CN110982330A - Lightfast pink primary pigment red for solvent type ink and preparation method thereof - Google Patents
Lightfast pink primary pigment red for solvent type ink and preparation method thereof Download PDFInfo
- Publication number
- CN110982330A CN110982330A CN201911086432.8A CN201911086432A CN110982330A CN 110982330 A CN110982330 A CN 110982330A CN 201911086432 A CN201911086432 A CN 201911086432A CN 110982330 A CN110982330 A CN 110982330A
- Authority
- CN
- China
- Prior art keywords
- parts
- red
- solvent
- pigment red
- fast pink
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
- C09D11/037—Printing inks characterised by features other than the chemical nature of the binder characterised by the pigment
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/32—Inkjet printing inks characterised by colouring agents
- C09D11/322—Pigment inks
Abstract
The invention relates to a fast pink primary pigment red for solvent type ink, which comprises the following components in parts by weight: 15-22 parts of alkaline red, 1-5 parts of glacial acetic acid, 1-6 parts of disodium hydrogen phosphate, 11-17 parts of sodium tungstate, 18-24 parts of sodium molybdate, 2-5 parts of pigment auxiliary agent, 25-35 parts of hydrochloric acid, 2-6 parts of rosin and 2-5 parts of liquid alkali; the pigment auxiliary agent comprises the following components in parts by weight: 2-6 parts of 3- (1-methylethyl) -1H-1,2, 4-triazole-5-amine, 1-3 parts of hyperbranched polyethyleneimine, 2-6 parts of hyperbranched polyglycidyl ether, 3-6 parts of olbetanine, 2-7 parts of disodium ethylenediamine tetraacetic acid, 3-5 parts of diazolidinyl urea, 55-65 parts of water, 1-2 parts of dispersing agent, 1-3 parts of emulsifier and 12-18 parts of cosolvent. The invention also discloses a preparation method of the fast pink primary pigment red for the solvent type ink. The light-fast pink primary pigment red for the solvent type ink disclosed by the invention has the advantages of low viscosity, good storage and transportation stability, good dispersion, large tinting strength, higher light fastness, weather fastness and solvent resistance, and bright color.
Description
Technical Field
The invention relates to the technical field of pigments, in particular to a fast pink chromogen pigment red for solvent type ink and a preparation method thereof.
Background
Printing is a technique of transferring ink to the surface of a material such as paper, fabric, plastic, or leather by performing processes such as plate making, inking, and pressing on an original such as characters, pictures, photographs, or forgery prevention, and thereby mass-transferring the content of the original. Printing is the process of transferring the approved printing plate to the printing stock by printing machine and special ink. Ink is an important material for printing, and is used for expressing patterns and characters on a printing material through printing or inkjet. The ink comprises main components and auxiliary components, is uniformly mixed and repeatedly rolled to form viscous colloidal fluid, consists of a binder, a pigment, a filler, an auxiliary agent, a solvent and the like, and is used for various printings such as books, periodicals, packaging decorations, building decorations, electronic circuit boards and the like. As social demands increase, ink varieties and yields also expand and grow accordingly. At present, common ink on the market is solvent-based ink, and a pigment for solvent-based ink applied to the ink is a substance capable of coloring an object and is a determining factor for endowing color and aesthetic feeling, so that the pigment for the solvent-based ink attracts wide attention of people.
The traditional pigment red is applied in more industry, and with the development of technology, more and more pigment red has certain application in ink materials, such as NC ink, PP ink, PA ink, PU ink and the like. In the ink material, the pigment needs to meet the requirements of low viscosity (high viscosity easily causes the caking phenomenon in the storage process and influences the use) and good stability, and the current pigment red is deficient in the aspects or cannot meet the aim of compatibility.
The invention patent of China with the application number of CN201610959477.1 provides 'a dispersible pigment red for food packaging and a preparation method thereof', the dispersible pigment red is prepared by occasional reaction with reasonable proportion control, and the problems that the pigment red cannot realize bright luster, high tinting strength and good dispersibility are solved, but the pigment red obtained by the method has higher viscosity and poorer dispersion stability and is not suitable for solvent-based ink, and besides, the pigment red also has the problem of poor light fastness.
