CN111281813A - Perfume and preparation method thereof - Google Patents
Perfume and preparation method thereof Download PDFInfo
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- CN111281813A CN111281813A CN202010203993.8A CN202010203993A CN111281813A CN 111281813 A CN111281813 A CN 111281813A CN 202010203993 A CN202010203993 A CN 202010203993A CN 111281813 A CN111281813 A CN 111281813A
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- perfume
- denatured ethanol
- hours
- daily essence
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- 239000002304 perfume Substances 0.000 title claims abstract description 56
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 49
- 229940075894 denatured ethanol Drugs 0.000 claims abstract description 28
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- TYYHDKOVFSVWON-UHFFFAOYSA-N 2-butyl-2-methoxy-1,3-diphenylpropane-1,3-dione Chemical compound C=1C=CC=CC=1C(=O)C(OC)(CCCC)C(=O)C1=CC=CC=C1 TYYHDKOVFSVWON-UHFFFAOYSA-N 0.000 claims abstract description 17
- FMRHJJZUHUTGKE-UHFFFAOYSA-N Ethylhexyl salicylate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1O FMRHJJZUHUTGKE-UHFFFAOYSA-N 0.000 claims abstract description 17
- YBGZDTIWKVFICR-JLHYYAGUSA-N Octyl 4-methoxycinnamic acid Chemical compound CCCCC(CC)COC(=O)\C=C\C1=CC=C(OC)C=C1 YBGZDTIWKVFICR-JLHYYAGUSA-N 0.000 claims abstract description 17
- 229960005193 avobenzone Drugs 0.000 claims abstract description 17
- 229940068171 ethyl hexyl salicylate Drugs 0.000 claims abstract description 17
- 229960001679 octinoxate Drugs 0.000 claims abstract description 17
- 239000000203 mixture Substances 0.000 claims abstract description 16
- 239000002994 raw material Substances 0.000 claims abstract description 14
- 239000007788 liquid Substances 0.000 claims abstract description 13
- 239000011521 glass Substances 0.000 claims description 19
- FLKPEMZONWLCSK-UHFFFAOYSA-N diethyl phthalate Chemical compound CCOC(=O)C1=CC=CC=C1C(=O)OCC FLKPEMZONWLCSK-UHFFFAOYSA-N 0.000 claims description 18
- 239000000463 material Substances 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 11
- RRAFCDWBNXTKKO-UHFFFAOYSA-N eugenol Chemical compound COC1=CC(CC=C)=CC=C1O RRAFCDWBNXTKKO-UHFFFAOYSA-N 0.000 claims description 8
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 claims description 8
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 7
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 claims description 4
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 claims description 4
- NPBVQXIMTZKSBA-UHFFFAOYSA-N Chavibetol Natural products COC1=CC=C(CC=C)C=C1O NPBVQXIMTZKSBA-UHFFFAOYSA-N 0.000 claims description 4
- 239000005770 Eugenol Substances 0.000 claims description 4
- BJIOGJUNALELMI-ONEGZZNKSA-N Isoeugenol Natural products COC1=CC(\C=C\C)=CC=C1O BJIOGJUNALELMI-ONEGZZNKSA-N 0.000 claims description 4
- UVMRYBDEERADNV-UHFFFAOYSA-N Pseudoeugenol Natural products COC1=CC(C(C)=C)=CC=C1O UVMRYBDEERADNV-UHFFFAOYSA-N 0.000 claims description 4
- BJIOGJUNALELMI-ARJAWSKDSA-N cis-isoeugenol Chemical compound COC1=CC(\C=C/C)=CC=C1O BJIOGJUNALELMI-ARJAWSKDSA-N 0.000 claims description 4
- 229960002217 eugenol Drugs 0.000 claims description 4
- 229940087305 limonene Drugs 0.000 claims description 4
- 235000001510 limonene Nutrition 0.000 claims description 4
- 229930007744 linalool Natural products 0.000 claims description 4
- BJIOGJUNALELMI-UHFFFAOYSA-N trans-isoeugenol Natural products COC1=CC(C=CC)=CC=C1O BJIOGJUNALELMI-UHFFFAOYSA-N 0.000 claims description 4
- 230000002045 lasting effect Effects 0.000 abstract description 4
- 238000001914 filtration Methods 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 238000003860 storage Methods 0.000 abstract description 2
- 239000003205 fragrance Substances 0.000 description 7
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- 238000004821 distillation Methods 0.000 description 2
- 241000205585 Aquilegia canadensis Species 0.000 description 1
- 244000068485 Convallaria majalis Species 0.000 description 1
- 235000009046 Convallaria majalis Nutrition 0.000 description 1
- 244000111489 Gardenia augusta Species 0.000 description 1
- 241001632576 Hyacinthus Species 0.000 description 1
- 235000010254 Jasminum officinale Nutrition 0.000 description 1
- 240000005385 Jasminum sambac Species 0.000 description 1
