CN110629542A - After-finishing method for improving flame resistance of fabric - Google Patents
After-finishing method for improving flame resistance of fabric Download PDFInfo
- Publication number
- CN110629542A CN110629542A CN201910772583.2A CN201910772583A CN110629542A CN 110629542 A CN110629542 A CN 110629542A CN 201910772583 A CN201910772583 A CN 201910772583A CN 110629542 A CN110629542 A CN 110629542A
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- Prior art keywords
- fabric
- flame
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- improving
- finishing method
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000004744 fabric Substances 0.000 title claims abstract description 124
- 238000000034 method Methods 0.000 title claims abstract description 36
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 claims abstract description 62
- 239000003063 flame retardant Substances 0.000 claims abstract description 62
- 239000007788 liquid Substances 0.000 claims abstract description 33
- ADCOVFLJGNWWNZ-UHFFFAOYSA-N antimony trioxide Chemical compound O=[Sb]O[Sb]=O ADCOVFLJGNWWNZ-UHFFFAOYSA-N 0.000 claims abstract description 28
- 238000001035 drying Methods 0.000 claims abstract description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 238000002791 soaking Methods 0.000 claims abstract description 16
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims abstract description 14
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims abstract description 14
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims abstract description 14
- 239000000347 magnesium hydroxide Substances 0.000 claims abstract description 14
- 239000003094 microcapsule Substances 0.000 claims abstract description 14
- BIKXLKXABVUSMH-UHFFFAOYSA-N trizinc;diborate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]B([O-])[O-].[O-]B([O-])[O-] BIKXLKXABVUSMH-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000004140 cleaning Methods 0.000 claims abstract description 12
- 239000012530 fluid Substances 0.000 claims abstract description 8
- 239000011248 coating agent Substances 0.000 claims abstract description 6
- 238000000576 coating method Methods 0.000 claims abstract description 6
- 238000002156 mixing Methods 0.000 claims abstract description 6
- 238000003756 stirring Methods 0.000 claims abstract description 6
- 230000002194 synthesizing effect Effects 0.000 claims abstract description 6
- 239000000463 material Substances 0.000 claims description 10
- 239000011265 semifinished product Substances 0.000 claims description 7
- 238000001125 extrusion Methods 0.000 claims description 5
- 238000009998 heat setting Methods 0.000 claims description 5
- 239000004753 textile Substances 0.000 abstract description 2
- 230000000694 effects Effects 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000009950 felting Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000010409 ironing Methods 0.000 description 1
- 239000008159 sesame oil Substances 0.000 description 1
- 235000011803 sesame oil Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000012209 synthetic fiber Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/44—Oxides or hydroxides of elements of Groups 2 or 12 of the Periodic Table; Zincates; Cadmates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/47—Oxides or hydroxides of elements of Groups 5 or 15 of the Periodic Table; Vanadates; Niobates; Tantalates; Arsenates; Antimonates; Bismuthates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
- D06M11/69—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with phosphorus; with halides or oxyhalides of phosphorus; with chlorophosphonic acid or its salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/80—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides
- D06M11/82—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides with boron oxides; with boric, meta- or perboric acids or their salts, e.g. with borax
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M23/00—Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
- D06M23/12—Processes in which the treating agent is incorporated in microcapsules
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/30—Flame or heat resistance, fire retardancy properties
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention provides an after-finishing method for improving flame resistance of fabric, and belongs to the technical field of textiles. It has solved the problem that prior art has had poor stability. The post-finishing method for improving the flame resistance of the fabric comprises the following steps: a: cleaning: putting the fabric into clean water for cleaning, and removing stains on the surface of the fabric; B. synthesizing a flame-retardant treatment fluid: stirring and mixing active magnesium hydroxide, microcapsule red phosphorus, antimony trioxide, zinc borate and water to obtain a flame-retardant treatment solution, wherein the active magnesium hydroxide is 20-25 parts by weight; 2-5 parts of microcapsule red phosphorus; 2-5 parts of antimony trioxide; 2-5 parts of zinc borate; 40-60 parts of water; C. coating: soaking the fabric in the flame-retardant treatment liquid to enable the flame-retardant treatment liquid to completely soak the fabric; D. and (5) drying. The post-finishing method for improving the flame resistance of the fabric has high stability.
