CN111534729A - Control method for transverse unevenness of high-strength aluminum alloy plate - Google Patents

Control method for transverse unevenness of high-strength aluminum alloy plate Download PDF

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CN111534729A
CN111534729A CN202010531157.2A CN202010531157A CN111534729A CN 111534729 A CN111534729 A CN 111534729A CN 202010531157 A CN202010531157 A CN 202010531157A CN 111534729 A CN111534729 A CN 111534729A
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plate
quenching
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aluminum alloy
unevenness
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CN111534729B (en
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李红萍
王凤春
章骏
吕新宇
王大伟
王旭
任伟才
王洪伍
金梅
张祥斌
吴沂哲
于莉莉
韩颖
左德运
藏家吉
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Comac Shanghai Aircraft Design & Research Institute
Northeast Light Alloy Co Ltd
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Comac Shanghai Aircraft Design & Research Institute
Northeast Light Alloy Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C21/00Alloys based on aluminium
    • C22C21/10Alloys based on aluminium with zinc as the next major constituent
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21CMANUFACTURE OF METAL SHEETS, WIRE, RODS, TUBES OR PROFILES, OTHERWISE THAN BY ROLLING; AUXILIARY OPERATIONS USED IN CONNECTION WITH METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL
    • B21C37/00Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape
    • B21C37/02Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape of sheets
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C1/00Making non-ferrous alloys
    • C22C1/02Making non-ferrous alloys by melting
    • C22C1/026Alloys based on aluminium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C1/00Making non-ferrous alloys
    • C22C1/02Making non-ferrous alloys by melting
    • C22C1/03Making non-ferrous alloys by melting using master alloys
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/002Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working by rapid cooling or quenching; cooling agents used therefor
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/04Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon
    • C22F1/053Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon of alloys with zinc as the next major constituent

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  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Straightening Metal Sheet-Like Bodies (AREA)
  • Metal Rolling (AREA)

Abstract

A method for controlling the transverse unevenness of a high-strength aluminum alloy plate relates to a technology for controlling the transverse unevenness of an aluminum alloy plate, and aims to solve the problem that the flatness of the conventional aluminum alloy plate cannot meet the requirement of being applied to a specific wing panel. The invention controls the direction and the size of the roll bending force of the rolling mill in the plate rolling process, controls the quenching water amount in the processes of roll straightening of the hot rolled plate before solid solution and cooling after solid solution so as to ensure uniform stress distribution of the quenched plate and reduce quenching deformation, and optimizes quenching parameters according to the test result of the residual stress of the plate after quenching so as to achieve the balanced control of the quenching stress of the plate and the action of the supporting force of a cross beam of a stretcher properly in the plate stretching process and improve the transverse flatness of the stretched plate. The transverse unevenness of the plate meets the ANSI H35.2 standard and meets the requirements of part processing and manufacturing.

