CN110859760A - Mild double-layer face-cleaning mousse and preparation method thereof - Google Patents
Mild double-layer face-cleaning mousse and preparation method thereof Download PDFInfo
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- CN110859760A CN110859760A CN201911207582.XA CN201911207582A CN110859760A CN 110859760 A CN110859760 A CN 110859760A CN 201911207582 A CN201911207582 A CN 201911207582A CN 110859760 A CN110859760 A CN 110859760A
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- mousse
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- 235000011929 mousse Nutrition 0.000 title claims abstract description 58
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- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims abstract description 21
- 229960005323 phenoxyethanol Drugs 0.000 claims abstract description 16
- 239000004094 surface-active agent Substances 0.000 claims abstract description 12
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims abstract description 10
- 235000010234 sodium benzoate Nutrition 0.000 claims abstract description 10
- 239000004299 sodium benzoate Substances 0.000 claims abstract description 10
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- 239000004519 grease Substances 0.000 claims abstract description 5
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid group Chemical group C(CC(O)(C(=O)O)CC(=O)O)(=O)O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 27
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 25
- 239000000203 mixture Substances 0.000 claims description 25
- BANXPJUEBPWEOT-UHFFFAOYSA-N 2-methyl-Pentadecane Chemical compound CCCCCCCCCCCCCC(C)C BANXPJUEBPWEOT-UHFFFAOYSA-N 0.000 claims description 24
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 15
- 238000003756 stirring Methods 0.000 claims description 15
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 claims description 13
- 229940073507 cocamidopropyl betaine Drugs 0.000 claims description 13
- KSAVQLQVUXSOCR-UHFFFAOYSA-M sodium lauroyl sarcosinate Chemical compound [Na+].CCCCCCCCCCCC(=O)N(C)CC([O-])=O KSAVQLQVUXSOCR-UHFFFAOYSA-M 0.000 claims description 13
- 229940043268 2,2,4,4,6,8,8-heptamethylnonane Drugs 0.000 claims description 12
- KUVMKLCGXIYSNH-UHFFFAOYSA-N isopentadecane Natural products CCCCCCCCCCCCC(C)C KUVMKLCGXIYSNH-UHFFFAOYSA-N 0.000 claims description 12
- 229940057995 liquid paraffin Drugs 0.000 claims description 12
- HXKKHQJGJAFBHI-UHFFFAOYSA-N 1-aminopropan-2-ol Chemical class CC(O)CN HXKKHQJGJAFBHI-UHFFFAOYSA-N 0.000 claims description 10
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- OQFSQFPPLPISGP-UHFFFAOYSA-N beta-carboxyaspartic acid Natural products OC(=O)C(N)C(C(O)=O)C(O)=O OQFSQFPPLPISGP-UHFFFAOYSA-N 0.000 claims description 10
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- 229940079886 disodium lauryl sulfosuccinate Drugs 0.000 claims description 9
- KHIQYZGEUSTKSB-UHFFFAOYSA-L disodium;4-dodecoxy-4-oxo-3-sulfobutanoate Chemical compound [Na+].[Na+].CCCCCCCCCCCCOC(=O)C(S(O)(=O)=O)CC([O-])=O.CCCCCCCCCCCCOC(=O)C(S(O)(=O)=O)CC([O-])=O KHIQYZGEUSTKSB-UHFFFAOYSA-L 0.000 claims description 9
- CNRDTAOOANTPCG-UHFFFAOYSA-N dodecyl carbamate Chemical compound CCCCCCCCCCCCOC(N)=O CNRDTAOOANTPCG-UHFFFAOYSA-N 0.000 claims description 9