Description
Technical Field
The invention belongs to the technical field of textiles, and relates to an after-finishing method for improving flame resistance of fabric.
Background
The post-finishing method is a technical treatment mode for endowing the fabric with color effect, shape effect (such as smoothness, suede, stiffness and smoothness) and effective effect (such as impermeability, non-felting, non-ironing, non-moth, flame resistance and the like), and the post-finishing of the fabric is a technological process for improving the appearance and the hand feeling of the fabric, enhancing the wearability or endowing special functions by a chemical or physical main method, and is a processing process for making the fabric more beautiful.
And (3) coating the synthetic fibers and the fabrics by using the uniform dispersion liquid of the flame-retardant treatment liquid to enable the flame-retardant treatment liquid to be attached to the fibers. The method is simple and easy to implement, and the flame retardant property of the fabric can be effectively improved.
However, the existing after-finishing method is to directly coat the flame-retardant treatment liquid on the fabric. The operation mode causes great operation difficulty and unstable flame retardant property of the fabric.
Disclosure of Invention
The invention aims to provide an after-finishing method for improving the flame resistance of fabric, which can effectively improve the flame resistance of the fabric, aiming at the problems in the prior art.
The purpose of the invention can be realized by the following technical scheme:
an after-finishing method for improving flame resistance of fabric is characterized by comprising the following steps:
a: cleaning: putting the fabric into clean water for cleaning, and removing stains on the surface of the fabric;
B. synthesizing a flame-retardant treatment fluid: stirring and mixing active magnesium hydroxide, microcapsule red phosphorus, antimony trioxide, zinc borate and water to obtain a flame-retardant treatment solution,
20-25 parts of the active magnesium hydroxide according to the weight ratio;
2-5 parts of microcapsule red phosphorus;
2-5 parts of antimony trioxide;
2-5 parts of zinc borate;
40-60 parts of water;
C. soaking: soaking the fabric in the flame-retardant treatment liquid to enable the flame-retardant treatment liquid to completely soak the fabric;
D. drying: and removing the flame-retardant treatment liquid on the fabric in a roll shaft extrusion manner to obtain a semi-finished fabric, and drying the semi-finished fabric to obtain a finished fabric.
The method creatively washes the fabric in advance, and the clean fabric is completely soaked in the flame-retardant treatment liquid, so that the flame-retardant treatment liquid can completely soak the fabric.
After drying treatment, redundant water on the fabric can be removed, and certainly, the flame-retardant material in the flame-retardant treatment liquid is stably adhered to the dried fabric, so that the flame-retardant property of the fabric is effectively improved.
In the post-finishing method for improving the flame resistance of the fabric, the flame-retardant treating fluid in the step B,
23 parts of active magnesium hydroxide according to the weight ratio;
3 parts of microcapsule red phosphorus;
4 parts of antimony trioxide;
3 parts of zinc borate;
51 parts of water;
in the post-finishing method for improving the flame resistance of the fabric, in the step C, the fabric is completely soaked in the flame-retardant treatment solution.
In the post-finishing method for improving the flame resistance of the fabric, the soaking time of the fabric in the step C is 30-50 minutes.
In the post-finishing method for improving the flame resistance of the fabric, the number of the roll shafts in the step D is two, the two roll shafts are fixedly connected to the support in parallel, and a material passing gap slightly smaller than the thickness of the fabric is formed between the two roll shafts.
In the post-finishing method for improving the flame resistance of the fabric, the semi-finished fabric in the step D is dried in a heat setting device.
In the post-finishing method for improving the flame resistance of the fabric, the drying environment temperature of the semi-finished product in the step D is 60-70 ℃, and the drying time of the semi-finished product is 30-50 minutes.
Compared with the prior art, the post-finishing method for improving the flame resistance of the fabric has the advantages that the fabric is soaked and then dried, and the flame-retardant material is stably adhered to the dried finished fabric, so that the soaking and drying treatment is simple and convenient to operate and easy to implement, and the stability is higher compared with the post-finishing method of mechanical and physical finishing of sesame oil.
