CN110623179A - Method for extracting mulberry juice - Google Patents

Method for extracting mulberry juice Download PDF

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Publication number
CN110623179A
CN110623179A CN201911063707.6A CN201911063707A CN110623179A CN 110623179 A CN110623179 A CN 110623179A CN 201911063707 A CN201911063707 A CN 201911063707A CN 110623179 A CN110623179 A CN 110623179A
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CN
China
Prior art keywords
enzymolysis
juice
steps
mulberry
juicing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201911063707.6A
Other languages
Chinese (zh)
Inventor
崔波
陶海腾
张建福
时今住
王涛
于滨
刘鹏飞
吴正宗
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shandong Shengyuan Green Food Technology Co Ltd
Qilu University of Technology
Original Assignee
Shandong Shengyuan Green Food Technology Co Ltd
Qilu University of Technology
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Filing date
Publication date
Application filed by Shandong Shengyuan Green Food Technology Co Ltd, Qilu University of Technology filed Critical Shandong Shengyuan Green Food Technology Co Ltd
Priority to CN201911063707.6A priority Critical patent/CN110623179A/en
Publication of CN110623179A publication Critical patent/CN110623179A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • A23L2/04Extraction of juices
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/70Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • A23L2/82Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by flocculation
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/70Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • A23L2/84Clarifying or fining of non-alcoholic beverages; Removing unwanted matter using microorganisms or biological material, e.g. enzymes

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Nutrition Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Microbiology (AREA)
  • Molecular Biology (AREA)
  • Zoology (AREA)
  • Non-Alcoholic Beverages (AREA)
  • Preparation Of Fruits And Vegetables (AREA)

Abstract

The invention provides a method for extracting mulberry juice, belongs to the field of food processing, and particularly comprises the following steps: the method comprises the steps of primary juicing, primary compound enzymolysis, fruit residue collection, secondary juicing, secondary compound enzymolysis and ultrasonic cavitation extraction. Mixing the two juices, colloid milling, and homogenizing. The method provided by the invention has simple steps, the juice yield of the mulberry fruit reaches 98%, and the final juice is clear and transparent, pure liquid, free of any residue feeling and suitable for drinking.

