CN111359335A - Ash discharge device and ash discharge method - Google Patents

Ash discharge device and ash discharge method Download PDF

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Publication number
CN111359335A
CN111359335A CN202010243369.0A CN202010243369A CN111359335A CN 111359335 A CN111359335 A CN 111359335A CN 202010243369 A CN202010243369 A CN 202010243369A CN 111359335 A CN111359335 A CN 111359335A
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China
Prior art keywords
intermediate tank
gas
dust
ash discharge
valve
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Pending
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CN202010243369.0A
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Chinese (zh)
Inventor
高麟
吴志强
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Intermet Technology Chengdu Co Ltd
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Intermet Technology Chengdu Co Ltd
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Priority to CN202010243369.0A priority Critical patent/CN111359335A/en
Publication of CN111359335A publication Critical patent/CN111359335A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • B01D46/42Auxiliary equipment or operation thereof
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00Phosphorus; Compounds thereof
    • C01B25/02Preparation of phosphorus
    • C01B25/027Preparation of phosphorus of yellow phosphorus
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D17/00Arrangements for using waste heat; Arrangements for using, or disposing of, waste gases
    • F27D17/008Arrangements for using waste heat; Arrangements for using, or disposing of, waste gases cleaning gases

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Environmental & Geological Engineering (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

The invention discloses an ash discharge device and an ash discharge method. This ash discharging device includes: the intermediate tank is used for receiving the dust collected by the dust removal device and discharging the dust; a replacement gas inlet pipe connected to the first gas inlet of the intermediate tank, for introducing replacement gas into the intermediate tank; and the balance pipe is connected with the air inlet of the dust removal device and the air outlet of the intermediate tank and is used for inputting the weight of the air discharged from the intermediate tank into the dust removal device again. The replacement gas is introduced into the intermediate tank through the replacement gas input pipe to replace the dangerous gas carried by the dust in the intermediate tank, so that the safety can be improved. The output of the target product obtained by condensing the dangerous gas can be obviously improved by inputting the replaced dangerous gas into the dust removal device again through the balance pipe.