Therefore, the development of the novel sunfast pink primary pigment red for the solvent type ink meets the market demand, has wide market value and application prospect, and has very important significance for promoting the development of the pigment red industry.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provide a fast pink primary pigment for solvent type ink and a preparation method thereof, and the preparation method has the advantages of simple formula and process, convenient operation, easy material acquisition, low preparation cost, small dependence on equipment, suitability for continuous industrial production, and higher economic value, social value and ecological value; the prepared sunfast pink primary pigment for the solvent type ink material has low viscosity, good storage and transportation stability, good dispersion, large tinting strength, strong crack resistance, higher light fastness, weather fastness and solvent resistance, and bright color.
In order to achieve the purpose, the invention adopts the technical scheme that:
a fast pink chromogen pigment red for solvent-based ink comprises the following components in parts by weight: 15-22 parts of alkaline red, 1-5 parts of glacial acetic acid, 1-6 parts of disodium hydrogen phosphate, 11-17 parts of sodium tungstate, 18-24 parts of sodium molybdate, 2-5 parts of pigment auxiliary agent, 25-35 parts of hydrochloric acid, 2-6 parts of rosin and 2-5 parts of liquid alkali; the pigment auxiliary agent comprises the following components in parts by weight: 2-6 parts of 3- (1-methylethyl) -1H-1,2, 4-triazole-5-amine, 1-3 parts of hyperbranched polyethyleneimine, 2-6 parts of hyperbranched polyglycidyl ether, 3-6 parts of olbetanine, 2-7 parts of disodium ethylenediamine tetraacetic acid, 3-5 parts of diazolidinyl urea, 55-65 parts of water, 1-2 parts of dispersing agent, 1-3 parts of emulsifier and 12-18 parts of cosolvent.
Further, the cosolvent is one of ethanol, isopropanol and butanone.
Further, the emulsifier is at least one of sodium dodecyl benzene sulfonate, polyoxypropylene polyoxyethylene glycerol ether and nonylphenol polyoxyethylene ether.
Further, the dispersant is at least one of 760W dispersant, sodium hexametaphosphate and sodium polycarboxylate.
Further, the hyperbranched polyethyleneimine is hyperbranched polyethyleneimine G4, which is purchased from alpha pharmaceutical industry; the hyperbranched polyglycidyl ether is prepared in advance, and the preparation method refers to the following steps: zhubao Kuo, Zhaoyonghong, Kong Li, et al, research progress of hyperbranched polyglycidyl ether [ J ] macromolecule report, 2007(04): 25-30.
Further, the fast pink primary pigment red for the solvent type ink comprises the following components in parts by weight: 17-18 parts of basic red; 3-4 parts of glacial acetic acid; 3-4 parts of disodium hydrogen phosphate; 12-13 parts of sodium tungstate; 22-23 parts of sodium molybdate; 3-4 parts of a pigment auxiliary agent; 32-33 parts of hydrochloric acid; 3-4 parts of rosin; 3-5 parts of liquid caustic soda.
Further, the fast pink primary pigment red for the solvent type ink comprises the following components in parts by weight: 17.5 parts of basic red; 4 parts of glacial acetic acid; 4 parts of disodium hydrogen phosphate; 12.5 parts of sodium tungstate; 22.5 parts of sodium molybdate; 3 parts of a pigment auxiliary agent; 32.5 parts of hydrochloric acid; 3.5 parts of rosin; 4 parts of liquid caustic soda.
Another object of the present invention is to provide a method for preparing the fast pink primary pigment red for the solvent-based ink, which comprises the following steps:
1) dissolving alkaline red in water at a certain temperature in a reaction barrel;
2) putting sodium tungstate, sodium molybdate and disodium hydrogen phosphate into another reaction barrel and dissolving;
3) adding the phosphorus, tungsten and molybdic acid solution dissolved in the step 2) into the alkaline red dissolved in the step 1);
4) after the reaction is finished, the materials are rinsed, dried and crushed in sequence.
Further, the certain temperature in the step 1) is 75-85 ℃.
Further, the certain temperature in the step 1) is 80 ℃.