Description

Control method for transverse unevenness of high-strength aluminum alloy plate
Technical Field
The invention relates to a technology for controlling the transverse unevenness of an aluminum alloy plate.
Background
The Al-Zn-Mg-Cu alloy belongs to a typical high-strength alloy in aluminum alloys, can be strengthened by heat treatment, and has the advantages of high strength, high toughness, good corrosion resistance, high specific strength, specific rigidity and the like; the alloy plates with different heat treatment states are widely applied to the field of aerospace as main structural materials; the width of the aluminum alloy plate which is produced at present and is installed and applied is basically below 2000mm, 2500mm ultra-wide plates are few, the flatness of the plate is a key index in the application process of the plate, the flatness of a plurality of large-size ultra-wide plates often meets the standard specification of materials but does not meet the processing conditions of parts, and installation and application of the plate cannot be achieved, so that the process of conversion of a plurality of research and development results and application of the plate are limited.
Disclosure of Invention
The invention aims to solve the problem that the flatness of the existing aluminum alloy plate cannot meet the requirement of being applied to a specific wing panel, and provides a method for controlling the transverse unevenness of a high-strength aluminum alloy plate.
The invention relates to a method for controlling the transverse unevenness of a high-strength aluminum alloy plate, which comprises the following steps of:
step one, according to the mass percentage of elements, Si is less than or equal to 0.10 percent, Fe is less than or equal to 0.15 percent, Cu: 2.0-2.6%, Mn less than or equal to 0.10%, Mg: 1.8-2.3%, Cr is less than or equal to 0.04%, Zn: 7.6-8.4%, Ti is less than or equal to 0.06%, Zr: 0.08 to 0.18 percent of Al and the balance of Al, weighing cathode copper, zinc ingots, primary magnesium ingots, aluminum-titanium intermediate alloys, aluminum-zirconium intermediate alloys and aluminum ingots, then adding the cathode copper, zinc ingots, primary magnesium ingots, aluminum-titanium intermediate alloys, aluminum-zirconium intermediate alloys and aluminum ingots into a dry smelting furnace, smelting, then casting into ingots with the specification of 420 multiplied by 1320 multiplied by 2000mm, 420 multiplied by 1620 multiplied by 2500mm or 450 multiplied by 1880 multiplied by 2100mm, and then carrying out homogenization annealing, face milling and saw cutting to obtain finished plate ingots;
step two, putting the finished plate ingot blank obtained in the step one into a resistance heating furnace, heating to 360-420 ℃, preserving heat for 8-13 hours, and then carrying out hot rolling on the finished plate ingot blank to obtain a prefabricated hot rolled plate;
thirdly, sawing the prefabricated hot rolled plate obtained in the second step, then placing the prefabricated hot rolled plate into a straightening machine for roll straightening, and adjusting the roll gap interval of the straightening machine to enable the transverse unevenness of the plate after roll straightening to be 5mm/2500 mm;
step four, carrying out solution treatment on the plate obtained in the step three in a roller hearth furnace, controlling the deformation degree of the plate after quenching through optimization of quenching cooling parameters of the plate after solution treatment, and optimizing and solidifying cooling conditions through a test result of residual stress after quenching;
step five, conveying the quenched plate obtained in the step four to a drawing machine for drawing;
step six, placing the plate stretched in the step five into an aging furnace, and performing aging treatment to obtain transverse unevenness: 0-5 mm/2m and longitudinal unevenness are: 0-3 mm/2m large-size aviation plates.
The invention has the beneficial effects that: by the transverse unevenness control method, large-size aviation plates with high flatness can be obtained; firstly, the roll bending force of a rolling mill is manually controlled in the plate rolling process, so that the metal flow of the whole transverse end face is uniform in the plate rolling hot processing deformation process, the deformation resistance difference is reduced, the cross section thickness of the plate is more uniform, and the deformation of a hot rolled plate after cooling is reduced; secondly, the internal stress of the hot rolled plate is more uniformly distributed by performing roll straightening before solid solution of the hot rolled plate, the cooling deformation in the solid solution quenching process is reduced, the deformation in the plate quenching process is improved by properly adjusting quenching cooling parameters, and the transverse unevenness of the plate is ensured to meet the ANSI H35.2 standard and the part processing and manufacturing requirements by combining the jacking action of a cross beam in the stretching process.
