CN111141332A - Flow guide device for liquor picking process of distilled liquor and online measurement system and method - Google Patents

Flow guide device for liquor picking process of distilled liquor and online measurement system and method Download PDF

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CN111141332A
CN111141332A CN202010048192.9A CN202010048192A CN111141332A CN 111141332 A CN111141332 A CN 111141332A CN 202010048192 A CN202010048192 A CN 202010048192A CN 111141332 A CN111141332 A CN 111141332A
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CN111141332B (en
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彭黎辉
马浩程
李群庆
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Tsinghua University
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    • G01MEASURING; TESTING
    • G01DMEASURING NOT SPECIALLY ADAPTED FOR A SPECIFIC VARIABLE; ARRANGEMENTS FOR MEASURING TWO OR MORE VARIABLES NOT COVERED IN A SINGLE OTHER SUBCLASS; TARIFF METERING APPARATUS; MEASURING OR TESTING NOT OTHERWISE PROVIDED FOR
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    • G01D21/02Measuring two or more variables by means not covered by a single other subclass
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    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12HPASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H6/00Methods for increasing the alcohol content of fermented solutions or alcoholic beverages
    • C12H6/02Methods for increasing the alcohol content of fermented solutions or alcoholic beverages by distillation

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Abstract

The invention relates to a flow guide device for a distilled liquor picking process, which comprises: the device comprises an inlet pipe, an outlet pipe, a first standard container, a second standard container and a plurality of control valves; the first standard container and the second standard container are spaced and independently arranged; the leading-in pipe comprises a first branch and a second branch, so that the wine body can flow into the first standard container from the first branch or flow into the second standard container from the second branch; the delivery pipe is arranged at the outlets of the first standard container and the second standard container, so that the wine in the first standard container and the second standard container can flow into the delivery pipe after flowing out; the control valves are used for controlling the wine bodies to alternately flow into the first standard container and the second standard container and enabling the wine bodies in the first standard container and the second standard container to alternately flow out. The invention also relates to an online measuring system and method for the flow and the alcoholic strength in the process of picking the distilled liquor.

Description

Flow guide device for liquor picking process of distilled liquor and online measurement system and method
Technical Field
The invention relates to the technical field of automatic machinery and equipment, in particular to a flow guide device used in a liquor-picking process of distilled liquor and an online measurement system and method for flow and alcoholic strength.
Background
The wine is the traditional culture of Chinese nationality and is a treasure in five thousand years of China civilization, but the existing Chinese liquor manufacturing industry also belongs to labor-intensive industry, the mechanization degree is low, and most liquor enterprises are in the original mode of manual operation production. In recent years, under the influence of the rising of labor cost, the increasing shortage of land resources and the national industrial policy of high efficiency and low consumption development, the Chinese liquor brewing production industry makes technological innovation and changes of the traditional production mode urgently.
The brewing industry has an old word: "producing fragrance depends on fermentation, extracting fragrance depends on distillation, and picking wine depends on wine picking workers", which shows the importance of the distillation wine picking process. In the process of distilling and picking wine, the wine yield and the wine quality of different vinasses are different, and the quality of the wine flowing at different moments of each vinasse in a retort is also different. The flow rate of the flowing wine and the alcoholic strength of the flowing wine are two important parameters in the process, and most of wineries adopt the traditional manual measurement mode at present, so that the development requirements of data generation, automation, intellectualization and fine management in the brewing industry are not met.
For flow and alcohol content measurement during liquor extraction, the following requirements are mainly set:
(1) the piping must be open so that the pressure in the piping does not affect the upstream distillation and condensation;
(2) the dynamic measurement range is large, the variation range can be from 0 to 10L/min or even higher, and the wine flowing time is an important index in production, so the flow of a few mL/min also needs to be measured more accurately;
(3) the requirement on the accuracy of accumulated flow measurement is high, the flow rate of wine is also an important index in production, and some alcohol degree measurement methods also depend on accurate accumulated flow measurement, so that the used flowmeter not only can accurately measure the real-time flow, but also has higher accuracy of accumulated flow measurement;
(4) the real-time requirement is high, and the real-time flow data of distilled liquor can be used for guiding retort loading and liquor grading, so that the flow and alcohol degree measurement must have high real-time performance.
However, the existing flow meter and alcohol meter cannot realize online real-time measurement of the flow rate and alcohol content of the wine body in an open pipeline.
Disclosure of Invention
Based on the background, the invention provides an online measurement system and method for the flow and the alcoholic strength of the flowing liquor in the liquor distilling and picking process, so that the real-time online monitoring of the flow and the alcoholic strength of the base liquor produced in the liquor picking process is realized, necessary data support is provided for liquor grading and fine management, and the 'picked liquor' does not depend on liquor picking workers any more. The method hopes to carry out some preliminary exploration on the datamation of the white spirit brewing process link in China through research, and plays a certain role in promoting the intellectualization of the brewing production and the refinement of the production management of the white spirit industry.
