CN111331143A - Vacuum gas atomization powder making barrel - Google Patents

Vacuum gas atomization powder making barrel Download PDF

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Publication number
CN111331143A
CN111331143A CN201811549023.2A CN201811549023A CN111331143A CN 111331143 A CN111331143 A CN 111331143A CN 201811549023 A CN201811549023 A CN 201811549023A CN 111331143 A CN111331143 A CN 111331143A
Authority
CN
China
Prior art keywords
spray gun
pressure gas
atomizing spray
atomizing
barrel
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811549023.2A
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Chinese (zh)
Inventor
高正江
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Aviation Maite Fine Metallurgical Technology Xuzhou Co ltd
Original Assignee
China Aviation Maite Fine Metallurgical Technology Xuzhou Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Aviation Maite Fine Metallurgical Technology Xuzhou Co ltd filed Critical China Aviation Maite Fine Metallurgical Technology Xuzhou Co ltd
Priority to CN201811549023.2A priority Critical patent/CN111331143A/en
Publication of CN111331143A publication Critical patent/CN111331143A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/06Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/06Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • B22F2009/0836Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid with electric or magnetic field or induction
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/06Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • B22F2009/0844Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid in controlled atmosphere
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/06Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • B22F2009/088Fluid nozzles, e.g. angle, distance
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/06Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • B22F2009/0892Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid casting nozzle; controlling metal stream in or after the casting nozzle

Abstract

A vacuum gas atomization powder making barrel relates to the technical field of alloy powder preparation. It contains the atomizing bucket, the transition material package, the eye leaks, the honeycomb duct, low pressure gas atomizing spray gun, high pressure gas atomizing spray gun, the cavity bucket wall, the heat preservation, the atomizing bucket top is equipped with the transition material package with electrode induction smelting pot intercommunication, be equipped with two eyes of leaking on the transition material package, the transition material package leaks the eye and passes through honeycomb duct and the inside intercommunication of atomizing bucket, honeycomb duct export both sides are equipped with low pressure gas atomizing spray gun and high pressure gas atomizing spray gun, the injection line focus of low pressure gas atomizing spray gun and high pressure gas atomizing spray gun all is located the guide pipe axis, the injection line focus of low pressure gas atomizing spray gun is higher than the injection line focus of high pressure gas atomizing spray gun, the atomizing bucket lateral wall is equipped with the cavity bucket wall. It can prevent the molten metal oxidation through the design of transition material package double-leakage hole, low pressure gas atomization spray gun and high pressure gas atomization spray gun, improves catalyst powder purity, promotes the work efficiency of vacuum gas atomization powder process.