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- JYJIGFIDKWBXDU-MNNPPOADSA-N inulin Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@]1(OC[C@]2(OC[C@]3(OC[C@]4(OC[C@]5(OC[C@]6(OC[C@]7(OC[C@]8(OC[C@]9(OC[C@]%10(OC[C@]%11(OC[C@]%12(OC[C@]%13(OC[C@]%14(OC[C@]%15(OC[C@]%16(OC[C@]%17(OC[C@]%18(OC[C@]%19(OC[C@]%20(OC[C@]%21(OC[C@]%22(OC[C@]%23(OC[C@]%24(OC[C@]%25(OC[C@]%26(OC[C@]%27(OC[C@]%28(OC[C@]%29(OC[C@]%30(OC[C@]%31(OC[C@]%32(OC[C@]%33(OC[C@]%34(OC[C@]%35(OC[C@]%36(O[C@@H]%37[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O%37)O)[C@H]([C@H](O)[C@@H](CO)O%36)O)[C@H]([C@H](O)[C@@H](CO)O%35)O)[C@H]([C@H](O)[C@@H](CO)O%34)O)[C@H]([C@H](O)[C@@H](CO)O%33)O)[C@H]([C@H](O)[C@@H](CO)O%32)O)[C@H]([C@H](O)[C@@H](CO)O%31)O)[C@H]([C@H](O)[C@@H](CO)O%30)O)[C@H]([C@H](O)[C@@H](CO)O%29)O)[C@H]([C@H](O)[C@@H](CO)O%28)O)[C@H]([C@H](O)[C@@H](CO)O%27)O)[C@H]([C@H](O)[C@@H](CO)O%26)O)[C@H]([C@H](O)[C@@H](CO)O%25)O)[C@H]([C@H](O)[C@@H](CO)O%24)O)[C@H]([C@H](O)[C@@H](CO)O%23)O)[C@H]([C@H](O)[C@@H](CO)O%22)O)[C@H]([C@H](O)[C@@H](CO)O%21)O)[C@H]([C@H](O)[C@@H](CO)O%20)O)[C@H]([C@H](O)[C@@H](CO)O%19)O)[C@H]([C@H](O)[C@@H](CO)O%18)O)[C@H]([C@H](O)[C@@H](CO)O%17)O)[C@H]([C@H](O)[C@@H](CO)O%16)O)[C@H]([C@H](O)[C@@H](CO)O%15)O)[C@H]([C@H](O)[C@@H](CO)O%14)O)[C@H]([C@H](O)[C@@H](CO)O%13)O)[C@H]([C@H](O)[C@@H](CO)O%12)O)[C@H]([C@H](O)[C@@H](CO)O%11)O)[C@H]([C@H](O)[C@@H](CO)O%10)O)[C@H]([C@H](O)[C@@H](CO)O9)O)[C@H]([C@H](O)[C@@H](CO)O8)O)[C@H]([C@H](O)[C@@H](CO)O7)O)[C@H]([C@H](O)[C@@H](CO)O6)O)[C@H]([C@H](O)[C@@H](CO)O5)O)[C@H]([C@H](O)[C@@H](CO)O4)O)[C@H]([C@H](O)[C@@H](CO)O3)O)[C@H]([C@H](O)[C@@H](CO)O2)O)[C@@H](O)[C@H](O)[C@@H](CO)O1 JYJIGFIDKWBXDU-MNNPPOADSA-N 0.000 claims description 9
- 229940029339 inulin Drugs 0.000 claims description 9
- 239000001509 sodium citrate Substances 0.000 claims description 9
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims description 9
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 8
- 108700004121 sarkosyl Proteins 0.000 claims description 7
- 229940045885 sodium lauroyl sarcosinate Drugs 0.000 claims description 7
- MTCFGRXMJLQNBG-REOHCLBHSA-N (2S)-2-Amino-3-hydroxypropansäure Chemical compound OC[C@H](N)C(O)=O MTCFGRXMJLQNBG-REOHCLBHSA-N 0.000 claims description 6
- HNDVDQJCIGZPNO-YFKPBYRVSA-N L-histidine Chemical compound OC(=O)[C@@H](N)CC1=CN=CN1 HNDVDQJCIGZPNO-YFKPBYRVSA-N 0.000 claims description 6
- AYFVYJQAPQTCCC-GBXIJSLDSA-N L-threonine Chemical compound C[C@@H](O)[C@H](N)C(O)=O AYFVYJQAPQTCCC-GBXIJSLDSA-N 0.000 claims description 6
- 238000009417 prefabrication Methods 0.000 claims description 6
- SFNALCNOMXIBKG-UHFFFAOYSA-N ethylene glycol monododecyl ether Chemical class CCCCCCCCCCCCOCCO SFNALCNOMXIBKG-UHFFFAOYSA-N 0.000 claims description 5
- 150000001413 amino acids Chemical class 0.000 claims description 4
- 229940079868 disodium laureth sulfosuccinate Drugs 0.000 claims description 4
- YGAXLGGEEQLLKV-UHFFFAOYSA-L disodium;4-dodecoxy-4-oxo-2-sulfonatobutanoate Chemical compound [Na+].[Na+].CCCCCCCCCCCCOC(=O)CC(C([O-])=O)S([O-])(=O)=O YGAXLGGEEQLLKV-UHFFFAOYSA-L 0.000 claims description 4
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- 238000007599 discharging Methods 0.000 claims description 3
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Images
Classifications
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
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Abstract
The invention discloses a mild double-layer face-cleaning mousse and a preparation method thereof, aiming at providing a face-cleaning mousse which can dynamically adjust the cleaning force and the moisture retention degree of the face-cleaning mousse according to the change of the using environment of a client, thereby meeting the using requirements of the client in different environments; the composite material consists of a phase A, a phase B, a phase C, a phase D, a phase E and a phase F; 10-25 parts of phase A liquid grease and 0.1-0.5 part of essence; the phase B comprises 40-60 parts of water and 0.5-2 parts of emulsifier; the phase C comprises 20-35 parts of composite surfactant; the phase D comprises 0.1-0.5 part of pH regulator and 1-2 parts of water; the phase E comprises 0.3-0.5 part of sodium benzoate, 1-2 parts of water and 0.3-0.5 part of phenoxyethanol; the phase F comprises 1-2 parts of hydrolyzed silk and 0.1-0.5 part of amino acid compound humectant; belongs to the technical field of cosmetics.
