CN111269753B - Essence, tobacco leaf winding formula and application thereof in tobacco products - Google Patents
Essence, tobacco leaf winding formula and application thereof in tobacco products Download PDFInfo
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- CN111269753B CN111269753B CN202010191768.7A CN202010191768A CN111269753B CN 111269753 B CN111269753 B CN 111269753B CN 202010191768 A CN202010191768 A CN 202010191768A CN 111269753 B CN111269753 B CN 111269753B
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/301—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by aromatic compounds
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/32—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by acyclic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention belongs to the technical field of essence and spice, and particularly relates to an essence which comprises components such as Tieguanyin extract, benzyl alcohol, benzaldehyde, phenylacetaldehyde, nerolidol, ethyl butyrate, amyl acetate, butyl acetate, methyl salicylate, ethyl caproate, butyl 2-methylbutanoate, linalool and the like, as well as a perfume fixative and a solvent. The invention also relates to a tobacco leaf rolling formula and application of the essence and the tobacco leaf rolling formula. The essence can endow the cigarette with the aroma characteristics of fruit aroma (citrus aroma, juicy peach aroma or coconut aroma) and the tea aroma of the iron goddess tea, and can improve the sensory quality of the cigarette.
Description
Technical Field
The invention belongs to the technical field of essence and spice, in particular relates to an essence, a tobacco-rolling formula containing the essence, and application of the essence and the tobacco-rolling formula in tobacco products.
Background
The essence is a mixture prepared by manually blending two or more fragrances and certain auxiliary agents according to a certain proportion and a blending process. The perfume is a substance with a certain fragrance or aroma for preparing various essences, and comprises natural perfume and synthetic perfume prepared by different methods. Wherein the natural perfume is an aromatic substance obtained by taking aromatic parts of animals and plants as raw materials and adopting corresponding processing means; the natural perfume has complex composition and rich fragrance, is an important raw material for preparing the essence, but has the following problems in application: firstly, the natural perfume is expensive, and the use amount and the use range of the natural perfume are limited; second, some natural fragrances contain forbidden components, the use of which is limited by safety; thirdly, due to the limitation of animal and plant protection, the supply amount of partial natural perfume is insufficient, and the use requirement cannot be met; fourth, the quality of natural plants is greatly affected by seasons, years, weather, temperature, humidity, etc., so that the quality of natural fragrances fluctuates greatly. Synthetic fragrances have become a current research focus as imitation natural fragrances can ameliorate the above problems.
The essence and spice are widely applied to the fields of tobacco, food, daily chemicals and the like. The essence and spice for cigarettes not only can endow the cigarette products with unique style characteristics, but also can improve the taste of the cigarettes, and are one of important connotations for constructing the core competitiveness of Chinese cigarettes. At present, domestic cigarette products still have defects in the aspects of aroma quality, sensory comfort and the like, and development of a new tobacco essence is urgently needed.
The Tieguanyin tea is originally produced in Anxi, known as tea king, and the Tieguanyin tea with excellent quality has unique taste, is fragrant and sweet, has special viewing sound charm, has residual fragrance after seven times of brewing, and has the expression that the Tieguanyin is more important than the Tieguanyin. Research shows that the main aroma components of the Tie Guanyin comprise alcohols (39.75%), acids (20.42%), esters (11.39%), ketones (9.38%) and other components (16.75%), and the various aroma components are compounded to form the special 'viewing sound rhyme' of the Tie Guanyin, and the special 'viewing sound rhyme' mainly comprises various aroma such as tea aroma, flower aroma, fruit aroma, faint scent, sweet aroma, milk aroma and the like, and has rich, elegant and attractive aroma.
The fruit fragrance is an important fragrance for cigarettes, is mainly used as the top fragrance and body fragrance of cigarettes, can endow the cigarettes with fruit fragrance characteristics, enrich the fragrance of the cigarettes, enable the smoke to be elegant and improve the smoking quality of the cigarettes.
The essence with the compound fruit flavor and Tieguanyin tea flavor is always a flavor blending target which is not achieved by a flavor blending engineer. Therefore, a tobacco essence with the combination of fruit flavor and Tieguanyin tea flavor is needed at present.
Disclosure of Invention
The essence provided by the invention has the aroma of fruit-aroma (citrus aroma, juicy peach aroma or coconut aroma) composite Tieguanyin tea aroma, and can be added into cigarette tobacco shreds to endow the cigarettes with the aroma characteristics of fruit-aroma composite Tieguanyin tea aroma and improve the sensory quality of cigarettes. On the basis, the invention provides a tobacco leaf rolling formula and application of essence and tobacco leaf rolling formula in tobacco products.
