CN110922644A - Cigarette capsule wall material capable of being dried quickly and cigarette capsule based on same - Google Patents
Cigarette capsule wall material capable of being dried quickly and cigarette capsule based on same Download PDFInfo
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- CN110922644A CN110922644A CN201911338358.4A CN201911338358A CN110922644A CN 110922644 A CN110922644 A CN 110922644A CN 201911338358 A CN201911338358 A CN 201911338358A CN 110922644 A CN110922644 A CN 110922644A
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- Prior art keywords
- capsule
- wall material
- cigarette
- coaxial double
- cigarette capsule
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L5/00—Compositions of polysaccharides or of their derivatives not provided for in groups C08L1/00 or C08L3/00
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/32—Phosphorus-containing compounds
- C08K2003/321—Phosphates
- C08K2003/324—Alkali metal phosphate
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a cigarette capsule wall material capable of being dried quickly and a cigarette capsule based on the same, wherein the cigarette capsule wall material comprises the following raw materials in parts by weight: 10-12 parts of carrageenan, 1 part of gelatin, 100 parts of deionized water, 0.2-0.4 part of sorbitol, 0.3 part of sodium pyrophosphate and 0.2 part of potassium chloride. The capsule wall material has low water content, the drying speed is shortened to 1/3-1/2 of the normal time, the production efficiency is greatly improved, and each quality index after the capsule is prepared can meet the requirement of industrially rolling the capsule filter stick.
Description
Technical Field
The invention belongs to the technical field of cigarettes, and particularly relates to a cigarette capsule wall material capable of being dried quickly and a cigarette capsule based on the same.
Background
The capsule for cigarette is prepared by embedding a semi-permeable membrane or a sealed capsule wrapped with liquid essence perfume into a cigarette filter tip by a filter stick bead embedding technology, and when the capsule is used, the capsule is broken by pinching the capsule, so that the liquid essence perfume in the capsule is fused into the fiber of the filter stick, and the effects of increasing the smoke humidity and improving the fragrance intercepting effect of the filter stick are achieved. Meanwhile, the aroma components in the capsule volatilize, so that the functions of cigarette aroma enhancement and taste level enrichment can be realized, and the capsule is wrapped by the outer wall, so that the capsule has the advantages of stable addition amount, difficult loss of effective components and the like, and is more and more widely applied.
Chinese patent CN12824887A discloses a capsule for tobacco prepared by an emulsification method: the oil-soluble essence, water and metal ions are made into emulsion, and the emulsion is dropped into the liquid using sodium alginate as main material, and the chemical action of sodium alginate and metal ions is utilized to form the outer wall of the capsule, and then the capsule is decolored, dehydrated and dried to prepare the capsule for cigarette. Chinese patent CN200910273417.4 discloses a dripping pill wrapping material for tobacco additives, dripping pills wrapped by the same and application of the dripping pills, wherein a dripping method is adopted, the dripping pill wrapping material and tobacco essence and spice are dripped from a concentric glue outlet and a discharge outlet at the same time and are solidified and formed in a curing agent, and finally, capsules for tobacco are prepared after drying and screening. The water content of the capsule wall material is more than 92 percent, the drying process takes about 4 to 8 hours, and if the water content is reduced, the viscosity of the packaging material of the dropping pill is improved, which brings difficulty to the subsequent industrial production.
Disclosure of Invention
In view of the above-mentioned shortcomings of the prior art, the present invention aims to provide a wall material for a cigarette capsule with low water content and capable of being dried quickly, and a cigarette capsule based on the wall material, so that the cigarette capsule dripped by the wall material can be dried quickly in the drying process.
In order to achieve the purpose, the invention adopts the following technical scheme:
the invention firstly discloses a cigarette capsule wall material capable of being dried quickly, which is characterized in that: the capsule wall material for the cigarettes comprises the following raw materials in parts by weight: 10-12 parts of carrageenan, 1 part of gelatin, 100 parts of deionized water, 0.2-0.4 part of sorbitol, 0.3 part of sodium pyrophosphate and 0.2 part of potassium chloride.
Further, according to actual production needs, the raw materials of the food-grade red-purple-brown-purple-red-purple-red-amaranth-purple-brown-chocolate-brown-red-yellow-red-purple-red-brown-red-yellow-red-brown.
The invention also discloses a cigarette capsule capable of being dried quickly, which is characterized in that: the wall material of the cigarette capsule is the wall material of the cigarette capsule.
