CN111281813A - Perfume and preparation method thereof - Google Patents

Perfume and preparation method thereof Download PDF

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Publication number
CN111281813A
CN111281813A CN202010203993.8A CN202010203993A CN111281813A CN 111281813 A CN111281813 A CN 111281813A CN 202010203993 A CN202010203993 A CN 202010203993A CN 111281813 A CN111281813 A CN 111281813A
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Prior art keywords
perfume
denatured ethanol
hours
daily essence
parts
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陈鹏
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Individual
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/35Ketones, e.g. benzophenone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31Hydrocarbons
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/342Alcohols having more than seven atoms in an unbroken chain
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/347Phenols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q13/00Formulations or additives for perfume preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Emergency Medicine (AREA)
  • Cosmetics (AREA)
  • Fats And Perfumes (AREA)

Abstract

The invention discloses perfume and a preparation method thereof, wherein the perfume is prepared from denatured ethanol, daily essence, water, ethylhexyl methoxycinnamate, butyl methoxy dibenzoyl methane and ethylhexyl salicylate. The preparation method comprises the steps of preparing the denatured ethanol and the daily essence according to a certain proportion and raw materials, facilitating the configuration of a user on specific perfume, and preparing the perfume by using the denatured ethanol, the daily essence, water, ethylhexyl methoxycinnamate, butyl methoxydibenzoylmethane and ethylhexyl salicylate according to a proportion of 80: 15: 4.7: 0.034: 0.033: 0.033's mode is accomplished perfume ratio, and it is extremely convenient to use, and for the time overlength of this kind of perfume storage simultaneously, fragrant smell is more strong lasting, adopts the liquid mode of filtering the mixture to make the precision of perfume purer, and the producer of can being convenient for is extremely simple and convenient to the mass production of this perfume.