The first aspect of the present invention relates to a fragrance comprising:
1 to 40 parts by weight of Tieguanyin extract (e.g., 5 parts by weight, 10 parts by weight, 15 parts by weight, 20 parts by weight, 25 parts by weight, 30 parts by weight, 35 parts by weight, 38 parts by weight)
0.05 to 5 parts by weight of benzyl alcohol (e.g., 0.1 part by weight, 0.2 part by weight, 0.5 part by weight, 0.7 part by weight, 1 part by weight, 2 parts by weight, 3 parts by weight, 4 parts by weight, 5 parts by weight)
0.05 to 6 parts by weight of benzaldehyde (e.g., 0.1 part by weight, 0.2 part by weight, 0.5 part by weight, 0.7 part by weight, 1 part by weight, 2 parts by weight, 3 parts by weight, 4 parts by weight, 5 parts by weight, 6 parts by weight)
0.05 to 5 parts by weight of phenylacetaldehyde (for example, 0.1 part by weight, 0.2 part by weight, 0.5 part by weight, 0.7 part by weight, 1 part by weight, 2 parts by weight, 3 parts by weight, 4 parts by weight, 5 parts by weight)
Nerolidol 0.1-6 parts by weight (e.g., 0.2 parts by weight, 0.3 parts by weight, 0.5 parts by weight, 0.7 parts by weight, 0.9 parts by weight, 1 part by weight, 2 parts by weight, 3 parts by weight, 4 parts by weight, 5 parts by weight, 5.5 parts by weight)
Ethyl butyrate 0.1-5 parts by weight (e.g., 0.2 parts by weight, 0.3 parts by weight, 0.5 parts by weight, 0.7 parts by weight, 0.9 parts by weight, 1 part by weight, 2 parts by weight, 3 parts by weight, 4 parts by weight, 4.5 parts by weight)
Amyl acetate 0.1-5 parts by weight (e.g., 0.2 parts by weight, 0.3 parts by weight, 0.5 parts by weight, 0.7 parts by weight, 0.9 parts by weight, 1 part by weight, 2 parts by weight, 3 parts by weight, 4 parts by weight, 4.5 parts by weight)
Butyl acetate 0.05-5 weight portions (e.g., 0.1 weight portion, 0.2 weight portion, 0.5 weight portion, 0.7 weight portion, 1 weight portion, 2 weight portions, 3 weight portions, 4 weight portions, 5 weight portions)
Methyl salicylate 0.05-6 weight portions (e.g., 0.1 weight portion, 0.2 weight portion, 0.5 weight portion, 0.7 weight portion, 1 weight portion, 2 weight portions, 3 weight portions, 4 weight portions, 5 weight portions, 6 weight portions)
Ethyl caproate 0.05 to 20 parts by weight (e.g., 0.1 part by weight, 0.2 part by weight, 0.5 part by weight, 0.7 part by weight, 1 part by weight, 2 parts by weight, 3 parts by weight, 4 parts by weight, 5 parts by weight, 6 parts by weight, 8 parts by weight, 10 parts by weight, 12 parts by weight, 15 parts by weight, 16 parts by weight, 18 parts by weight)
0.05 to 5 parts by weight of butyl 2-methylbutyrate (for example, 0.1 part by weight, 0.2 part by weight, 0.5 part by weight, 0.7 part by weight, 1 part by weight, 2 parts by weight, 3 parts by weight, 4 parts by weight, 5 parts by weight)
Linalool 0.1-20 parts by weight (e.g., 0.1 part by weight, 0.2 parts by weight, 0.5 parts by weight, 0.7 parts by weight, 1 part by weight, 2 parts by weight, 3 parts by weight, 4 parts by weight, 5 parts by weight, 6 parts by weight, 8 parts by weight, 10 parts by weight, 12 parts by weight, 15 parts by weight, 16 parts by weight, 18 parts by weight)
5 to 50 parts by weight of a perfume fixative (for example, 10 parts by weight, 15 parts by weight, 20 parts by weight, 25 parts by weight, 30 parts by weight, 35 parts by weight, 40 parts by weight, 45 parts by weight)
20 to 90 parts by weight of a solvent (for example, 25 parts by weight, 30 parts by weight, 35 parts by weight, 40 parts by weight, 45 parts by weight, 50 parts by weight, 55 parts by weight, 60 parts by weight, 65 parts by weight, 70 parts by weight, 75 parts by weight, 80 parts by weight, 82 parts by weight, 87 parts by weight);
and, the essence further comprises a component as defined in any one of the following (1) to (3):
(1)
0.01 to 4 parts by weight of hexanal (for example, 0.03 parts by weight, 0.05 parts by weight, 0.08 parts by weight, 0.1 parts by weight, 0.3 parts by weight, 0.5 parts by weight, 0.7 parts by weight, 1 parts by weight, 1.3 parts by weight, 1.6 parts by weight, 2 parts by weight, 2.1 parts by weight, 2.3 parts by weight, 2.5 parts by weight, 2.7 parts by weight, 3 parts by weight, 3.2 parts by weight, 3.4 parts by weight, 3.6 parts by weight, 3.8 parts by weight)
Citral 0.05 to 5 parts by weight (e.g., 0.05 part by weight, 0.08 part by weight, 0.1 part by weight, 0.3 part by weight, 0.5 part by weight, 0.7 part by weight, 1 part by weight, 1.3 parts by weight, 1.6 parts by weight, 2 parts by weight, 2.1 parts by weight, 2.3 parts by weight, 2.5 parts by weight, 2.7 parts by weight, 3 parts by weight, 3.2 parts by weight, 3.4 parts by weight, 3.6 parts by weight, 3.8 parts by weight, 4 parts by weight, 4.2 parts by weight, 4.4 parts by weight, 4.6 parts by weight, 4.8 parts by weight)
