raw materials in parts by mass: grape seed oil: 35 parts of (B); sunflower seed oil: 32 parts of (1); mountain golden car oil: 13 parts; sesame oil: 7 parts; ligusticum wallichii: 0.5 part; notopterygium root: 0.3 part; radix angelicae pubescentis: 0.3 part; wind prevention: 0.4 part; chinese angelica: 0.3 part; pseudo-ginseng: 0.4 part; white peony root: 0.3 part; licorice root: 0.02 part; herba schizonepetae: 0.03 part; vitamin E: 0.08 portion.
The preparation method of the massage essential oil comprises the following steps:
1) cleaning rhizoma Ligustici Chuanxiong rhizome, Notopterygii rhizoma rhizome, radix Angelicae Pubescentis root, radix Saposhnikoviae root, radix Angelicae sinensis rhizome, Notoginseng radix root, radix Paeoniae alba root, Glycyrrhrizae radix rhizome and herba Schizonepetae whole plant respectively, air drying naturally and pulverizing to obtain rhizoma Ligustici Chuanxiong powder, Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Angelicae sinensis powder, Notoginseng radix powder, radix Paeoniae alba powder, Glycyrrhrizae radix powder and herba Schizonepetae powder with particle diameter less than 0.5 mm;
2) respectively extracting rhizoma Ligustici Chuanxiong powder, Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Angelicae sinensis powder, Notoginseng radix powder, radix Paeoniae alba powder and herba Schizonepetae powder with supercritical carbon dioxide fluid (pressure 20MPa, temperature 40 deg.C) to obtain rhizoma Ligustici Chuanxiong essential oil, Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Angelicae sinensis essential oil, Notoginseng radix essential oil, radix Paeoniae alba essential oil and herba Schizonepetae essential oil, and distilling Glycyrrhrizae radix powder with water to obtain Glycyrrhrizae radix essential oil;
3) adding grape seed oil, sunflower seed oil, Arnica oil and sesame oil into a stirrer, adjusting the rotation speed of the stirrer to 1800r/min, and stirring for 4 min;
4) adding rhizoma Ligustici Chuanxiong essential oil, Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Angelicae sinensis essential oil, Notoginseng radix essential oil, radix Paeoniae alba essential oil, herba Schizonepetae essential oil and Glycyrrhrizae radix essential oil into a blender, adjusting the rotation speed of the blender to 1800r/min, and stirring for 4 min;
5) adding vitamin E into a stirrer, adjusting the rotation speed of the stirrer to 1800r/min, and stirring for 5min to obtain massage essential oil.
Comparative example 2:
the massage essential oil is prepared from the following raw materials in parts by mass: grape seed oil: 37 parts of; sunflower seed oil: 32 parts of (1); mountain golden car oil: 9 parts of (1); sesame oil: 10 parts of (A); ligusticum wallichii: 3.1 parts; notopterygium root: 2.3 parts of a mixture; radix angelicae pubescentis: 2.2 parts of; wind prevention: 2.3 parts of a mixture; chinese angelica: 2.3 parts of a mixture; pseudo-ginseng: 2.2 parts of; white peony root: 2.1 parts; licorice root: 1.4 parts; herba schizonepetae: 1.4 parts; vitamin E: 0.21 part.