A flow guide device for a liquor extracting process of distilled liquor comprises: the device comprises an inlet pipe, an outlet pipe, a first standard container, a second standard container and a plurality of control valves; the first standard container and the second standard container are spaced and independently arranged; the leading-in pipe comprises a first branch and a second branch; the first branch is suspended and arranged at the inlet of the first standard container at intervals, so that wine can flow into the first standard container from the first branch; the second branch is suspended and arranged at the inlet of the second standard container at intervals, so that wine can flow into the second standard container from the second branch; the delivery pipe is arranged at the outlets of the first standard container and the second standard container, so that the wine in the first standard container and the second standard container can flow into the delivery pipe after flowing out; the control valves are used for controlling the wine bodies to alternately flow into the first standard container and the second standard container and enabling the wine bodies in the first standard container and the second standard container to alternately flow out.
A flow guide device for a liquor extracting process of distilled liquor comprises: the device comprises an inlet pipe, an outlet pipe, a first standard container, a second standard container, a moving device and a plurality of control valves; the first standard container and the second standard container are spaced and independently arranged; the leading-in pipe is arranged at the inlets of the first standard container and the second standard container in a suspending way; the moving device is used for moving the introducing pipe above the first standard container and the second standard container so as to make the wine body alternately flow into the first standard container and the second standard container; the delivery pipe is arranged at the outlets of the first standard container and the second standard container, so that the wine in the first standard container and the second standard container can flow into the delivery pipe after flowing out; the control valves are used for controlling the alternating outflow of the wine bodies in the first standard container and the second standard container.
An online measurement system for flow and alcoholic strength of distilled liquor in a liquor-picking process, comprising: the flow guide device is any one of the flow guide devices in the distilled liquor picking process; the mass measuring device is used for measuring the weight of the wine bodies in the first standard container and the second standard container in real time; the liquid level measuring device is used for measuring the liquid levels of the wine bodies in the first standard container and the second standard container in real time; the temperature measuring device is used for measuring the temperature of the wine bodies in the first standard container and the second standard container in real time; the control device is electrically connected with the liquid level measuring device and the gravity measuring device and is used for acquiring weight data and liquid level height data of wine bodies in the first standard container and the second standard container; the control device is also electrically connected with the control valves respectively, and controls the control valves to be opened and closed according to the liquid level heights of the wine bodies in the first standard container and the second standard container; the control device is also used for calculating the flow and the alcoholic strength of the wine body according to the weight data and the liquid level height data.
An online measuring method for flow and alcoholic strength in the process of picking distilled liquor comprises the following steps: controlling by a computer to alternately flow the influent liquid into a first standard container and a second standard container and alternately flow the wine bodies in the first standard container and the second standard container; respectively measuring the liquid level heights of the wine bodies in the first standard container and the second standard container in real time through a liquid level measuring device and sending liquid level height data to the computer; respectively measuring the weight of the wine in the first standard container and the second standard container in real time through the gravity measuring device and sending the readings of the gravity measuring device to the computer; and the computer calculates the flow and the alcoholic strength of the distilled liquor in the liquor-picking process according to the liquid level height data and the indication number of the gravity measuring device.
Compared with the prior art, in the flow and alcohol content online measurement system and method, the two standard containers alternately collect liquid and discharge liquid, so that parameters such as volume flow, mass flow, density, temperature, alcohol content and the like of the wine body can be stably measured in an open pipeline, the measurement result can guide the distilled grain steaming and wine product primary grading, manual wine picking and metering used in a large number of wineries at present are replaced, the measurement speed is ensured, automatic and online measurement is realized, and technical support is provided for intelligent production and fine management in the brewing industry.
Drawings
Fig. 1 is a schematic structural diagram of a diversion device for a distilled liquor picking process provided in embodiment 1 of the present invention.
Fig. 2 is a schematic structural diagram of an online measurement system for flow rate and alcohol content in a process of extracting distilled liquor provided in embodiment 1 of the present invention.
Fig. 3 is a schematic structural diagram of a sensor for detecting a liquid level using a camera according to embodiment 1 of the present invention.
Fig. 4 is a photograph taken and a processing result in the method for detecting a liquid level using a camera according to embodiment 1 of the present invention.
FIG. 5 is a schematic structural diagram of a sensor for detecting liquid level by measuring electrical impedance characteristics, provided in embodiment 1 of the present invention.
FIG. 6 is a photograph of a sensor for detecting liquid level by measuring electrical impedance characteristics, provided in example 1 of the present invention.
FIG. 7 is a graph showing the variation of equivalent series capacitance and resistance with liquid level in the method for detecting liquid level by measuring electrical impedance characteristics provided in example 1 of the present invention.
FIG. 8 is a schematic diagram of two principles of detecting liquid level by ultrasonic waves according to embodiment 1 of the present invention.
Fig. 9 is a functional block diagram of a control device provided in embodiment 1 of the present invention.