Methyl jasmonate 0.03-4 parts by weight (e.g., 0.04 parts by weight, 0.05 parts by weight, 0.08 parts by weight, 0.1 parts by weight, 0.3 parts by weight, 0.5 parts by weight, 0.7 parts by weight, 1 parts by weight, 1.3 parts by weight, 1.6 parts by weight, 2 parts by weight, 2.1 parts by weight, 2.3 parts by weight, 2.5 parts by weight, 2.7 parts by weight, 3 parts by weight, 3.2 parts by weight, 3.4 parts by weight, 3.6 parts by weight, 3.8 parts by weight)
Jasmone 0.01-3 parts by weight (e.g., 0.03 parts by weight, 0.05 parts by weight, 0.08 parts by weight, 0.1 parts by weight, 0.3 parts by weight, 0.5 parts by weight, 0.7 parts by weight, 1 parts by weight, 1.3 parts by weight, 1.6 parts by weight, 2 parts by weight, 2.1 parts by weight, 2.3 parts by weight, 2.5 parts by weight, 2.7 parts by weight, 3 parts by weight)
(Z) -3-hexenyl propionate 0.05-8 parts by weight (e.g., 0.05 parts by weight, 0.08 parts by weight, 0.1 parts by weight, 0.3 parts by weight, 0.5 parts by weight, 0.7 parts by weight, 1 parts by weight, 1.3 parts by weight, 1.6 parts by weight, 2 parts by weight, 2.1 parts by weight, 2.3 parts by weight, 2.5 parts by weight, 2.7 parts by weight, 3 parts by weight, 3.2 parts by weight, 3.4 parts by weight, 3.6 parts by weight, 3.8 parts by weight, 4 parts by weight, 4.5 parts by weight, 5 parts by weight, 5.5 parts by weight, 6 parts by weight, 6.5 parts by weight, 7 parts by weight, 7.5 parts by weight, 7.8 parts by weight)
0.05 to 4 parts by weight of sweet orange oil (for example, 0.05 part by weight, 0.08 part by weight, 0.1 part by weight, 0.3 part by weight, 0.5 part by weight, 0.7 part by weight, 1 part by weight, 1.3 parts by weight, 1.6 parts by weight, 2 parts by weight, 2.1 parts by weight, 2.3 parts by weight, 2.5 parts by weight, 2.7 parts by weight, 3 parts by weight, 3.2 parts by weight, 3.4 parts by weight, 3.6 parts by weight, 3.8 parts by weight)
0.05 to 4 parts by weight (for example, 0.05 part by weight, 0.08 part by weight, 0.1 part by weight, 0.3 part by weight, 0.5 part by weight, 0.7 part by weight, 1 part by weight, 1.3 parts by weight, 1.6 parts by weight, 2 parts by weight, 2.1 parts by weight, 2.3 parts by weight, 2.5 parts by weight, 2.7 parts by weight, 3 parts by weight, 3.2 parts by weight, 3.4 parts by weight, 3.6 parts by weight, 3.8 parts by weight) of lime oil;
(2)
1 to 22 parts by weight of tetradecaldehyde (for example, 3 parts by weight, 5 parts by weight, 7 parts by weight, 8 parts by weight, 10 parts by weight, 11 parts by weight, 13 parts by weight, 15 parts by weight, 17 parts by weight, 19 parts by weight, 21 parts by weight)
Gamma-undecalactone 0.05-4 parts by weight (e.g., 0.05 parts by weight, 0.08 parts by weight, 0.1 parts by weight, 0.3 parts by weight, 0.5 parts by weight, 0.7 parts by weight, 1 parts by weight, 1.3 parts by weight, 1.6 parts by weight, 2 parts by weight, 2.1 parts by weight, 2.3 parts by weight, 2.5 parts by weight, 2.7 parts by weight, 3 parts by weight, 3.2 parts by weight, 3.4 parts by weight, 3.6 parts by weight, 3.8 parts by weight)
0.05 to 3 parts by weight of sweet orange oil (for example, 0.05 part by weight, 0.08 part by weight, 0.1 part by weight, 0.3 part by weight, 0.5 part by weight, 0.7 part by weight, 1 part by weight, 1.3 parts by weight, 1.6 parts by weight, 2 parts by weight, 2.1 parts by weight, 2.3 parts by weight, 2.5 parts by weight, 2.7 parts by weight, 3 parts by weight)
0.1 to 16 parts by weight (for example, 0.3 parts by weight, 0.5 parts by weight, 0.7 parts by weight, 1 part by weight, 2 parts by weight, 4 parts by weight, 6 parts by weight, 8 parts by weight, 10 parts by weight, 11 parts by weight, 13 parts by weight, 15 parts by weight, 16 parts by weight) of benzyl benzoate;
(3)
0.01 to 4 parts by weight of hexanal (for example, 0.02 part by weight, 0.03 part by weight, 0.05 part by weight, 0.08 part by weight, 0.1 part by weight, 0.3 part by weight, 0.5 part by weight, 0.7 part by weight, 1 part by weight, 1.3 part by weight, 1.6 part by weight, 2 parts by weight, 2.1 parts by weight, 2.3 parts by weight, 2.5 parts by weight, 2.7 parts by weight, 3 parts by weight, 3.2 parts by weight, 3.4 parts by weight, 3.6 parts by weight, 3.8 parts by weight)
Heliotropin 0.05-6 weight parts (e.g., 0.05 weight parts, 0.08 weight parts, 0.1 weight parts, 0.3 weight parts, 0.5 weight parts, 0.7 weight parts, 1 weight parts, 1.3 weight parts, 1.6 weight parts, 2 weight parts, 2.1 weight parts, 2.3 weight parts, 2.5 weight parts, 2.7 weight parts, 3 weight parts, 3.2 weight parts, 3.4 weight parts, 3.6 weight parts, 3.8 weight parts, 4 weight parts, 4.3 weight parts, 4.5 weight parts, 4.7 weight parts, 5 weight parts, 5.2 weight parts, 5.4 weight parts, 5.6 weight parts, 5.8 weight parts)