Description

Ash discharge device and ash discharge method
Technical Field
The invention relates to the technical field of dust treatment, in particular to an ash discharge device and an ash discharge method.
Background
At present, the technological process of yellow phosphorus production system is to send the mixture of phosphate rock, silica and coke in proportion into electric furnace, the mixture in the electric furnace is reduced to produce furnace gas, the furnace gas escapes from the reaction melting zone, the furnace gas passes through the furnace gas filtering layer formed by continuously supplemented mixture at the upper part of the furnace and then carries with part of the impurities in the mixture to be discharged from the electric furnace, and then the yellow phosphorus product is obtained by dedusting, filtering, condensing, washing, refining and separating, and the tail gas is recycled or discharged. In the production system, the dust removal system is arranged between the electric furnace and the washing tower, and furnace gas in the electric furnace overcomes the resistance of a filter assembly in the filter system through a blower or a draught fan so as to remove dust and filter.
Since the dust removing gas contains yellow phosphorus vapor, the yellow phosphorus vapor is inevitably mixed into the dust intercepted by the dust removing device. Since yellow phosphorus is a phase-change-prone substance and has a risk of explosion, it is highly dangerous to directly discharge the dust carrying yellow phosphorus vapor. However, there is no mature and complete treatment technology for dust discharge after filtering dust-removing gas containing yellow phosphorus vapor and the like with easy phase change and explosion risks in the prior art.
Disclosure of Invention
The invention mainly aims to provide an ash discharge device and an ash discharge method, so as to solve the problem of poor ash discharge safety in the prior art.
In order to achieve the above object, according to one aspect of the present invention, an ash discharge apparatus is provided. This ash discharging device includes:
the intermediate tank is used for receiving the dust collected by the dust removal device and discharging the dust;
a replacement gas inlet pipe connected to the first gas inlet of the intermediate tank, for introducing replacement gas into the intermediate tank;
and the balance pipe is connected with the air inlet of the dust removal device and the air outlet of the intermediate tank and is used for inputting the weight of the air discharged from the intermediate tank into the dust removal device again.
The replacement gas is introduced into the intermediate tank through the replacement gas input pipe to replace the dangerous gas carried by the dust in the intermediate tank, so that the safety can be improved. The output of the target product obtained by condensing the dangerous gas can be obviously improved by inputting the replaced dangerous gas into the dust removal device again through the balance pipe.
The sealing gas input pipe is connected with the second gas inlet of the intermediate tank. Therefore, the sealing gas can isolate the external gas, and the amount of gas carried by dust entering the intermediate tank is reduced.
Furthermore, the dust removing device also comprises a dust vibrating gas input pipe for inputting dust vibrating gas to the dust hopper of the dust removing device. From this, the dust that shakes of letting in can make the caking scatter, and the dust of not only being convenient for falls into the pans, can prevent moreover that the dust accumulation piece from causing mechanical damage to striking the pans.
Furthermore, the first air inlet and the exhaust port are arranged at the upper part of the intermediate tank; the second air inlet is arranged at the lower part of the intermediate tank. Therefore, the replacement effect and the sealing effect are good.
Further, the replaceable gas input pipe, the sealing gas input pipe and the ash vibrating gas input pipe are connected with the same inert gas storage tank, and inert gas is input into the intermediate tank. The inert gas is a gas that does not react with the dust or the gas entrained with the dust, such as nitrogen, helium, argon, and the like.
Furthermore, a first valve bank is arranged on a pipeline connecting the intermediate tank and the dust removal device, and the first valve bank comprises at least two valves. Therefore, the valve group strengthens sealing and avoids external air from entering a system in the ash discharge process.
And a second valve group is arranged on an ash discharge pipeline of the intermediate tank, and comprises at least two valves. Therefore, the valve group strengthens sealing and avoids external air from entering a system in the ash discharge process.
Further, a material level detection mechanism is arranged on the intermediate tank. Therefore, the start and stop of the feeding and ash discharging of the intermediate tank can be controlled conveniently according to the detection result of the material level detection mechanism.
Further, a pressure detection mechanism is arranged on the intermediate tank, a first valve is arranged on the replaceable gas input pipe, and the pressure detection mechanism is interlocked with the first valve. Therefore, safety accidents caused by overpressure of the intermediate tank are prevented, and safety of the intermediate tank is guaranteed.
Furthermore, a pressure control mechanism for controlling the input speed of the replaceable gas is arranged on the replaceable gas input pipe. This prevents the occurrence of a safety problem due to an excessively large or small flow rate of the replacement gas.
Furthermore, the dust removal device is connected with the gas outlet of a combustion furnace used for producing yellow phosphorus. In this case, the inert gas is preferably a hot gas having a temperature of 60 ℃ or higher, whereby condensation of the yellow phosphorus vapor can be prevented. The yellow phosphorus vapor can also be prevented from condensing by arranging heat-insulating jackets on the intermediate tank and the pipeline.