- 244000178870 Lavandula angustifolia Species 0.000 description 1
- 235000010663 Lavandula angustifolia Nutrition 0.000 description 1
- 240000007472 Leucaena leucocephala Species 0.000 description 1
- 235000010643 Leucaena leucocephala Nutrition 0.000 description 1
- 241000218378 Magnolia Species 0.000 description 1
- 241000234479 Narcissus Species 0.000 description 1
- 239000008896 Opium Substances 0.000 description 1
- 244000014047 Polianthes tuberosa Species 0.000 description 1
- 235000016067 Polianthes tuberosa Nutrition 0.000 description 1
- 241000220317 Rosa Species 0.000 description 1
- 235000004338 Syringa vulgaris Nutrition 0.000 description 1
- 244000297179 Syringa vulgaris Species 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 239000003899 bactericide agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000008451 emotion Effects 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- -1 iso-methyl ionone Chemical compound 0.000 description 1
- 239000001102 lavandula vera Substances 0.000 description 1
- 235000018219 lavender Nutrition 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229960001027 opium Drugs 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/347—Phenols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q13/00—Formulations or additives for perfume preparations
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses perfume and a preparation method thereof, wherein the perfume is prepared from denatured ethanol, daily essence, water, ethylhexyl methoxycinnamate, butyl methoxy dibenzoyl methane and ethylhexyl salicylate. The preparation method comprises the steps of preparing the denatured ethanol and the daily essence according to a certain proportion and raw materials, facilitating the configuration of a user on specific perfume, and preparing the perfume by using the denatured ethanol, the daily essence, water, ethylhexyl methoxycinnamate, butyl methoxydibenzoylmethane and ethylhexyl salicylate according to a proportion of 80: 15: 4.7: 0.034: 0.033: 0.033's mode is accomplished perfume ratio, and it is extremely convenient to use, and for the time overlength of this kind of perfume storage simultaneously, fragrant smell is more strong lasting, adopts the liquid mode of filtering the mixture to make the precision of perfume purer, and the producer of can being convenient for is extremely simple and convenient to the mass production of this perfume.
Description
Technical Field
The invention relates to the technical field related to perfume preparation, in particular to perfume and a preparation method thereof.
Background
The perfume is an alcohol solution of essence, and is added with a proper amount of perfume and the like to form a mixture, so that the perfume has strong fragrance, has the main function of being sprayed on parts such as lappets, handkerchiefs, hairlines and the like to emit pleasant fragrance, is one of important cosmetics, and is simply one of volatile substances; they have certain fragrance and flavor, and can be perceived by people in smelling or taste; the perfume is a product with perfume dissolved in ethanol, and can be added with trace additives such as pigment, antioxidant, bactericide, glycerol, surfactant and the like according to needs, different types of perfumes are prepared by blending, the perfume can be divided into two categories of floral perfume and fantasy perfume according to the fragrance, the fragrance of the floral perfume is mostly prepared by simulating natural floral fragrance, and the fantasy perfume mainly comprises rose, jasmine, narcissus, magnolia, lily of the valley, gardenia, orange flower, lilac, tuberose, acacia, honeysuckle, hyacinth, lavender and the like, the fantasy perfume is a new fragrance created by a blender through the artistic imagination in the aspects of natural phenomena, customs, scenery, geographical names, characters, emotions, music, painting and the like, fantasy-type perfumes often have very nice names such as naxinlan, xiangnell five, night voyage, night paris, nighttime on christmas, joy, castrate, poison, opium, sand dune, etc.
In the existing perfume preparation methods, the perfume is prepared in a distillation mode, the operation is extremely complicated, and the lasting strength of the perfume is low.
