CN111110619B - Oil-control acne-removing composition and application thereof in cosmetics - Google Patents
Oil-control acne-removing composition and application thereof in cosmetics Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
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Abstract
The invention provides an oil-controlling acne-removing composition and application thereof in cosmetics. The composition comprises zedoary, bark of black willow, devil's-tongue stem/root, hawthorn and kaempferia galanga root. Through the synergistic effect of various plants, the composition disclosed by the invention can effectively control oil and remove acnes, is mild and non-irritant, and is suitable for long-term use.
Description
Technical Field
The invention belongs to a composition in the technical field of cosmetic compositions, and particularly relates to an oil-controlling acne-removing composition, a preparation method thereof and application thereof in cosmetics.
Background
Acne is commonly known as acne, also called as "whelk", "pimple" or "comedo", and is a skin disease caused by the blockage and inflammation of hair follicles and sebaceous glands. In adolescence, excessive hormone in the body can stimulate the hair to grow rapidly, sebaceous glands secrete more oil, and the hair and the sebaceous glands accumulate excessive substances, so that the oil and bacteria are more easily attached to the hair, and the skin is red and swollen. A number of microorganisms in the hair follicle, particularly propionibacterium acnes, multiply in number, and lipases produced by propionibacterium acnes break down sebum to produce free fatty acids, while chemotactic inflammatory cells and mediators, ultimately inducing and exacerbating the inflammatory response.
The existing acne removing methods and the types of medicines are also many, such as: laser therapy, western medicines such as salicylic acid, clindamycin, metronidazole, dexamethasone and plant essential oil such as rose essential oil. In the above treatment method, laser treatment cannot eradicate acne and has a destructive effect on skin tissues; the single western medicine treatment easily causes drug dependence on patients and has large side effect; the plant essential oil has good treatment effect, but has long treatment time and high price and cannot be accepted by the public.
Disclosure of Invention
Problems to be solved by the invention
In view of the defects in the prior art, the invention aims to provide an effective oil-controlling acne-removing composition capable of being used for a long time, and a preparation method of the oil-controlling acne-removing composition in a mask.
< first aspect >
A first aspect of the invention provides an oil-controlling acne-removing composition comprising: zedoary, bark of black willow, stem/root of amorphophallus virosus, hawthorn and root of kaempferia galanga.
Bark of black willow
The bark of the black willow has strong antibacterial activity on staphylococcus aureus and propionibacterium acnes. These two microorganisms are one of the major causes of acne formation.
Stem/root of devil's-tongue
The devil's jaborage stem/root helps control sebum and reduce microorganisms associated with acne spots.
Hawthorn fruit
The hawthorn can reduce inflammation and cool the skin, and has an antibacterial effect on acne-forming microorganisms, particularly Propionibacterium acnes.
Root of Kaempferia galanga
The kaempferia galanga root can accelerate the healing of acne skin and prevent the generation of acne marks.
Rhizoma Curcumae
Zedoary has strong oil control and antioxidant effects.
The Curcumae rhizoma used in the present invention comprises one or more of Curcuma zedoaria (Curcuma phaeocaulis) belonging to Zingiberaceae family, Curcuma zedoaria Kwangsiensis, or Curcuma zedoaria Wenyujin (Curcuma wenyujin) prepared by Curcuma wenyujin. In a preferred embodiment, the curcuma zedoary is prepared from one or more of curcuma zedoaria, curcuma kwangsiensis and curcuma wenyujin.
In some specific embodiments of the present invention, curcuma kwangsiensis is added to the oil-controlling acne-removing composition. Specifically, the oil-controlling acne-removing composition is prepared from dried rhizome of curcuma kwangsiensis.
Oil-control acne-removing composition
The specific formula of the oil-controlling acne-removing composition comprises the following components in parts by weight: 15-45 parts of curcuma zedoary, 15-40 parts of black willow bark, 5-25 parts of verruca stipes stem/root, 3-40 parts of hawthorn and 15-45 parts of kaempferia galanga root.