Due to the application of the technical scheme, compared with the prior art, the invention has the following advantages: the preparation method has the advantages of simple formula and process, convenient operation, easy material acquisition, low preparation cost, small dependence on equipment, suitability for continuous industrial production and higher economic value, social value and ecological value; the prepared sunfast pink primary pigment for the solvent type ink material has low viscosity, good storage and transportation stability, good dispersion, large tinting strength, strong crack resistance, higher light fastness, weather fastness and solvent resistance, and bright color; effectively solves the problem that the pigment red in the prior art can not realize low viscosity and good stability.
Detailed Description
The invention relates to a fast pink primary pigment red for solvent type ink, which comprises the following components in parts by weight: 15-22 parts of alkaline red, 1-5 parts of glacial acetic acid, 1-6 parts of disodium hydrogen phosphate, 11-17 parts of sodium tungstate, 18-24 parts of sodium molybdate, 2-5 parts of pigment auxiliary agent, 25-35 parts of hydrochloric acid, 2-6 parts of rosin and 2-5 parts of liquid alkali; the pigment auxiliary agent comprises the following components in parts by weight: 2-6 parts of 3- (1-methylethyl) -1H-1,2, 4-triazole-5-amine, 1-3 parts of hyperbranched polyethyleneimine, 2-6 parts of hyperbranched polyglycidyl ether, 3-6 parts of olbetanine, 2-7 parts of disodium ethylenediamine tetraacetic acid, 3-5 parts of diazolidinyl urea, 55-65 parts of water, 1-2 parts of dispersing agent, 1-3 parts of emulsifier and 12-18 parts of cosolvent.
Further, the cosolvent is one of ethanol, isopropanol and butanone; the emulsifier is at least one of sodium dodecyl benzene sulfonate, polyoxypropylene polyoxyethylene glycerol ether and nonylphenol polyoxyethylene ether; the dispersant is at least one of 760W dispersant, sodium hexametaphosphate and sodium polycarboxylate; the hyperbranched polyethyleneimine is hyperbranched polyethyleneimine G4 and is purchased from alpha pharmaceutical industry; the hyperbranched polyglycidyl ether is prepared in advance, and the preparation method refers to the following steps: zhubao Kuo, Zhaoyonghong, Kong Li, et al, research progress of hyperbranched polyglycidyl ether [ J ] macromolecule report, 2007(04): 25-30.
Further, the fast pink primary pigment red for the solvent type ink comprises the following components in parts by weight: 17-18 parts of basic red; 3-4 parts of glacial acetic acid; 3-4 parts of disodium hydrogen phosphate; 12-13 parts of sodium tungstate; 22-23 parts of sodium molybdate; 3-4 parts of a pigment auxiliary agent; 32-33 parts of hydrochloric acid; 3-4 parts of rosin; 3-5 parts of liquid caustic soda.
Further, the fast pink primary pigment red for the solvent type ink comprises the following components in parts by weight: 17.5 parts of basic red; 4 parts of glacial acetic acid; 4 parts of disodium hydrogen phosphate; 12.5 parts of sodium tungstate; 22.5 parts of sodium molybdate; 3 parts of a pigment auxiliary agent; 32.5 parts of hydrochloric acid; 3.5 parts of rosin; 4 parts of liquid caustic soda.
Another object of the present invention is to provide a method for preparing the fast pink primary pigment red for the solvent-based ink, which comprises the following steps:
1) dissolving alkaline red in water at a certain temperature in a reaction barrel;
2) putting sodium tungstate, sodium molybdate and disodium hydrogen phosphate into another reaction barrel and dissolving;
3) adding the phosphorus, tungsten and molybdic acid solution dissolved in the step 2) into the alkaline red dissolved in the step 1);
4) after the reaction is finished, the materials are rinsed, dried and crushed in sequence.
Further, the certain temperature in the step 1) is 75-85 ℃; preferably, the certain temperature in the step 1) is 80 ℃.
Due to the application of the technical scheme, compared with the prior art, the invention has the following advantages: the preparation method has the advantages of simple formula and process, convenient operation, easy material acquisition, low preparation cost, small dependence on equipment, suitability for continuous industrial production and higher economic value, social value and ecological value; the prepared sunfast pink primary pigment for the solvent type ink material has low viscosity, good storage and transportation stability, good dispersion, large tinting strength, strong crack resistance, higher light fastness, weather fastness and solvent resistance, and bright color; effectively solves the problem that the pigment red in the prior art can not realize low viscosity and good stability.