Jasmine lactone 0-4 weight parts (for example, 0.5 weight parts, 1 weight parts, 1.3 weight parts, 1.6 weight parts, 2 weight parts, 2.2 weight parts, 2.5 weight parts, 2.7 weight parts, 3 weight parts, 3.1 weight parts, 3.3 weight parts, 3.5 weight parts, 3.7 weight parts, 3.9 weight parts)
0.5 to 20 parts by weight of propionolactone (for example, 0.7 part by weight, 1 part by weight, 2 parts by weight, 3 parts by weight, 5 parts by weight, 7 parts by weight, 9 parts by weight, 10 parts by weight, 12 parts by weight, 14 parts by weight, 16 parts by weight, 18 parts by weight, 19 parts by weight)
Vanillin 0.01-3 parts by weight (e.g., 0.02 part by weight, 0.03 part by weight, 0.05 part by weight, 0.08 part by weight, 0.1 part by weight, 0.3 part by weight, 0.5 part by weight, 0.7 part by weight, 1 part by weight, 1.3 part by weight, 1.6 part by weight, 2 parts by weight, 2.1 parts by weight, 2.3 parts by weight, 2.5 parts by weight, 2.7 parts by weight, 3 parts by weight)
0.05 to 6 parts by weight of ethyl vanillin (e.g., 0.05 part by weight, 0.08 part by weight, 0.1 part by weight, 0.3 part by weight, 0.5 part by weight, 0.7 part by weight, 1 part by weight, 1.3 part by weight, 1.6 part by weight, 2 parts by weight, 2.1 parts by weight, 2.3 parts by weight, 2.5 parts by weight, 2.7 parts by weight, 3 parts by weight, 3.2 parts by weight, 3.4 parts by weight, 3.6 parts by weight, 3.8 parts by weight, 4 parts by weight, 4.3 parts by weight, 4.5 parts by weight, 4.7 parts by weight, 5 parts by weight, 5.2 parts by weight, 5.4 parts by weight, 5.6 parts by weight, 5.8 parts by weight).
In some embodiments of the first aspect of the present invention, the perfume comprises:
in some embodiments of the first aspect of the present invention, the perfume comprises:
in some embodiments of the first aspect of the present invention, the perfume comprises:
in some embodiments of the first aspect of the invention, one or more of the following a to F are included:
A. the perfume fixing agent is selected from propylene glycol, glycerol and sorbitol, preferably propylene glycol;
B. the solvent is selected from ethanol and aqueous solutions thereof, preferably ethanol aqueous solutions;
more preferably, the concentration of the aqueous ethanol solution is 30% (W/W) to 90% (W/W), for example 50% (W/W), 70% (W/W), 80% (W/W);
C. the Tieguanyin extract is prepared by the following steps:
(1) Directly steam distilling Tieguanyin tea, and collecting distillate;
(2) Separating oil from water of the distillate, and collecting water phase to obtain Tieguanyin extract;
preferably, in step (1), the distillation flow rate of the direct steam distillation is 20 to 40Kg/h, for example 25Kg/h, 30Kg/h, 35Kg/h;
preferably, in step (1), the time of the direct steam distillation is from 2 to 4 hours, for example 2.5 hours, 3 hours, 3.5 hours;
preferably, the weight of the Tie Guanyin extract is 4-8 times, such as 5 times, 6 times, 7 times, the weight of the Tie Guanyin finished tea;
preferably, in step (1), the direct steam distillation is performed by a steam distillation still;
D. the essence is tobacco essence;
E. the first perfume of the essence is selected from benzyl alcohol, benzaldehyde, phenylacetaldehyde, nerolidol, ethyl butyrate, amyl acetate, butyl acetate, n-hexanal, citral, tetradecal, heliotropin, sweet orange oil, white lemon oil, vanillin and ethyl vanillin;
F. the body aroma of the essence is selected from Tieguanyin extract, methyl salicylate, ethyl caproate, butyl 2-methylbutyrate, linalool, methyl jasmonate, jasmone, (Z) -propionic acid-3-hexenyl ester, gamma-undecalactone, benzyl benzoate, jasmonate, propionolactone, sweet orange oil, white lemon oil, vanillin and ethyl vanillin.
In some embodiments of the first aspect of the present invention, the iron goddess tea finished product refers to a finished tea produced by the steps of picking, sun-drying, making, deactivating enzyme, kneading, drying, sorting and the like of the iron goddess fresh leaves.
In some embodiments of the first aspect of the present invention, the top note of the perfume comprises benzyl alcohol, benzaldehyde, phenylacetaldehyde, nerolidol, ethyl butyrate, amyl acetate, butyl acetate, n-hexanal, citral, sweet orange oil, and white lemon oil.
In some embodiments of the first aspect of the present invention, the top note of the flavour comprises benzyl alcohol, benzaldehyde, phenylacetaldehyde, nerolidol, ethyl butyrate, amyl acetate, butyl acetate, tetradecaldehyde, and orange oil.
In some embodiments of the first aspect of the present invention, the top note of the perfume comprises benzyl alcohol, benzaldehyde, phenylacetaldehyde, nerolidol, ethyl butyrate, amyl acetate, butyl acetate, n-hexanal, heliotropin, vanillin, and ethyl vanillin.