As a preferred embodiment, the oil-controlling and acne-removing composition comprises the following components in parts by weight: 17-40 parts of curcuma zedoary, 16-35 parts of black willow bark, 8-24 parts of verruca pedunculata stem/root, 5-35 parts of hawthorn and 18-43 parts of kaempferia galanga root.
As another preferred embodiment, the oil-controlling and acne-removing composition comprises the following components in parts by weight: 20-40 parts of curcuma zedoary, 16-35 parts of black willow bark, 10-24 parts of verruca pedunculata stem/root, 8-35 parts of hawthorn and 20-43 parts of kaempferia galanga root.
As a further preferred embodiment, the oil-controlling and acne-removing composition comprises the following components in parts by weight: 25 parts of curcuma zedoary, 20 parts of black willow bark, 18 parts of verruca vulgaris stem/root, 24 parts of hawthorn and 23 parts of kaempferia galanga root; or preferably, 30 parts of curcuma zedoary, 25 parts of black willow bark, 12 parts of verruca stipes stem/root, 27 parts of hawthorn and 31 parts of kaempferia galanga root; or preferably, 37 parts of curcuma zedoary, 22 parts of black willow bark, 15 parts of verruca stipes stem/root, 30 parts of hawthorn and 37 parts of kaempferia galanga root.
On the other hand, the invention also provides a preparation method for preparing the oil-controlling acne-removing composition, which comprises the following steps:
(1) pretreating plant raw materials: weighing each plant raw material, crushing, grinding, sieving and uniformly mixing;
(2) extraction: adding the mixture into 60% ethanol solution at a ratio of 1 (8-14), preferably 1:14, and extracting for 3 times at 50-80 deg.C; preferably 75 deg.C, extracting for 20-40min, preferably 30min, and filtering to obtain extractive solution;
(3) And (3) concentrating: concentrating the extracting solution by reduced pressure distillation to obtain a concentrated solution;
(4) and (3) drying: and (4) freeze-drying the concentrated solution obtained in the step (3).
The oil-controlling acne-removing composition is mainly applied to cosmetics, but the specific cosmetics are not particularly limited. The cosmetic can be facial cleanser, facial mask, cosmetic water or lotion; preferably, the cosmetic is a facial mask.
< second aspect >
The second aspect of the invention provides an application of the composition containing the oil-controlling acne-removing agent in cosmetics.
In some embodiments, there is provided a cosmetic comprising the above composition, wherein the composition is present in the cosmetic in an amount of 1 to 30% by weight; preferably, the composition is contained in an amount of 5-20% by weight.
In some embodiments, the cosmetic is selected from one or more of a facial cleanser, a facial mask, a lotion, or an emulsion; preferably, the cosmetic is selected from a mask.
In some embodiments, there is also provided a facial mask comprising the above oil-controlling and acne-removing composition, wherein the facial mask comprises the following components in parts by weight: 0.01-1 part of allantoin, 0.001-0.025 part of hyaluronic acid, 1-7 parts of glycerol, 0.5-10 parts of butanediol, 0.01-0.5 part of carbomer, 0.01-0.7 part of triethanolamine, 1-30 parts of an oil-controlling and acne-removing composition, 0.01-0.1 part of ethylhexylglycerin, 0.01-1 part of phenoxyethanol and 50-80 parts of deionized water.
Detailed Description
The present invention will be described in detail below. The technical features described below are explained based on typical embodiments and specific examples of the present invention, but the present invention is not limited to these embodiments and specific examples.
Furthermore, in the following detailed description, numerous specific details are set forth in order to provide a better understanding of the present invention. It will be understood by those skilled in the art that the present invention may be practiced without some of these specific details. In other instances, methods, means, devices and steps which are well known to those skilled in the art have not been described in detail so as not to obscure the invention.
Examples
Embodiments of the present invention will be described in detail below with reference to examples, but those skilled in the art will appreciate that the following examples are only illustrative of the present invention and should not be construed as limiting the scope of the present invention. The examples, in which specific conditions are not specified, were conducted under conventional conditions or conditions recommended by the manufacturer. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products commercially available.