The invention will be further described with reference to specific examples, but the scope of the invention is not limited thereto.
Example 1
Embodiment 1 provides a fast pink primary pigment red for solvent-based ink, which comprises the following components in parts by weight: 15 parts of alkaline red, 1 part of glacial acetic acid, 1 part of disodium hydrogen phosphate, 11 parts of sodium tungstate, 18 parts of sodium molybdate, 2 parts of pigment auxiliary agent, 25 parts of hydrochloric acid, 2 parts of rosin and 2 parts of liquid alkali; the pigment auxiliary agent comprises the following components in parts by weight: 2 parts of 3- (1-methylethyl) -1H-1,2, 4-triazole-5-amine, 1 part of hyperbranched polyethyleneimine, 2 parts of hyperbranched polyglycidyl ether, 3 parts of olbetaine, 2 parts of disodium ethylene diamine tetraacetate, 3 parts of diazolidinyl urea, 55 parts of water, 1 part of sodium hexametaphosphate, 1 part of sodium dodecyl benzene sulfonate and 12 parts of ethanol; the hyperbranched polyethyleneimine is hyperbranched polyethyleneimine G4.
The preparation method of the fast pink primary pigment red for the solvent type ink is characterized by comprising the following steps:
1) dissolving alkaline red in water at 80 ℃ in a reaction barrel;
2) putting sodium tungstate, sodium molybdate and disodium hydrogen phosphate into another reaction barrel and dissolving;
3) adding the phosphorus, tungsten and molybdic acid solution dissolved in the step 2) into the alkaline red dissolved in the step 1);
4) after the reaction is finished, the materials are rinsed, dried and crushed in sequence.
Example 2
Example 2 provides a fast pink primary pigment red for solvent-based ink, which has the same formula and preparation method as those of example 1, except that the pigment red comprises the following components in parts by weight: 17 parts of alkaline red, 2 parts of glacial acetic acid, 2 parts of disodium hydrogen phosphate, 12 parts of sodium tungstate, 20 parts of sodium molybdate, 3 parts of pigment auxiliary agent, 27 parts of hydrochloric acid, 3 parts of rosin and 3 parts of liquid alkali.
Example 3
Example 3 provides a fast pink primary pigment red for solvent-based ink, which has the same formula and preparation method as example 1, except that the pigment red comprises the following components in parts by weight: 19 parts of alkaline red, 3.5 parts of glacial acetic acid, 4 parts of disodium hydrogen phosphate, 15 parts of sodium tungstate, 21 parts of sodium molybdate, 4 parts of pigment auxiliary agent, 30 parts of hydrochloric acid, 4 parts of rosin and 3.5 parts of liquid alkali.
Example 4
Example 4 provides a fast pink primary pigment red for solvent-based ink, which has the same formula and preparation method as example 1, except that the pigment red comprises the following components in parts by weight: 21 parts of basic red, 4.5 parts of glacial acetic acid, 5.5 parts of disodium hydrogen phosphate, 16 parts of sodium tungstate, 23 parts of sodium molybdate, 4.5 parts of pigment auxiliary agent, 33 parts of hydrochloric acid, 5.5 parts of rosin and 4.5 parts of liquid alkali.
Example 5
Example 5 provides a fast pink primary pigment red for solvent-based ink, which has the same formula and preparation method as example 1, except that the pigment red comprises the following components in parts by weight: 22 parts of basic red, 5 parts of glacial acetic acid, 6 parts of disodium hydrogen phosphate, 17 parts of sodium tungstate, 24 parts of sodium molybdate, 5 parts of pigment auxiliary agent, 35 parts of hydrochloric acid, 6 parts of rosin and 5 parts of liquid alkali.
Comparative example 1
Comparative example 1 provides a fast pink primary pigment red for solvent-based inks, which was formulated and prepared substantially the same as in example 1, except that glacial acetic acid, disodium hydrogen phosphate, rosin, and liquid alkali were not added.