In order to achieve the above object, according to another aspect of the present invention, an ash discharge method is provided. The ash discharge method comprises the following steps:
(1) first-stage ash discharge: opening a second valve on the balance pipe, then opening a first valve group on a pipeline connecting the intermediate tank and the dust removal device, so that dust in an ash hopper of the dust removal device falls into the intermediate tank, and then closing the first valve group;
(2) and (3) replacement: opening a first valve on the replacement gas input pipe, inputting the gas in the intermediate tank into the dust removal device again through the balance pipe, and then closing the first valve and the second valve;
(3) secondary ash discharge: closing a third valve on the sealing gas input pipe, then opening a second valve group on an ash discharge pipeline of the intermediate tank to discharge ash, closing the second valve group after the ash discharge is finished, and opening the third valve;
and (3) repeating the steps (1) to (3) in the ash discharging process.
The replacement gas is introduced into the intermediate tank through the replacement gas input pipe to replace the dangerous gas carried by the dust in the intermediate tank, so that the safety can be improved. The output of the target product obtained by condensing the dangerous gas can be obviously improved by inputting the replaced dangerous gas into the dust removal device again through the balance pipe. The ash discharging process is carried out in two stages, and the two stages of ash discharging are interlocked, so that the system safety in the ash discharging process is further ensured.
Further, the second valve is intermittently opened during the secondary ash discharge. Therefore, the pressure of the intermediate tank can be balanced, and the stability of the ash discharge process is improved.
Further, the dust-containing gas treated by the dust removing device contains yellow phosphorus vapor. Therefore, the yellow phosphorus belongs to a phase-change-prone substance and has a burning explosion risk, and the yellow phosphorus steam can be prevented from being discharged by adopting the ash discharge method, so that the yield of the yellow phosphorus is improved.
In summary, the dust discharging device and the dust discharging method are particularly suitable for discharging dust intercepted after the dust removing device filters furnace gas of a combustion furnace in yellow phosphorus production, and certainly, are also suitable for discharging dust after the dust removing device filters dust-containing gas containing other flammable and explosive substances.
The invention is further described with reference to the following figures and detailed description. Additional aspects and advantages of the invention will be set forth in part in the description which follows and, in part, will be obvious from the description, or may be learned by practice of the invention.
Drawings
The accompanying drawings, which are incorporated in and constitute a part of this specification, are included to assist in understanding the invention, and are included to explain the invention and their equivalents and not limit it unduly. In the drawings:
fig. 1 is a schematic structural view of an ash discharge apparatus according to embodiment 1 of the present invention.
Fig. 2 is a schematic structural view of an ash discharge apparatus according to embodiment 2 of the present invention.
Fig. 3 is a schematic structural view of an ash discharge apparatus according to embodiment 3 of the present invention.
The relevant references in the above figures are:
110: a dust removal device;
111: an ash hopper;
120: an intermediate tank;
121: a material level detection mechanism;
122: a pressure detection mechanism;
123: a heat-preserving jacket;
130: a replacement gas inlet tube;
131: a first valve;
132: a pressure control mechanism;
140: a balance tube;
141: a second valve;
150: a sealing gas input tube;
151: a third valve;
160: ash vibration gas input pipe;
161: a fourth valve;
170: an inert gas storage tank;
180: a first valve block;
190: a second valve block.
Detailed Description
The invention will be described more fully hereinafter with reference to the accompanying drawings. Those skilled in the art will be able to implement the invention based on these teachings. Before the present invention is described in detail with reference to the accompanying drawings, it is to be noted that:
the technical solutions and features provided in the present invention in the respective sections including the following description may be combined with each other without conflict.
Moreover, the embodiments of the present invention described in the following description are generally only some embodiments of the present invention, and not all embodiments. Therefore, all other embodiments obtained by a person of ordinary skill in the art based on the embodiments of the present invention without any creative effort shall fall within the protection scope of the present invention.
With respect to terms and units in the present invention. The terms "comprising," "having," and any variations thereof in the description and claims of this invention and the related sections are intended to cover non-exclusive inclusions.
Example 1
Fig. 1 is a schematic structural diagram of an ash discharge device in this embodiment, which is used for dust removal of dust intercepted after a dust removal device 110 filters furnace gas of a combustion furnace in yellow phosphorus production, wherein the furnace gas contains yellow phosphorus vapor.
As shown in fig. 1, the ash discharging apparatus includes a tundish 120, a replacement gas inlet pipe 130, and a balance pipe 140.
The intermediate tank 120 is used for receiving the dust collected by the dust removal device 110 and discharging the dust; the intermediate tank 120 is provided with a heat insulating jacket 123, a material level detection mechanism 121, and a pressure detection mechanism 122.
The replacement gas input pipe 130 is connected to the first gas inlet of the intermediate tank 120, and is configured to input replacement gas into the intermediate tank 120; the replacement gas input pipe 130 is provided with a first valve 131, and the pressure detection mechanism 122 is interlocked with the first valve 131. The replacement gas input pipe 130 is provided with a pressure control mechanism 132 for controlling the input speed of the replacement gas.