Drawings
Fig. 1 is a flow chart of a method for controlling the transverse unevenness of a high-strength aluminum alloy plate according to a first embodiment;
fig. 2 is a comparison graph of a real object before and after optimization of quenching parameters of a plate in the first embodiment, where a is a real object graph before optimization of quenching parameters of the plate, and b is a real object graph after optimization of quenching parameters of the plate.
Detailed Description
The first embodiment is as follows: the present embodiment is described with reference to fig. 1 and 2, and the method for controlling the transverse unevenness of the high-strength aluminum alloy sheet according to the present embodiment includes the steps of:
step one, according to the mass percentage of elements, Si is less than or equal to 0.10 percent, Fe is less than or equal to 0.15 percent, Cu: 2.0-2.6%, Mn less than or equal to 0.10%, Mg: 1.8-2.3%, Cr is less than or equal to 0.04%, Zn: 7.6-8.4%, Ti is less than or equal to 0.06%, Zr: 0.08 to 0.18 percent of Al and the balance of Al, weighing cathode copper, zinc ingots, primary magnesium ingots, aluminum-titanium intermediate alloys, aluminum-zirconium intermediate alloys and aluminum ingots, then adding the cathode copper, zinc ingots, primary magnesium ingots, aluminum-titanium intermediate alloys, aluminum-zirconium intermediate alloys and aluminum ingots into a dry smelting furnace, smelting, then casting into ingots with the specification of 420 multiplied by 1320 multiplied by 2000mm, 420 multiplied by 1620 multiplied by 2500mm or 450 multiplied by 1880 multiplied by 2100mm, and then carrying out homogenization annealing, face milling and saw cutting to obtain finished plate ingots;
step two, putting the finished plate ingot blank obtained in the step one into a resistance heating furnace, heating to 360-420 ℃, preserving heat for 8-13 hours, and then carrying out hot rolling on the finished plate ingot blank to obtain a prefabricated hot rolled plate;
thirdly, sawing the prefabricated hot rolled plate obtained in the second step, then placing the prefabricated hot rolled plate into a straightening machine for roll straightening, and adjusting the roll gap interval of the straightening machine to enable the transverse unevenness of the plate after roll straightening to be 5mm/2500 mm; after the hot rolled plate is straightened by the roller, the transverse unevenness at different positions is 1-4 mm/2m, and the longitudinal unevenness is 0-3 mm/2 m; then loading the mixture into a roller hearth furnace for solid solution;
step four, carrying out solution treatment on the plate obtained in the step three in a roller hearth furnace, controlling the deformation degree of the plate after quenching through optimization of quenching cooling parameters of the plate after solution treatment, and optimizing and solidifying cooling conditions through a test result of residual stress after quenching;
step five, conveying the quenched plate obtained in the step four to a drawing machine for drawing;
step six, placing the plate stretched in the step five into an aging furnace, and performing aging treatment to obtain transverse unevenness: 0-5 mm/2m and longitudinal unevenness are: 0-3 mm/2m large-size aviation plates.
In the embodiment, the transverse unevenness control method selects a reasonable process flow, and realizes the optimized control of the transverse unevenness of the ultra-wide large-size plate through the control of the roll force in the rolling process, the roll straightening of the hot rolled plate before solid solution, the allocation of cooling parameters in the quenching and cooling process and the support of a cross beam in the stretching process; the prepared ultrahigh-strength alloy large-size wide plate has the advantages of transverse unevenness less than or equal to 5mm/2000m, uniform thickness and good surface, meets the requirements of use conditions in the processing process of plate parts, provides important guarantee for improving the localization rate of certain type passenger plane materials in China, and widens the channel for selecting materials of other subsequent machine types.
The aluminum alloy ultrahigh-strength large-size pre-stretched plate which is produced by the method for controlling the transverse unevenness and has the advantages of flat plate surface, uniform thickness, good surface and stable performance is adopted, the maximum value of the transverse unevenness of the plate is 5mm/2m, and the maximum value of the longitudinal unevenness of the plate is 3mm/2 m; the method is widely applied to various fields of aerospace, aviation, military and civil large-scale airplanes and the like.
The second embodiment is as follows: in this embodiment, the method for controlling the transverse unevenness of the high-strength aluminum alloy sheet according to the first embodiment is further defined, and in the second embodiment, when the finished sheet ingot is hot-rolled, the direction of the bending force is a forward direction, and the magnitude of the bending force is 2700 to 3000 KN.