Comparative example 2
Comparative example 2 provides a fast pink-red chromogen pigment red for solvent-based inks, having substantially the same formulation and preparation method as in example 1, except that 3- (1-methylethyl) -1H-1,2, 4-triazol-5-amine and hyperbranched polyethyleneimine are not added.
Comparative example 3
Comparative example 3 provides a fast pink chromogen pigment red for solvent-based inks, having substantially the same formulation and preparation as in example 1, except that no hyperbranched polyglycidyl ether and no olbetanin were added.
Comparative example 4
Comparative example 4 provides a fast pink-red chromogen pigment red for solvent-based inks, having substantially the same formulation and preparation method as in example 1, except that disodium ethylenediaminetetraacetate and diazolidinyl urea were not added.
To further illustrate the technical effects of the embodiments of the present invention, the high strength pigment red prepared in the embodiments 1 to 5 and the comparative examples 1 to 4 of the present invention is tested, the test results are shown in table 1, and the test method is performed by referring to the existing measurement conditions for pigment red in the prior art, such as those described in the national standards and the industry standards, and will not be described herein again.
TABLE 1
| Detecting items | Viscosity of the oil | Degree of gloss | Color strength value |
| Example 1 | 46 | 5 | 111 |
| Example 2 | 37 | 5 | 109 |
| Example 3 | 40 | 4 | 113 |
| Example 4 | 35 | 5 | 115 |
| Example 5 | 45 | 5 | 113 |
| Comparative example 1 | 1000 | 2 | 98 |
| Comparative example 2 | 325 | 3 | 95 |
| Comparative example 3 | 370 | 3 | 96 |
| Comparative example 4 | 280 | 2 | 93 |
As can be seen from Table 1, the fast pink chromogen pigment red for the solvent type ink and the preparation method thereof provided by the invention have the advantages that the obtained high strength pigment red has low viscosity, good storage and transportation stability and better glossiness through the proportion and the preparation method; the 3- (1-methylethyl) -1H-1,2, 4-triazole-5-amine, hyperbranched polyethyleneimine, hyperbranched polyglycidyl ether, sodium aspartame, disodium ethylenediamine tetraacetate and diazolidinyl urea in the pigment auxiliary agent have synergistic effect, and the performance can be improved.
The above embodiments are merely illustrative of the technical ideas and features of the present invention, and the purpose thereof is to enable those skilled in the art to understand the contents of the present invention and implement the present invention, and not to limit the protection scope of the present invention. All equivalent changes and modifications made according to the spirit of the present invention should be covered within the protection scope of the present invention.
Claims (10)
1. The fast pink chromogen pigment red for the solvent type ink is characterized by comprising the following components in parts by weight: 15-22 parts of alkaline red, 1-5 parts of glacial acetic acid, 1-6 parts of disodium hydrogen phosphate, 11-17 parts of sodium tungstate, 18-24 parts of sodium molybdate, 2-5 parts of pigment auxiliary agent, 25-35 parts of hydrochloric acid, 2-6 parts of rosin and 2-5 parts of liquid alkali; the pigment auxiliary agent comprises the following components in parts by weight: 2-6 parts of 3- (1-methylethyl) -1H-1,2, 4-triazole-5-amine, 1-3 parts of hyperbranched polyethyleneimine, 2-6 parts of hyperbranched polyglycidyl ether, 3-6 parts of olbetanine, 2-7 parts of disodium ethylenediamine tetraacetic acid, 3-5 parts of diazolidinyl urea, 55-65 parts of water, 1-2 parts of dispersing agent, 1-3 parts of emulsifier and 12-18 parts of cosolvent.
2. The fast pink chromogen pigment red for solvent-based inks according to claim 1, wherein the cosolvent is one of ethanol, isopropanol and butanone.
3. The fast pink chromogen pigment red for solvent-based inks according to claim 1, wherein the emulsifier is at least one of sodium dodecylbenzene sulfonate, polyoxypropylene polyoxyethylene glyceryl ether and nonylphenol polyoxyethylene ether.
4. The fast pink chromogen pigment red for solvent-based inks according to claim 1, wherein the dispersant is at least one of 760W dispersant, sodium hexametaphosphate, and sodium polycarboxylate.