Description

Vacuum gas atomization powder making barrel
Technical Field
The invention relates to the technical field of alloy powder preparation, in particular to a vacuum gas atomization powder preparation barrel.
Background
Gas atomization powder production is a powder production process in which a rapidly moving fluid (atomizing medium) impacts or otherwise breaks up a metal or alloy liquid into fine droplets, which are subsequently condensed into a solid powder. Atomization is the best method for producing fully alloyed powders, the product of which is known as pre-alloyed powder. Each particle of this powder not only has exactly the same uniform chemical composition as a given molten alloy, but also refines the crystalline structure due to rapid solidification; eliminating macro-segregation of the second phase.
The atomization powder-making method is divided into two major categories, the "two-stream method" (crushing the alloy stream with an atomizing medium stream) and the "one-stream method" (crushing the alloy stream in other ways). 846 the former atomizing medium is divided into gas (helium, , nitrogen, air) and liquid (water, oil); the latter is e.g. centrifugal atomization and dissolved air vacuum atomization.
At present, when gas atomization powder process equipment is used for manufacturing alloy powder, molten metal is easy to oxidize, the purity of the obtained catalyst powder is insufficient, subsequent production is influenced, and the production efficiency is low.
Disclosure of Invention
The invention aims to provide a vacuum gas atomization powder making barrel aiming at the defects and shortcomings of the prior art, and the vacuum gas atomization powder making barrel can be used for solving the defects that when alloy powder is made by existing gas atomization powder making equipment, metal liquid is easy to oxidize, so that the purity of the obtained catalyst powder is insufficient, subsequent production is influenced, and the production efficiency is low.
In order to achieve the purpose, the invention adopts the following technical scheme: it contains atomizing barrel, transition material package, leaks eye, honeycomb duct, low pressure gas atomizing spray gun, high pressure gas atomizing spray gun, cavity bucket wall, heat preservation, the top of atomizing barrel is provided with the transition material package that communicates with electrode induction smelting pot, be provided with two on the transition material package and leak the eye, the inside intercommunication of honeycomb duct and atomizing barrel is passed through to the eye that leaks of transition material package, the both sides in honeycomb duct exit are provided with low pressure gas atomizing spray gun and high pressure gas atomizing spray gun respectively, the injection line focus of low pressure gas atomizing spray gun and high pressure gas atomizing spray gun all is located the axis of honeycomb duct, and the injection line focus of low pressure gas atomizing spray gun is higher than the injection line focus of high pressure gas atomizing spray gun, the lateral wall of atomizing barrel is provided with the cavity bucket wall, the outside of cavity bucket wall is provided with.
Furthermore, the honeycomb duct is arranged in parallel with the inner wall of the atomizing barrel, and the low-pressure gas atomizing spray gun and the high-pressure gas atomizing spray gun respectively form an included angle of 45-75 degrees with the honeycomb duct.
Furthermore, the focal point of the injection line of the low-pressure gas atomization spray gun is 5-25cm higher than that of the high-pressure gas atomization spray gun.
Further, the bottom of atomizing bucket is provided with the buffer portion of loudspeaker form, the bottom of buffer portion is provided with the discharge gate, discharge gate department is provided with electric control valve.
Furthermore, the outer side walls of the hollow barrel wall and the heat preservation layer are provided with a fixing support and a plurality of pipeline interfaces communicated with the inside of the atomizing barrel.
The working principle of the invention is as follows: during operation, through the evacuation system evacuation earlier in the atomizing bucket, the liquid metal that electrode induction smelting pot smelted gets into in the transition material package through crossing material package entry, it opens to leak the eye after the seal of transition material package entry, the liquid metal that leaks the eye and flow through the honeycomb duct sprays inert gas respectively through low pressure gas atomizing spray gun and high pressure gas atomizing spray gun and atomizes, liquid metal leaks in the eye and the honeycomb duct entering atomizing bucket that can be quick through two, prevent the oxidation of liquid metal, low pressure gas atomizing spray gun and high pressure gas atomizing spray gun spray inert gas to liquid metal simultaneously fast, further prevent the oxidation of liquid metal, can effectively improve catalyst powder purity, promote the work efficiency of vacuum gas atomization powder process.
After the technical scheme is adopted, the invention has the beneficial effects that: its simple structure, reasonable in design through the design of transition material package two hourglass eyes, low pressure gas atomization spray gun and high pressure gas atomization spray gun, can prevent the molten metal oxidation, improves catalyst powder purity, promotes the work efficiency of vacuum gas atomization powder process.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to these drawings without creative efforts.
FIG. 1 is a schematic structural view of the present invention;
fig. 2 is an enlarged view of a portion a in fig. 1.
Description of reference numerals: atomizing bucket 1, transition material package 2, hourglass eye 3, honeycomb duct 4, low pressure gas atomizing spray gun 5, high pressure gas atomizing spray gun 6, cavity bucket wall 7, heat preservation 8, buffer 9, discharge gate 10, fixed bolster 11.
Detailed Description
Referring to fig. 1 to 2, the technical solution adopted by the present embodiment is: it contains atomizing barrel 1, transition material package 2, leaks hole 3, honeycomb duct 4, low pressure gas atomizing spray gun 5, high pressure gas atomizing spray gun 6, cavity bucket wall 7, heat preservation 8, the top of atomizing barrel 1 is provided with transition material package 2 with electrode induction smelting pot intercommunication, transition material package 2 casing and atomizing barrel 1 casing welding, liquid metal that electrode induction smelting pot smelted gets into in transition material package 2 through transition material package 2 entry, be provided with two on the transition material package 2 and leak the hole 3, increase the circulation rate of liquid metal through setting up two and leak the hole 3, prevent liquid metal oxidation, the hole 3 that leaks of transition material package 2 communicates with the inside of atomizing barrel 1 through honeycomb duct 4, the both sides in honeycomb duct 4 exit are provided with low pressure gas atomizing spray gun 5 and high pressure gas atomizing spray gun 6 respectively, the injection line focus of low pressure gas atomizing spray gun 5 and high pressure gas atomizing spray gun 6 all is located the axis of honeycomb duct 4, the spray line focus of low pressure gas atomizing spray gun 5 is higher than the spray line focus of high pressure gas atomizing spray gun 6, the lateral wall of atomizing bucket 1 is provided with cavity bucket wall 7, the outside of cavity bucket wall 7 is provided with heat preservation 8, and cavity bucket wall 7 and heat preservation 8 can prevent 1 inside thermal losses of atomizing bucket.
The honeycomb duct 4 and the inner wall parallel arrangement of atomizing bucket 1, low pressure gas atomizing spray gun 5 and high pressure gas atomizing spray gun 6 are 45-75 contained angles with honeycomb duct 4 respectively, and during the concrete implementation, preferred low pressure gas atomizing spray gun 5 and high pressure gas atomizing spray gun 6 are 60 contained angles with honeycomb duct 4 respectively.
The focal point of the injection line of the low-pressure gas atomization spray gun 5 is 5-25cm higher than that of the high-pressure gas atomization spray gun 6, and in specific implementation, the focal point of the injection line of the low-pressure gas atomization spray gun 5 is preferably 15cm higher than that of the high-pressure gas atomization spray gun 6.
The bottom of atomizing bucket 1 is provided with tubaeform buffering portion 9, the bottom of buffering portion 9 is provided with discharge gate 10, discharge gate 9 department is provided with electric control valve.
The lateral wall of cavity bucket wall 7 and heat preservation 8 is provided with the pipeline interface of fixed bolster 11 and a plurality of and the inside intercommunication of atomizing bucket, and fixed bolster 11 welds on the lateral wall of cavity bucket wall 7 and heat preservation 8 for fix atomizing bucket 1, the pipeline interface of a plurality of and the inside intercommunication of atomizing bucket 1 is used for being connected with external pipeline.
During specific work, through the earlier evacuation of evacuation system in the atomizing bucket 1, the liquid metal that the electrode induction smelting pot smelted gets into in transition material package 2 through crossing material package 2 entries, 2 entries of transition material package are sealed the back and are leaked eye 3 and open, it sprays inert gas respectively through low pressure gas atomizing spray gun 5 and high pressure gas atomizing spray gun 6 to leak the liquid metal that eye 3 flows out through honeycomb duct 4 and atomize, liquid metal leaks in the entering atomizing bucket 1 that eye 3 and honeycomb duct 4 can be quick through two, prevent the oxidation of liquid metal, simultaneously low pressure gas atomizing spray gun 5 and high pressure gas atomizing spray gun 6 spray inert gas to liquid metal fast simultaneously, further prevent the oxidation of liquid metal, can effectively improve catalyst powder purity, promote the work efficiency of vacuum gas atomization powder process.
The above description is only for the purpose of illustrating the technical solutions of the present invention and not for the purpose of limiting the same, and other modifications or equivalent substitutions made by those skilled in the art to the technical solutions of the present invention should be covered within the scope of the claims of the present invention without departing from the spirit and scope of the technical solutions of the present invention.