Fig. 10 is a schematic view of a dynamic weighing model for correcting the reading of the pressure sensor according to embodiment 1 of the present invention.
Fig. 11 is a schematic structural diagram of a diversion device for a distilled liquor picking process provided in embodiment 2 of the present invention.
Fig. 12 is a schematic structural diagram of a diversion device for a distilled liquor picking process provided in embodiment 3 of the present invention.
Fig. 13 is a schematic structural diagram of a diversion device for a distilled liquor picking process provided in embodiment 4 of the present invention.
Description of the main elements
Figure BDA0002370175300000041
Figure BDA0002370175300000051
Detailed Description
The diversion device for the liquor-extracting process of distilled liquor and the online measuring system and method for the flow and the alcoholic strength provided by the invention are further described in detail with reference to the accompanying drawings and specific embodiments.
Referring to fig. 1, an embodiment 1 of the present invention provides a diversion device 100 for a distilled spirit picking process, where the diversion device 100 includes a guiding pipe 101, a guiding pipe 102, a first standard container 103, a second standard container 104, a first control valve 105, a second control valve 106, a third control valve 107, and a fourth control valve 108. The first control valve 105, the second control valve 106, the third control valve 107, and the fourth control valve 108 are single-channel control valves.
The inlet tube 101 includes a first leg 1011 and a second leg 1012. The first branch 1011 is suspended and spaced apart from the inlet of the first standard container 103, so that the wine body 109 can flow into the first standard container 103 from the first branch 1011. The second branch 1012 is suspended and spaced apart from the inlet of the second standard container 104, so that the wine body 109 can flow into the second standard container 104 from the second branch 1012. The first branch 1011 is suspended and spaced from the first standard container 103, so as to avoid considering the influence of the pressure or the supporting force of the first branch 1011 when the quality of the wine body 109 in the first standard container 103 is measured subsequently. The same is true of the second branch 1012 being suspended and spaced apart.
The delivery tube 102 includes a third branch 1021 and a fourth branch 1022. The first standard container 103 is suspended and spaced at the inlet of the third branch 1021, so that the wine 109 flowing out of the first standard container 103 can flow into the third branch 1021. The second standard container 104 is suspended and spaced apart from the inlet of the fourth branch 1022, so that the wine body 109 flowing out of the second standard container 104 can flow into the fourth branch 1022. The first standard container 103 is suspended and spaced from the third branch 1021, so that the influence of the supporting force of the third branch 1021 is avoided being considered when the quality of the wine body 109 in the first standard container 103 is measured subsequently. The same is true of the second standard container 104 being suspended and spaced apart.
The first control valve 105 is disposed on the first branch 1011, the second control valve 106 is disposed on the second branch 1012, the third control valve 107 is disposed at the outlet of the first standard container 103, and the fourth control valve 108 is disposed at the outlet of the second standard container 104. Specifically, a first flow guide pipe 1030 is connected to the bottom of the first standard container 103, and the third control valve 107 is disposed on the first flow guide pipe 1030; a second flow pipe 1040 is connected to the bottom of the second standard container 104, and the fourth control valve 108 is disposed on the second flow pipe 1040. The first flow guide pipe 1030 is suspended and disposed at an entrance of the third branch 1021 at intervals, and the second flow guide pipe 1040 is suspended and disposed at an entrance of the fourth branch 1022 at intervals.
When the diversion device 100 works, the first control valve 105 and the fourth control valve 108 are firstly opened, the second control valve 106 and the third control valve 107 are closed, and the wine 109 flows into the first standard container 103; when the first standard container 103 is full, the first control valve 105 and the fourth control valve 108 are closed, the second control valve 106 is opened, new wine 109 flows into the second standard container 104, and then the third control valve 107 is opened, so that the wine 109 in the first standard container 103 flows out; when the wine body 109 in the first standard container 103 completely flows out, the third control valve 107 is closed; when the second standard container 104 is full, the second control valve 106 is closed, the first control valve 105 is opened, new wine 109 flows into the first standard container 103 again, and then the fourth control valve 108 is opened, so that the wine 109 in the second standard container 104 flows out; when the wine 109 in the second standard container 104 is completely discharged, the fourth control valve 108 is closed. The above steps are repeated in a circulating way.
Referring to fig. 2, embodiment 1 of the present invention further provides an online measurement system 10 for measuring flow rate and alcohol content of distilled spirit during a process of extracting distilled spirit, wherein the measurement system 10 includes the diversion device 100, a measurement device 110 and a control device 120.
The measuring device 110 includes a first pressure sensor 111, a second pressure sensor 112, a first liquid level sensor 113, and a second liquid level sensor 114. The first pressure sensor 111 and the second pressure sensor 112 are used for measuring the mass of the wine 109 in the first standard container 103 and the second standard container 104 in real time respectively. The first liquid level sensor 113 and the second liquid level sensor 114 are respectively used for measuring the liquid level height of the wine body 109 in the first standard container 103 and the second standard container 104 in real time. The structures of the first pressure sensor 111 and the second pressure sensor 112 are not limited, and the structures may be the same or different. The first liquid level sensor 113 and the second liquid level sensor 114 are not limited in structure, and may have the same or different structures. It is understood that the first fluid level sensor 113 and the second fluid level sensor 114 may be the same fluid level sensor.