Example 1
The oil-control acne-removing composition comprises the following components in parts by weight: 25 parts of curcuma zedoary, 20 parts of black willow bark, 18 parts of verruca vulgaris stem/root, 24 parts of hawthorn and 23 parts of kaempferia galanga root.
The preparation method of the oil-controlling acne-removing composition comprises the following steps:
(1) pretreating plant raw materials: weighing 25 parts of curcuma zedoary, 20 parts of black willow bark, 18 parts of verruca vulgaris stem/root, 24 parts of hawthorn and 23 parts of kaempferia galanga root, crushing, grinding, sieving by a 80-mesh sieve, and uniformly mixing;
(2) extraction: adding the mixture into 60% ethanol solution at a ratio of 1:14, extracting for 3 times at 75 deg.C for 30min, and filtering to obtain extractive solution;
(3) concentration: concentrating the extractive solution by vacuum distillation;
(4) and (3) drying: freeze drying the concentrated solution.
Example 2
The oil-control acne-removing composition comprises the following components in parts by weight: 30 parts of curcuma zedoary, 25 parts of black willow bark, 12 parts of verruca vulgaris stem/root, 27 parts of hawthorn and 31 parts of kaempferia galanga root.
The preparation method of the oil-controlling acne-removing composition comprises the following steps:
(1) pretreating plant raw materials: weighing 30 parts of curcuma zedoary, 25 parts of black willow bark, 12 parts of verruca vulgaris stem/root, 27 parts of hawthorn and 31 parts of kaempferia galanga root, crushing, grinding, sieving by a 80-mesh sieve, and uniformly mixing;
(2) extraction: adding the mixture into 60% ethanol solution at a ratio of 1:14, extracting for 3 times at 75 deg.C for 30min, and filtering to obtain extractive solution.
(3) And (3) concentrating: the extract was concentrated by distillation under reduced pressure.
(4) And (3) drying: freeze drying the concentrated solution.
Example 3
The oil-control acne-removing composition comprises the following components in parts by weight: 37 parts of curcuma zedoary, 22 parts of black willow bark, 15 parts of verruca vulgaris stem/root, 30 parts of hawthorn and 37 parts of kaempferia galanga root.
The preparation method of the oil-controlling acne-removing composition comprises the following steps:
(1) pretreating plant raw materials: weighing 37 parts of curcuma zedoary, 22 parts of black willow bark, 15 parts of verruca vulgaris stem/root, 30 parts of hawthorn and 37 parts of kaempferia galanga root, crushing, grinding, sieving by a 80-mesh sieve, and uniformly mixing;
(2) extraction: adding the mixture into 60% ethanol solution at a ratio of 1:14, extracting for 3 times at 75 deg.C for 30min, and filtering to obtain extractive solution.
(3) Concentration: the extract was concentrated by distillation under reduced pressure.
(4) And (3) drying: freeze drying the concentrated solution.
Example 4 oil-controlling acne-removing mask
TABLE 1 oil-controlling acne-removing mask
The preparation method of the oil-control acne-removing mask comprises the following steps:
dissolving allantoin, hyaluronic acid, glycerol, butanediol, and carbomer in deionized water, stirring, heating to 80 deg.C, keeping the temperature for 15min, cooling to 45 deg.C, adding ethylhexyl glycerol, phenoxyethanol, oil-controlling and acne-removing composition, mixing, adding triethanolamine, and stirring.
Comparative example 1
Comparative example 1 differs from example 1 only in that comparative example 1 does not contain a composition.
Comparative example 2
Comparative example 2 differs from example 1 only in that the composition of comparative example 2 does not contain zedoary.
Comparative example 3
Comparative example 3 differs from example 1 only in that the composition of comparative example 2 does not contain black willow bark.
Comparative example 4
Comparative example 4 differs from example 1 only in that the composition of comparative example 3 does not contain the verruca stalk/root.
Comparative example 5
Comparative example 5 differs from example 1 only in that the composition of comparative example 4 does not contain hawthorn.