Disclosure of Invention
The invention aims to solve the problems that in the existing perfume preparation method, the perfume is prepared in a distillation mode, the operation is extremely complicated, and the lasting strength of the perfume is low, and provides the perfume and the preparation method thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
the perfume consists of the following raw materials in parts by weight: 75-80 parts of denatured ethanol, 12-16 parts of daily essence, 4.5-4.8 parts of water, 0.033-0.035 part of ethylhexyl methoxycinnamate, 0.032-0.034 part of butyl methoxydibenzoylmethane and 0.032-0.034 part of ethylhexyl salicylate.
As a further description of the above technical solution, the method comprises the following steps:
(1) preparing denatured ethanol raw materials: pouring 100ml of one hundred percent or ninety five percent of medicinal ethanol into a beaker prepared previously slowly, sucking 5ml of diethyl phthalate through a suction pipe, slowly dropping the diethyl phthalate in the suction pipe into the beaker containing the ethanol, and sufficiently and uniformly stirring through a glass rod, wherein light force is needed in the stirring process, the mixture is stirred slowly and finely for three minutes to be sufficiently mixed, and then the mixture is kept stand for 48 hours.
(2) Blending raw materials of the daily essence: measuring 5ml of limonene, 5ml of eugenol, 5ml of iso-methyl ionone, 5ml of iso-eugenol and 5ml of linalool by using a suction tube, uniformly dropping the materials into a measuring cylinder in sequence, fully and uniformly stirring the materials for three minutes by using a glass rod to fully mix the materials, and then standing the materials for 48 hours;
(3) selecting raw materials: mixing 75-80 parts of denatured ethanol, 12-16 parts of daily essence, 4.5-4.8 parts of water, 0.033-0.035 part of ethylhexyl methoxycinnamate, 0.032-0.034 part of butyl methoxy dibenzoyl methane and 0.032-0.034 part of ethylhexyl salicylate, wherein the ratio of the denatured ethanol to the daily essence to the water to the ethylhexyl methoxycinnamate to the butyl methoxy dibenzoyl methane to the ethylhexyl salicylate is 80: 15: 4.7: 0.034: 0.033: 0.033;
as a further description of the above solution, the method involves a tool: measuring cylinder, rubber head dropper, glass rod, flask, filter paper, and collecting bottle.
As a further description of the above technical solution, the perfume preparation method comprises the steps of:
(1) selecting a flask with the volume of 150 ml;
(2) and (3) sequentially and slowly injecting 80ml of denatured ethanol and 15ml of daily essence into the flask through the port at the top end of the flask, and slowly stirring for five minutes by using a glass rod to completely dissolve the daily essence in the denatured ethanol.
(3) After standing for 48 hours, 4.7ml of water was then poured into the flask and stirred again with a glass rod so that the water was thoroughly mixed with the mixed liquid of denatured ethanol and daily essence, and then allowed to stand for 48 hours.
(4) After 48 hours, 0.034ml of ethylhexyl methoxycinnamate, 0.033ml of butyl methoxydibenzoylmethane and 0.033ml of ethylhexyl salicylate were successively charged into the flask, stirred uniformly with a glass rod and left to stand for another 48 hours.
(5) And after 48 hours, injecting the mixed liquid into a collecting bottle with filter paper, injecting the filtered liquid in the collecting bottle into a perfume bottle, and plugging the perfume bottle opening by using a plug.
In summary, due to the adoption of the technical scheme, the invention has the beneficial effects that: the preparation method comprises the steps of preparing denatured ethanol and daily essence according to a certain proportion and raw materials, facilitating the preparation of a user for specific perfume, and preparing the perfume by using the denatured ethanol, the daily essence, water, ethylhexyl methoxycinnamate, butyl methoxydibenzoylmethane and ethylhexyl salicylate according to the proportion of 80: 15: 4.7: 0.034: 0.033: 0.033's mode is accomplished perfume proportion, and it is extremely convenient to use, and for the time overlength of this kind of perfume storage simultaneously, fragrant smell is more strong lasting, adopts the liquid mode of filtering the mixture to make the precision of perfume purer, can be convenient for the producer to the mass production of this perfume.