Description
Technical Field
The invention discloses a face-cleaning mousse, in particular to a mild double-layer face-cleaning mousse, and also discloses a preparation method of the mild double-layer face-cleaning mousse, belonging to the technical field of cosmetics.
Background
The cleansing mousse is generally a single phase homogeneous liquid containing a complex surfactant which is pressed by a pump head to produce a fine foam. Compared with facial cleanser, the facial cleanser is more and more popular with consumers because the facial cleanser does not need to be added with water, rubbed and foamed and is convenient to use. Similar to other face cleaning products, the face cleaning agent has the advantages of strong degreasing force, insufficient moisture retention force, weak cleaning force and no clean feeling during cleaning. The cleaning force and the humidity can not be freely selected according to the use environment or scene. For example, the skin produces more oil in summer than in autumn and winter, and the cleaning force is relatively strong at this time. In autumn and winter, due to dry climate, skin cleaning requires a little weak cleaning force and the moisture retention is relatively high. The cleansing power and moisture retention required of the skin also varies in the morning and evening. And few single-support facial cleansing products on the market can solve all the problems, namely the cleaning strength and the moisture retention degree are freely selected according to the use environment or scene, and the cleaning degree and the moisture retention degree are mild enough, good experience feeling and available sensitive muscles. The double-layer face cleaning mousse on the market is few, the cleaning component is single, and the defects of difficult water passing, slow layering after shaking, poor low-temperature stability and the like exist. The main difficulty lies in the selection and collocation among the emulsifier, the surfactant and the grease. The three components can achieve ideal effects, namely cleaning force, humidity preservation and foam, only by accurate matching, and excellent use experience is provided for consumers.
Disclosure of Invention
In view of the above problems, the present invention provides a face-cleaning mousse capable of dynamically adjusting its own cleaning power and moisture-keeping degree according to the change of the using environment of the client, so as to meet the using requirements of the client in different environments.
In order to solve the above technical problem, a first technical solution provided by the present invention is as follows:
therefore, the first technical scheme provided by the invention is as follows:
a mild double-layer face cleaning mousse comprises phase A, phase B, phase C, phase D, phase E and phase F; each phase comprises the following components in parts by weight:
the phase A comprises 10-25 parts of liquid grease and 0.1-0.5 part of essence;
the phase B comprises 40-60 parts of water and 0.5-2 parts of emulsifier;
the phase C comprises 20-35 parts of composite surfactant;
the phase D comprises 0.1-0.5 part of pH regulator and 1-2 parts of water;
the phase E comprises 0.3-0.5 part of sodium benzoate, 1-2 parts of water and 0.3-0.5 part of phenoxyethanol;
the phase F comprises 1-2 parts of hydrolyzed silk and 0.1-0.5 part of amino acid compound humectant.