The preparation method of the capsule for the cigarette comprises the following steps:
(1) adding the raw materials of the wall material of the cigarette capsule into a glue melting tank according to a ratio, heating to 75-85 ℃, stirring at constant temperature until the mixture is completely dissolved, adding the colorant, continuously stirring at constant temperature until the colorant is completely dissolved and uniformly dispersed, stopping stirring, keeping the temperature, standing, removing bubbles, and sieving with a 80-mesh sieve to obtain a wall material glue solution;
(2) adopting a dripping device with a coaxial double-layer dripper, wherein the coaxial double-layer dripper has an internal pulse function; adding the wall material glue solution and the capsule content into a corresponding storage tank of dripping equipment, and conveying the wall material glue solution and the capsule content to a coaxial double-layer dripper through a pipeline; setting the outlet temperature of a coaxial double-layer dripper to be 75-95 ℃, when the wall material glue solution and the capsule content pass through the coaxial double-layer dripper, performing pulse cutting on the capsule content to form liquid drops, and dripping the liquid drops into paraffin oil at 15-18 ℃ for cooling to form spherical wet capsules;
(3) taking out the wet capsule, and cleaning with edible ethanol;
(4) putting the washed wet capsules into drying equipment, and shaping and drying at 38 ℃ for 1-3 h to obtain dry capsules;
(5) and (3) balancing the dry capsule for more than 72 hours in an environment with the temperature of 22 +/-2 ℃ and the humidity of 50 +/-5 percent to obtain a finished product.
Further, the content of the capsule is a cigarette additive and is an essence and flavor meeting YCT164-2012 standard.
Compared with the prior art, the invention has the beneficial effects that:
1. according to the invention, the water content of the capsule wall material raw material is reduced, the potassium salt is added to adjust the capsule wall material raw material to the viscosity suitable for production, so that the capsule wall material raw material has low water content and viscosity suitable for production, the drying speed is shortened to 1/3-1/2 of normal time, the production efficiency is greatly improved, and each quality index after the capsule is prepared can meet the requirement of industrially rolling the capsule filter stick.
2. The capsule drying speed is high, the drying time and energy consumption are reduced, and the production cost can be reduced.
3. The preparation method is simple and can meet the industrial production requirement.
Detailed Description
The following examples are given for the detailed implementation and specific operation of the present invention, but the scope of the present invention is not limited to the following examples.
Example 1
(1) Respectively weighing 10kg of carrageenan, 1kg of gelatin, 100kg of deionized water, 0.2kg of sorbitol, 0.3kg of sodium pyrophosphate and 0.2kg of potassium chloride, adding the materials into a gelatin melting tank, heating to 80 ℃, stirring at constant temperature until the mixture is completely dissolved, adding 15g of brilliant blue, continuously stirring at constant temperature until the brilliant blue is completely dissolved and uniformly dispersed, stopping stirring, keeping the temperature and standing for 1h to remove bubbles, and sieving with an 80-mesh sieve to obtain a wall material gelatin solution.
(2) Adopting a dripping device with a coaxial double-layer dripper, wherein the coaxial double-layer dripper has an internal pulse function; adding wall material glue solution and capsule content (essence for orange flavor cigarette) into a corresponding storage tank of dripping equipment, and conveying to a coaxial double-layer dripper through a pipeline; the mass ratio of the wall material glue solution to the capsule content is 4:1, the outlet temperature of the coaxial double-layer dripper is set to be 85 ℃, when the wall material glue solution and the capsule content pass through the coaxial double-layer dripper, the capsule content is subjected to pulse cutting to form liquid drops, and the liquid drops are dripped into paraffin oil at the temperature of 16 ℃ for cooling to form spherical wet capsules.
(3) Taking out the wet capsule, and cleaning with 99% edible ethanol;
(4) putting the washed wet capsules into drying equipment, and shaping and drying at 38 ℃ for 2h to obtain dry capsules;
(5) and (3) balancing the dry capsules for more than 72 hours in an environment with the temperature of 22 +/-2 ℃ and the humidity of 50 +/-5 percent to obtain the finished product.
The final capsule weight of the present example is 12.0 + -1.0 mg, wherein the content weight is 10.8 + -1.0 mg, the capsule particle size is 2.70 + -0.2 mm, and the capsule pressure mean value is 1.2 + -0.2 kg.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents and improvements made within the spirit and principle of the present invention are intended to be included within the scope of the present invention.
Claims (4)
1. The cigarette capsule wall material capable of being dried quickly is characterized in that: the capsule wall material for the cigarettes comprises the following raw materials in parts by weight: 10-12 parts of carrageenan, 1 part of gelatin, 100 parts of deionized water, 0.2-0.4 part of sorbitol, 0.3 part of sodium pyrophosphate and 0.2 part of potassium chloride.