The preparation method of the massage essential oil comprises the following steps:
1) cleaning rhizoma Ligustici Chuanxiong rhizome, Notopterygii rhizoma rhizome, radix Angelicae Pubescentis root, radix Saposhnikoviae root, radix Angelicae sinensis rhizome, Notoginseng radix root, radix Paeoniae alba root, Glycyrrhrizae radix rhizome and herba Schizonepetae whole plant respectively, air drying naturally and pulverizing to obtain rhizoma Ligustici Chuanxiong powder, Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Angelicae sinensis powder, Notoginseng radix powder, radix Paeoniae alba powder, Glycyrrhrizae radix powder and herba Schizonepetae powder with particle diameter less than 0.5 mm;
2) respectively extracting rhizoma Ligustici Chuanxiong powder, Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Angelicae sinensis powder, Notoginseng radix powder, radix Paeoniae alba powder and herba Schizonepetae powder with supercritical carbon dioxide fluid (pressure 20MPa, temperature 40 deg.C) to obtain rhizoma Ligustici Chuanxiong essential oil, Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Angelicae sinensis essential oil, Notoginseng radix essential oil, radix Paeoniae alba essential oil and herba Schizonepetae essential oil, and distilling Glycyrrhrizae radix powder with water to obtain Glycyrrhrizae radix essential oil;
3) adding grape seed oil, sunflower seed oil, Arnica oil and sesame oil into a stirrer, adjusting the rotation speed of the stirrer to 1800r/min, and stirring for 4 min;
4) adding rhizoma Ligustici Chuanxiong essential oil, Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Angelicae sinensis essential oil, Notoginseng radix essential oil, radix Paeoniae alba essential oil, herba Schizonepetae essential oil and Glycyrrhrizae radix essential oil into a blender, adjusting the rotation speed of the blender to 1800r/min, and stirring for 4 min;
5) adding vitamin E into a stirrer, adjusting the rotation speed of the stirrer to 1800r/min, and stirring for 5min to obtain massage essential oil.
Comparative example 3:
jingtongling (Jilin Wantong pharmaceutical Co., Ltd.).
Comparative example 4:
the massage essential oil is prepared from the following raw materials in parts by mass: grape seed oil: 40 parts of a mixture; sunflower seed oil: 30 parts of (1); mountain golden car oil: 15 parts of (1); sesame oil: 6 parts of (1); notopterygium root: 1 part; radix angelicae pubescentis: 1 part; wind prevention: 1 part; white peony root: 1 part; licorice root: 0.5 part; herba schizonepetae: 0.5 part; vitamin E: 0.1 part.
The preparation method of the massage essential oil comprises the following steps:
1) respectively cleaning rhizome of Notopterygii rhizoma, radix Angelicae Pubescentis, radix Saposhnikoviae, radix Paeoniae alba, Glycyrrhrizae radix and herba Schizonepetae, air drying, and pulverizing to obtain Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Paeoniae alba powder, Glycyrrhrizae radix powder and herba Schizonepetae powder with particle size less than 0.5 mm;
2) respectively extracting Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Paeoniae alba powder, Glycyrrhrizae radix powder and herba Schizonepetae powder with supercritical carbon dioxide fluid (pressure 20MPa, temperature 40 deg.C) to obtain Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Paeoniae alba essential oil and herba Schizonepetae essential oil, and distilling Glycyrrhrizae radix powder with water to obtain Glycyrrhrizae radix essential oil;
3) adding grape seed oil, sunflower seed oil, Arnica oil and sesame oil into a stirrer, adjusting the rotation speed of the stirrer to 1800r/min, and stirring for 4 min;
4) adding Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Paeoniae alba essential oil, herba Schizonepetae essential oil and Glycyrrhrizae radix essential oil into a blender, adjusting the rotation speed of the blender to 1800r/min, and stirring for 4 min;
5) adding vitamin E into a stirrer, adjusting the rotation speed of the stirrer to 1800r/min, and stirring for 5min to obtain massage essential oil.
Note:
the grape seed oil in the above examples and comparative examples was prepared from grape seeds by cold pressing and preliminary pressing;
the sunflower seed oil in the above examples and comparative examples was prepared from sunflower seeds by cold pressing and preliminary pressing;
the arnica oil in the above examples and comparative examples is prepared by soaking and extracting arnica;
the sesame oil in the above examples and comparative examples was prepared from sesame seeds by cold-pressing preliminary pressing.