Further, the measuring device 110 further comprises a resistance sensor (not shown) for measuring the temperature of the wine 109 in the first standard container 103 and the second standard container 104. Preferably, the resistance sensor is a non-contact resistance sensor.
In one embodiment, the first pressure sensor 111 and the second pressure sensor 112 are identical in structure. The first standard container 103 is fixed to the first pressure sensor 111 by a first support mechanism (not shown), and the second standard container 104 is fixed to the second pressure sensor 112 by a second support mechanism (not shown). According to the indication of the first pressure sensor 111 and the instantaneous flow of the wine body 109, the impact of the wine body 109 flowing into the first standard container 103 is corrected, and the weight of the first standard container 103 is subtracted, namely the weight of the wine body 109 in the first standard container 103. Similarly, the weight of the wine body 109 in the second standard container 104 can be obtained.
In one embodiment, the liquid level is detected using a camera. Referring to fig. 3, the first liquid level sensor 113 includes a surface light source 1131, a light shielding strip 1132 and a camera 1133. The surface light source 1131 and the camera 1133 are respectively disposed on two sides of the first standard container 103, and the light shielding strip 1132 is disposed on one side of the surface light source 1131 close to the first standard container 103. For example, a black shielding strip 1132 is attached to the surface light source 1131. The camera 1133 photographs the surface light source 1131 and the light shielding strip 1132 through the first standard container 103 containing the wine 109. The width of the part of the light shielding strip 1132 without liquid is normal, and the width of the part with liquid is obviously widened due to the refraction effect of the liquid, so that the liquid level height of the wine body 109 can be obtained after the image processing processes such as binarization, morphological processing and statistical analysis are carried out on the width of the light shielding strip 1132 in the picture shot by the camera 1133. Fig. 4 shows a sample of photographs taken by the camera and the processing results. The first liquid level sensor 113 and the second liquid level sensor 114 have the same structure. The first liquid level sensor 113 and the second liquid level sensor 114 may be provided with one camera.
In another embodiment, the liquid level is detected by measuring electrical impedance characteristics (including resistance, capacitance, etc.). Fig. 5 and 6 show a schematic diagram and a physical photograph of an apparatus for measuring the liquid level of the wine body 109 by measuring electrical impedance characteristics, respectively. The first liquid level sensor 113 includes a first electrode 1134, a second electrode 1135 and a detecting device 1136. The first electrode 1134 and the second electrode 1135 are two strip-shaped metal sheets with the same shape, and are symmetrically adhered to two sides of the outer tube wall of the first standard container 103 at intervals. The detecting device 1136 applies an ac signal to the first electrode 1134 and the second electrode 1135 (while attenuating electromagnetic noise by using a shielding layer), and detects impedance characteristics between the first electrode 1134 and the second electrode 1135. The impedance between the first electrode 1134 and the second electrode 1135 is found to be capacitive, and the modulus | Z | of the impedance is in a relatively good inverse proportion to the liquid level in the tube. The impedance is equivalent to a series circuit of a resistor and a capacitor, and the measured equivalent series resistance R is in a better inverse proportional relation with the liquid level of the wine body 109. As shown in fig. 7, the equivalent series capacitance C has a good linear relationship with the liquid level.
In another embodiment, the liquid level is measured by ultrasound. FIG. 8 shows a schematic view of two devices for detecting liquid level by using ultrasonic waves. The first level sensor 113 includes an ultrasonic transducer 1137. The ultrasonic transducer 1137 may be mounted on the bottom or top of the first modular container 103. When the ultrasonic transducer 1137 is installed at the bottom of the first standard container 103, ultrasonic waves are emitted upwards and reflected at the liquid level of the wine body 109, so that the propagation time of the ultrasonic waves in the wine body 109 can be measured, and the liquid level height can be calculated according to the sound velocity in the liquid. When the ultrasonic transducer 1137 is installed on the top of the first standard container 103, ultrasonic waves are emitted downwards and reflected at the liquid level of the wine body 109, so that the time of the ultrasonic waves propagating in the air above the liquid level of the wine body 109 can be measured, and the liquid level height of the wine body 109 can be calculated according to the sound velocity in the air.
The control device 120 is electrically connected to the first pressure sensor 111, the second pressure sensor 112, the first liquid level sensor 113 and the second liquid level sensor 114, respectively, and is configured to obtain mass data and liquid level height data of the wine body 109 in the first standard container 103 and the second standard container 104, and calculate a flow rate and an alcohol content of the wine body 109 according to the mass data and the liquid level height data. Further, the control device 120 is connected to the first control valve 105, the second control valve 106, the third control valve 107 and the fourth control valve 108, and controls the opening and closing of the first control valve 105, the second control valve 106, the third control valve 107 and the fourth control valve 108 according to the liquid level heights of the wine bodies 109 in the first standard container 103 and the second standard container 104.