Specifically, the mild double-layer face cleaning mousse is prepared by mixing isohexadecane and liquid paraffin.
Specifically, the mild double-layer cleansing mousse has the following mass ratio of isohexadecane to liquid paraffin: 7.
specifically, the mild double-layer cleansing mousse comprises a composition of glycerin and inulin lauryl carbamate as an emulsifier.
Specifically, the mild double-layer cleansing mousse is characterized in that the composite surfactant is a mixture of sodium lauroyl sarcosine, cocamidopropyl betaine, MIPA salt of lauryl polyether sulfate and propylene glycol, disodium lauryl sulfosuccinate.
Specifically, the mild double-layer cleansing mousse comprises sodium lauroyl sarcosinate, cocamidopropyl betaine, laureth sulfate MIPA salt and disodium laurylsulfosuccinate in a mass ratio of: 10: 5: 3: 10.
specifically, the mild double-layer cleansing mousse comprises citric acid and sodium citrate as pH agents.
Specifically, the mild double-layer cleansing mousse is characterized in that the amino acid compound humectant is a mixture of serine, threonine, aspartic acid and histidine.
Specifically, the mild double-layer cleansing mousse comprises the following components in percentage by mass: 1:1:1: 1.
the second technical scheme provided by the invention is as follows:
a preparation method of a mild double-layer face-cleaning mousse sequentially comprises the following steps:
1) adding D-phase citric acid and sodium citrate into water to be completely dissolved into a transparent solution, and filtering the solution through a 300-mesh 400-mesh filter screen for later use to be recorded as prefabrication (1);
2) adding E-phase sodium benzoate into water to be completely dissolved into a transparent solution, and recording as a prefabrication (2) for later use;
3) adding the isohexadecane of phase A, liquid paraffin and essence into a clean sterilized oil phase pot in proportion, stirring for 3-5min at 20-25Hz, and sieving with 100 mesh filter screen to obtain oil phase mixture;
4) adding the deionized water of the phase B into a clean and disinfected emulsifying pot, stirring for 25-30Hz, adding the composition of the glycerol and the inulin lauryl carbamate, heating to 75-80 ℃, vacuumizing to-0.03-0.05 MPa, homogenizing for 3000r/min and homogenizing for 2-3min, and cooling;
5) cooling to 55-60 deg.C, adding mixture of C-phase sodium lauroyl sarcosine, cocamidopropyl betaine, MIPA salt of laureth sulfate, propylene glycol, and disodium laureth sulfosuccinate, stirring at 25-30Hz for 3-5 min;
6) maintaining stirring at 25-30Hz, adding preformed phenoxyethanol (1), preformed phenoxyethanol (2) and phenoxyethanol (E) phase, hydrolyzed silk (F) phase, serine, threonine, aspartic acid and histidine, and stirring for 2-3 min;
7) cooling to 40 ℃, sampling and detecting, and discharging through a 300-mesh and 400-mesh filter screen after the sample is qualified to obtain a water phase mixture;
8) filling the oil phase mixture and the water phase mixture into a packaging bottle according to the required proportion to obtain the face cleaning mousse with double-layer appearance.
Compared with the prior art, the technical scheme provided by the invention is as follows:
1. the double-layer face-cleaning mousse provided by the invention takes the mixture of isohexadecane and liquid paraffin as the liquid oil component, and is compounded with the composite surfactant, so that the defects that other similar double-layer face-cleaning mousses are not easy to wash water, slow in layering and the like are effectively overcome, and the double-layer face-cleaning mousse has better experience feeling and stability.