2. A cigarette capsule capable of being dried quickly is characterized in that: the wall material of the cigarette capsule is the wall material of the cigarette capsule in claim 1.
3. A preparation method of the capsule for the cigarette as claimed in claim 2, which is characterized by comprising the following steps:
(1) adding the raw materials of the wall material of the cigarette capsule into a glue melting tank according to a ratio, heating to 75-85 ℃, stirring at constant temperature until the mixture is completely dissolved, adding the colorant, continuously stirring at constant temperature until the colorant is completely dissolved and uniformly dispersed, stopping stirring, keeping the temperature, standing, removing bubbles, and sieving with a 80-mesh sieve to obtain a wall material glue solution;
(2) adopting a dripping device with a coaxial double-layer dripper, wherein the coaxial double-layer dripper has an internal pulse function; adding the wall material glue solution and the capsule content into a corresponding storage tank of dripping equipment, and conveying the wall material glue solution and the capsule content to a coaxial double-layer dripper through a pipeline; setting the outlet temperature of a coaxial double-layer dripper to be 75-95 ℃, when the wall material glue solution and the capsule content pass through the coaxial double-layer dripper, performing pulse cutting on the capsule content to form liquid drops, and dripping the liquid drops into paraffin oil at 15-18 ℃ for cooling to form spherical wet capsules;
(3) taking out the wet capsule, and cleaning with edible ethanol;
(4) putting the washed wet capsules into drying equipment, and shaping and drying at 38 ℃ for 1-3 h to obtain dry capsules;
(5) and (3) balancing the dry capsule for more than 72 hours in an environment with the temperature of 22 +/-2 ℃ and the humidity of 50 +/-5 percent to obtain a finished product.
4. The production method according to claim 3, characterized in that: the using amount of the colorant is 0-0.05 part.
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CN201911338358.4A CN110922644A (en) | 2019-12-23 | 2019-12-23 | Cigarette capsule wall material capable of being dried quickly and cigarette capsule based on same |
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CN201911338358.4A CN110922644A (en) | 2019-12-23 | 2019-12-23 | Cigarette capsule wall material capable of being dried quickly and cigarette capsule based on same |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN117099998A (en) * | 2023-08-23 | 2023-11-24 | 广州科百欣香料有限公司 | Essence microbead for flower-fragrance type cigarettes and preparation method and application thereof |
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CN101406704A (en) * | 2008-11-25 | 2009-04-15 | 吴国庆 | Novel plant capsule film material and method for producing the same |
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CN207665976U (en) * | 2017-12-21 | 2018-07-31 | 将军烟草集团有限公司 | A kind of quick-fried droplet water dropper of cigarette |
CN108578381A (en) * | 2018-02-27 | 2018-09-28 | 广州彤博士健康科技有限公司 | The formula and preparation method of chewable property soft capsule crust |
CN109549249A (en) * | 2018-12-11 | 2019-04-02 | 云南巴菰生物科技有限公司 | A kind of preparation method of cigarette preservation antioxidation capsule |
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2019
- 2019-12-23 CN CN201911338358.4A patent/CN110922644A/en active Pending
Patent Citations (10)
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CN101406704A (en) * | 2008-11-25 | 2009-04-15 | 吴国庆 | Novel plant capsule film material and method for producing the same |
CN102499910A (en) * | 2011-12-15 | 2012-06-20 | 山西吉呈生物技术有限公司 | Hard-shell capsule based on pullulan |
CN104479870A (en) * | 2014-12-03 | 2015-04-01 | 湖北中烟工业有限责任公司 | Water capsule for cigarettes using compound salts as wall material and preparation method thereof |
CN107847455A (en) * | 2015-08-05 | 2018-03-27 | 富士胶囊股份有限公司 | Soft capsule is by film composition |
CN105400215A (en) * | 2015-12-14 | 2016-03-16 | 贵州中烟工业有限责任公司 | Heatproof and moisture-proof cigarette capsule material and applications thereof |
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CN108578381A (en) * | 2018-02-27 | 2018-09-28 | 广州彤博士健康科技有限公司 | The formula and preparation method of chewable property soft capsule crust |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN117099998A (en) * | 2023-08-23 | 2023-11-24 | 广州科百欣香料有限公司 | Essence microbead for flower-fragrance type cigarettes and preparation method and application thereof |
CN117099998B (en) * | 2023-08-23 | 2024-02-20 | 广州科百欣香料有限公司 | Essence microbead for flower-fragrance type cigarettes and preparation method and application thereof |
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