The balance pipe 140 connects an air inlet of the dust removing device 110 with an air outlet of the intermediate tank 120, and is used for newly inputting the gas exhausted from the intermediate tank 120 into the dust removing device 110.
The replacement gas input pipe 130 is connected to an inert gas storage tank 170 and inputs an inert gas into the intermediate tank 120. The inert gas is nitrogen with the temperature more than or equal to 60 ℃.
The first air inlet and the exhaust port are provided at an upper portion of the middle tank 120.
A first valve set 180 is provided on a pipeline connecting the intermediate tank 120 and the dust removing device 110, and the first valve set 180 includes two valves.
A second valve group 190 is arranged on the ash discharge pipeline of the intermediate tank 120, and the second valve group 190 comprises two valves.
The ash discharge method adopting the ash discharge device shown in FIG. 1 comprises the following steps:
(1) first-stage ash discharge: opening a second valve 141 on the balance pipe 140, then opening a first valve group 180 on a pipeline connecting the intermediate tank 120 and the dust removal device 110, so that dust in the dust hopper 111 of the dust removal device 110 falls into the intermediate tank 120, and then closing the first valve group 180;
(2) and (3) replacement: opening the first valve 131 on the replacement gas input pipe 130 to re-input the gas in the intermediate tank 120 into the dust removing device 110 through the balance pipe 140, and then closing the first valve 131 and the second valve 141;
(3) secondary ash discharge: opening a second valve group 190 on an ash discharge pipeline of the intermediate tank 120 for ash discharge, and closing the second valve group 190 after the ash discharge is finished;
and (3) repeating the steps (1) to (3) in the ash discharging process.
Example 2
Compared with embodiment 1, the ash discharging device and the ash discharging method of the present embodiment have the following differences: as shown in fig. 2, the ash discharging apparatus further includes a sealing gas inlet pipe 150, and the sealing gas inlet pipe 150 is connected to the second gas inlet of the intermediate tank 120, and is used for supplying a sealing gas to the intermediate tank 120 through the sealing gas inlet pipe 150. The second inlet is provided at the lower portion of the middle tank 120. The replacement gas input pipe 130 and the sealing gas input pipe 150 are connected to the same inert gas storage tank 170 and input the inert gas into the middle tank 120.
The ash discharge method comprises the following steps:
(1) first-stage ash discharge: opening a second valve 141 on the balance pipe 140, then opening a first valve group 180 on a pipeline connecting the intermediate tank 120 and the dust removal device 110, so that dust in the dust hopper 111 of the dust removal device 110 falls into the intermediate tank 120, and then closing the first valve group 180;
(2) and (3) replacement: opening the first valve 131 on the replacement gas input pipe 130 to re-input the gas in the intermediate tank 120 into the dust removing device 110 through the balance pipe 140, and then closing the first valve 131 and the second valve 141;
(3) secondary ash discharge: closing a third valve 151 on the sealing gas input pipe 150, then opening a second valve set 190 on an ash discharge pipeline of the intermediate tank 120 for ash discharge, closing the second valve set 190 after the ash discharge is finished, and opening the third valve 151;
and (3) repeating the steps (1) to (3) in the ash discharging process.
Example 3
Compared with embodiment 2, the ash discharging device and the ash discharging method of the present embodiment have the following differences: as shown in fig. 3, the ash discharging device further has an ash vibrating gas input pipe 160, and the ash vibrating gas input pipe 160 is used for inputting ash vibrating gas to the ash bucket 111 of the dust removing device 110. The replacement gas inlet pipe 130, the sealing gas inlet pipe 150, and the ash shaking gas inlet pipe 160 are connected to the same inert gas storage tank 170 and supply inert gas into the intermediate tank 120.
The ash discharge method comprises the following steps:
(1) loosening ash: opening a fourth valve 161 on the ash vibrating gas input pipe 160, and introducing hot nitrogen gas to loosen ash deposited at the bottom of the ash hopper 111 of the dust removal device 110;
(2) first-stage ash discharge: opening a second valve 141 on the balance pipe 140, then opening a first valve group 180 on a pipeline connecting the intermediate tank 120 and the dust removal device 110, so that dust in the dust hopper 111 of the dust removal device 110 falls into the intermediate tank 120, and then closing the first valve group 180;
(3) and (3) replacement: opening the first valve 131 on the replacement gas input pipe 130 to re-input the gas in the intermediate tank 120 into the dust removing device 110 through the balance pipe 140, and then closing the first valve 131 and the second valve 141;
(4) secondary ash discharge: closing a third valve 151 on the sealing gas input pipe 150, then opening a second valve set 190 on an ash discharge pipeline of the intermediate tank 120 for ash discharge, closing the second valve set 190 after the ash discharge is finished, and opening the third valve 151;
and (4) repeating the steps (1) to (4) in the ash discharging process.
Example 4
Compared with the ash discharge method of any of embodiments 1 to 3, the ash discharge method of the present embodiment has the differences: the second valve 141 is intermittently opened during the secondary ash discharge.
The contents of the present invention have been explained above. Those skilled in the art will be able to implement the invention based on these teachings. All other embodiments, which can be derived by a person skilled in the art from the above description without inventive step, shall fall within the scope of protection of the present invention.