2. According to the technical scheme provided by the invention, the composite surfactant is formed by adopting sodium lauroyl sarcosine, cocamidopropyl betaine, lauryl polyether sulfate (MIPA) salt, propylene glycol and disodium lauryl sulfosuccinate according to a specific proportion, and has the advantages of mildness, easiness in water passing and abundant foam. Sodium lauroyl sarcosinate and cocamidopropyl betaine are good in mildness and rich in foam but not easy to wash out, disodium lauryl sulfosuccinate has excellent cleaning power and is easy to wash out, but the degreasing power is strong, and the MIPA salt of lauryl polyether sulfate can further improve the overall foam and mildness. The combination makes up the defects of a single surfactant, combines the advantages of the surfactants, is mild, has abundant foam and is easy to wash. Good low-temperature stability and difficult precipitation.
3. The technical scheme provided by the invention has an oil-water two-layer structure, and the layering is rapid. The lower layer is water phase containing mild composite surfactant for cleaning, and the upper layer is oil phase for moistening skin. Can be according to service environment or scene through whether rock the clean dynamics and the degree of moisturizing of the selection of oil water biphase freedom, for example need clean dynamics better when clean face evening, can choose not to rock or rock lightly. The foam that presses out at this time is clean dynamics better, can satisfy the demand, and when the face of cleaning in the morning in autumn and winter, needs the moisture retention degree better, can rock the profit two-phase and make its homogeneity, the foam that presses out at this time keeps the moisture better, also can satisfy the demand. Therefore, the invention can better solve the problem that a single facial cleaning product can not freely select cleaning strength and humidity according to the use environment or scene.
4. According to the technical scheme provided by the invention, the hydrolyzed silk and amino acid compound humectant is selected to be compounded, has the effects of reducing stimulation and repairing damaged cuticle, is really mild, is usable for sensitive muscles, and solves the problem that the cuticle is thinner and thinner when other face cleaning products stimulate.
Drawings
FIG. 1 is a radar chart of the customer feedback indicators of the present application and its commercial products.
Detailed Description
The following claims are presented in further detail with reference to the embodiments, but not to be construed as limiting the invention in any way, and any number of modifications which may be made by anyone within the scope of the claims are within the scope of the claims.
Example 1
The invention provides a mild double-layer face-cleaning mousse which consists of a phase A, a phase B, a phase C, a phase D, a phase E and a phase F; each phase comprises the following components in parts by weight:
the phase A comprises 8 parts of isohexadecane, 7 parts of liquid paraffin and 0.2 part of essence;
the phase B comprises 50.5 parts of water and 0.75 part of glycerol; 0.25 part of inulin lauryl carbamate;
the phase C comprises 10 parts of sodium lauroyl sarcosinate, 5 parts of cocamidopropyl betaine, 3 parts of laureth sulfate MIPA salt and 10 parts of disodium laureth sulfosuccinate.
The phase D comprises 0.1 part of citric acid, 0.1 part of sodium citrate and 2 parts of water;
the phase E comprises 0.5 part of sodium benzoate, 1 part of water and 0.5 part of phenoxyethanol;
the phase F comprises 1 part of hydrolyzed silk, 0.025 part of serine, 0.025 part of threonine, 0.025 part of aspartic acid and 0.025 part of histidine.
Example 2
The invention provides a mild double-layer face-cleaning mousse which consists of a phase A, a phase B, a phase C, a phase D, a phase E and a phase F; each phase comprises the following components in parts by weight:
the phase A comprises 5.33 parts of isohexadecane, 4.67 parts of liquid paraffin and 0.1 part of essence;
the phase B comprises 47.8 parts of water, 0.375 part of glycerol and 0.125 part of inulin lauryl carbamate;
the phase C comprises 12.5 parts of sodium lauroyl sarcosinate, 6.25 parts of cocamidopropyl betaine, 3.75 parts of MIPA (lauryl polyether sulfate) salt and 12.5 parts of disodium lauryl sulfosuccinate.
The phase D comprises 0.25 part of citric acid, 0.25 part of sodium citrate and 1 part of water;
the phase E comprises 0.3 part of sodium benzoate, 2 parts of water and 0.3 part of phenoxyethanol;
the phase F comprises 2 parts of hydrolyzed silk, 0.125 part of serine, 0.125 part of threonine, 0.125 part of aspartic acid and 0.125 part of histidine.