As shown in fig. 9, the control device 120 includes a computer 121, a valve control circuit 122, a sensor interface 123, and a display device 124. The valve control circuit 122, the sensor interface 123 and the display device 124 are electrically connected to the computer 121, respectively. The computer 121 is used to control the operation of the entire measuring system 10 and to calculate the flow rate and the alcohol content of the wine body 109. The computer 121 may be a Personal Computer (PC), a Microcontroller (MCU), a Programmable Logic Controller (PLC), or the like.
The flow rate of the wine body 109 may be a mass flow rate or a volume flow rate. The volume flow rate is obtained by dividing the volume of the wine bodies 109 in the standard container by the time t during which these wine bodies are collected, and the mass flow rate is obtained by dividing the mass of the wine bodies 109 in the standard container by the time t during which these wine bodies are collected. The volume is obtained by means of a level sensor and the mass of the wine body 109 is obtained by means of a pressure sensor. The time t is obtained by the computer 121. For example, taking the calculation of the volume flow rate of the wine 109 in the first standard container 103 as an example, when the computer 121 controls the first control valve 105 to open, the timing is started to obtain the time t, and the first liquid level sensor 113 reads the liquid level height in real time and obtains the volume of the wine 109 in the first standard container 103.
The method for measuring the alcoholic strength of the wine body 109 comprises the following steps: the alcohol content of the wine body 109 can be obtained by calculating the mass of the wine body, calculating the density of the wine body 109, obtaining the temperature of the wine body 109, and looking up tables according to density and temperature, an alcohol water solution density and alcohol content (alcohol content) comparison table (20 ℃) in GB 5009.225-2016 (measurement of alcohol concentration in national standard wine for food safety), and an alcohol content conversion table (conversion table of alcohol meter temperature and alcohol content (alcohol content) at 20 ℃). The computer 121 may store the comparison table and the conversion table, or may query the comparison table and the conversion table through a network.
Wherein the density of the wine body 109 is obtained by dividing the mass by the volume. The volume is obtained by a level sensor. The mass is obtained by means of a pressure sensor. In one embodiment, the computer 121 corrects the pressure sensor readings by using the dynamic weighing model shown in FIG. 10. Taking the calculation of the mass of the wine body 109 in the first standard container 103 as an example, the method specifically includes: let the first reference container 103 have a mass moThe mass of the wine body 109 in the first standard container 103 is mlThe bottom area of the first standard container 103 is S, the height of the wine outlet of the first branch 1011 from the liquid surface of the wine body 109 in the first standard container 103 is h, and the speed of the inflow liquid 109a leaving the wine outlet of the first branch 1011 and reaching the liquid surface of the wine body 109 is v0And v1The first pressure sensor 111 has a value of N, and the instantaneous volume flow rate of the inflow liquid 109a is qv
Wherein m isoAnd S is a vessel parameter, which can be measured in advance, h and N can be measured in real time, v0And q isvThe relationship of (c) can be calculated. q. q.svThe calculation can be performed by using equation (1).
Figure BDA0002370175300000101
Ignoring the air resistance experienced by the drops as they fall,
v1 2-v0 2=2gh#(2)
according to the theorem of momentum,
N=(m0+ml)g+qvv1#(3)
therefore, the first and second electrodes are formed on the substrate,
Figure BDA0002370175300000102
the above expression contains the differential term of the liquid level, and the noise of the liquid level measurement has a great influence on the precision of the quality measurement, so that when the method is applied, a proper filtering algorithm needs to be designed to more accurately measure the quality of the wine body 109 in the first standard container 103.
In one embodiment, the measurement data is filtered using an Extended Kalman Filter (EKF) algorithm, comprising: selecting the accumulated mass flow M, the accumulated volume flow V, the instantaneous wine density rho and the instantaneous volume flow qvAnd selecting the liquid level h and the index N of the first pressure sensor 111 as observed quantities as state quantities, establishing an extended Kalman filtering model, and estimating the value of each state quantity in real time.
Calculating the mass m of the wine body 109 in the first standard container 103 according to the formula (4)lThe density of the wine body 109 in the first standard container 103 may then be calculated from the volume of the wine body 109 in the first standard container 103.
After the density of the wine body 109 in the first standard container 103 is measured, the density temperature of the wine body 109 in the first standard container 103 is measured, and then the alcoholic strength can be calculated. In one embodiment, the alcohol content of the wine body 109 in the first standard container 103 is determined by measuring the temperature of the wine body 109 in the first standard container 103 by a thermal resistance sensor, and looking up the table according to the density and temperature of the wine body 109 in the first standard container 103, the comparison table of the density of the aqueous alcohol solution and the alcohol content (ethanol content) in GB 5009.225-2016 (measurement of ethanol concentration in national standard wine for food safety) "(20 ℃), and the conversion table of the alcohol temperature and the alcohol content (ethanol content) at 20 ℃).