In the embodiment, the direction of the bending roll force is adjusted to be the positive direction, and the force is 2700-3000 KN, so that the fine thickness difference of the cross section of the plate is finely controlled, the uniform thermal deformation of the whole transverse end face of the plate is ensured, and the deformation of the hot rolled plate after cooling is reduced.
The third concrete implementation mode: in the present embodiment, the method for controlling the transverse unevenness of the high-strength aluminum alloy sheet according to the first embodiment is further defined, and in the third step, the range of the set displacement value of the first roll in the leveler is: 17.0-25.0 mm; the displacement set value range of the two rollers on the straightening machine is as follows: 10.0-23.0 mm; the three-roller displacement set value range on the straightening machine is as follows: 10.0-20.5 mm; the displacement set value range of the four rollers on the straightening machine is as follows: 13.5-16.5 mm; the displacement set value range of the upper five rollers of the straightening machine is as follows: 13.5-16.5 mm; the displacement set value range of the six rollers on the straightening machine is as follows: 17.5-25.5 mm.
In the present embodiment, the upper roll displacement setting range of the leveler when the hot rolled sheet is roll-corrected is shown in table 1;
sequence of straightening rolls Set value range/mm of upper roll displacement
Last roller 17.0~25.0
Upper two rollers 10.0~23.0
Upper three-roller 10.0~20.5
Upper four rollers 13.5~16.5
Upper five rollers 13.5~16.5
Upper six rollers 17.5~25.5
TABLE 1
The fourth concrete implementation mode: in this embodiment, the method for controlling the transverse unevenness of the high-strength aluminum alloy plate according to the first embodiment is further defined, and in the fourth embodiment, the quenching cooling parameters of the plate include the thickness of a finished product, the water content control of the forced cooling zone i, the water content control of the forced cooling zone ii and the quenching speed;
the thickness control range of the finished product is as follows: 19.05 mm-25.4 mm;
the water quantity control of the strong cooling zone I comprises the flow control of an upper nozzle of the zone I and the flow control of a lower nozzle of the zone I; wherein, nozzle flow control scope on I district is: 100L/s-220L/s; the flow control range of the nozzle under the zone I is as follows: 200-300L/s;
the water flow control of the forced cooling area II comprises flow control of an upper nozzle of the area II and flow control of a lower nozzle of the area II; wherein, the flow control range of the nozzle on the II area is as follows: 240-280 l/s; the flow control range of the nozzle under the zone II is as follows: 300-340L/s;
the quenching speed control range is as follows: 170 mm/s-200 mm/s.
In the present embodiment, the process parameters of the plate quenching zone are shown in table 2;
Figure BDA0002535470360000041
TABLE 2
The fifth concrete implementation mode: in this embodiment, the method for controlling the transverse unevenness of the high-strength aluminum alloy sheet according to the first embodiment is further limited, and in this embodiment, when the sheet after quenching is sent to a stretcher and stretched, the height of the cross beam of the stretcher is 10mm to 25 mm.
In the embodiment, the height of the beam is increased to 10-15 mm, so that the plate is acted by an upward force in the stretching process, and the effect of correcting the transverse unevenness is achieved; the transverse unevenness of the sheet was measured after the sheet was stretched.
According to the control method for the transverse unevenness of the high-strength aluminum alloy plate, the large-specification high-flatness aviation plate is obtained, firstly, the bending force of a rolling mill is manually controlled in the plate rolling process, the bending force is positive bending, and the force value is 2900KN, so that the metal flow of the whole transverse end face in the plate rolling, heating and processing deformation process is uniform, the deformation resistance difference is reduced, the thickness of the cross section of the plate is more uniform, and the deformation of the hot rolled plate after cooling is reduced; the stress distribution in the plate is more uniform by the solid solution front roller correction of the hot rolled plate, the cooling deformation in the solid solution quenching process is reduced, the deformation in the plate quenching process is improved by properly adjusting the quenching cooling parameters, and the transverse unevenness of the plate is ensured to meet the ANSI H35.2 standard and the part processing and manufacturing requirements at the same time by combining the jacking action of a cross beam in the stretching process.