Example 3
The invention provides a mild double-layer face-cleaning mousse which consists of a phase A, a phase B, a phase C, a phase D, a phase E and a phase F; each phase comprises the following components in parts by weight:
the phase A comprises 13.33 parts of isohexadecane, 11.67 parts of liquid paraffin and 0.5 part of essence;
the phase B comprises 46.81 parts of water and 1.5 parts of glycerol; 0.5 part of inulin lauryl carbamate;
the phase C comprises 7.14 parts of sodium lauroyl sarcosinate, 3.57 parts of cocamidopropyl betaine, 2.14 parts of laureth sulfate MIPA salt and 7.14 parts of disodium laurylsulfosuccinate.
The phase D comprises 0.05 part of citric acid, 0.05 part of sodium citrate and 2 parts of water;
the phase E comprises 0.5 part of sodium benzoate, 1.5 parts of water and 0.5 part of phenoxyethanol;
the phase F comprises 1 part of hydrolyzed silk, 0.025 part of serine, 0.025 part of threonine, 0.025 part of aspartic acid and 0.025 part of histidine.
Example 4
The invention provides a mild double-layer face-cleaning mousse which consists of a phase A, a phase B, a phase C, a phase D, a phase E and a phase F; each phase comprises the following components in parts by weight:
the phase A comprises 10.67 parts of isohexadecane, 9.33 parts of liquid paraffin and 0.3 part of essence;
the phase B comprises 42.41 parts of water and 1.125 parts of glycerol; inulin lauryl carbamate 0.375 parts;
the phase C comprises 10.71 parts of sodium lauroyl sarcosinate, 5.36 parts of cocamidopropyl betaine, 3.21 parts of MIPA (lauryl polyether sulfate) salt and 10.71 parts of disodium lauryl sulfosuccinate.
The phase D comprises 0.15 part of citric acid, 0.15 part of sodium citrate and 1.5 parts of water;
the phase E comprises 0.4 part of sodium benzoate, 1.5 parts of water and 0.4 part of phenoxyethanol;
the phase F comprises 1.5 parts of hydrolyzed silk, 0.05 part of amino acid compound humectant serine, 0.05 part of threonine, 0.05 part of aspartic acid and 0.05 part of histidine.
In order to better prepare a mild double-layer cleansing mousse provided by the application, a preparation method of the mild double-layer cleansing mousse is given below, and the method sequentially comprises the following steps:
1) adding D-phase citric acid and sodium citrate into water to be completely dissolved into a transparent solution, and filtering the solution through a 300-mesh 400-mesh filter screen for later use to be recorded as prefabrication (1);
2) adding E-phase sodium benzoate into water to be completely dissolved into a transparent solution, and recording as a prefabrication (2) for later use;
3) adding the isohexadecane of phase A, liquid paraffin and essence into a clean sterilized oil phase pot in proportion, stirring for 3-5min at 20-25Hz, and sieving with 100 mesh filter screen to obtain oil phase mixture;
4) adding the deionized water of the phase B into a clean and disinfected emulsifying pot, stirring for 25-30Hz, adding the composition of the glycerol and the inulin lauryl carbamate, heating to 75-80 ℃, vacuumizing to-0.03-0.05 MPa, homogenizing for 3000r/min and homogenizing for 2-3min, and cooling;
5) cooling to 55-60 deg.C, adding mixture of C-phase sodium lauroyl sarcosine, cocamidopropyl betaine, MIPA salt of laureth sulfate, propylene glycol, and disodium laureth sulfosuccinate, stirring at 25-30Hz for 3-5 min;
6) maintaining stirring at 25-30Hz, adding preformed phenoxyethanol (1), preformed phenoxyethanol (2) and phenoxyethanol (E) phase, hydrolyzed silk (F) phase, serine, threonine, aspartic acid and histidine, and stirring for 2-3 min;
7) cooling to 40 ℃, sampling and detecting, and discharging through a 300-mesh and 400-mesh filter screen after the sample is qualified to obtain a water phase mixture;
8) filling the oil phase mixture and the water phase mixture into a packaging bottle according to the required proportion to obtain the face cleaning mousse with double-layer appearance.