Claims (5)

1. The utility model provides a vacuum gas atomization system powder bucket which characterized in that: it contains atomizing barrel, transition material package, leaks eye, honeycomb duct, low pressure gas atomizing spray gun, high pressure gas atomizing spray gun, cavity bucket wall, heat preservation, the top of atomizing barrel is provided with the transition material package that communicates with electrode induction smelting pot, be provided with two on the transition material package and leak the eye, the inside intercommunication of honeycomb duct and atomizing barrel is passed through to the eye that leaks of transition material package, the both sides in honeycomb duct exit are provided with low pressure gas atomizing spray gun and high pressure gas atomizing spray gun respectively, the injection line focus of low pressure gas atomizing spray gun and high pressure gas atomizing spray gun all is located the axis of honeycomb duct, and the injection line focus of low pressure gas atomizing spray gun is higher than the injection line focus of high pressure gas atomizing spray gun, the lateral wall of atomizing barrel is provided with the cavity bucket wall, the outside of cavity bucket wall is provided with.
2. The vacuum atomization powder making barrel of claim 1, wherein: the honeycomb duct is arranged parallel to the inner wall of the atomizing barrel, and the low-pressure gas atomizing spray gun and the high-pressure gas atomizing spray gun respectively form an included angle of 45-75 degrees with the honeycomb duct.
3. The vacuum atomization powder making barrel of claim 1, wherein: the focal point of the injection line of the low-pressure gas atomization spray gun is 5-25cm higher than that of the high-pressure gas atomization spray gun.
4. The vacuum atomization powder making barrel of claim 1, wherein: the bottom of atomizing bucket is provided with tubaeform buffering portion, the bottom of buffering portion is provided with the discharge gate, discharge gate department is provided with electric control valve.
5. The vacuum atomization powder making barrel of claim 1, wherein: the outer side walls of the hollow barrel wall and the heat preservation layer are provided with fixing supports and a plurality of pipeline connectors communicated with the inside of the atomization barrel.
CN201811549023.2A 2018-12-18 2018-12-18 Vacuum gas atomization powder making barrel Pending CN111331143A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811549023.2A CN111331143A (en) 2018-12-18 2018-12-18 Vacuum gas atomization powder making barrel

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811549023.2A CN111331143A (en) 2018-12-18 2018-12-18 Vacuum gas atomization powder making barrel

Publications (1)

Publication Number Publication Date
CN111331143A true CN111331143A (en) 2020-06-26

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Application Number Title Priority Date Filing Date
CN201811549023.2A Pending CN111331143A (en) 2018-12-18 2018-12-18 Vacuum gas atomization powder making barrel

Country Status (1)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112893855A (en) * 2021-01-15 2021-06-04 江苏威拉里新材料科技有限公司 Electrode induction gas atomization powder making equipment
CN115351284A (en) * 2022-10-20 2022-11-18 湖南特种金属材料有限责任公司 Be applied to multistage processing unit of sendust powder of metal magnetic powder core

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112893855A (en) * 2021-01-15 2021-06-04 江苏威拉里新材料科技有限公司 Electrode induction gas atomization powder making equipment
CN115351284A (en) * 2022-10-20 2022-11-18 湖南特种金属材料有限责任公司 Be applied to multistage processing unit of sendust powder of metal magnetic powder core
CN115351284B (en) * 2022-10-20 2022-12-20 湖南特种金属材料有限责任公司 Be applied to multistage processing unit of sendust powder of metal magnetic powder core

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Application publication date: 20200626

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