Claims (5)

1. A transverse unevenness control method for a high-strength aluminum alloy plate is characterized by comprising the following steps:
step one, according to the mass percentage of elements, Si is less than or equal to 0.10 percent, Fe is less than or equal to 0.15 percent, Cu: 2.0-2.6%, Mn less than or equal to 0.10%, Mg: 1.8-2.3%, Cr is less than or equal to 0.04%, Zn: 7.6-8.4%, Ti is less than or equal to 0.06%, Zr: 0.08 to 0.18 percent of Al and the balance of Al, weighing cathode copper, zinc ingots, primary magnesium ingots, aluminum-titanium intermediate alloys, aluminum-zirconium intermediate alloys and aluminum ingots, then adding the cathode copper, zinc ingots, primary magnesium ingots, aluminum-titanium intermediate alloys, aluminum-zirconium intermediate alloys and aluminum ingots into a dry smelting furnace, smelting, then casting into ingots with the specification of 420 multiplied by 1320 multiplied by 2000mm, 420 multiplied by 1620 multiplied by 2500mm or 450 multiplied by 1880 multiplied by 2100mm, and then carrying out homogenization annealing, face milling and saw cutting to obtain finished plate ingots;
step two, putting the finished plate ingot blank obtained in the step one into a resistance heating furnace, heating to 360-420 ℃, preserving heat for 8-13 hours, and then carrying out hot rolling on the finished plate ingot blank to obtain a prefabricated hot rolled plate;
thirdly, sawing the prefabricated hot rolled plate obtained in the second step, then placing the prefabricated hot rolled plate into a straightening machine for roll straightening, and adjusting the roll gap interval of the straightening machine to enable the transverse unevenness of the plate after roll straightening to be 5mm/2500 mm;
step four, carrying out solution treatment on the plate obtained in the step three in a roller hearth furnace, controlling the deformation degree of the plate after quenching through optimization of quenching cooling parameters of the plate after solution treatment, and optimizing and solidifying cooling conditions through a test result of residual stress after quenching;
step five, conveying the quenched plate obtained in the step four to a drawing machine for drawing;
step six, placing the plate stretched in the step five into an aging furnace, and performing aging treatment to obtain transverse unevenness: 0-5 mm/2m and longitudinal unevenness are: 0-3 mm/2m large-size aviation plates.
2. The method for controlling the transverse unevenness of the high-strength aluminum alloy sheet according to claim 1, wherein in the second step, the direction of the bending roll force is positive and the magnitude of the bending roll force is 2700 to 3000KN when the finished sheet ingot is hot-rolled.
3. The method for controlling the transverse unevenness of the high-strength aluminum alloy sheet according to claim 1, wherein in the third step, the range of the set displacement value of a roller on the straightener is as follows: 17.0-25.0 mm; the displacement set value range of the two rollers on the straightening machine is as follows: 10.0-23.0 mm; the three-roller displacement set value range on the straightening machine is as follows: 10.0-20.5 mm; the displacement set value range of the four rollers on the straightening machine is as follows: 13.5-16.5 mm; the displacement set value range of the upper five rollers of the straightening machine is as follows: 13.5-16.5 mm; the displacement set value range of the six rollers on the straightening machine is as follows: 17.5-25.5 mm.
4. The method for controlling the transverse unevenness of the high-strength aluminum alloy plate according to claim 1, wherein in the fourth step, the quenching cooling parameters of the plate comprise the thickness of a finished product, the water content control of a strong cooling area I, the water content control of a strong cooling area II and the quenching speed;
the thickness control range of the finished product is as follows: 19.05 mm-25.4 mm;
the water quantity control of the strong cooling zone I comprises the flow control of an upper nozzle of the zone I and the flow control of a lower nozzle of the zone I; wherein, nozzle flow control scope on I district is: 100L/s-220L/s; the flow control range of the nozzle under the zone I is as follows: 200-300L/s;
the water flow control of the forced cooling area II comprises flow control of an upper nozzle of the area II and flow control of a lower nozzle of the area II; wherein, the flow control range of the nozzle on the II area is as follows: 240-280 l/s; the flow control range of the nozzle under the zone II is as follows: 300-340L/s;
the quenching speed control range is as follows: 170 mm/s-200 mm/s.
5. The method for controlling the transverse unevenness of the high-strength aluminum alloy sheet according to claim 1, wherein in the fifth step, when the sheet after quenching is sent to a stretcher for stretching, the rise height of a cross beam of the stretcher is 10mm to 25 mm.
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Cited By (1)

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Publication number Priority date Publication date Assignee Title
CN112207522A (en) * 2020-10-26 2021-01-12 许晨玲 Flatness control method for large aluminum alloy integral wall plate

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CN110042333A (en) * 2019-04-26 2019-07-23 东北轻合金有限责任公司 A kind of manufacturing method of 625MPa grades of large-size aluminum alloy pre-stretching plates of aviation
CN110241337A (en) * 2019-06-25 2019-09-17 天津忠旺铝业有限公司 A kind of preparation method of super large wide cut aluminum alloy plate materials
CN110453121A (en) * 2019-09-09 2019-11-15 广西南南铝加工有限公司 A kind of 7xxx line aluminium alloy plate of high brightness and preparation method thereof

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Publication number Priority date Publication date Assignee Title
US6193818B1 (en) * 1995-12-12 2001-02-27 Pechiney Rhenalu Method for making thin, high-strength, highly formable aluminium alloy strips
JP2006199978A (en) * 2005-01-18 2006-08-03 Furukawa Sky Kk Method for producing aluminum alloy hot rolled sheet for welded structure
CN101037747A (en) * 2007-04-29 2007-09-19 东北轻合金有限责任公司 Aviation aluminum alloy pre-stretching plate and production method thereof
JP2009256782A (en) * 2008-03-28 2009-11-05 Kobe Steel Ltd Aluminum alloy plate, and method for producing the same
CN107236883A (en) * 2017-06-29 2017-10-10 广西南南铝加工有限公司 A kind of preparation technology of aluminum alloy plate materials
CN110042333A (en) * 2019-04-26 2019-07-23 东北轻合金有限责任公司 A kind of manufacturing method of 625MPa grades of large-size aluminum alloy pre-stretching plates of aviation
CN110241337A (en) * 2019-06-25 2019-09-17 天津忠旺铝业有限公司 A kind of preparation method of super large wide cut aluminum alloy plate materials
CN110453121A (en) * 2019-09-09 2019-11-15 广西南南铝加工有限公司 A kind of 7xxx line aluminium alloy plate of high brightness and preparation method thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112207522A (en) * 2020-10-26 2021-01-12 许晨玲 Flatness control method for large aluminum alloy integral wall plate

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