Description

Perfume and preparation method thereof
Technical Field
The invention relates to the technical field related to perfume preparation, in particular to perfume and a preparation method thereof.
Background
The perfume is an alcohol solution of essence, and is added with a proper amount of perfume and the like to form a mixture, so that the perfume has strong fragrance, has the main function of being sprayed on parts such as lappets, handkerchiefs, hairlines and the like to emit pleasant fragrance, is one of important cosmetics, and is simply one of volatile substances; they have certain fragrance and flavor, and can be perceived by people in smelling or taste; the perfume is a product with perfume dissolved in ethanol, and can be added with trace additives such as pigment, antioxidant, bactericide, glycerol, surfactant and the like according to needs, different types of perfumes are prepared by blending, the perfume can be divided into two categories of floral perfume and fantasy perfume according to the fragrance, the fragrance of the floral perfume is mostly prepared by simulating natural floral fragrance, and the fantasy perfume mainly comprises rose, jasmine, narcissus, magnolia, lily of the valley, gardenia, orange flower, lilac, tuberose, acacia, honeysuckle, hyacinth, lavender and the like, the fantasy perfume is a new fragrance created by a blender through the artistic imagination in the aspects of natural phenomena, customs, scenery, geographical names, characters, emotions, music, painting and the like, fantasy-type perfumes often have very nice names such as naxinlan, xiangnell five, night voyage, night paris, nighttime on christmas, joy, castrate, poison, opium, sand dune, etc.
In the existing perfume preparation methods, the perfume is prepared in a distillation mode, the operation is extremely complicated, and the lasting strength of the perfume is low.
Disclosure of Invention
The invention aims to solve the problems that in the existing perfume preparation method, the perfume is prepared in a distillation mode, the operation is extremely complicated, and the lasting strength of the perfume is low, and provides the perfume and the preparation method thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
the perfume consists of the following raw materials in parts by weight: 75-80 parts of denatured ethanol, 12-16 parts of daily essence, 4.5-4.8 parts of water, 0.033-0.035 part of ethylhexyl methoxycinnamate, 0.032-0.034 part of butyl methoxydibenzoylmethane and 0.032-0.034 part of ethylhexyl salicylate.
As a further description of the above technical solution, the method comprises the following steps:
(1) preparing denatured ethanol raw materials: pouring 100ml of one hundred percent or ninety five percent of medicinal ethanol into a beaker prepared previously slowly, sucking 5ml of diethyl phthalate through a suction pipe, slowly dropping the diethyl phthalate in the suction pipe into the beaker containing the ethanol, and sufficiently and uniformly stirring through a glass rod, wherein light force is needed in the stirring process, the mixture is stirred slowly and finely for three minutes to be sufficiently mixed, and then the mixture is kept stand for 48 hours.
(2) Blending raw materials of the daily essence: measuring 5ml of limonene, 5ml of eugenol, 5ml of iso-methyl ionone, 5ml of iso-eugenol and 5ml of linalool by using a suction tube, uniformly dropping the materials into a measuring cylinder in sequence, fully and uniformly stirring the materials for three minutes by using a glass rod to fully mix the materials, and then standing the materials for 48 hours;
(3) selecting raw materials: mixing 75-80 parts of denatured ethanol, 12-16 parts of daily essence, 4.5-4.8 parts of water, 0.033-0.035 part of ethylhexyl methoxycinnamate, 0.032-0.034 part of butyl methoxy dibenzoyl methane and 0.032-0.034 part of ethylhexyl salicylate, wherein the ratio of the denatured ethanol to the daily essence to the water to the ethylhexyl methoxycinnamate to the butyl methoxy dibenzoyl methane to the ethylhexyl salicylate is 80: 15: 4.7: 0.034: 0.033: 0.033;
as a further description of the above solution, the method involves a tool: measuring cylinder, rubber head dropper, glass rod, flask, filter paper, and collecting bottle.
As a further description of the above technical solution, the perfume preparation method comprises the steps of:
(1) selecting a flask with the volume of 150 ml;
(2) and (3) sequentially and slowly injecting 80ml of denatured ethanol and 15ml of daily essence into the flask through the port at the top end of the flask, and slowly stirring for five minutes by using a glass rod to completely dissolve the daily essence in the denatured ethanol.
(3) After standing for 48 hours, 4.7ml of water was then poured into the flask and stirred again with a glass rod so that the water was thoroughly mixed with the mixed liquid of denatured ethanol and daily essence, and then allowed to stand for 48 hours.
(4) After 48 hours, 0.034ml of ethylhexyl methoxycinnamate, 0.033ml of butyl methoxydibenzoylmethane and 0.033ml of ethylhexyl salicylate were successively charged into the flask, stirred uniformly with a glass rod and left to stand for another 48 hours.
(5) And after 48 hours, injecting the mixed liquid into a collecting bottle with filter paper, injecting the filtered liquid in the collecting bottle into a perfume bottle, and plugging the perfume bottle opening by using a plug.