To better illustrate the advantages of the technical solution provided by the present application, experimental data of the mild double-layer cleansing mousse provided by the present application are given below:
1. the prepared cleansing mousse and the commercially available cleansing mousse are tested according to the evaluation standard of the internal mild cleansing products of the company, and the mildness of the cleansing mousse is evaluated mainly by a chick embryo chorioallantoic membrane vascular test (CAMVA), and the specific experimental method and the evaluation standard are as follows:
the experimental principle is as follows: the chick embryo chorioallantoic membrane is a chick embryo respirator, has abundant blood vessels, is similar to the conjunctiva of human and mammals, and can predict the eye irritation of a test object. The experimental method comprises the following steps: a certain amount of test substances (300ul) are directly contacted with chick embryo allantoic membrane, after a period of action (3min), the change of chorioallantoic membrane toxicity effect indexes (bleeding, coagulation and vessel thawing) is observed, the indexes reflect the change of morphological structures, colors and permeability of vessels and a vessel network, reflect phenomena such as chorioallantoic membrane protein denaturation and damage degree thereof, and then a score is obtained by combination for evaluating the eye irritation of the test substances.
Evaluation standard of mild cleansing product: each chick embryo score is the sum of the extent of bleeding, vascular thawing, and clotting observed for each chick embryo. ES-the mathematical sum of scores for 6 chick embryos.
| Serial number | Date of testing | Test sample | ES value | Determination of results |
| 1 | 2019.10.25 | Example 1 | 13 | Qualified |
| 2 | 2019.10.25 | Example 2 | 16 | Fail to be qualified |
| 3 | 2019.10.25 | Example 3 | 13 | Qualified |
| 4 | 2019.10.25 | Example 4 | 15 | Qualified |
| 2 | 2019.10.25 | Multi-fragrance moist cleansing mousse | 17 | Fail to be qualified |
| 3 | 2019.10.25 | Youfei amino acid double-layer face-cleaning liquid | 16 | Fail to be qualified |
2. Case (2): 26 volunteers, 9 volunteers containing sensitive muscles, were selected and used for 7 days in the face cleaning mousse of example 1 of the invention, and 0 person with discomfort or allergy symptoms and 0 allergy rate were selected. Meanwhile, 26 volunteers including 8 sensitive muscle volunteers are selected, and 3 allergic persons are sold on the market in 1 day and 7 days, wherein 2 sensitive muscle volunteers are selected, and 1 non-sensitive muscle volunteer is selected. And then, 26 volunteers are alternatively taken, wherein 5 sensitive muscle volunteers are contained, 2 allergic persons are sold on the market for 2 days and 7 allergic persons are contained, and 2 sensitive muscle volunteers are contained. Namely, the mild performance of the double-layer cleansing mousse is obviously superior to that of the commercial product.
3. Sensory evaluation test: the two-layer mildy wash mousse examples 1-4 and a commercially available mildy wash mousse according to the invention were evaluated for product trial use by 15 trained panelists. The questionnaire was counted, and the following radar chart was prepared for the product foam richness, eye-entering mildness, ease of rinsing, moisture retention after rinsing, and overall product preference, see fig. 1. That is, the overall performance of example 1 of the present invention is significantly better than the commercial product.
4. Physical and chemical tests: including stability testing and delamination speed testing. The sample to be tested is examined for heat resistance (40 +/-1) DEG C, cold resistance (5 +/-1) DEG C and cold resistance (-8 +/-2) DEG C for 2 months to test the stability of the sample. The layering speed is also an important index for inspecting the double-layer face-cleaning mousse, namely the time for recovering to two phases after uniform shaking is related to selection and matching of the emulsifier and the grease, and the consumer experience is influenced by too slow layering speed. The layering speed is generally higher when the formula is designed well. The cleansing mousse of the embodiment 1 and the yoffie amino acid double-layer cleansing mousse are subjected to a stability comparison test and a layering speed comparison test. The test results were as follows:
the results show that example 1 of the present invention is significantly superior to the comparative product in terms of stability and delamination rate.
5. And (3) freely selecting cleaning force and moisture retention test: the cleaning force and the moisture retention of the facial mousse and the yuffy amino acid double-layer facial mousse in example 1 were tested by selecting 15 trained testers, and the cleaning force and the moisture retention of the duffy moist facial mousse were also tested. The test is carried out in a scoring mode, the total score is 10, and the higher the score is, the better the corresponding cleaning strength and the moisture retention are. The test results are statistically as follows:
the results show that example 1 of the present invention gives consumers more choice in cleaning power and moisture retention, i.e., the cleaning power and moisture retention can be freely selected according to the use environment or scene. Is obviously superior to other comparative products.