Description

Method for extracting mulberry juice
Technical Field
The invention relates to mulberry juice, and belongs to the technical field of food.
Background
The mulberry contains 80-86% of moisture, sugar, organic acid, crude fiber, protein, mineral, 18 kinds of amino acids, vitamins, anthocyanidin and trace elements. Since the mulberry belongs to the berry type, the fresh mulberry is not easy to preserve and has a short marketing period, the fresh mulberry is often processed into various products in the industrial production of the mulberry. Liquid processed products of fresh morous alba (e.g. morous alba juice) are generally obtained by squeezing fresh morous alba to obtain raw juice of morous alba, then storing the raw juice, and when a specific product is required in the market, the stored raw juice of morous alba is further processed, so that the juice yield determines the processing and utilization degree of morous alba. However, the mulberry cell wall and cell membrane contain abundant pectin and cellulose, and the network structure formed by the substances is difficult to destroy by physical squeezing; pectin has a thickening effect, and the mulberry juice obtained by squeezing has high viscosity and is difficult to filter and extract.
Disclosure of Invention
Aiming at the condition of incomplete utilization of the mulberries in the prior art, the invention provides a high-efficiency and simple mulberry juice extraction technology.
A mulberry juice extraction technology comprises the following steps:
(1) primary juicing: fresh mulberry: water = 1: 1, stirring for 10-15 minutes at 3000-;
(2) primary composite enzymolysis: the compound enzymolysis process comprises the following steps: the cellulase ratio is 1: 2, the addition amount of the complex enzyme is 0.2-0.4%, the enzymolysis temperature is 50 ℃, and the enzymolysis time is 2-3 h;
(3) storing the filtered juice at 40-50 deg.C, and collecting the residue;
(4) secondary juicing: superfine grinding of fruit residues, mulberry fruit residues: the mass ratio of water is 1: 2, micronizing the mixture to 100-120 meshes at the temperature of between 20 and 30 ℃;
(5) secondary composite enzymolysis: the compound enzymolysis process comprises the following steps: the cellulase ratio is 1: 2, the addition amount of the complex enzyme is 0.2-0.4%, the enzymolysis temperature is 50 ℃, and the enzymolysis time is 2-3 h;
(6) ultrasonic extracting with water and pomace at a mass ratio of 2.5:1, adding pectin 5% of pomace volume, ultrasonic cell disruption at 20-40 deg.C under 25 ~ 30KHz frequency and 500 ~ 1000W power for 30min-1h, filtering to obtain juice;
concentration:
(7) mixing the two squeezed juices, concentrating at 40-50 deg.C to concentration of about 70-80%, colloid milling, homogenizing, bottling, and sterilizing.
According to the method, the cell walls of the mulberries are fully destroyed by combining technologies such as superfine grinding, compound enzymolysis and ultrasonic extraction, the juice yield of the mulberries is improved, after the superfine grinding and the compound enzymolysis, the cells of the mulberries are dispersed, most of juice enters water, the cells are crushed by an ultrasonic extraction technology, nutrient components and fruit juice remained in the cells are completely dissolved out, and at the moment, the liquid is not clear and transparent. Pectin is added in the ultrasonic process, residues which are not utilized completely are agglomerated again through the coagulation effect of the pectin, the filtering is convenient, and the final product is clear and transparent and has no residue feeling when being tasted.
The invention has the beneficial effects
1. The juice yield of the mulberry fruits is greatly improved to 98%;
2. the final juice is clear and transparent, pure liquid, has no residue feeling, and is suitable for drinking.
Examples
Example 1
A mulberry juice extraction technology comprises the following steps:
(1) primary juicing: fresh mulberry: water = 1: 1, stirring for 15 minutes at the temperature of 20 ℃ at 5000 r/min, and beating into homogenate;
(2) primary composite enzymolysis: the compound enzymolysis process comprises the following steps: the cellulase ratio is 1: 2, adding 0.2 percent of complex enzyme, carrying out enzymolysis at 50 ℃ for 2 hours;
(3) storing the filtered juice at 50 deg.C, and collecting the residue;
(4) secondary juicing: superfine grinding of fruit residues, mulberry fruit residues: the mass ratio of water is 1: 2, micronizing the mixture to 100-120 meshes at 30 ℃;
(5) secondary composite enzymolysis: the compound enzymolysis process comprises the following steps: the cellulase ratio is 1: 2, adding 0.2 percent of complex enzyme, carrying out enzymolysis at 50 ℃ for 3 hours;
(6) ultrasonic extraction: adding pectin accounting for 5% of the fruit residue volume, extracting at 40 deg.C for 1 hr with ultrasonic cell disruptor frequency of 30KHz and power of 1000W, and filtering to retain fruit juice;
concentration:
(7) mixing the two squeezed juices, concentrating at 50 deg.C to a concentration of about 80%, colloid milling, homogenizing, bottling, and sterilizing.
The juice is clear and transparent, and has no fine residue, and the juice yield is 99 percent.
Example 2
A mulberry juice extraction technology comprises the following steps:
(1) primary juicing: fresh mulberry: water = 1: 1, stirring for 15 minutes at 3000 r/min 30 ℃, and beating into homogenate;
(2) primary composite enzymolysis: the compound enzymolysis process comprises the following steps: the cellulase ratio is 1: 2, adding 0.4 percent of complex enzyme, carrying out enzymolysis at 50 ℃ for 3 hours;
(3) storing the filtered juice at 50 deg.C, and collecting the residue;
(4) secondary juicing: superfine grinding of fruit residues, mulberry fruit residues: the mass ratio of water is 1: 2, micronizing the mixture to 100-120 meshes at 20 ℃;
(5) secondary composite enzymolysis: the compound enzymolysis process comprises the following steps: the cellulase ratio is 1: 2, adding 0.2 percent of complex enzyme, carrying out enzymolysis at 50 ℃ for 3 hours;
(6) ultrasonic extraction: adding pectin accounting for 5% of the fruit residue volume, extracting at 40 deg.C for 30min with ultrasonic cell disruptor frequency of 30KHz and power of 1000W, and filtering to retain fruit juice, wherein the mass ratio of water to fruit residue is 2.5: 1;
concentration:
(7) mixing the two squeezed juices, concentrating at 40 deg.C to a concentration of about 80%, colloid milling, homogenizing, bottling, and sterilizing.
The juice is clear and transparent, and has no fine residue, and the juice yield is 98%.
Comparative example 1
The superfine grinding and compound enzymolysis are not used for the pomace, pectin is not added in the ultrasonic cavitation, and other steps are the same as the example 1.
In the presence of pectin and cellulose, the juice extraction rate is only 90%, and there is a fine residue.
Comparative example 2
During the ultrasonic cavitation process, pectin was not added, and the other steps were the same as in example 1.
The extraction rate of the fruit juice is 98 percent, and the final product has tiny residues.
Comparative example 3
The compound enzymolysis is not used for the pomace, only the ultramicro crushing and the ultrasonic cavitation are used, pectin is not added in the ultrasonic cavitation process, and other steps are the same as the example 1.
The extraction rate of the juice is 94%, and the final product has tiny residue feeling.
Comparative example 4
The ultrasonic cavitation is not used for the pomace, and only the ultramicro crushing and the compound enzymolysis are used, and other steps are the same as the example 1.
The extraction rate of the fruit juice is 96 percent, and the final product has tiny residue feeling.
Comparative example 5
The pomace is not subjected to superfine grinding, and only composite enzymolysis and ultrasonic cavitation are used (pectin is not required to be added under the condition of not using superfine grinding). The other steps are the same as in example 1.
The extraction rate of the fruit juice is 95 percent, and the final product has tiny residue feeling.