In summary, due to the adoption of the technical scheme, the invention has the beneficial effects that: the preparation method comprises the steps of preparing denatured ethanol and daily essence according to a certain proportion and raw materials, facilitating the preparation of a user for specific perfume, and preparing the perfume by using the denatured ethanol, the daily essence, water, ethylhexyl methoxycinnamate, butyl methoxydibenzoylmethane and ethylhexyl salicylate according to the proportion of 80: 15: 4.7: 0.034: 0.033: 0.033's mode is accomplished perfume proportion, and it is extremely convenient to use, and for the time overlength of this kind of perfume storage simultaneously, fragrant smell is more strong lasting, adopts the liquid mode of filtering the mixture to make the precision of perfume purer, can be convenient for the producer to the mass production of this perfume.
Detailed Description
The technical solutions in the embodiments of the present invention will be described below clearly and completely in connection with the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The perfume consists of the following raw materials in parts by weight: 75-80 parts of denatured ethanol, 12-16 parts of daily essence, 4.5-4.8 parts of water, 0.033-0.035 part of ethylhexyl methoxycinnamate, 0.032-0.034 part of butyl methoxydibenzoylmethane and 0.032-0.034 part of ethylhexyl salicylate.
The first embodiment is as follows: a preparation method of perfume comprises the following steps:
(1) preparing denatured ethanol raw materials: pouring 100ml of one hundred percent or ninety five percent of medicinal ethanol into a beaker prepared previously slowly, sucking 5ml of diethyl phthalate through a suction pipe, slowly dropping the diethyl phthalate in the suction pipe into the beaker containing the ethanol, and sufficiently and uniformly stirring through a glass rod, wherein light force is needed in the stirring process, the mixture is stirred slowly and finely for three minutes to be sufficiently mixed, and then the mixture is kept stand for 48 hours.
Proportion table of ethanol and diethyl phthalate
Figure BDA0002420328510000051
(2) Blending raw materials of the daily essence: measuring 5ml of limonene, 5ml of eugenol, 5ml of iso-methyl ionone, 5ml of iso-eugenol and 5ml of linalool by using a suction tube, uniformly dropping the materials into a measuring cylinder in sequence, fully and uniformly stirring the materials for three minutes by using a glass rod to fully mix the materials, and then standing the materials for 48 hours;
proportioning proportion table of limonene, eugenol, iso-methyl ionone, isoeugenol and linalool
Figure BDA0002420328510000052
(3) Selecting raw materials: mixing 75-80 parts of denatured ethanol, 12-16 parts of daily essence, 4.5-4.8 parts of water, 0.033-0.035 part of ethylhexyl methoxycinnamate, 0.032-0.034 part of butyl methoxy dibenzoyl methane and 0.032-0.034 part of ethylhexyl salicylate, wherein the ratio of the denatured ethanol to the daily essence to the water to the ethylhexyl methoxycinnamate to the butyl methoxy dibenzoyl methane to the ethylhexyl salicylate is 80: 15: 4.7: 0.034: 0.033: 0.033;
proportion of denatured ethanol, daily essence, water, ethylhexyl methoxycinnamate, butyl methoxydibenzoylmethane and ethylhexyl salicylate
Figure BDA0002420328510000061
Example two: the method involves a tool: measuring cylinder, rubber head dropper, glass rod, flask, filter paper, collecting bottle.
Example three: the preparation method of the perfume comprises the following steps:
(1) selecting a flask with the volume of 150 ml;
(2) and (3) sequentially and slowly injecting 80ml of denatured ethanol and 15ml of daily essence into the flask through the port at the top end of the flask, and slowly stirring for five minutes by using a glass rod to completely dissolve the daily essence in the denatured ethanol.
(3) After standing for 48 hours, 4.7ml of water was then poured into the flask and stirred again with a glass rod so that the water was thoroughly mixed with the mixed liquid of denatured ethanol and daily essence, and then allowed to stand for 48 hours.
(4) After 48 hours, 0.034ml of ethylhexyl methoxycinnamate, 0.033ml of butyl methoxydibenzoylmethane and 0.033ml of ethylhexyl salicylate were successively charged into the flask, stirred uniformly with a glass rod and left to stand for another 48 hours.
(5) And after 48 hours, injecting the mixed liquid into a collecting bottle with filter paper, injecting the filtered liquid in the collecting bottle into a perfume bottle, and plugging the perfume bottle opening by using a plug.
The working principle is as follows: when the daily essence is used, firstly 100ml of one-hundred percent or ninety-five percent of medicinal ethanol is slowly poured into a beaker prepared previously, then 5ml of diethyl phthalate is absorbed by a suction pipe, then the diethyl phthalate in the suction pipe is slowly dripped into the beaker containing ethanol, and then the mixture is fully and uniformly stirred by a glass rod, wherein light force is needed in the stirring process, the mixture is slowly and finely stirred for three minutes to be fully mixed, then the mixture is kept stand for 48 hours, then the daily essence is prepared according to the method, and then the denatured ethanol, the daily essence, water, ethylhexyl methoxycinnamate, butyl methoxydibenzoylmethane and ethyl hexyl salicylate are mixed according to the proportion of 80: 15: 4.7: 0.034: 0.033: 0.033, finally injecting the mixed liquid into a collecting bottle with filter paper, injecting the filtered liquid in the collecting bottle into a perfume bottle, and plugging the perfume bottle mouth with a plug.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and equivalent alternatives or modifications according to the technical solution and the inventive concept of the present invention should be covered by the scope of the present invention.