In some embodiments of the first aspect of the present invention, the body note of the essence comprises Tieguanyin extract, methyl salicylate, ethyl caproate, butyl 2-methylbutanoate, linalool, methyl jasmonate, jasmone, (Z) -prop-3-enyl ester, sweet orange oil and white lemon oil.
In some embodiments of the first aspect of the present invention, the body note of the essence comprises Tieguanyin extract, methyl salicylate, ethyl caproate, butyl 2-methylbutanoate, linalool, gamma-undecalactone, benzyl benzoate, and orange oil.
In some embodiments of the first aspect of the present invention, the body note of the essence comprises Tieguanyin extract, methyl salicylate, ethyl caproate, butyl 2-methylbutanoate, linalool, jasmonate, propionolactone, vanillin, and ethyl vanillin.
In some embodiments of the first aspect of the present invention, any one or more of orange oil, lime oil, vanillin and ethyl vanillin may be used as both the top note fragrance and the body note fragrance.
The second aspect of the invention relates to a tobacco leaf rolling formula comprising the essence according to the first aspect of the invention.
In some embodiments of the second aspect of the invention, the flavour comprises 0.005% to 15%, for example 0.01%, 0.02%, 0.05%, 0.06%, 0.08%, 0.1%, 0.3%, 0.5%, 0.7%, 1%, 2%, 3%, 5%, 6%, 7%, 9%, 10%, 11%, 12%, 13%, 14%, 15% by weight of the total weight of the tobacco leaf group formulation.
A third aspect of the invention relates to a tobacco product comprising the flavour according to the first aspect of the invention or the tobacco leaf roller formula according to the second aspect of the invention.
In some embodiments of the third aspect of the present invention, the tobacco product is a cigarette.
A fourth aspect of the invention relates to the use of a flavour according to the first aspect of the invention or a tobacco leaf roller formula according to the second aspect of the invention in tobacco products.
In some embodiments of the fourth aspect of the invention, the tobacco product is a cigarette.
A fifth aspect of the invention relates to the use of the essence according to the first aspect of the invention or the tobacco leaf set formulation according to the second aspect of the invention for improving the sensory quality of cigarettes or for imparting a aroma profile to cigarettes with a fruit aroma compound Tieguanyin tea aroma.
In some embodiments of the fifth aspect of the invention, the fruit aroma is selected from citrus, juicy peach and coconut.
In some embodiments of the fifth aspect of the invention, the fruit note is a citrus note, a juicy peach note, or a coconut note.
In some embodiments of the fifth aspect of the invention, the evaluation index of the sensory quality of the cigarette is selected from the group consisting of gloss, aroma, harmony, miscellaneous gases, irritation and aftertaste.
In the invention, the sweet orange oil is obtained by cold grinding fresh whole fruits, cold pressing fresh fruit peels or distilling residues or broken fruit peels after cold pressing through water vapor. Belongs to conventional food flavor and can be directly purchased from the market.
In the invention, white lemon oil belongs to one of essential oils, and is obtained by steam distillation or cold pressing of fruits or peels of white lemon which is an aromatic plant. Belongs to conventional food flavor and can be directly purchased from the market.
In the present invention, "top note" is also referred to as top note, a structural term of fragrance. Refers to the characteristic fragrance of the product which is smelled initially. Mainly the fragrance feeling represented by some low boiling point and volatile odor molecules, and the fragrance style of the product can be represented most. Its corresponding perfume is known as a top note perfume.
In the present invention, "body note" is also referred to as a middle or middle note. The main fragrance of the product is the main component of the fragrance type, and represents the most main fragrance characteristic of the product. Is smelled after the first fragrance, and can be kept stable or consistent for a long time. Its corresponding perfume is called body perfume.
In the present invention, the "tobacco product" is a preference commodity produced from tobacco leaves. According to the characteristics of different types of tobacco leaves, different processing and manufacturing methods are applied to produce various tobacco products so as to meet the hobby requirements of different consumers. Among them, cigarettes account for the vast majority.
The invention has at least one of the following beneficial effects:
1. the essence provided by the invention has the aroma of fruit-aroma (citrus aroma, juicy peach aroma or coconut aroma) composite Tieguanyin tea aroma, and can endow the cigarette with the aroma characteristic of fruit-aroma composite Tieguanyin tea aroma.
2. The essence of the invention can improve the sensory quality of cigarettes when being added into cigarettes.
Detailed Description
Embodiments of the present invention will now be described more fully hereinafter with reference to the accompanying examples, in which it is shown, however, that the examples are shown, and in which the invention is practiced. The following description of at least one exemplary embodiment is merely exemplary in nature and is in no way intended to limit the invention, its application, or uses. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Sweet orange oil is purchased from Huabao edible essence and spice (Shanghai) limited company;
white lemon oil was purchased from Shenzhen Boton fragrance Co.
Example 1 citrus fruit-aroma composite essence with Tieguanyin tea aroma characteristics
The components are mixed according to the formula shown in the table 1-1 to prepare the No. 1-5 essence respectively. The No. 1 essence is a control sample. Wherein benzyl alcohol, benzaldehyde, phenylacetaldehyde, n-hexanal, citral, nerolidol, ethyl butyrate, amyl acetate and butyl acetate are used as top-note perfume, tieguanyin extract, methyl jasmonate, jasmone, methyl salicylate, ethyl caproate, butyl 2-methylbutyrate, linalool and (Z) -3-hexenyl propionate are used as body-note perfume, sweet orange oil and white lemon oil are used as top-note perfume and body-note perfume, propylene glycol is used as a perfume fixative, and 70% ethanol aqueous solution is used as solvent.