Claims (10)

1. Ash discharging device, its characterized in that: comprises that
A middle tank (120) for receiving the dust collected by the dust removing device (110) and discharging the dust;
a replacement gas inlet pipe (130), the replacement gas inlet pipe (130) being connected to the first gas inlet of the intermediate tank (120) and being configured to introduce replacement gas into the intermediate tank (120);
and the balance pipe (140) is connected with the air inlet of the dust removal device (110) and the air outlet of the intermediate tank (120), and is used for inputting the air discharged from the intermediate tank (120) into the dust removal device (110) again.
2. The ash discharge device of claim 1, wherein: the sealing gas input pipe (150) is used for inputting sealing gas into the intermediate tank (120), and the sealing gas input pipe (150) is connected with a second gas inlet of the intermediate tank (120); the dust removing device also comprises a dust vibrating gas input pipe (160) for inputting dust vibrating gas to the dust hopper (111) of the dust removing device (110).
3. The ash discharge device according to claim 2, wherein: the first air inlet and the first air outlet are arranged at the upper part of the intermediate tank (120); the second air inlet is arranged at the lower part of the intermediate tank (120).
4. The ash discharge device according to claim 2, wherein: the replaceable gas input pipe (130), the sealing gas input pipe (150) and the ash vibrating gas input pipe (160) are connected with the same inert gas storage tank (170) and input inert gas into the intermediate tank (120).
5. The ash discharge device of claim 1, wherein: a first valve group (180) is arranged on a pipeline connecting the intermediate tank (120) and the dust removal device (110), and the first valve group (180) comprises at least two valves; and a second valve group (190) is arranged on an ash discharge pipeline of the intermediate tank (120), and the second valve group (190) comprises at least two valves.
6. The ash discharge device of claim 1, wherein: a material level detection mechanism (121) is arranged on the intermediate tank (120); and/or a pressure detection mechanism (122) is arranged on the intermediate tank (120), a first valve (131) is arranged on the replaceable gas input pipe (130), and the pressure detection mechanism (122) is interlocked with the first valve (131).
7. The ash discharge device of claim 1, wherein: the pressure control mechanism (132) for controlling the input speed of the replacement gas is arranged on the replacement gas input pipe (130).
8. The ash discharge device of claim 1, wherein: the dust removal device (110) is connected with the gas outlet of a combustion furnace used for producing yellow phosphorus.
9. An ash discharge method comprising the steps of:
(1) first-stage ash discharge: opening a second valve (141) on the balance pipe (140), then opening a first valve group (180) on a pipeline connecting the intermediate tank (120) and the dust removal device (110), so that dust in the dust hopper (111) of the dust removal device (110) falls into the intermediate tank (120), and then closing the first valve group (180);
(2) and (3) replacement: opening a first valve (131) on a replaceable gas input pipe (130), enabling the gas in the intermediate tank (120) to be input into the dust removal device (110) again through a balance pipe (140), and then closing the first valve (131) and a second valve (141);
(3) secondary ash discharge: closing a third valve (151) on the sealing gas input pipe (150), then opening a second valve group (190) on an ash discharge pipeline of the intermediate tank (120) for ash discharge, closing the second valve group (190) after the ash discharge is finished, and opening the third valve (151);
and (3) repeating the steps (1) to (3) in the ash discharging process.
10. The ash discharge method according to claim 9, wherein: intermittently opening the second valve (141) during the secondary ash discharge; the dust-containing gas treated by the dust removing device (110) contains yellow phosphorus vapor.
CN202010243369.0A 2020-03-31 2020-03-31 Ash discharge device and ash discharge method Pending CN111359335A (en)