Detailed Description
Example one
The post-finishing method for improving the flame resistance of the fabric comprises the following steps:
a: cleaning: putting the fabric into clean water for cleaning, and removing stains on the surface of the fabric;
B. synthesizing a flame-retardant treatment fluid: stirring and mixing active magnesium hydroxide, microcapsule red phosphorus, antimony trioxide, zinc borate and water to obtain a flame-retardant treatment solution,
20 parts of the active magnesium hydroxide according to the weight ratio;
2 parts of microcapsule red phosphorus;
2 parts of antimony trioxide;
2 parts of zinc borate;
40 parts of water;
C. coating: soaking the fabric in the flame-retardant treatment liquid to enable the flame-retardant treatment liquid to completely soak the fabric;
and C, completely soaking the fabric in the flame-retardant treatment solution.
And C, soaking the fabric in the step C for 30 minutes.
D. Drying: and removing the flame-retardant treatment liquid on the fabric in a roll shaft extrusion manner to obtain a semi-finished fabric, and drying the semi-finished fabric to obtain a finished fabric.
And D, the number of the roll shafts in the step D is two, the two roll shafts are fixedly connected to the support in parallel, and a material passing gap slightly smaller than the thickness of the fabric is formed between the two roll shafts.
And D, drying the semi-finished fabric in the step D in a heat setting device.
And D, drying the semi-finished product in the step D at the ambient temperature of 60 ℃ for 30 minutes.
The method creatively washes the fabric in advance, and the clean fabric is completely soaked in the flame-retardant treatment liquid, so that the flame-retardant treatment liquid can completely soak the fabric.
After drying treatment, redundant water on the fabric can be removed, and certainly, the flame-retardant material in the flame-retardant treatment liquid is stably adhered to the dried fabric, so that the flame-retardant property of the fabric is effectively improved.
Example two
The post-finishing method for improving the flame resistance of the fabric comprises the following steps:
a: cleaning: putting the fabric into clean water for cleaning, and removing stains on the surface of the fabric;
B. synthesizing a flame-retardant treatment fluid: stirring and mixing active magnesium hydroxide, microcapsule red phosphorus, antimony trioxide, zinc borate and water to obtain a flame-retardant treatment solution,
25 parts of the active magnesium hydroxide according to the weight ratio;
5 parts of microcapsule red phosphorus;
5 parts of antimony trioxide;
5 parts of zinc borate;
60 parts of water;
C. coating: soaking the fabric in the flame-retardant treatment liquid to enable the flame-retardant treatment liquid to completely soak the fabric;
and C, completely soaking the fabric in the flame-retardant treatment solution.
And C, soaking the fabric in the step C for 50 minutes.
D. Drying: and removing the flame-retardant treatment liquid on the fabric in a roll shaft extrusion manner to obtain a semi-finished fabric, and drying the semi-finished fabric to obtain a finished fabric.
And D, the number of the roll shafts in the step D is two, the two roll shafts are fixedly connected to the support in parallel, and a material passing gap slightly smaller than the thickness of the fabric is formed between the two roll shafts.
And D, drying the semi-finished fabric in the step D in a heat setting device.
And D, drying the semi-finished product in the step D at the ambient temperature of 70 ℃ for 50 minutes.
The method creatively washes the fabric in advance, and the clean fabric is completely soaked in the flame-retardant treatment liquid, so that the flame-retardant treatment liquid can completely soak the fabric.
After drying treatment, redundant water on the fabric can be removed, and certainly, the flame-retardant material in the flame-retardant treatment liquid is stably adhered to the dried fabric, so that the flame-retardant property of the fabric is effectively improved.
EXAMPLE III
The post-finishing method for improving the flame resistance of the fabric comprises the following steps:
a: cleaning: putting the fabric into clean water for cleaning, and removing stains on the surface of the fabric;
B. synthesizing a flame-retardant treatment fluid: stirring and mixing active magnesium hydroxide, microcapsule red phosphorus, antimony trioxide, zinc borate and water to obtain a flame-retardant treatment solution,
22 parts of active magnesium hydroxide according to the weight ratio;
3 parts of microcapsule red phosphorus;
3 parts of antimony trioxide;
4 parts of zinc borate;
47 parts of water;
C. coating: soaking the fabric in the flame-retardant treatment liquid to enable the flame-retardant treatment liquid to completely soak the fabric;
and C, completely soaking the fabric in the flame-retardant treatment solution.