The preparation method of the Tieguanyin extract comprises the following steps: 15Kg of Tieguanyin tea leaves are weighed and placed on a sieve plate of a steam distillation kettle, steam enters the distillation kettle from the lower part and fully contacts, disperses and gasifies with a tea material layer, mixed steam of formed water and volatile essential oil is led out from a steam outlet at the upper part of the distillation kettle, condensed by a condenser and then enters an oil-water separator for separation, the steaming flow is controlled at 25Kg/h, the distillation time is 2.5h, and distillation is finished when the weight of the pure dew of the Tieguanyin tea leaves is 62.5Kg, so that the Tieguanyin extract is obtained.
Table 1-1 1# 5 essence formulations
Referring to the odor and fragrance index evaluation in YC/T497-2014 of Chinese style sensory evaluation method of cigarette, 12 professional odor and fragrance evaluation operators evaluate the fragrance characteristics of No. 1-No. 5 essence, the fragrance is divided into 5 minutes, and the average result is shown in tables 1-2.
The intensity of fruit fragrance of the No. 1-5 essence is compared and evaluated by 12 professional fragrance evaluation workers, an average result is obtained and is recorded as a fragrance holding capacity score, the fragrance holding capacity score is divided into 5 scores, and the average result is shown in tables 1-2.
Table 1-2 1# 5 evaluation results of fragrance characteristics and fragrance-holding ability of fragrances
As can be seen from tables 1-2, the fruit note and the holding power of the No. 2, no. 3, no. 4 and No. 5 essences are stronger than those of the No. 1 essence, and the fruit note and the holding power of the No. 3 essence are best. The citrus fruit-flavored composite Tieguanyin tea with 2# essence, 3# essence, 4# essence and 5# essence has outstanding flavor, and lasting and stable flavor.
And respectively applying the prepared No. 1-No. 5 essence to cigarettes to evaluate the aroma characteristics and the sensory quality of the cigarettes. Uniformly spraying No. 1-No. 5 essence on tobacco shreds according to the weight of 0.1% of the tobacco shreds, baking, and rolling into cigarettes; the blank sample was applied with a 70% ethanol solution at 0.1% by weight of tobacco. The aroma characteristics of the cigarettes are evaluated according to YC/T497-2014 'sensory evaluation method of Chinese style of cigarettes'; sensory quality is according to GB 5606.4-2005 "fourth part of cigarette: sensory technology requirements, evaluation; the average results are shown in tables 1-3 and 1-4, as assessed by 13 professionals.
Table 1-3 evaluation results of aroma characteristics of cigarettes
As can be seen from tables 1-3, the cigarettes with the 2# essence, 3# essence, 4# essence, and 5# essence applied had stronger fruit flavor characteristics than the 1# essence and the blank, and the cigarette samples with the 3# essence applied had the strongest fruit flavor characteristics. The fragrance characteristics of the cigarette and citrus fruit-flavor composite Tieguanyin tea flavor can be endowed by applying No. 2, no. 3, no. 4 and No. 5 essence.
Tables 1 to 4 sensory quality evaluation results of cigarettes
As can be seen from tables 1-4, the sensory quality of cigarettes with the No. 2, no. 3, no. 4 and No. 5 flavors is higher than that of cigarettes with the No. 1 flavors and the blank, and the smoking quality and the sensory comfort of the cigarettes can be effectively improved. Wherein, the cigarettes with the No. 2, no. 3 and No. 4 flavors are more remarkable in the aspects of improving aroma, reducing miscellaneous gases, reducing irritation and other sensory evaluation indexes.
Example 2 juicy peach fruit-aroma composite Tieguanyin tea aromaEssence for symptom
The components are mixed according to the formula shown in the table 2-1 to prepare the No. 1 and No. 6-9 essence respectively.
The No. 1 essence is a control sample. Wherein benzyl alcohol, benzaldehyde, phenylacetaldehyde, tetradecyl aldehyde, nerolidol, ethyl butyrate, amyl acetate and butyl acetate are used as top-note perfume, tieguanyin extract, methyl salicylate, ethyl caproate, butyl 2-methylbutyrate, gamma-undecalactone, linalool and benzyl benzoate are used as body-note perfume, sweet orange oil is used as top-note perfume and body-note perfume, propylene glycol is used as a perfume fixative, and 70% ethanol aqueous solution is used as solvent.
The preparation method of the Tieguanyin extract comprises the following steps: 15Kg of Tieguanyin tea leaves are weighed and placed on a sieve plate of a steam distillation kettle, steam enters the distillation kettle from the lower part and fully contacts, disperses and gasifies with a tea material layer, mixed steam of formed water and volatile essential oil is led out from a steam outlet at the upper part of the distillation kettle, condensed by a condenser and then enters an oil-water separator for separation, the steaming flow is controlled to be 30Kg/h, the distillation time is 2.5h, and distillation is finished when the weight of the pure dew of the Tieguanyin tea leaves is 75Kg, so that the Tieguanyin extract is obtained.
Table 2-1 1# and 6# to 9# essence formulations
Referring to the odor index judgment in YC/T497-2014' method for evaluating Chinese style sensory evaluation of cigarette, 12 professional odor evaluation staff evaluate the odor characteristics of No. 1 and No. 6-9 essence, the odor is divided into 5 minutes, and average results are shown in Table 2-2.