5. The fast pink-red-base pigment red for solvent-based inks according to claim 1, wherein the hyperbranched polyethyleneimine is hyperbranched polyethyleneimine G4.
6. The fast pink-red-base pigment red for the solvent-based ink according to claim 1, which is characterized by comprising the following components in parts by weight: 17-18 parts of basic red; 3-4 parts of glacial acetic acid; 3-4 parts of disodium hydrogen phosphate; 12-13 parts of sodium tungstate; 22-23 parts of sodium molybdate; 3-4 parts of a pigment auxiliary agent; 32-33 parts of hydrochloric acid; 3-4 parts of rosin; 3-5 parts of liquid caustic soda.
7. The fast pink-red-base pigment red for the solvent-based ink according to claim 1, which is characterized by comprising the following components in parts by weight: 17.5 parts of basic red; 4 parts of glacial acetic acid; 4 parts of disodium hydrogen phosphate; 12.5 parts of sodium tungstate; 22.5 parts of sodium molybdate; 3 parts of a pigment auxiliary agent; 32.5 parts of hydrochloric acid; 3.5 parts of rosin; 4 parts of liquid caustic soda.
8. The fast pink-red-chromogen pigment red for solvent-based inks according to any one of claims 1 to 7, wherein the preparation method of the fast pink-red-chromogen pigment red for solvent-based inks comprises the following steps:
1) dissolving alkaline red in water at a certain temperature in a reaction barrel;
2) putting sodium tungstate, sodium molybdate and disodium hydrogen phosphate into another reaction barrel and dissolving;
3) adding the phosphorus, tungsten and molybdic acid solution dissolved in the step 2) into the alkaline red dissolved in the step 1);
4) after the reaction is finished, the materials are rinsed, dried and crushed in sequence.
9. The fast pink color primary pigment red for solvent-based inks according to claim 8, wherein said certain temperature in step 1) is 75-85 ℃.
10. The fast pink color primary pigment red for solvent-based inks according to claim 8, wherein said certain temperature in step 1) is 80 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911086432.8A CN110982330A (en) | 2019-11-08 | 2019-11-08 | Lightfast pink primary pigment red for solvent type ink and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911086432.8A CN110982330A (en) | 2019-11-08 | 2019-11-08 | Lightfast pink primary pigment red for solvent type ink and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110982330A true CN110982330A (en) | 2020-04-10 |
Family
ID=70083583
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201911086432.8A Pending CN110982330A (en) | 2019-11-08 | 2019-11-08 | Lightfast pink primary pigment red for solvent type ink and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110982330A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113637230A (en) * | 2021-09-15 | 2021-11-12 | 吴江山湖颜料有限公司 | Peach red chromogen with high temperature resistance and preparation method thereof |
| CN113773669A (en) * | 2021-09-15 | 2021-12-10 | 吴江山湖颜料有限公司 | High-light-resistance green lotus chromogen and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0135083A2 (en) * | 1983-08-11 | 1985-03-27 | Bayer Ag | 3-Cycloalkyl-1-(1,3-dioxan-5-yl)-2-(1,2,4-triazol-1-yl)-propan-1-ones and -propan-1-ols |
| CN1919942A (en) * | 2005-08-23 | 2007-02-28 | 富士胶片株式会社 | Curable composition, ink composition, inkjet recording method |
| CN102702327A (en) * | 2012-06-20 | 2012-10-03 | 吉尔生化（上海）有限公司 | Solid-liquid phase synthesis method for alarelin acetate |
| CN108017934A (en) * | 2016-11-03 | 2018-05-11 | 吴江山湖颜料有限公司 | A kind of ink sun-proof pink chromogen paratonere and preparation method |
| CN108017932A (en) * | 2016-11-03 | 2018-05-11 | 吴江山湖颜料有限公司 | A kind of ink everbright fast violet toner paratonere and preparation method |
-
2019
- 2019-11-08 CN CN201911086432.8A patent/CN110982330A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0135083A2 (en) * | 1983-08-11 | 1985-03-27 | Bayer Ag | 3-Cycloalkyl-1-(1,3-dioxan-5-yl)-2-(1,2,4-triazol-1-yl)-propan-1-ones and -propan-1-ols |