Further, embodiment 1 of the present invention further provides an online measurement method for flow and alcohol content during liquor-taking process of distilled liquor, including the following steps:
a step S10 of controlling, by the computer 121, the inflow liquid 109a to alternately flow into the first standard container 103 and the second standard container 104 and alternately flow out the wine bodies 109 in the first standard container 103 and the second standard container 104;
step S20, measuring the liquid level heights of the wine bodies 109 in the first standard container 103 and the second standard container 104 in real time through the first liquid level sensor 113 and the second liquid level sensor 114, respectively, and sending the liquid level height data to the computer 121;
step S30, measuring the weight of the wine 109 in the first standard container 103 and the second standard container 104 respectively in real time through the first pressure sensor 111 and the second pressure sensor 112 and sending the pressure sensor readings to the computer 121; and
in step S40, the computer 121 calculates the flow rate and alcohol content of the distilled spirit during the process of extracting the distilled spirit according to the liquid level height data and the pressure sensor readings.
It should be understood that the diversion device 100 is not limited to the above-mentioned structure, as long as the inflow liquid 109a alternately flows into the first standard container 103 and the second standard container 104 and the wine 109 in the first standard container 103 and the second standard container 104 alternately flows out can be realized. Several other configurations of deflector device 100 are provided below.
Referring to fig. 11, an embodiment 2 of the present invention provides a diversion device 100A for a distilled spirit picking process, where the diversion device 100A includes a guiding pipe 101, a guiding pipe 102, a first standard container 103, a second standard container 104, a first control valve 105, a third control valve 107, and a fourth control valve 108.
The diversion device 100A of embodiment 2 of the present invention has substantially the same structure as the diversion device 100 of embodiment 1 of the present invention, except that the first control valve 105 of the diversion device 100A of embodiment 2 of the present invention is a multi-channel control valve directly disposed on the main branch of the inlet pipe 101, and can control the wine 109 to alternately flow into the first standard container 103 and the second standard container 104 through the first branch 1011 and the second branch 1012.
Referring to fig. 12, embodiment 3 of the present invention provides a diversion device 100B for a distilled spirit picking process, the diversion device 100B includes a guiding pipe 101, a guiding pipe 102, a first standard container 103, a second standard container 104, a third control valve 107, a fourth control valve 108, and a moving device 130.
The deflector 100B according to embodiment 3 of the present invention has substantially the same structure as the deflector 100 according to embodiment 1 of the present invention, except that the inlet pipe 101 of the deflector 100B according to embodiment 3 of the present invention is not provided with a plurality of branches and is not provided with a control valve, and the inlet pipe 101 is swung or moved above the first standard container 103 and the second standard container 104 by the moving device 130, so that the wine 109 is alternately introduced into the first standard container 103 and the second standard container 104.
Referring to fig. 13, embodiment 4 of the present invention provides a diversion device 100C for a distilled spirit picking process, wherein the diversion device 100C includes a guiding pipe 101, a guiding pipe 102, a first standard container 103, a second standard container 104, a first control valve 105, a second control valve 106, a third control valve 107, and a fourth control valve 108.
The deflector 100C of embodiment 4 of the present invention is substantially the same as the deflector 100 of embodiment 1 of the present invention, except that the delivery pipe 102 is not provided with a branch, and the wine 109 flowing out from the first standard container 103 and the second standard container 104 is directly flowed into the delivery pipe 102 through a large funnel (not shown).
In the flow and alcohol content on-line measuring system and method, the two standard containers alternately collect liquid and discharge liquid, so that parameters such as volume flow, mass flow, density, temperature, alcohol content and the like of a wine body can be stably measured in an open pipeline, the measurement result can guide the distilled grain steaming and wine primary grading, manual wine picking and metering used in a large number of wineries at present are replaced, the measurement speed is ensured, automatic and on-line measurement is realized, and technical support is provided for intelligent production and fine management in the brewing industry.
In addition, other modifications within the spirit of the invention may occur to those skilled in the art, and such modifications within the spirit of the invention are intended to be included within the scope of the invention as claimed.

Claims (10)

1. A flow guide device for a liquor extracting process of distilled liquor comprises: the device comprises an inlet pipe, an outlet pipe, a first standard container, a second standard container and a plurality of control valves; the device is characterized in that the first standard container and the second standard container are arranged at intervals and independently; the leading-in pipe comprises a first branch and a second branch; the first branch is suspended and arranged at the inlet of the first standard container at intervals, so that wine can flow into the first standard container from the first branch; the second branch is suspended and arranged at the inlet of the second standard container at intervals, so that wine can flow into the second standard container from the second branch; the delivery pipe is arranged at the outlets of the first standard container and the second standard container, so that the wine in the first standard container and the second standard container can flow into the delivery pipe after flowing out; the control valves are used for controlling the wine bodies to alternately flow into the first standard container and the second standard container and enabling the wine bodies in the first standard container and the second standard container to alternately flow out.