And (3) performance testing:
1) selecting 180 neck and shoulder strain patients (excluding patients with more basic diseases, age greater than 65 years and existing suspicious drug allergy history) conforming to wind-cold collateral obstruction physique, dividing into 9 groups at random, carrying out massage on the first 8 groups by special people by using the same massage manipulation in combination with the massage essential oils of examples 1-5, comparative examples 1-2 and comparative example 4 for 1 time every day for 45min, wherein the treatment course is 3 days, the 9 th group takes the cervicodynia remedy of comparative example 3 (after meals) and takes 15-20 mL every time for 3 times every day, the treatment course is 3 days, and then evaluating the treatment effect, and the evaluation result of the treatment effect is shown in the following table:
TABLE 1 evaluation results of therapeutic effects
Figure BDA0002580846000000091
Note:
the therapeutic effect judgment standard of neck and shoulder strain is as follows:
and (3) curing: compared with the treatment before, the positive symptoms disappear completely, the pain disappears, and the neck and shoulder joints move normally;
improvement: compared with the treatment before, the positive symptoms basically disappear, the pain basically disappears, and the neck-shoulder joint movement is basically normal;
and (4) invalidation: compared with the treatment before, the positive symptoms are not obviously improved, the pain is still obvious, and the neck and shoulder joint movement is still obviously obstructed.
Effective rate (%) - (number of cured cases + number of improved cases)/total number of people per group × 100%.
As can be seen from Table 1: compared with the comparative example 1, the analysis of the example 1 shows that when the proportion of the raw materials is lower than the protection range, the curative effect is obviously reduced, and the difference has statistical significance (P is less than 0.01); compared with the comparative example 2, the analysis of the example 2 and the comparative example 2 shows that when the proportion of the raw materials is higher than the protection range, the curative effect is obviously reduced, and the difference has statistical significance (P is less than 0.05); compared with the comparative example 3, the analysis of the example 3 and the comparative example 3 shows that when the mixture ratio of the raw materials is in the optimal matching, the curative effect is higher than that of the current common treatment mode, and the difference has statistical significance (P is less than 0.01); compared with the comparative example 4, the analysis of the example 3 shows that the effective rate is obviously reduced after the core components are removed, and the difference has statistical significance (P is less than 0.01).
Therefore, the massage essential oil has excellent repair treatment effect on neck and shoulder strain, has a curative effect obviously superior to that of a common oral analgesic drug treatment mode, and is particularly suitable for neck and shoulder strain patients with wind-cold arthralgia type physique.
2) Typical cases are as follows:
case 1: a patient, 34 years old, has shoulder pain of 1 month, is obvious after fatigue, has repeated attacks, can get better after rest, has the symptoms of shoulder and neck muscle tension, has obvious thirst, has upper limb traction pain on one side, can be seen through physical examination, has the symptoms of shoulder and neck muscle tension, slight tenderness of cervical vertebra, red tongue, white fur and tight pulse. The subjective symptoms are relieved obviously after the treatment by using 10mL of massage essential oil of the example 3 and proper massage manipulation to massage the neck and the shoulder for 3 days. Can reach the standard of cure.
Case 2: patients, women, 48 years old, had repeated neck pain with upper limb traction pain on both sides for 3 months, the pain often appeared after work, the rest was slightly relieved, the body was examined to see that the neck and shoulder muscles were tense, the neck and shoulder had light pressure pain, the tongue was pale red, the tongue was white, and the pulse was tight. The subjective symptoms are relieved obviously after the treatment by using 10mL of massage essential oil of the example 3 and proper massage manipulation to massage the neck and the shoulder for 3 days. Can reach the standard of cure.
The above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such changes, modifications, substitutions, combinations, and simplifications are intended to be included in the scope of the present invention.

Claims (10)

1. The neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstructing collaterals is characterized by comprising the following components in parts by weight: comprises base oil, Chinese medicinal components and vitamin E; the base oil comprises grape seed oil, sunflower seed oil, arnica oil and sesame oil; the Chinese medicinal components comprise rhizoma Ligustici Chuanxiong, Notopterygii rhizoma, radix Angelicae Pubescentis, radix Saposhnikoviae, radix Angelicae sinensis, Notoginseng radix, radix Paeoniae alba, Glycyrrhrizae radix and herba Schizonepetae.
2. The neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstruction in collaterals as claimed in claim 1, which is characterized in that: the feed is prepared from the following raw materials in parts by mass: grape seed oil: 30-50 parts of a solvent; sunflower seed oil: 20-40 parts of a solvent; mountain golden car oil: 5-25 parts; sesame oil: 5-15 parts of a solvent; ligusticum wallichii: 0.5-3 parts; notopterygium root: 0.5-2 parts; radix angelicae pubescentis: 0.5-2 parts; wind prevention: 0.5-2 parts; chinese angelica: 0.5-2 parts; pseudo-ginseng: 0.5-2 parts; white peony root: 0.5-2 parts; licorice root: 0.05-1.5 parts; herba schizonepetae: 0.05-1.5 parts; vitamin E: 0.05 to 0.2 portion.