| CN1919942A (en) * | 2005-08-23 | 2007-02-28 | 富士胶片株式会社 | Curable composition, ink composition, inkjet recording method |
| CN102702327A (en) * | 2012-06-20 | 2012-10-03 | 吉尔生化（上海）有限公司 | Solid-liquid phase synthesis method for alarelin acetate |
| CN108017934A (en) * | 2016-11-03 | 2018-05-11 | 吴江山湖颜料有限公司 | A kind of ink sun-proof pink chromogen paratonere and preparation method |
| CN108017932A (en) * | 2016-11-03 | 2018-05-11 | 吴江山湖颜料有限公司 | A kind of ink everbright fast violet toner paratonere and preparation method |
Non-Patent Citations (3)
| Title |
|---|
| 朱宝库等: "超支化聚缩水甘油醚研究进展", 《高分子通报》 * |
| 禹茂章等，: "《国外药品商品名辞典》", 31 December 1995, 中国医药科技出版社 * |
| 赵洪波等: "《胶体与表面化学理论及应用研究》", 31 March 2016, 黑龙江大学出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113637230A (en) * | 2021-09-15 | 2021-11-12 | 吴江山湖颜料有限公司 | Peach red chromogen with high temperature resistance and preparation method thereof |
| CN113773669A (en) * | 2021-09-15 | 2021-12-10 | 吴江山湖颜料有限公司 | High-light-resistance green lotus chromogen and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103756410B (en) | A kind of PE plastics film gravure use ink and preparation method thereof | |
| CN110982330A (en) | Lightfast pink primary pigment red for solvent type ink and preparation method thereof | |
| CN104861778A (en) | Water-based ink for grainy paper printing and preparation method thereof | |
| CN111518433A (en) | Printing ink for anti-counterfeiting embossed tipping paper and preparation method thereof | |
| CN103451998B (en) | A kind of colored dust-free paper top sizing dyeing | |
| CN112480743A (en) | Weather-proof thermal sublimation thermal transfer printing ink and preparation method thereof | |
| CN110885588A (en) | Aqueous glazing-free printing material for preprinting and preparation method thereof | |
| CN114958084B (en) | Preparation method of low-viscosity high-solid-content anti-offset composite ink for flexography | |
| CN106543807A (en) | A kind of preparation method that high safety redness mill base is printed for medicated napkin | |
| CN107286743A (en) | A kind of boiling water resistance water-based ink printed applied to PVC | |
| CN113072840A (en) | Thermal sublimation ink based on compound disperse black dye and preparation method thereof | |
| CN107059425A (en) | A kind of preparation method and applications of ink-jet printing ink composition suitable for tricot de laine | |
| CN105348913A (en) | Environment-friendly water-soluble gravure paper blue ink and preparation method thereof | |
| CN111995904A (en) | Water-based environment-friendly ink and preparation method thereof | |
| CN101469155A (en) | Environment friendly transparent iron oxide yellow superfine aqueous color sizing dispersion and preparation thereof | |
| CN110982331A (en) | Pigment violet for PP ink and preparation method thereof | |
| CN111019391A (en) | Pigment violet for PA ink and preparation method thereof | |
| CN110964360A (en) | High-strength pigment red and preparation method thereof | |
| CN113388285B (en) | Water-based ink with good initial drying property, strong adhesion fastness and adhesion resistance and preparation method thereof | |
| CN108948866A (en) | One kind becoming special printing inks and preparation method thereof for the aqueous light of intaglio plate green | |
| CN104263066A (en) | Anti-yellowing multipurpose environment-friendly white printing ink | |
| CN106433297A (en) | Waterborne polyurethane plastic ink and preparation method thereof | |
| CN104231734A (en) | Anti-clogging and high-temperature-resisting polyvinyl butyral spray ink | |
| CN114702860A (en) | Improved water-based anti-counterfeiting ink for paperboard printing and preparation method thereof | |
| CN104877447A (en) | Anti-stripping non-staining water-based ink for paper printing |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20200410 |
|
| RJ01 | Rejection of invention patent application after publication |