2. The apparatus for guiding a distilled spirit tapping process according to claim 1, wherein the plurality of control valves includes a first control valve disposed on the first branch, a second control valve disposed on the second branch, a third control valve disposed at an outlet of the first standard container, and a fourth control valve disposed at an outlet of the second standard container.
3. The diversion device for liquor extraction process according to claim 2, wherein a first diversion pipe is connected to the bottom of the first standard container, and the third control valve is disposed in the first diversion pipe; the bottom of the second standard container is connected with a second flow guide pipe, and the fourth control valve is arranged on the second flow guide pipe; the delivery pipe comprises a third branch and a fourth branch; the first guide pipe is suspended in the air and arranged at the inlet of the third branch at intervals, so that the wine body flowing out of the first standard container can flow into the third branch; the second guide pipe is suspended in the air and arranged at the inlet of the fourth branch at intervals, so that the wine body flowing out of the second standard container can flow into the fourth branch.
4. The apparatus for guiding a distilled spirit tapping process according to claim 1, wherein said plurality of control valves includes a multi-channel control valve directly provided on a trunk line of said inlet pipe for controlling the alternating flow of the spirit body into said first and second standard containers through said first and second branches; the control valves also comprise two single-channel control valves which are respectively arranged at the outlets of the first standard container and the second standard container and are used for controlling the alternating outflow of the wine bodies in the first standard container and the second standard container.
5. A flow guide device for a liquor extracting process of distilled liquor comprises: the device comprises an inlet pipe, an outlet pipe, a first standard container, a second standard container, a moving device and a plurality of control valves; the device is characterized in that the first standard container and the second standard container are arranged at intervals and independently; the leading-in pipe is arranged at the inlets of the first standard container and the second standard container in a suspending way; the moving device is used for moving the introducing pipe above the first standard container and the second standard container so as to make the wine body alternately flow into the first standard container and the second standard container; the delivery pipe is arranged at the outlets of the first standard container and the second standard container, so that the wine in the first standard container and the second standard container can flow into the delivery pipe after flowing out; the control valves are used for controlling the alternating outflow of the wine bodies in the first standard container and the second standard container.
6. An online measurement system for flow and alcoholic strength in a liquor-picking process of distilled liquor is characterized by comprising:
a diversion device, which is any one of the diversion devices in the distilled liquor extraction process according to the claims 1 to 5;
the mass measuring device is used for measuring the weight of the wine bodies in the first standard container and the second standard container in real time;
the liquid level measuring device is used for measuring the liquid levels of the wine bodies in the first standard container and the second standard container in real time;
the temperature measuring device is used for measuring the temperature of the wine bodies in the first standard container and the second standard container in real time; and
the control device is electrically connected with the liquid level measuring device and the gravity measuring device and is used for acquiring weight data and liquid level height data of wine bodies in the first standard container and the second standard container; the control device is also electrically connected with the control valves respectively, and controls the control valves to be opened and closed according to the liquid level heights of the wine bodies in the first standard container and the second standard container; the control device is also used for calculating the flow and the alcoholic strength of the wine body according to the weight data and the liquid level height data.
7. The system for on-line measurement of flow and alcohol content of a liquor extraction process as claimed in claim 6, wherein said gravity measuring means comprises a first pressure sensor and a second pressure sensor; the first standard container is fixed on the first pressure sensor, and the second standard container is fixed on the second pressure sensor; the liquid level measuring device is a measuring device for detecting liquid level by using a camera, a measuring device for detecting liquid level by measuring electrical impedance characteristics, or a measuring device for detecting liquid level by ultrasonic waves.
8. An online measuring method for flow and alcoholic strength in the process of picking distilled liquor is characterized by comprising the following steps:
controlling by a computer to alternately flow the influent liquid into a first standard container and a second standard container and alternately flow the wine bodies in the first standard container and the second standard container;
respectively measuring the liquid level heights of the wine bodies in the first standard container and the second standard container in real time through a liquid level measuring device and sending liquid level height data to the computer;
respectively measuring the weight of the wine in the first standard container and the second standard container in real time through the gravity measuring device and sending the readings of the gravity measuring device to the computer; and
and the computer calculates the flow and the alcoholic strength of the distilled liquor in the liquor-picking process according to the liquid level height data and the indication number of the gravity measuring device.
9. The method for on-line measurement of flow and alcohol content of a liquor extraction process as claimed in claim 8, wherein the method for calculating alcohol content of a liquor extraction process from said liquid level height data and said gravity measurement device readings by said computer comprises: calculating the mass of the wine body; calculating the density of the wine body; acquiring the temperature of the wine body; and calculating the alcoholic strength through the density and the temperature of the wine body, the standard comparison table and the conversion table.