Claims (1)

1. A mulberry juice extraction technology is characterized by comprising the following steps:
(1) primary juicing: fresh mulberry: water = 1: 1, stirring for 10-15 minutes at 3000-;
(2) primary composite enzymolysis: the compound enzymolysis process comprises the following steps: the cellulase ratio is 1: 2, the addition amount of the complex enzyme is 0.2-0.4%, the enzymolysis temperature is 50 ℃, and the enzymolysis time is 2-3 h;
(3) storing the filtered juice at 40-50 deg.C, and collecting the residue;
(4) secondary juicing: superfine grinding of fruit residues, mulberry fruit residues: the mass ratio of water is 1: 2, micronizing the mixture to 100-120 meshes at the temperature of between 20 and 30 ℃;
(5) secondary composite enzymolysis: the compound enzymolysis process comprises the following steps: the cellulase ratio is 1: 2, the addition amount of the complex enzyme is 0.2-0.4%, the enzymolysis temperature is 50 ℃, and the enzymolysis time is 2-3 h;
(6) ultrasonic extracting with water and pomace at a mass ratio of 2.5:1, adding pectin 5% of pomace volume, ultrasonic cell disruption at 20-40 deg.C under 25 ~ 30KHz frequency and 500 ~ 1000W power for 30min-1h, filtering to obtain juice;
concentration:
(7) mixing the two squeezed juices, concentrating at 40-50 deg.C to concentration of about 70-80%, colloid milling, homogenizing, bottling, and sterilizing.
CN201911063707.6A 2019-11-04 2019-11-04 Method for extracting mulberry juice Pending CN110623179A (en)

Priority Applications (1)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111838483A (en) * 2020-07-20 2020-10-30 安徽康之味生物科技有限公司 Preparation process of ultra-micro extracted fruit juice beverage
CN114304452A (en) * 2022-01-27 2022-04-12 夏津素源生物科技有限公司 Clarification process and device based on Xiazhi white mulberry fresh juice

Citations (9)

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Publication number Priority date Publication date Assignee Title
CN102188027A (en) * 2011-04-02 2011-09-21 四川省蚕业科技开发总公司 Method for making mulberry juice
KR20130059662A (en) * 2011-11-29 2013-06-07 경상북도 상주시 Mulberry juice and fabricating method thereof
CN104256801A (en) * 2014-10-13 2015-01-07 宁波海通食品科技有限公司 Method for increasing juice yield and anthocyanidin content of blueberry pulp
CN105724999A (en) * 2016-03-22 2016-07-06 广东省农业科学院蚕业与农产品加工研究所 Method for increasing blueberry juicing rate and blueberry juice anthocyanin content
CN107668437A (en) * 2017-11-20 2018-02-09 齐宏伟 A kind of preparation method of alcohol-decomposing beverage
CN107927513A (en) * 2017-12-20 2018-04-20 徐州世缘食品有限公司 A kind of preparation method of instant burdock solid beverage
CN108179091A (en) * 2018-01-29 2018-06-19 广西壮歌农业科技桑博园有限责任公司 A kind of production method of mulberry fruit wine
CN109170404A (en) * 2018-10-18 2019-01-11 徐州工程学院 A kind of processing method of the Black Mulberry Juice
CN110122708A (en) * 2019-05-20 2019-08-16 山东圣源绿色食品科技有限公司 A kind of preparation method of full mulberry beverage

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Publication number Priority date Publication date Assignee Title
CN102188027A (en) * 2011-04-02 2011-09-21 四川省蚕业科技开发总公司 Method for making mulberry juice
KR20130059662A (en) * 2011-11-29 2013-06-07 경상북도 상주시 Mulberry juice and fabricating method thereof
CN104256801A (en) * 2014-10-13 2015-01-07 宁波海通食品科技有限公司 Method for increasing juice yield and anthocyanidin content of blueberry pulp
CN105724999A (en) * 2016-03-22 2016-07-06 广东省农业科学院蚕业与农产品加工研究所 Method for increasing blueberry juicing rate and blueberry juice anthocyanin content
CN107668437A (en) * 2017-11-20 2018-02-09 齐宏伟 A kind of preparation method of alcohol-decomposing beverage
CN107927513A (en) * 2017-12-20 2018-04-20 徐州世缘食品有限公司 A kind of preparation method of instant burdock solid beverage
CN108179091A (en) * 2018-01-29 2018-06-19 广西壮歌农业科技桑博园有限责任公司 A kind of production method of mulberry fruit wine
CN109170404A (en) * 2018-10-18 2019-01-11 徐州工程学院 A kind of processing method of the Black Mulberry Juice
CN110122708A (en) * 2019-05-20 2019-08-16 山东圣源绿色食品科技有限公司 A kind of preparation method of full mulberry beverage

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111838483A (en) * 2020-07-20 2020-10-30 安徽康之味生物科技有限公司 Preparation process of ultra-micro extracted fruit juice beverage
CN114304452A (en) * 2022-01-27 2022-04-12 夏津素源生物科技有限公司 Clarification process and device based on Xiazhi white mulberry fresh juice

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