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CN202010243369.0A CN111359335A (en) 2020-03-31 2020-03-31 Ash discharge device and ash discharge method

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Application Number Priority Date Filing Date Title
CN202010243369.0A CN111359335A (en) 2020-03-31 2020-03-31 Ash discharge device and ash discharge method

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113295012A (en) * 2021-05-26 2021-08-24 无锡锡南铸造机械股份有限公司 Flue gas treatment system based on automatic hanging
CN114314536A (en) * 2021-12-07 2022-04-12 成都易态科技有限公司 Mud phosphorus evaporation plant
CN114870533A (en) * 2022-05-23 2022-08-09 成都易态科技有限公司 Ash discharge balancing device and filter
CN114870532A (en) * 2022-05-23 2022-08-09 成都易态科技有限公司 Ash discharge balancing device and filter

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CN204952524U (en) * 2015-05-21 2016-01-13 成都易态科技有限公司 Hot precipitator unloads grey system
CN105438849A (en) * 2015-10-29 2016-03-30 成都易态科技有限公司 Dust discharging process and dust discharging structure used for yellow phosphorus gas purifying
CN205313119U (en) * 2015-12-10 2016-06-15 成都易态膜分离技术有限公司 Arrange grey structure and antimony smelting burner gas processing system who constitutes thereof
CN109158212A (en) * 2018-10-08 2019-01-08 浙江大学 The wide temperature high leakproofness dust-extraction unit of self-sustaining and technique
CN212236466U (en) * 2020-03-31 2020-12-29 成都易态科技有限公司 Ash discharging device

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EP1469173A1 (en) * 2003-04-16 2004-10-20 Arvin Technologies, Inc. An exhaust emission reduction system
CN103816740A (en) * 2012-06-29 2014-05-28 邹岳明 Phosphorus steam dust-removing device capable of realizing high-purity phosphorus recovery
KR20140038132A (en) * 2012-09-20 2014-03-28 고등기술연구원연구조합 Ash discharging apparatus and method of the high pressure dust collector
CN104623991A (en) * 2015-02-15 2015-05-20 北京烨晶科技有限公司 High-temperature gas-solid filtering separation process
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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113295012A (en) * 2021-05-26 2021-08-24 无锡锡南铸造机械股份有限公司 Flue gas treatment system based on automatic hanging
CN114314536A (en) * 2021-12-07 2022-04-12 成都易态科技有限公司 Mud phosphorus evaporation plant
CN114314536B (en) * 2021-12-07 2024-02-02 成都易态科技有限公司 Mud phosphorus evaporation plant
CN114870533A (en) * 2022-05-23 2022-08-09 成都易态科技有限公司 Ash discharge balancing device and filter
CN114870532A (en) * 2022-05-23 2022-08-09 成都易态科技有限公司 Ash discharge balancing device and filter
CN114870533B (en) * 2022-05-23 2023-07-04 成都易态科技有限公司 Ash discharging balancing device and filter
CN114870532B (en) * 2022-05-23 2023-08-04 成都易态科技有限公司 Ash discharging balancing device and filter

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