Claims (10)
1. A mild double-layer cleansing mousse is characterized by consisting of a phase A, a phase B, a phase C, a phase D, a phase E and a phase F; each phase comprises the following components in parts by weight:
the phase A comprises 10-25 parts of liquid grease and 0.1-0.5 part of essence;
the phase B comprises 40-60 parts of water and 0.5-2 parts of emulsifier;
the phase C comprises 20-35 parts of composite surfactant;
the phase D comprises 0.1-0.5 part of pH regulator and 1-2 parts of water;
the phase E comprises 0.3-0.5 part of sodium benzoate, 1-2 parts of water and 0.3-0.5 part of phenoxyethanol;
the phase F comprises 1-2 parts of hydrolyzed silk and 0.1-0.5 part of amino acid compound humectant.
2. The mild, double-layered facial mousse according to claim 1, wherein the liquid oil is a mixture of isohexadecane and liquid paraffin.
3. The mild dual-layer cleansing mousse according to claim 2, wherein the weight ratio of isohexadecane to liquid paraffin is 8: 7.
4. the mild, bi-layer facial mousse according to claim 1, wherein the emulsifier is a combination of glycerin and inulin lauryl carbamate.
5. The mild dual-layer cleansing mousse according to claim 1, wherein the complex surfactant is a mixture of sodium lauroyl sarcosinate, cocamidopropyl betaine, MIPA salts of laureth sulfate, disodium lauryl sulfosuccinate.
6. The mild dual-layer cleansing mousse according to claim 1, wherein the sodium lauroyl sarcosine, cocamidopropyl betaine, MIPA salt of laureth sulfate, disodium lauryl sulfosuccinate are in the following mass ratio: 10: 5: 3: 10.
7. the mild dual-layer cleansing mousse according to claim 1, wherein the pH agent is citric acid and sodium citrate.
8. The mild dual-layer cleansing mousse according to claim 1, wherein the amino acid complex humectant is a mixture of serine, threonine, aspartic acid and histidine.
9. The mild dual-layer cleansing mousse according to claim 1, wherein the serine, threonine, aspartic acid and histidine are in the following mass ratio: 1:1:1:1.
10. A method of preparing a mild dual-layer cleansing mousse according to claim 1, comprising the steps of, in order:
1) adding D-phase citric acid and sodium citrate into water to be completely dissolved into a transparent solution, and filtering the solution through a 300-mesh 400-mesh filter screen for later use to be recorded as prefabrication (1);
2) adding E-phase sodium benzoate into water to be completely dissolved into a transparent solution, and recording as a prefabrication (2) for later use;
3) adding the isohexadecane of phase A, liquid paraffin and essence into a clean sterilized oil phase pot in proportion, stirring for 3-5min at 20-25Hz, and sieving with 100 mesh filter screen to obtain oil phase mixture;
4) adding the deionized water of the phase B into a clean and disinfected emulsifying pot, stirring for 25-30Hz, adding the composition of the glycerol and the inulin lauryl carbamate, heating to 75-80 ℃, vacuumizing to-0.03-0.05 MPa, homogenizing for 3000r/min and homogenizing for 2-3min, and cooling;
5) cooling to 55-60 deg.C, adding mixture of C-phase sodium lauroyl sarcosine, cocamidopropyl betaine, MIPA salt of laureth sulfate, propylene glycol, and disodium laureth sulfosuccinate, stirring at 25-30Hz for 3-5 min;
6) maintaining stirring at 25-30Hz, adding preformed phenoxyethanol (1), preformed phenoxyethanol (2) and phenoxyethanol (E) phase, hydrolyzed silk (F) phase, serine, threonine, aspartic acid and histidine, and stirring for 2-3 min;
7) cooling to 40 ℃, sampling and detecting, and discharging through a 300-mesh and 400-mesh filter screen after the sample is qualified to obtain a water phase mixture;
8) filling the oil phase mixture and the water phase mixture into a packaging bottle according to the required proportion to obtain the face cleaning mousse with double-layer appearance.
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