Detailed Description
The technical solutions in the embodiments of the present invention will be described below clearly and completely in connection with the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The perfume consists of the following raw materials in parts by weight: 75-80 parts of denatured ethanol, 12-16 parts of daily essence, 4.5-4.8 parts of water, 0.033-0.035 part of ethylhexyl methoxycinnamate, 0.032-0.034 part of butyl methoxydibenzoylmethane and 0.032-0.034 part of ethylhexyl salicylate.
The first embodiment is as follows: a preparation method of perfume comprises the following steps:
(1) preparing denatured ethanol raw materials: pouring 100ml of one hundred percent or ninety five percent of medicinal ethanol into a beaker prepared previously slowly, sucking 5ml of diethyl phthalate through a suction pipe, slowly dropping the diethyl phthalate in the suction pipe into the beaker containing the ethanol, and sufficiently and uniformly stirring through a glass rod, wherein light force is needed in the stirring process, the mixture is stirred slowly and finely for three minutes to be sufficiently mixed, and then the mixture is kept stand for 48 hours.
Proportion table of ethanol and diethyl phthalate
(2) Blending raw materials of the daily essence: measuring 5ml of limonene, 5ml of eugenol, 5ml of iso-methyl ionone, 5ml of iso-eugenol and 5ml of linalool by using a suction tube, uniformly dropping the materials into a measuring cylinder in sequence, fully and uniformly stirring the materials for three minutes by using a glass rod to fully mix the materials, and then standing the materials for 48 hours;
proportioning proportion table of limonene, eugenol, iso-methyl ionone, isoeugenol and linalool
(3) Selecting raw materials: mixing 75-80 parts of denatured ethanol, 12-16 parts of daily essence, 4.5-4.8 parts of water, 0.033-0.035 part of ethylhexyl methoxycinnamate, 0.032-0.034 part of butyl methoxy dibenzoyl methane and 0.032-0.034 part of ethylhexyl salicylate, wherein the ratio of the denatured ethanol to the daily essence to the water to the ethylhexyl methoxycinnamate to the butyl methoxy dibenzoyl methane to the ethylhexyl salicylate is 80: 15: 4.7: 0.034: 0.033: 0.033;
proportion of denatured ethanol, daily essence, water, ethylhexyl methoxycinnamate, butyl methoxydibenzoylmethane and ethylhexyl salicylate
Example two: the method involves a tool: measuring cylinder, rubber head dropper, glass rod, flask, filter paper, collecting bottle.
Example three: the preparation method of the perfume comprises the following steps:
(1) selecting a flask with the volume of 150 ml;
(2) and (3) sequentially and slowly injecting 80ml of denatured ethanol and 15ml of daily essence into the flask through the port at the top end of the flask, and slowly stirring for five minutes by using a glass rod to completely dissolve the daily essence in the denatured ethanol.
(3) After standing for 48 hours, 4.7ml of water was then poured into the flask and stirred again with a glass rod so that the water was thoroughly mixed with the mixed liquid of denatured ethanol and daily essence, and then allowed to stand for 48 hours.
(4) After 48 hours, 0.034ml of ethylhexyl methoxycinnamate, 0.033ml of butyl methoxydibenzoylmethane and 0.033ml of ethylhexyl salicylate were successively charged into the flask, stirred uniformly with a glass rod and left to stand for another 48 hours.
(5) And after 48 hours, injecting the mixed liquid into a collecting bottle with filter paper, injecting the filtered liquid in the collecting bottle into a perfume bottle, and plugging the perfume bottle opening by using a plug.
The working principle is as follows: when the daily essence is used, firstly 100ml of one-hundred percent or ninety-five percent of medicinal ethanol is slowly poured into a beaker prepared previously, then 5ml of diethyl phthalate is absorbed by a suction pipe, then the diethyl phthalate in the suction pipe is slowly dripped into the beaker containing ethanol, and then the mixture is fully and uniformly stirred by a glass rod, wherein light force is needed in the stirring process, the mixture is slowly and finely stirred for three minutes to be fully mixed, then the mixture is kept stand for 48 hours, then the daily essence is prepared according to the method, and then the denatured ethanol, the daily essence, water, ethylhexyl methoxycinnamate, butyl methoxydibenzoylmethane and ethyl hexyl salicylate are mixed according to the proportion of 80: 15: 4.7: 0.034: 0.033: 0.033, finally injecting the mixed liquid into a collecting bottle with filter paper, injecting the filtered liquid in the collecting bottle into a perfume bottle, and plugging the perfume bottle mouth with a plug.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and equivalent alternatives or modifications according to the technical solution and the inventive concept of the present invention should be covered by the scope of the present invention.