Claims (4)

1. The perfume is characterized by comprising the following raw materials in parts by weight: 75-80 parts of denatured ethanol, 12-16 parts of daily essence, 4.5-4.8 parts of water, 0.033-0.035 part of ethylhexyl methoxycinnamate, 0.032-0.034 part of butyl methoxydibenzoylmethane and 0.032-0.034 part of ethylhexyl salicylate.
2. A preparation method of perfume comprises the following steps:
(1) preparing denatured ethanol raw materials: 100ml of one hundred percent or ninety-five percent of medicinal ethanol is slowly poured into a beaker prepared previously, 5ml of diethyl phthalate is absorbed by a suction pipe, the diethyl phthalate in the suction pipe is slowly dripped into the beaker containing the ethanol, and the mixture is fully and uniformly stirred by a glass rod, wherein light force is needed in the stirring process, the mixture is slowly and finely stirred for three minutes to be fully mixed, and then the mixture is kept stand for 48 hours.
(2) Blending raw materials of the daily essence: measuring 5ml of limonene, 5ml of eugenol, 5ml of iso-methyl ionone, 5ml of iso-eugenol and 5ml of linalool by using a suction tube, sequentially and uniformly dropping the materials into a measuring cylinder, fully and uniformly stirring the materials for three minutes by using a glass rod to fully mix the materials, and then standing the materials for 48 hours;
(3) selecting raw materials: mixing 75-80 parts of denatured ethanol, 12-16 parts of daily essence, 4.5-4.8 parts of water, 0.033-0.035 part of ethylhexyl methoxycinnamate, 0.032-0.034 part of butyl methoxy dibenzoyl methane and 0.032-0.034 part of ethylhexyl salicylate, wherein the ratio of the denatured ethanol to the daily essence to the water to the ethylhexyl methoxycinnamate to the butyl methoxy dibenzoyl methane to the ethylhexyl salicylate is 80: 15: 4.7: 0.034: 0.033: 0.033.
3. a perfume and a process for its preparation according to claim 1, characterized in that: the method involves a tool: measuring cylinder, rubber head dropper, glass rod, flask, filter paper, and collecting bottle.
4. A perfume and a process for its preparation according to claim 1, wherein the perfume preparation process comprises the steps of:
(1) selecting a flask with the volume of 150 ml;
(2) and (3) sequentially and slowly injecting 80ml of denatured ethanol and 15ml of daily essence into the flask through the port at the top end of the flask, and slowly stirring for five minutes by using a glass rod to completely dissolve the daily essence in the denatured ethanol.
(3) After standing for 48 hours, 4.7ml of water was then poured into the flask and stirred again with a glass rod so that the water was thoroughly mixed with the mixed liquid of denatured ethanol and daily essence, and then allowed to stand for 48 hours.
(4) After 48 hours, 0.034ml of ethylhexyl methoxycinnamate, 0.033ml of butyl methoxydibenzoylmethane and 0.033ml of ethylhexyl salicylate were successively charged into the flask, stirred uniformly with a glass rod, and left to stand for another 48 hours.
(5) And after 48 hours, injecting the mixed liquid into a collecting bottle with filter paper, injecting the filtered liquid in the collecting bottle into a perfume bottle, and plugging the perfume bottle opening by using a plug.
CN202010203993.8A 2020-03-21 2020-03-21 Perfume and preparation method thereof Pending CN111281813A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112022743A (en) * 2020-09-11 2020-12-04 广州简灿生物科技有限公司 Liquid layered perfume and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5968535A (en) * 1997-04-09 1999-10-19 Haarmann & Reimer Gmbh Denaturant for ethanol
CN106474009A (en) * 2016-11-16 2017-03-08 纪绥粧 A kind of fall fire cologne
CN107106470A (en) * 2015-01-19 2017-08-29 科思创德国股份有限公司 For active composition or the polyurethane urea solutions of the composition of spices
CN109199929A (en) * 2018-11-07 2019-01-15 上海芬尚生物科技有限公司 perfume and preparation method thereof
CN109310601A (en) * 2016-06-08 2019-02-05 高砂香料工业株式会社 Spices material

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5968535A (en) * 1997-04-09 1999-10-19 Haarmann & Reimer Gmbh Denaturant for ethanol
CN107106470A (en) * 2015-01-19 2017-08-29 科思创德国股份有限公司 For active composition or the polyurethane urea solutions of the composition of spices
CN109310601A (en) * 2016-06-08 2019-02-05 高砂香料工业株式会社 Spices material
CN106474009A (en) * 2016-11-16 2017-03-08 纪绥粧 A kind of fall fire cologne
CN109199929A (en) * 2018-11-07 2019-01-15 上海芬尚生物科技有限公司 perfume and preparation method thereof

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
武汉市税务局江汉分局 *
裘炳毅等: "《现代化妆品科学与技术 上》", 31 March 2016, 中国轻工业出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112022743A (en) * 2020-09-11 2020-12-04 广州简灿生物科技有限公司 Liquid layered perfume and preparation method thereof

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Application publication date: 20200616