The fruit fragrance intensity of the No. 1 and No. 6-9 essences is compared and evaluated by 12 professional fragrance evaluation staff, the average result is recorded as fragrance holding capacity score, the fragrance holding capacity score is divided into 5 points, and the average result is shown in tables 2-2.
Evaluation results of fragrance characteristics and fragrance holding ability of fragrances in tables 2 to 21 #, 6# to 9#
As can be seen from tables 2-2, the fruit note and the holding power of the 6# essence, the 7# essence, the 8# essence and the 9# essence are stronger than those of the 1# essence, wherein the fruit note and the holding power of the 6# essence are best. The juicy peach fruit flavor compound Tieguanyin tea flavor of the No. 6, no. 7, no. 8 and No. 9 essence has outstanding flavor, and the flavor is more durable and stable.
And respectively applying the prepared No. 1 and No. 6-No. 9 essences into cigarettes to evaluate the aroma characteristics and the sensory quality of the cigarettes. Uniformly spraying No. 1 and No. 6-No. 9 essence on tobacco shreds according to the weight of 0.1% of the tobacco shreds, baking, and rolling into cigarettes; the blank sample was applied with a 70% ethanol solution at 0.1% by weight of tobacco. The aroma characteristics of the cigarettes are evaluated according to YC/T497-2014 'sensory evaluation method of Chinese style of cigarettes'; sensory quality is according to GB 5606.4-2005 "fourth part of cigarette: sensory technology requirements, evaluation; the average results are shown in tables 2-3 and 2-4, as assessed by 13 professionals.
Table 2-3 evaluation results of aroma characteristics of cigarettes
As can be seen from tables 2-3, the cigarettes with the No. 6, no. 7, no. 8, no. 9 flavors had stronger fruit flavor characteristics than the No. 1 flavors and the blank, and the cigarette samples with the No. 6 flavors had the strongest fruit flavor characteristics. The fragrance characteristics of the juicy peach fruit-flavored composite Tieguanyin tea flavor of the cigarettes can be endowed by applying No. 6, no. 7, no. 8 and No. 9 essence.
Table 2-4 sensory quality evaluation results of cigarettes
As can be seen from tables 2-4, the sensory quality of cigarettes with the No. 6, no. 7, no. 8 and No. 9 flavors is higher than that of cigarettes with the No. 1 flavors and the blank, and the smoking quality and the sensory comfort of the cigarettes can be effectively improved. Wherein, the cigarettes with the No. 6, no. 7, no. 8 and No. 9 essences have more remarkable performances in the aspects of improving aroma, improving smoke harmony, reducing miscellaneous gases, reducing irritation and other sensory quality.
Example 3 Cocois fruit fragrance essence with characteristics of Tieguanyin tea fragrance
The components are mixed according to the formula shown in the table 3-1 to prepare the No. 1 and No. 10-No. 13 essence respectively. The No. 1 essence is a control sample. Wherein benzyl alcohol, benzaldehyde, phenylacetaldehyde, n-hexanal, heliotropin, nerolidol, ethyl butyrate, amyl acetate and butyl acetate are used as top-note perfume, tieguanyin extract, jasmine lactone, methyl salicylate, ethyl caproate, butyl 2-methylbutyrate, propionolactone and linalool are used as body-note perfume, vanillin and ethyl vanillin are used as top-note perfume and body-note perfume, propylene glycol is used as perfume fixative, and 70% ethanol aqueous solution is used as solvent.
The preparation method of the Tieguanyin extract comprises the following steps: 15Kg of Tieguanyin tea leaves are weighed and placed on a sieve plate of a steam distillation kettle, steam enters the distillation kettle from the lower part and fully contacts, disperses and gasifies with a tea material layer, mixed steam of formed water and volatile essential oil is led out from a steam outlet at the upper part of the distillation kettle, condensed by a condenser and then enters an oil-water separator for separation, the steaming flow is controlled at 35Kg/h, the distillation time is 3h, and distillation is finished when the weight of the pure dew of the tea leaves of the Tieguanyin tea leaves is 105Kg, so that the Tieguanyin extract is obtained.
Table 3-1 1# and 10# to 13# essence formulations
Referring to the odor index judgment in YC/T497-2014' method for evaluating Chinese style sensory evaluation of cigarette, 12 professional odor evaluation staff evaluate the odor characteristics of No. 1 and No. 10-No. 13 essence, the odor is divided into 5, and the average result is shown in Table 3-2.
The fruit fragrance intensity of the No. 1 and No. 10-No. 13 essences is compared and evaluated by 12 professional evaluation staff, the average result is recorded as fragrance holding capacity score, the fragrance holding capacity score is divided into 5 points, and the average result is shown in Table 3-2.
Evaluation results of fragrance characteristics and fragrance holding ability of fragrances in tables 3 to 21 #, 10# to 13#
As can be seen from tables 3-2, the fruit note and the holding power of the No. 10, no. 11, no. 12 and No. 13 essences were stronger than those of the No. 1 essence, and the fruit note and the holding power of the No. 12 essence were best shown. The coconut fruit-flavored compound Tieguanyin tea with 10# essence, 11# essence, 12# essence and 13# essence has outstanding flavor, and the flavor is more durable and stable.