Comparative example 6
Comparative example 6 differs from example 1 only in that the composition of comparative example 5 does not contain kaempferia galanga roots.
Comparative example 7 differs from example 1 only in that the composition of comparative example 7 is entirely zedoary.
Comparative example 8 differs from example 1 only in that the composition of comparative example 8 is entirely black willow bark.
Comparative example 9 differs from example 1 only in that the composition of comparative example 9 is entirely devil's verrucose stalk/root.
Comparative example 10 differs from example 1 only in that the composition of comparative example 10 is entirely hawthorn.
Comparative example 11 differs from example 1 only in that the composition of comparative example 11 is entirely kaempferia galanga root.
Masks 4 to 14 were prepared using the compositions of comparative examples 1 to 11, and the kinds, contents and preparation methods of the remaining components except for the compositions were the same as those of mask 1.
Efficacy testing
Patch test of human body
1. The test substance: inventive examples 1-3;
2. subject: a total of 34 men, 26 women, age 20-40 years, who meet the volunteer enrollment criteria of the subject;
3. the test method comprises the following steps: placing the tested object in a proper spot sticking device by adopting a closed test method, sticking the tested object on the arm curve side of the tested object by using a hypoallergenic adhesive tape, and lightly pressing the tested object by using a palm to uniformly stick the tested object on the skin for 24 hours; the blank control group was subject without product;
4. and (4) observing results: the test devices were removed after 24 hours, skin reactions were observed after 0.5h, 24h, 48h, respectively, and the results were recorded. The grade of the adverse reaction of the skin is shown in Table 2, and the test results are shown in Table 3.
TABLE 2 skin response grading Standard for skin Enclosed Patch test
TABLE 3 test results of human skin patches
The results show that 0 of 34 subjects showed adverse reactions on the skin, namely mask 1, mask 2 and mask 3, and show that the oil-controlling and acne-removing mask disclosed by the invention in the examples 1-3 is safe and non-irritant.
Acne-removing clinical effect observation
Subjects: 225 vaccinia muscle test subjects were selected and randomized into 15 groups of 15 persons each. The application time is 28 days, and the control group uses the commercial facial mask with acne removing function for 28 days.
And (4) judging the standard:
high efficiency: facial acne heals without new red pimples, and clinical symptoms disappear.
The method has the following advantages: facial acne basically heals, no new red pimple appears, and clinical symptoms basically disappear.
And (4) invalidation: facial acne and clinical symptoms are not obvious before treatment, and new red pimples still exist.
The results of the 28-day performance comparisons for the 15 groups of users are shown in the following table.
TABLE 4
| Group of | Efficient | Is effective | Invalidation |
| Control group | 0 | 6 | 9 |
| Face pack 1 | 10 | 5 | 0 |
| Face pack 2 | 12 | 3 | 0 |
| Face pack 3 | 10 | 5 | 0 |
| Face pack 4 | 0 | 0 | 15 |
| Face pack 5 | 7 | 8 | 0 |
| Face pack 6 | 4 | 6 | 5 |
| Face pack 7 | 5 | 7 | 3 |
| Face pack 8 | 5 | 8 | 2 |
| Face pack 9 | 6 | 8 | 1 |
| Mask 10 | 0 | 4 | 11 |
| Face pack 11 | 2 | 5 | 8 |
| Face pack 12 | 1 | 4 | 10 |
| Face pack 13 | 2 | 4 | 9 |
| Face mask 14 | 0 | 6 | 9 |
Compared with the oil-control acne-removing masks 4-14 prepared by the comparative examples 1-11, the oil-control acne-removing masks 1-3 prepared by the examples 1-3 of the invention have high acne-removing effect, which shows that the oil-control acne-removing composition has remarkable acne-removing effect compared with any four combined or single plant extracts. In addition, compared with the commercially available oil-controlling acne-removing mask, the oil-controlling acne-removing mask 1-3 provided by the invention has an obvious use effect.