3. The neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstruction of collaterals as claimed in claim 2, which is characterized in that: the feed is prepared from the following raw materials in parts by mass: grape seed oil: 40 parts of a mixture; sunflower seed oil: 30 parts of (1); mountain golden car oil: 15 parts of (1); sesame oil: 6 parts of (1); ligusticum wallichii: 2 parts of (1); notopterygium root: 1 part; radix angelicae pubescentis: 1 part; wind prevention: 1 part; chinese angelica: 1 part; pseudo-ginseng: 1 part; white peony root: 1 part; licorice root: 0.5 part; herba schizonepetae: 0.5 part; vitamin E: 0.1 part.
4. The neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstructing collaterals as claimed in any one of claims 1-3, characterized in that: the grape seed oil is prepared from grape seeds through cold pressing and preliminary pressing.
5. The neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstructing collaterals as claimed in any one of claims 1-3, characterized in that: the sunflower seed oil is prepared by cold pressing and primary pressing of sunflower seeds.
6. The neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstructing collaterals as claimed in any one of claims 1-3, characterized in that: the arnica oil is prepared by soaking and extracting arnica.
7. The neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstructing collaterals as claimed in any one of claims 1-3, characterized in that: the sesame oil is prepared from sesame seeds by cold pressing and preliminary pressing.
8. The preparation method of the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstructing collaterals as claimed in any one of claims 1 to 7, characterized by comprising the following steps: the method comprises the following steps:
1) cleaning rhizoma Ligustici Chuanxiong, Notopterygii rhizoma, radix Angelicae Pubescentis, radix Saposhnikoviae, radix Angelicae sinensis, Notoginseng radix, radix Paeoniae alba, Glycyrrhrizae radix and herba Schizonepetae, drying and pulverizing to obtain rhizoma Ligustici Chuanxiong powder, Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Angelicae sinensis powder, Notoginseng radix powder, radix Paeoniae alba powder, Glycyrrhrizae radix powder and herba Schizonepetae powder;
2) respectively performing supercritical extraction on rhizoma Ligustici Chuanxiong powder, Notopterygii rhizoma powder, radix Angelicae Pubescentis powder, radix Saposhnikoviae powder, radix Angelicae sinensis powder, Notoginseng radix powder, radix Paeoniae alba powder and herba Schizonepetae powder to obtain rhizoma Ligustici Chuanxiong essential oil, Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Angelicae sinensis essential oil, Notoginseng radix essential oil, radix Paeoniae alba essential oil and herba Schizonepetae essential oil, and distilling Glycyrrhrizae radix powder to obtain Glycyrrhrizae radix essential oil;
3) adding grape seed oil, sunflower seed oil, arnica oil and sesame oil into a stirrer, and stirring;
4) adding rhizoma Ligustici Chuanxiong essential oil, Notopterygii rhizoma essential oil, radix Angelicae Pubescentis essential oil, radix Saposhnikoviae essential oil, radix Angelicae sinensis essential oil, Notoginseng radix essential oil, radix Paeoniae alba essential oil, herba Schizonepetae essential oil and Glycyrrhrizae radix essential oil into a blender, and stirring;
5) adding vitamin E into a stirrer, and stirring to obtain the neck and shoulder strain rehabilitation essential oil for the physique of wind-cold obstruction of collaterals.
9. The method of claim 8, wherein: and 2) the supercritical extraction is supercritical carbon dioxide fluid extraction.
10. The production method according to claim 8 or 9, characterized in that: the rotating speed of the stirrer during stirring in the steps 3) to 5) is 1500-3000 r/min.
CN202010666991.2A 2020-07-13 2020-07-13 Neck and shoulder strain rehabilitation essential oil for physique of wind-cold obstructing collaterals and preparation method thereof Pending CN111588781A (en)

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Application publication date: 20200828