And respectively applying the prepared No. 1 and No. 10-No. 13 essences into cigarettes to evaluate the aroma characteristics and the sensory quality of the cigarettes. Uniformly spraying No. 1 and No. 10-No. 13 essence on tobacco shreds according to the weight of 0.1% of the tobacco shreds, baking, and rolling into cigarettes; the blank sample was applied with a 70% ethanol solution at 0.1% by weight of tobacco. The aroma characteristics of the cigarettes are evaluated according to YC/T497-2014 'sensory evaluation method of Chinese style of cigarettes'; sensory quality is according to GB 5606.4-2005 "fourth part of cigarette: sensory technology requirements, evaluation; the average results are shown in tables 3-3 and 3-4, as assessed by 13 professionals.
TABLE 3-3 evaluation results of aroma characteristics of cigarettes
As can be seen from tables 3-3, the cigarettes with applied No. 10, no. 11, no. 12, no. 13 flavors exhibited stronger fruit flavor characteristics than the No. 1 flavors and the blank, and the cigarette samples with applied No. 12 flavors exhibited the strongest fruit flavor characteristics. The 10# essence, the 11# essence, the 12# essence and the 13# essence can be applied to endow the cigarettes with the aroma characteristics of the coconut aroma and the iron goddess tea aroma.
Tables 3-4 sensory quality evaluation results of cigarettes
As can be seen from tables 3-4, the sensory quality of cigarettes with 10#, 11#, 12#, 13# flavors was higher than that of cigarettes with 1# flavors and blank, and the smoking quality and sensory comfort of cigarettes were effectively improved. Wherein, the cigarettes with 10#, 11#, 12#, 13# essence are more remarkable in the aspects of improving aroma, improving smoke harmony, reducing miscellaneous gases, reducing irritation and other sensory quality.
It is apparent that the above examples are given by way of illustration only and are not limiting of the embodiments. Other variations or modifications of the above teachings will be apparent to those of ordinary skill in the art. It is not necessary here nor is it exhaustive of all embodiments. While still being apparent from variations or modifications that may be made by those skilled in the art are within the scope of the invention.
Claims (18)
1. An essence consists of fruit-flavor characteristic components and Tieguanyin tea-flavor characteristic components, wherein the Tieguanyin tea-flavor characteristic components are as follows:
and, the fruity characteristic component is any one of the following (1) to (3):
(1)
(2)
(3)
2. the flavour concentrate of claim 1, wherein the flavour concentrate consists of the following components:
3. the flavour concentrate of claim 1, wherein the flavour concentrate consists of the following components:
4. the flavour concentrate of claim 1, wherein the flavour concentrate consists of the following components:
5. the flavour according to any one of claims 1 to 4, characterized by one or more of the following a to F:
A. the perfume fixing agent is selected from propylene glycol, glycerol and sorbitol;
B. the solvent is selected from ethanol and aqueous solutions thereof;
C. the Tieguanyin extract is prepared by the following steps:
1) Directly steam distilling Tieguanyin tea, and collecting distillate;
2) Oil-water separation is carried out on the distillate, and water phase matters are collected to obtain the Tieguanyin extract;
D. the essence is tobacco essence;
E. the first perfume of the essence is selected from benzyl alcohol, benzaldehyde, phenylacetaldehyde, nerolidol, ethyl butyrate, amyl acetate, butyl acetate, n-hexanal, citral, tetradecal, heliotropin, sweet orange oil, white lemon oil, vanillin and ethyl vanillin;
F. the body aroma of the essence is selected from Tieguanyin extract, methyl salicylate, ethyl caproate, butyl 2-methylbutyrate, linalool, methyl jasmonate, jasmone, (Z) -propionic acid-3-hexenyl ester, gamma-undecalactone, benzyl benzoate, jasmonate, propionolactone, sweet orange oil, white lemon oil, vanillin and ethyl vanillin.
6. The essence according to claim 5, wherein in item B, the concentration of the aqueous ethanol solution is 30% (W/W) to 90% (W/W).
7. The essence according to claim 5, wherein in the item C, in the step 1), the distilled flow rate of the direct steam distillation is 20 to 40Kg/h.
8. The flavor according to claim 5, wherein in item C, in step 1), the direct steam distillation is carried out for a period of 2 to 4 hours.
9. The essence according to claim 5, wherein in item C, the weight of the Tieguanyin extract is 4 to 8 times the weight of the Tieguanyin tea leaves.
10. A tobacco leaf winding composition comprising the flavour of any one of claims 1 to 9.
11. A wrapped tobacco leaf group composition according to claim 10 wherein the flavour comprises 0.005% to 15% by weight of the total wrapped tobacco leaf group composition.
12. A tobacco product comprising the flavour of any one of claims 1 to 9 or the tobacco leaf winding composition of claim 10 or 11.
13. A smoking article according to claim 12, which is a cigarette.
14. Use of the flavour of any one of claims 1 to 9 or the tobacco leaf winding composition of claim 10 or 11 in tobacco products.
15. The use according to claim 14, wherein the tobacco product is a cigarette.
16. Use of the essence of any one of claims 1 to 9 or the tobacco leaf set composition of claim 10 or 11 for improving the sensory quality of cigarettes or for imparting a aroma profile to cigarettes with a fruit aroma composite Tie Guanyin tea aroma.
17. Use according to claim 16, wherein the fruit aroma is selected from citrus, juicy peach and coconut aroma.
18. The use according to claim 16, wherein the evaluation index of the sensory quality of the cigarette is selected from the group consisting of gloss, aroma, harmony, miscellaneous gases, irritation and aftertaste.
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