10. The method for on-line measurement of flow and alcohol content in liquor-extracting process according to claim 8, wherein the method for calculating the mass of the liquor body is to calculate the mass m of the liquor body in the first standard container by the formulas (1) to (4)l
Figure FDA0002370175290000031
v1 2-v0 2=2gh# (2)
N=(m0+ml)g+qVv1# (3)
Figure FDA0002370175290000032
Wherein g is the acceleration of gravity, N is the reading of the gravity measuring device to the first standard container, moThe mass of the first standard container, S the bottom area of the first standard container, h the height of the wine outlet of the first branch from the liquid level of the wine in the first standard container, and v0Leaving the first leg for incoming liquidSpeed of the outlet of the road, v1The speed of the inflowing liquid reaching the surface of the wine body in the first standard container qvIs the instantaneous volumetric flow rate of the influent liquid.
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112746004A (en) * 2021-02-03 2021-05-04 河北工业大学 Alcohol content online detection segmented liquor picking equipment based on density
CN113390747A (en) * 2021-06-09 2021-09-14 劲牌有限公司 Method and device for detecting and grading alcohol content on line in process of brewing and distilling white spirit
CN113484189A (en) * 2021-07-02 2021-10-08 中国电信股份有限公司 Online alcoholic strength acquisition system and method

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2682410Y (en) * 2004-03-17 2005-03-02 田鹰 On-line measuring apparatus for alcohol content and alcohol quantity of spirit
CN201097192Y (en) * 2007-09-03 2008-08-06 吴行友 Distilled spirit online detection dosage control device
DE102010008511A1 (en) * 2010-02-18 2011-08-18 Bundesrepublik Deutschland, vertr.d.d. Bundesministerium für Wirtschaft und Technologie, d.vertr.d.d. Präsidenten der Physikalisch-Technischen Bundesanstalt, 38116 Liquid volume measuring device e.g. liquid flow meter, for determination of e.g. volumetric measured variable, has control device switching switch, so that measured variable is determined by summing filling volumes of containers
US20160232997A1 (en) * 2015-02-10 2016-08-11 Korea Atomic Energy Research Institute Measuring device for micro flow rate and nuclear power plant having the same
CN106338323A (en) * 2016-09-07 2017-01-18 武汉市度量衡管理所 Site calibration method and calibration system of flowmeter
CN106742890A (en) * 2017-01-10 2017-05-31 苏州苏净保护气氛有限公司 The safety monitoring system and its control method of a kind of device for recovering oil and gas
CN108507630A (en) * 2018-03-12 2018-09-07 清华大学 Positive displacement oil gas water three phase flow separate phase flow rate on-line measurement devices and methods therefor
CN110382103A (en) * 2017-05-11 2019-10-25 株式会社堀场Stec Liquid material gasifying feedway and control program
CN211824530U (en) * 2020-01-16 2020-10-30 清华大学 Guiding device and online measurement system for liquor picking process of distilled liquor

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2682410Y (en) * 2004-03-17 2005-03-02 田鹰 On-line measuring apparatus for alcohol content and alcohol quantity of spirit
CN201097192Y (en) * 2007-09-03 2008-08-06 吴行友 Distilled spirit online detection dosage control device
DE102010008511A1 (en) * 2010-02-18 2011-08-18 Bundesrepublik Deutschland, vertr.d.d. Bundesministerium für Wirtschaft und Technologie, d.vertr.d.d. Präsidenten der Physikalisch-Technischen Bundesanstalt, 38116 Liquid volume measuring device e.g. liquid flow meter, for determination of e.g. volumetric measured variable, has control device switching switch, so that measured variable is determined by summing filling volumes of containers
US20160232997A1 (en) * 2015-02-10 2016-08-11 Korea Atomic Energy Research Institute Measuring device for micro flow rate and nuclear power plant having the same
CN106338323A (en) * 2016-09-07 2017-01-18 武汉市度量衡管理所 Site calibration method and calibration system of flowmeter
CN106742890A (en) * 2017-01-10 2017-05-31 苏州苏净保护气氛有限公司 The safety monitoring system and its control method of a kind of device for recovering oil and gas
CN110382103A (en) * 2017-05-11 2019-10-25 株式会社堀场Stec Liquid material gasifying feedway and control program
CN108507630A (en) * 2018-03-12 2018-09-07 清华大学 Positive displacement oil gas water three phase flow separate phase flow rate on-line measurement devices and methods therefor
CN211824530U (en) * 2020-01-16 2020-10-30 清华大学 Guiding device and online measurement system for liquor picking process of distilled liquor

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112746004A (en) * 2021-02-03 2021-05-04 河北工业大学 Alcohol content online detection segmented liquor picking equipment based on density
CN113390747A (en) * 2021-06-09 2021-09-14 劲牌有限公司 Method and device for detecting and grading alcohol content on line in process of brewing and distilling white spirit
CN113484189A (en) * 2021-07-02 2021-10-08 中国电信股份有限公司 Online alcoholic strength acquisition system and method

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