The results show that the oil-control acne-removing composition has remarkable acne-removing efficacy, and the components have synergistic effect
Skin oil content test
Selecting 140 volunteers with the age of 18-40 years, male and female, and the screening conditions are as follows: sebum level after three hours of early morning cleansing is more than 150 mu g/cm2. The test pieces were randomly divided into 14 groups, each of which was 10 subjects, and the masks 1 to 3 prepared in examples 1 to 3 and the masks 4 to 14 prepared in comparative examples 1 to 11 were applied, respectively. The using method comprises the following steps: after cleaning face, each group was individuallyThe facial mask is applied on the whole face, is washed off by clear water after waiting for 25 minutes, and is used once a day. The average sebum reduction (%) after day 28 was measured using MPA580 skin elasticity (oil) tester (Probe: Sebumeter SM 815). The test results are shown in table 5:
TABLE 5 mean sebum reduction after 28 days of use for each group
| Group of | Sebum reduction ratio (%) | Group of | Sebum reduction ratio (%) |
| Face pack 1 | 49.62 | Face pack 8 | 36.71 |
| Face pack 2 | 48.51 | Face pack 9 | 40.36 |
| Face pack 3 | 55.33 | Mask 10 | 46.57 |
| Face pack 4 | -0.18 | Face pack 11 | 2.88 |
| Face pack 5 | 2.55 | Face pack 12 | 3.51 |
| Face pack 6 | 40.70 | Face pack 13 | 3.08 |
| Face pack 7 | 38.93 | Face mask 14 | 1.84 |
According to the data in table 5, the oil control effect of the oil control and acne removal composition added into the mask is stronger than that of cosmetics which are single in component and lack of any active component, which indicates that the five active components cooperate with each other, and after synergistic interaction, the oil secretion can be effectively inhibited.
The above description is only for the specific embodiments of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art can easily think of the changes or substitutions within the technical scope of the present invention, and shall cover the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the claims.
Claims (15)
1. The oil-controlling acne-removing composition is characterized by comprising the following components in parts by weight: 15-45 parts of curcuma zedoary, 15-40 parts of salix nigra bark, 5-25 parts of verruca stipes stem/root, 3-40 parts of hawthorn and 15-45 parts of kaempferia galanga root;
the preparation method of the oil-controlling acne-removing composition comprises the following steps:
(1) pretreating plant raw materials: weighing each plant raw material, crushing, grinding, sieving and uniformly mixing;
(2) extraction: adding the mixture into 60% ethanol solution at a ratio of 1 (8-14) for extraction at 50-80 deg.C for 3 times; extracting for 20-40 min each time, and filtering to obtain extractive solution;
(3) concentration: concentrating the extracting solution by reduced pressure distillation to obtain a concentrated solution;
(4) and (3) drying: and (4) freeze-drying the concentrated solution obtained in the step (3).
2. The composition for controlling oil and removing acne according to claim 1, which comprises the following components in parts by weight: 17-40 parts of curcuma zedoary, 16-35 parts of black willow bark, 8-24 parts of verruca pedunculata stem/root, 5-35 parts of hawthorn and 18-43 parts of kaempferia galanga root.
3. The oil-controlling acne-removing composition according to claim 1, which comprises the following components in parts by weight: 20-40 parts of curcuma zedoary, 16-35 parts of black willow bark, 10-24 parts of verruca pedunculata stem/root, 8-35 parts of hawthorn and 20-43 parts of kaempferia galanga root.
4. The oil-controlling acne-removing composition according to claim 1, which comprises the following components in parts by weight: 25 parts of curcuma zedoary, 20 parts of black willow bark, 18 parts of verruca vulgaris stem/root, 24 parts of hawthorn and 23 parts of kaempferia galanga root.
5. The composition for controlling oil and removing acne according to claim 1, which comprises the following components, by weight, 30 parts of curcuma zedoary, 25 parts of black willow bark, 12 parts of devil's-tongue stem/root, 27 parts of hawthorn and 31 parts of kaempferia galanga root.