Claims (4)
1. The perfume is characterized by comprising the following raw materials in parts by weight: 75-80 parts of denatured ethanol, 12-16 parts of daily essence, 4.5-4.8 parts of water, 0.033-0.035 part of ethylhexyl methoxycinnamate, 0.032-0.034 part of butyl methoxydibenzoylmethane and 0.032-0.034 part of ethylhexyl salicylate.
2. A preparation method of perfume comprises the following steps:
(1) preparing denatured ethanol raw materials: 100ml of one hundred percent or ninety-five percent of medicinal ethanol is slowly poured into a beaker prepared previously, 5ml of diethyl phthalate is absorbed by a suction pipe, the diethyl phthalate in the suction pipe is slowly dripped into the beaker containing the ethanol, and the mixture is fully and uniformly stirred by a glass rod, wherein light force is needed in the stirring process, the mixture is slowly and finely stirred for three minutes to be fully mixed, and then the mixture is kept stand for 48 hours.
(2) Blending raw materials of the daily essence: measuring 5ml of limonene, 5ml of eugenol, 5ml of iso-methyl ionone, 5ml of iso-eugenol and 5ml of linalool by using a suction tube, sequentially and uniformly dropping the materials into a measuring cylinder, fully and uniformly stirring the materials for three minutes by using a glass rod to fully mix the materials, and then standing the materials for 48 hours;
(3) selecting raw materials: mixing 75-80 parts of denatured ethanol, 12-16 parts of daily essence, 4.5-4.8 parts of water, 0.033-0.035 part of ethylhexyl methoxycinnamate, 0.032-0.034 part of butyl methoxy dibenzoyl methane and 0.032-0.034 part of ethylhexyl salicylate, wherein the ratio of the denatured ethanol to the daily essence to the water to the ethylhexyl methoxycinnamate to the butyl methoxy dibenzoyl methane to the ethylhexyl salicylate is 80: 15: 4.7: 0.034: 0.033: 0.033.
3. a perfume and a process for its preparation according to claim 1, characterized in that: the method involves a tool: measuring cylinder, rubber head dropper, glass rod, flask, filter paper, and collecting bottle.
4. A perfume and a process for its preparation according to claim 1, wherein the perfume preparation process comprises the steps of:
(1) selecting a flask with the volume of 150 ml;
(2) and (3) sequentially and slowly injecting 80ml of denatured ethanol and 15ml of daily essence into the flask through the port at the top end of the flask, and slowly stirring for five minutes by using a glass rod to completely dissolve the daily essence in the denatured ethanol.
(3) After standing for 48 hours, 4.7ml of water was then poured into the flask and stirred again with a glass rod so that the water was thoroughly mixed with the mixed liquid of denatured ethanol and daily essence, and then allowed to stand for 48 hours.
(4) After 48 hours, 0.034ml of ethylhexyl methoxycinnamate, 0.033ml of butyl methoxydibenzoylmethane and 0.033ml of ethylhexyl salicylate were successively charged into the flask, stirred uniformly with a glass rod, and left to stand for another 48 hours.
(5) And after 48 hours, injecting the mixed liquid into a collecting bottle with filter paper, injecting the filtered liquid in the collecting bottle into a perfume bottle, and plugging the perfume bottle opening by using a plug.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN112022743A (en) * | 2020-09-11 | 2020-12-04 | 广州简灿生物科技有限公司 | Liquid layered perfume and preparation method thereof |
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CN106474009A (en) * | 2016-11-16 | 2017-03-08 | 纪绥粧 | A kind of fall fire cologne |
CN107106470A (en) * | 2015-01-19 | 2017-08-29 | 科思创德国股份有限公司 | For active composition or the polyurethane urea solutions of the composition of spices |
CN109199929A (en) * | 2018-11-07 | 2019-01-15 | 上海芬尚生物科技有限公司 | perfume and preparation method thereof |
CN109310601A (en) * | 2016-06-08 | 2019-02-05 | 高砂香料工业株式会社 | Spices material |
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2020
- 2020-03-21 CN CN202010203993.8A patent/CN111281813A/en active Pending
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