And C, soaking the fabric in the step C for 41 minutes.
D. Drying: and removing the flame-retardant treatment liquid on the fabric in a roll shaft extrusion manner to obtain a semi-finished fabric, and drying the semi-finished fabric to obtain a finished fabric.
And D, the number of the roll shafts in the step D is two, the two roll shafts are fixedly connected to the support in parallel, and a material passing gap slightly smaller than the thickness of the fabric is formed between the two roll shafts.
And D, drying the semi-finished fabric in the step D in a heat setting device.
And D, drying the semi-finished product in the step D at the ambient temperature of 62 ℃ for 37 minutes.
The method creatively washes the fabric in advance, and the clean fabric is completely soaked in the flame-retardant treatment liquid, so that the flame-retardant treatment liquid can completely soak the fabric.
After drying treatment, redundant water on the fabric can be removed, and certainly, the flame-retardant material in the flame-retardant treatment liquid is stably adhered to the dried fabric, so that the flame-retardant property of the fabric is effectively improved.
Claims (7)
1. An after-finishing method for improving flame resistance of fabric is characterized by comprising the following steps:
a: cleaning: putting the fabric into clean water for cleaning, and removing stains on the surface of the fabric;
B. synthesizing a flame-retardant treatment fluid: stirring and mixing active magnesium hydroxide, microcapsule red phosphorus, antimony trioxide, zinc borate and water to obtain a flame-retardant treatment solution,
20-25 parts of the active magnesium hydroxide according to the weight ratio;
2-5 parts of microcapsule red phosphorus;
2-5 parts of antimony trioxide;
2-5 parts of zinc borate;
40-60 parts of water;
C. coating: soaking the fabric in the flame-retardant treatment liquid to enable the flame-retardant treatment liquid to completely soak the fabric;
D. drying: and removing the flame-retardant treatment liquid on the fabric in a roll shaft extrusion manner to obtain a semi-finished fabric, and drying the semi-finished fabric to obtain a finished fabric.
2. The post-finishing method for improving the flame resistance of the fabric according to claim 1, wherein the flame-retardant treating fluid in the step B,
23 parts of active magnesium hydroxide according to the weight ratio;
3 parts of microcapsule red phosphorus;
4 parts of antimony trioxide;
3 parts of zinc borate;
51 parts of water.
3. The after-finishing method for improving the flame resistance of the fabric according to claim 2, wherein the fabric in the step C is completely soaked in the flame-retardant treatment solution.
4. The after-finishing method for improving the flame resistance of the fabric according to claim 3, wherein the soaking time of the fabric in the step C is 30-50 minutes.
5. The post-finishing method for improving the flame resistance of the fabric according to claim 4, wherein the number of the rollers in the step D is two, the two rollers are fixedly connected to the bracket in parallel, and a material passing gap slightly smaller than the thickness of the fabric is formed between the two rollers.
6. The finishing method for improving the flame resistance of the fabric according to claim 5, wherein the semi-finished fabric is dried in a heat setting device in the step D.
7. The post-finishing method for improving the flame resistance of the fabric according to claim 6, wherein the drying environment temperature of the semi-finished product in the step D is 60-70 ℃, and the drying time of the semi-finished product is 30-50 minutes.
Priority Applications (1)
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CN201910772583.2A CN110629542A (en) | 2019-08-21 | 2019-08-21 | After-finishing method for improving flame resistance of fabric |
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CN201910772583.2A CN110629542A (en) | 2019-08-21 | 2019-08-21 | After-finishing method for improving flame resistance of fabric |
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2019
- 2019-08-21 CN CN201910772583.2A patent/CN110629542A/en active Pending
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CN101285246A (en) * | 2008-05-28 | 2008-10-15 | 镇江通达内饰材料有限公司 | Carbonizing meshy fire retardant felt and method for preparing same |
US20100285313A1 (en) * | 2009-05-11 | 2010-11-11 | Eternal Chemical Co., Ltd. | Microencapsulated fire retardants and the uses thereof |
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Application publication date: 20191231 |