6. The composition for controlling oil and removing acne according to claim 1, which comprises the following components, by weight, 37 parts of curcuma zedoary, 22 parts of bark of black willow, 15 parts of stem/root of amorphophallus virosus, 30 parts of hawthorn and 37 parts of kaempferia galanga root.
7. The composition for controlling oil and removing acne according to claim 1, wherein in the preparation method, in the step (2), the mixture is added into a 60% ethanol solution for extraction for 3 times in a ratio of 1: 14.
8. The composition for controlling oil and removing acne according to claim 1, wherein in the preparation method, in the step (2), the extraction temperature is 75 ℃.
9. The composition for controlling oil and removing acne according to claim 1, wherein in the preparation method, in the step (2), each extraction time is 30 min.
10. Use of the composition for controlling oil and removing acne according to any one of claims 1 to 9 in the preparation of cosmetics.
11. A cosmetic product comprising the composition for controlling oil and removing acne according to any one of claims 1 to 9, wherein the composition is contained in the cosmetic product in an amount of 1 to 30% by weight.
12. The cosmetic composition according to claim 11, wherein said composition is present in an amount of 5 to 20% by weight.
13. The use of claim 10, wherein the cosmetic is selected from one or more of a facial cleanser, a facial mask, a lotion, or an emulsion.
14. Use according to claim 10, characterized in that the cosmetic product is selected from face masks.
15. The use according to claim 14, wherein the mask comprises the following components in parts by weight: 0.01-1 part of allantoin, 0.001-0.025 part of hyaluronic acid, 1-7 parts of glycerol, 0.5-10 parts of butanediol, 0.01-0.5 part of carbomer, 0.01-0.7 part of triethanolamine, 1-30 parts of the oil-controlling and acne-removing composition according to any one of claims 1-9, 0.01-0.1 part of ethylhexylglycerin, 0.01-1 part of phenoxyethanol and 50-80 parts of deionized water.
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| CN112043655A (en) * | 2020-09-21 | 2020-12-08 | 东晟源研究院(广州)有限公司 | Plant anti-dandruff composition, silicone oil-free shampoo and preparation method thereof |
| CN114767603A (en) * | 2022-03-11 | 2022-07-22 | 彭氏(惠州)实业发展有限公司 | Acne-removing cosmetic composition containing red ginseng extract |
| CN115337252A (en) * | 2022-08-22 | 2022-11-15 | 广州药妆日用化工有限公司 | Acne-removing cream with acne-removing, inflammation-diminishing and skin-repairing effects and preparation method thereof |
| CN115364002B (en) * | 2022-09-30 | 2024-04-12 | 丽鑫生技化妆品（上海）有限公司 | Foundation liquid with acne removing effect and preparation method thereof |
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| CN104688811A (en) * | 2014-12-29 | 2015-06-10 | 昆明皕凯科技有限公司 | Acne removal composition based on natural plant raw materials and application thereof |
| CN104707057A (en) * | 2015-03-30 | 2015-06-17 | 广州市络捷生物科技有限公司 | Composition with acne removing effect as well as preparation method and application thereof |
| CN108210389A (en) * | 2018-03-08 | 2018-06-29 | 佛山市汇汾化妆品科技有限公司 | A kind of oil control and acne removal composition |
| KR20180077755A (en) * | 2016-12-29 | 2018-07-09 | 정윤주 | Cosmetic composition comprising rx complex |
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2020
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104688811A (en) * | 2014-12-29 | 2015-06-10 | 昆明皕凯科技有限公司 | Acne removal composition based on natural plant raw materials and application thereof |
| CN104707057A (en) * | 2015-03-30 | 2015-06-17 | 广州市络捷生物科技有限公司 | Composition with acne removing effect as well as preparation method and application thereof |
| KR20180077755A (en) * | 2016-12-29 | 2018-07-09 | 정윤주 | Cosmetic composition comprising rx complex |
| CN108210389A (en) * | 2018-03-08 | 2018-06-29 | 佛山市汇汾化妆品科技有限公司 | A kind of oil control and acne removal composition |
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